CN207950754U - Two-phase mixtures liquid separating appts - Google Patents
Two-phase mixtures liquid separating appts Download PDFInfo
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- CN207950754U CN207950754U CN201721906668.8U CN201721906668U CN207950754U CN 207950754 U CN207950754 U CN 207950754U CN 201721906668 U CN201721906668 U CN 201721906668U CN 207950754 U CN207950754 U CN 207950754U
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Abstract
The utility model discloses a kind of two-phase mixtures liquid separating appts, includes tank body equipped with sealing cover and be located in tank body and the vertical inner cylinder being connected on tank body bottom wall；The inner cylinder has cylinder lumen helically linear under vertical view state, the inlet tube for stretching into cylinder lumen centre is connected on the sealing cover, the cylinder lumen is connected to by being located at the side opening of inner cylinder side with tank inner chamber, to make the liquid into lumen centers position that can flow into tank inner chamber through side opening after interior intracavitary circuitous flow；Tank body is equipped with for the upper leakage fluid dram of the small liquid discharge of proportion and for the lower leakage fluid dram of heavy liquid discharge.The device can make two-phase mixtures liquid separating rate fast, good separating effect.
Description
Technical field
The utility model is related to a kind of devices that can detach two-phase mixtures liquid.
Background technology
In organic synthesis and Polymer Synthesizing, it is frequently encountered the problem of two-phase liquid mixes, such as extraction and washing
Process just will produce the problem of two-phase liquid mixing.Extraction is to utilize solubility of the substance in two kinds of mutual exclusive solvents not
Together, substance is extracted to the separation method for detaching solute and solvent in another solvent, extraction process meeting in a kind of solvent
Generate two kinds of immiscible liquid；Feed liquid washing mainly by salt in the reaction material liquid with solvent or impurity water or other not
Mutual solvents carrying out washing treatment, feed liquid washing process also will produce two kinds of mutual exclusive liquid.Currently, generally use mixes two-phase
It closes liquid and is passed through standing slot（Tank）It is interior, after through a long time stewing process makes the layering completely of two-phase liquid, then it is isolated.Above-mentioned point
From mode, disengaging time is long, low separation efficiency, is unfavorable for carrying out continuous production, therefore want a kind of structure of necessary utility model
The device of simple and high separative efficiency two-phase mixtures liquid separation.
Utility model content
The technical problems to be solved in the utility model is to provide a kind of two-phase mixtures liquid separating appts.
In order to solve the above-mentioned technical problem, the utility model provides a kind of two-phase mixtures liquid separation dress such as lower structure
It sets, is structurally characterized in that：Include tank body equipped with sealing cover and is located in tank body and the vertical inner cylinder being connected on tank body bottom wall；
The inner cylinder has cylinder lumen helically linear under vertical view state, is connected on the sealing cover and stretches into cylinder lumen center
The inlet tube at position, the cylinder lumen are connected to by being located at the side opening of inner cylinder side with tank inner chamber, interior to make to enter
The liquid in chamber centre can flow into tank inner chamber after interior intracavitary circuitous flow through side opening；Tank body is equipped with small for proportion
The upper leakage fluid dram of liquid discharge and the lower leakage fluid dram being discharged for heavy liquid.
The bottom wall of the tank body is equipped with slot corresponding with inner cylinder cross-sectional shape, and the inner cylinder is inserted into slot.
The bottom wall of the tank body is equipped in the low skewed setting in the high other side in side, tank wall close to tank body bottom wall
The slag-drip opening of downside setting.
The tank wall is equipped with the observation window for observing liquid interface.
It is connected with hose on the lower leakage fluid dram, in order to adjust the outflow height of the liquid flowed out from lower leakage fluid dram.
The inner cylinder for made of plank and since one side of plank outside from coil to coil curl up the cylinder to be formed, institute
Cylinder lumen and side opening is stated to be formed during plank curls up to form inner cylinder.
Several pieces of baffles for slowing down flow rate of liquid and being connected on cylinder lumen wall surface are equipped in the cylinder lumen
Plate, the flow-stopping plate short transverse is consistent with the short transverