CN208482463U - A kind of I-131 production destructive distillation absorber - Google Patents
A kind of I-131 production destructive distillation absorber Download PDFInfo
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- CN208482463U CN208482463U CN201821133230.5U CN201821133230U CN208482463U CN 208482463 U CN208482463 U CN 208482463U CN 201821133230 U CN201821133230 U CN 201821133230U CN 208482463 U CN208482463 U CN 208482463U
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Abstract
The utility model discloses a kind of I-131 production destructive distillation absorber, the destructive distillation absorber includes the absorption slot and horizontally disposed distillation cascade being vertically arranged;Wherein, the absorption slot contains alkali liquid tank, water-bath tank, coil pipe, and distillation cascade one end is horn mouth.The distillation cascade other end is fixedly connected with lye pot sidewall by casing;The water-bath tank is placed in alkali liquid tank, and coil pipe is placed in water-bath tank;The upper end pipeline of the coil pipe sequentially passes through water-bath tank obliquely, alkali liquid tank, casing, pierces into distillation cascade and leakproofness is fixedly connected respectively with water-bath tank, alkali liquid tank, distillation cascade, there is an angle between coil pipe upper end pipeline and horizontal line;Coil pipe lower channel is vertically pierced by water-bath pot bottom center and is fixedly connected with water-bath tank leakproofness.The destructive distillation absorber of the utility model can distill and rapid acquiring heap is according to TeO2The high temperature I-131 steam distillated, more conducively raising Na131I production efficiency and safety.
Description
Technical field
The utility model belongs to radioactive isotope preparation technical field, and in particular to a kind of I-131 production is inhaled with destructive distillation
Receive device.
Background technique
For producing the Na of radioactive drugs131After I raw material mainly passes through the irradiation of high temperature (about 750 DEG C) dry distillation reactor heap
TeO2(tellurium dioxide) and the radioactivity I in carrier gas is absorbed with sig water (generally NaOH solution of the concentration less than 0.5mol/L)
(iodine) -131 steam is made.Inst. of Nuclear Physics and Chemistry, Chinese Engineering Physics Research Ins, and domestic Chinese atomic energy science
Research institute and Chinese nuclear power research institute, once in its Na131In I production technology by the way of vacuum pump pumping, by retort
Interior high temperature carrier gas is introduced directly into absorption bottle bottom by pipeline and is bubbled, and the iodine -131 steam in carrier gas is turned by the sig water in bottle
Chemical conversion is Na131I solution.But since very high and the absorbing liquid in absorption bottle the small volume of carrier gas temperature (is usually no more than
20mL), it is easy to during iodine -131 is extracted in distillation so that the temperature of absorbing liquid quickly increases and occurs on absorption bottle top
" fog ", and exhaust gas processing device is entered by tail gas carrier band, cause I-131 vapor adsorption inefficiency and absorbing liquid in carrier gas to be steamed
Hair loses more radioiodine, and bigger pressure is also caused for the online processing of tail gas and qualified discharge.Reduce flow rate of carrier gas
Advantageously reducing heat exchange leads to the evaporation of absorbing liquid, but is unfavorable for preventing iodine -131 steam mistake temperature in gas-guide tube from being adsorbed by tube wall
And lose, also it is unfavorable for setting out in time for the intracavitary a large amount of iodine -131s of retort, causes production (distillation or heat preservation) time and carrier gas
The absorbing liquid continuous heating time is extended, and there are the greater risks that iodine -131 steam is leaked from feed inlet, especially in dioxy
Change tellurium and reaches the fusing point moment.Since domestic destructive distillation heap shines TeO2Produce Na131The device of I is all made of vacuum pump pumping and keeps carrying
Gas directed flow, and keep the intracavitary certain negative pressure of retort to prevent iodine -131 vapour leakage, and higher in order to meet product
The requirement of radioactive concentration, the diluted alkaline liquid measure being added in the absorption bottle of tubulose are less.On the other hand, existing heap shines TeO2It is dry
Furnace is without charging and material unloading function online, it is necessary to be down at least 150 DEG C or less (distillations of iodine in upper batch production furnace temperature
Temperature is about 185 DEG C, preferably close to room temperature), it could charge again after taking out residue and carry out lower batch production, batch production time
Often it is no less than 6 hours, and wherein about 80% time is used for furnace body natural cooling.Since iodine is easily evaporated and is inhaled
It is attached, directly the bottoms of high temperature are taken out, or remove the plug of distillation cascade bottoms are placed on nozzle cooling is to be prohibited
, and absorbing liquid evaporation, and high-temperature furnace body holding to distillation cascade and its interior bottoms can be accelerated by improving flow rate of carrier gas
The time of continuous heat supply can't be significantly affected by flow rate of carrier gas, unless using heat-insulated to distillation cascade or furnace body can be made quick
Otherwise the method for heat dissipation is difficult to significantly shorten the production time.Based on previous reasons, the iodine -131 yield of the prior art is often below
90%, the batch production time is long and the risk of iodine -131 vapour leakage pollution environment is higher, is unfavorable for implementing continuous multiple batches of height
Effect, safety in production.Although reducing the temperature of distillation outlet of still carrier gas by using one section of low-temperature space is increased behind high temperature distillation area
Degree is not carried pipe before by lye absorption processing for iodine -131 in guarantee carrier gas to cut down the heating effect to absorbing liquid
Road inner wall is adsorbed and is caused damages, and the temperature general control of carrier gas is still bright to the effect of absorbing liquid heating evaporation at 300 DEG C or so
It is aobvious.Moreover, the distillation cascade of the prior art and absorber be it is split type, connected using plastic tube or rubber tube, the radiation in carrier gas
The intense gamma radiation of property iodine -131 and high temperature have larger impact to the service life of connecting tube, are easy to appear season cracking in practice
And lead to radioactivity iodine -131 vapour leakage accident, it shortens service life and increases production equipment maintenance and repair personnel receiving
The risk of more dose of radiations, is unfavorable for keeping the safety in production.There is efficiently cooling and quickening distillation cascade drop to Alkali absorption liquid using setting
Temperature function, and be suitable for hot cell or shield compact-sized, the small and exquisite distillation cascade and absorber of production environment condition in work box
Integration-in-one destructive distillation absorber is the main path for solving prior art defect.
Summary of the invention
In order to improve Na131The production efficiency of I solution, reduces security risk, and the utility model provides a kind of I-131 production
With destructive distillation absorber.
The destructive distillation absorber of the utility model using compressed air stream it is heat-insulated and to absorbing liquid it is cooling by the way of and distillation cascade
With the structure of absorber integration-in-one, the height distilled from the tellurium dioxide raw material that reactor activates can be efficiently trapped
Warm radioactivity iodine -131 steam, so that the high income of iodine -131 is of about 98%, the batch production time is foreshortened to about 2 hours, extends life
It produces device lifetime and the security risk of production is effectively reduced.
The technical scheme for implementing the utility model is as follows:
A kind of I-131 production destructive distillation absorber of the utility model, its main feature is that, the destructive distillation absorber includes perpendicular
The absorption slot and horizontally disposed distillation cascade being directly arranged.Wherein, the absorption slot contains alkali liquid tank, water-bath tank, coil pipe, distillation
Pipe one end is horn mouth.The connection relationship of above-mentioned destructive distillation absorber is that the distillation cascade other end passes through with lye pot sidewall
Casing is fixedly connected;The water-bath tank is placed in alkali liquid tank, and coil pipe is placed in water-bath tank;The upper end pipeline of the coil pipe is oblique
Water-bath tank is sequentially passed through upwards, alkali liquid tank, casing, is pierced into distillation cascade and is consolidated with water-bath tank, alkali liquid tank, distillation cascade difference leakproofness
Fixed connection, there is an angle between coil pipe upper end pipeline and horizontal line;Coil pipe lower channel is vertically pierced by water-bath pot bottom center simultaneously
It is fixedly connected with water-bath tank leakproofness.
Laterally the triple valve being connected to, two-way valve are fixedly installed respectively with bottom center at the top of the alkali liquid tank, three
The baffle of circular ring shape is fixedly installed on alkali liquid tank inner sidewall between port valve and water-bath tank deck;It is provided in the water-bath tank
The charge pipe of L-type, water inlet pipe, L-type drainpipe, the upper end level of charge pipe be pierced by lye pot sidewall and with alkali liquid tank leakproofness
It is fixedly connected, the lower end of charge pipe is pierced by water-bath tank vertically downward and is fixedly connected with water-bath tank leakproofness, water inlet pipe and draining
The lower end side-by-side horizontal of pipe is through water-bath tank and alkali liquid tank lower part and is fixedly connected respectively with water-bath tank, alkali liquid tank leakproofness, arranges
The upper port of water pipe is placed in water-bath tank and has a gap with water-bath tank top.
Plug is equipped in the distillation cascade horn mouth;The alkali liquid tank and water-bath pot sidewall passes through link block
It is fixedly connected, steel wire is provided between alkali liquid tank and water-bath pot sidewall, steel wire connects respectively with alkali liquid tank (1) and water-bath tank
Touching.
Angle between the coil pipe upper end pipeline and horizontal line is 5 ° ~ 10 °.
The horizontal axis line of the casing, distillation cascade is to be overlapped setting;The alkali liquid tank, water-bath tank, coil pipe it is vertical
Axial line is to be overlapped setting;The horizontal axis line of the casing and the vertical axis line of alkali liquid tank are arranged in a crossed manner.
The alkali liquid tank, water-bath tank, coil pipe, triple valve, two-way valve, baffle, charge pipe, water inlet pipe, drainpipe, set
Pipe, distillation cascade, plug and link block are all made of quartz glass production;The steel wire is made of stainless steel.
A kind of brief working principle of I-131 production destructive distillation absorber of the utility model is: under vacuum pump twitch,
The heap in distillation cascade is placed according to TeO2The high temperature iodine -131 steams that about 750 DEG C of meltings are overflowed are heated to, by carrier gas from distillation cascade
Interior carrier band is sent into lye pot bottom by way of the coil pipe being placed in water-bath tank and is bubbled, and carrier gas is in coil pipe by gradually cold in flow process
But, the heat release that carrier gas contacts the disproportionated reaction that heat exchange and I-131 and alkali occurs with lye passes through tube wall heat exchange by water-bath tank
Middle cold water is quickly taken away, and making the temperature of absorbing liquid, the temperature remains within the normal range in entire production process or increasing extent of temperature is smaller, residual distilling
After slag temperature is down to specified value, the iodine -131 that elution condenses in coil pipe inner wall is impregnated by back pressure absorbing liquid, realizes and high temperature is carried
The efficient absorption and Na of iodine -131 steam in gas131Efficient, the safety in production of I solution.
The destructive distillation absorber of the utility model uses the absorption slot of two-stage cooling sandwith layer structure, first will be high in absorption slot
Warm carrier gas substantially cools down, then the heat of the remaining heat for passing to absorbing liquid and disproportionated reaction is taken away to greatest extent, cold
But in the case of the general running water pressure of water holding, it is ensured that small size is inhaled in the high temperature carrier gas under high flow velocities (or larger flow)
The heating for receiving liquid is unobvious, prevents or reduce to greatest extent the loss of iodine -131 caused by the generation of " fog ";Using in alkali
What is be arranged between flow container and water-bath tank is immersed in steel wire intensive in absorbing liquid, and biggish carrier gas bubble is split increase and is inhaled
It receives liquid contact area and increases time of contact (increasing bubble moving distance), I-131 in high flow velocities carrier gas has been effectively ensured
The absorption efficiency of steam.The destructive distillation absorber of the utility model it is compact-sized, small and exquisite, safety and reliability is good.
Detailed description of the invention
Fig. 1 is a kind of general structure schematic diagram of I-131 production destructive distillation absorber of the utility model;
Fig. 2 is the overlooking structure diagram of the absorption slot in the utility model;
Fig. 3 is the A-A schematic cross-sectional view of the absorption slot in the utility model;
Fig. 4 is the B-B schematic cross-sectional view of the absorption slot in Fig. 1;
Fig. 5 is the C-C schematic cross-sectional view of the absorption slot in the utility model;
1. alkali liquid tank, 2. water-bath tank, 3. coil pipe, 4. steel wire, 5. triple valve, 6. two-way valve, 7. baffle 8. adds in figure
12. distillation cascade of expects pipe 9. water inlet pipe, 10. drainpipe, 11. connecting tube, 13. plug.
Specific embodiment
The present invention will be further described with reference to the accompanying drawings and examples.
Embodiment 1
Fig. 1 is a kind of general structure schematic diagram of I-131 production destructive distillation absorber of the utility model, and Fig. 2 is this reality
With the overlooking structure diagram of the absorption slot in novel, Fig. 3 is the A-A sectional structure signal of the absorption slot in the utility model
Figure, Fig. 4 are the B-B schematic cross-sectional views of the absorption slot in Fig. 1, and Fig. 5 is the C-C section view knot of the absorption slot in the utility model
Structure schematic diagram.In Fig. 1 ~ Fig. 5, a kind of I-131 production destructive distillation absorber of the utility model is absorbed including the destructive distillation
Device includes the absorption slot and horizontally disposed distillation cascade 12 being vertically arranged;Wherein, the absorption slot contains alkali liquid tank 1, water-bath
Tank 2, coil pipe 3,12 one end of distillation cascade are horn mouth;The connection relationship of above-mentioned destructive distillation absorber is that the distillation cascade 12 is another
End is fixedly connected with 1 side wall of alkali liquid tank by casing 11.The water-bath tank 2 is placed in alkali liquid tank 1, and coil pipe 3 is placed in water-bath tank 2
It is interior.The upper end pipeline of the coil pipe 3 sequentially pass through obliquely water-bath tank 2, alkali liquid tank 1, casing 11, pierce into distillation cascade 12 and with
Leakproofness is fixedly connected respectively for water-bath tank 2, alkali liquid tank 1, distillation cascade 12, has an angle between 3 upper end pipeline of coil pipe and horizontal line;
3 lower channel of coil pipe is vertically pierced by 2 bottom center of water-bath tank and is fixedly connected with 2 leakproofness of water-bath tank.The alkali liquid tank 1 pushes up
Portion is laterally fixedly installed the triple valve 5 being connected to, two-way valve 6 with bottom center respectively, between triple valve 5 and the top of water-bath tank 2
1 inner sidewall of alkali liquid tank on be fixedly installed the baffle 7 of circular ring shape.Be provided in the water-bath tank 2 L-type charge pipe 8, into
The drainpipe 10 of water pipe 9, L-type, the upper end level of charge pipe 8, which is pierced by 1 side wall of alkali liquid tank and fixes with 1 leakproofness of alkali liquid tank, to be connected
It connects, the lower end of charge pipe 8 is pierced by water-bath tank 2 vertically downward and is fixedly connected with 2 leakproofness of water-bath tank, water inlet pipe 9 and drainpipe
10 lower end side-by-side horizontal fixes company through water-bath tank 2 and 1 lower part of alkali liquid tank and respectively with water-bath tank 2,1 leakproofness of alkali liquid tank
Connect, the upper port of drainpipe 10 be placed in water-bath tank 2 and with have a gap at the top of water-bath tank 2.12 horn mouth of distillation cascade
Inside it is equipped with plug 13.The alkali liquid tank 1 is fixedly connected with 2 side wall of water-bath tank by link block, in alkali liquid tank 1 and water
It is provided with steel wire 4 between bath 2 side wall of tank, steel wire 4 contacts respectively with alkali liquid tank 1 and water-bath tank 2.3 upper end of coil pipe
Angle between pipeline and horizontal line is 5 ° ~ 10 °.The horizontal axis line of the casing 11, distillation cascade 12 is to be overlapped setting.Institute
The alkali liquid tank 1 stated, water-bath tank 2, coil pipe 3 vertical axis line to be overlapped setting.The horizontal axis line and lye of the casing 11
The vertical axis line of tank 1 is arranged in a crossed manner.The alkali liquid tank 1, water-bath tank 2, coil pipe 3, triple valve 5, two-way valve 6, baffle 7 plus
Expects pipe 8, water inlet pipe 9, drainpipe 10, casing 11, distillation cascade 12, plug 13 and link block are all made of quartz glass production.It is described
Steel wire 4 using stainless steel make.As shown in Fig. 1 ~ Fig. 5.
The part of horizontal of the distillation cascade 12 is placed in external heating furnace, is placed on steaming by being heated to about 750 DEG C
The heap in pipe 12 is evaporated according to TeO2Melting, the iodine -131 distillated, which is included in constantly to be loaded into pipe and by carrier gas, absorbs slot.The alkali
The external bigeminy ball of a branch pipe of triple valve 5 on flow container 1, for making it to absorbing liquid pressurization in alkali liquid tank 1, liquid impregnates from bottom to up
Elution condenses in the iodine -131 of 3 inner wall of coil pipe, advantageously reduces the adsorption loss of iodine -131;Another branch pipe of triple valve 5 is successively
External exhaust gas processing device, vacuum pump drive carrier gas to flow through coil pipe 3, alkali liquid tank 1 and tail from the orientation of distillation cascade 12 using vacuum pump
Flash Gas Compression Skid System is to handle high temperature carrier gas.The bottom and the distance between side and alkali liquid tank 1 of the water-bath tank 2 compared with
It is small, the loading amount of absorbing liquid is advantageously reduced to realize high concentration Na131I production.The upper end pipeline of the coil pipe 3 is with certain angle
Degree is arranged obliquely, is beneficial to prevent absorption when pressurization drives the absorbing liquid elution of liquid immersion from bottom to up to condense in 3 inner wall of coil pipe
Liquid, which covers coil pipe and enters distillation cascade 12, to cause damages.The external peristaltic pump of charge pipe 8, it is fixed to alkali liquid tank 1 using peristaltic pump
Amount plus absorbing liquid.The water inlet pipe 9, the external recirculated cooling water device of drainpipe 10, guarantee in water-bath tank 2 cooling water from lower and
Upper quickly flowing is to take away heat transfer of the high temperature carrier gas to absorbing liquid.The effect that the baffle 7 is arranged is to prevent excessive air-flow from leading
It causes absorbing liquid to be acutely bubbled to pour in 5 branch pipe of triple valve and lose.
In the present embodiment, angle of the upper end pipeline of the coil pipe 3 obliquely between horizontal line is 5 °.
The workflow of the utility model is as follows, opens peristaltic pump for a certain amount of absorbing liquid and injects lye through charge pipe 8
In tank 1, then opens recirculated cooling water device and pass through cooling water from the injection of 2 bottom of water-bath tank, at the top of water-bath tank 2 through water inlet pipe 9
Drainpipe 10 be discharged, respectively in alkali liquid tank 1 absorbing liquid and coil pipe 3 cool down.Heating furnace is opened to being placed in distillation cascade 12
Interior heap shines TeO2750 DEG C are heated to about, vacuum pump pumping is opened simultaneously, the high temperature that iodine -131 steam is loaded in distillation cascade 12 carries
Coil pipe 3 of the gas through being placed in water-bath tank 2 is sent into 1 bottom of alkali liquid tank and is bubbled, and carrier gas is in coil pipe 3 in top-down flow process
It is gradually cooled down, absorbing liquid of the bubble in contact alkali liquid tank 1, and is upward through and is immersed in absorbing liquid from 1 bottom of alkali liquid tank
Steel wire 4, then during being discharged from triple valve 5, exchange to the heat and I-131 of absorbing liquid and the reaction heat of alkali all passes through heat
Exchange is taken away rapidly by the cold water in water-bath tank 2, and making the temperature of absorbing liquid, the temperature remains within the normal range in entire production process or heating width
It spends smaller.Distillation terminates after closing heating power supply, and after 12 temperature of distillation cascade is lower than 150 DEG C (preferably close to room temperature), closes
The connection of triple valve 5 and exhaust gas processing device is simultaneously connected to bigeminy ball, is washed using the liquid immersion from bottom to up of bigeminy ball back pressure absorbing liquid
The de- iodine -131 for condensing in 3 inner wall of coil pipe, then removal bigeminy ball pressure, impregnates eluent and flows back to alkali liquid tank 1.Open two-way valve
6 are put into the absorbing liquid in alkali liquid tank 1 in special glass bottle, take out bottoms and deal carefully with.So far, it realizes and high temperature is carried
The high yield and Na of iodine -131 steam in gas131Efficient, the safety in production of I solution.
Embodiment 2
The present embodiment is identical as the structure of embodiment 1, except that the upper end pipeline of coil pipe 3 obliquely with horizontal line
Between angle be 10 °.
Claims (3)
1. a kind of I-131 production destructive distillation absorber, it is characterised in that: the destructive distillation absorber includes the absorption being vertically arranged
Slot and horizontally disposed distillation cascade (12);Wherein, the absorption slot contains alkali liquid tank (1), water-bath tank (2), coil pipe (3), steams
Evaporating pipe (12) one end is horn mouth;The connection relationship of above-mentioned destructive distillation absorber is the distillation cascade (12) other end and lye
Tank (1) side wall is fixedly connected by casing (11);The water-bath tank (2) is placed in alkali liquid tank (1), and coil pipe (3) is placed in water-bath
In tank (2);The upper end pipeline of the coil pipe (3) sequentially passes through water-bath tank (2) obliquely, alkali liquid tank (1), casing (11), wears
Into distillation cascade (12) and with water-bath tank (2), alkali liquid tank (1), distillation cascade (12), leakproofness is fixedly connected respectively, coil pipe (3) upper end
There is an angle between pipeline and horizontal line;Coil pipe (3) lower channel be vertically pierced by water-bath tank (2) bottom center and with water-bath tank
(2) leakproofness is fixedly connected;
Laterally the triple valve (5) being connected to, two-way valve (6) are fixedly installed respectively with bottom center at the top of the alkali liquid tank (1),
The baffle (7) of circular ring shape is fixedly installed on alkali liquid tank (1) inner sidewall between triple valve (5) and water-bath tank (2) top;It is described
Water-bath tank (2) in be provided with the charge pipe (8) of L-type, water inlet pipe (9), L-type drainpipe (10), the upper end water of charge pipe (8)
Flat to be pierced by alkali liquid tank (1) side wall and be fixedly connected with alkali liquid tank (1) leakproofness, the lower end of charge pipe (8) is pierced by water vertically downward
Bath tank (2) is simultaneously fixedly connected with water-bath tank (2) leakproofness, and the lower end side-by-side horizontal of water inlet pipe (9) and drainpipe (10) runs through water
Bath tank (2) and alkali liquid tank (1) lower part are simultaneously fixedly connected with water-bath tank (2), alkali liquid tank (1) leakproofness respectively, drainpipe (10)
Upper port is placed in water-bath tank (2) and has a gap with water-bath tank (2) top;
Plug (13) are equipped in described distillation cascade (12) horn mouth;The alkali liquid tank (1) and water-bath tank (2) side wall
Be fixedly connected by link block, be provided with steel wire (4) between alkali liquid tank (1) and water-bath tank (2) side wall, steel wire (4) with
Alkali liquid tank (1) and water-bath tank (2) contact respectively.
2. a kind of I-131 production destructive distillation absorber according to claim 1, it is characterised in that: on the coil pipe (3)
Angle between end pipe road and horizontal line is 5 ° ~ 10 °.
3. a kind of I-131 production destructive distillation absorber according to claim 1, it is characterised in that: the casing (11),
The horizontal axis line of distillation cascade (12) is to be overlapped setting;The alkali liquid tank (1), water-bath tank (2), coil pipe (3) vertical axis line
To be overlapped setting;The vertical axis line of the horizontal axis line of the casing (11) and alkali liquid tank (1) is arranged in a crossed manner.
Priority Applications (1)
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CN201821133230.5U CN208482463U (en) | 2018-07-18 | 2018-07-18 | A kind of I-131 production destructive distillation absorber |
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CN201821133230.5U CN208482463U (en) | 2018-07-18 | 2018-07-18 | A kind of I-131 production destructive distillation absorber |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108686610A (en) * | 2018-07-18 | 2018-10-23 | 中国工程物理研究院核物理与化学研究所 | A kind of I-131 productions destructive distillation absorber |
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2018
- 2018-07-18 CN CN201821133230.5U patent/CN208482463U/en not_active Withdrawn - After Issue
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108686610A (en) * | 2018-07-18 | 2018-10-23 | 中国工程物理研究院核物理与化学研究所 | A kind of I-131 productions destructive distillation absorber |
CN108686610B (en) * | 2018-07-18 | 2023-09-19 | 中国工程物理研究院核物理与化学研究所 | Destructive distillation absorber for I-131 production |
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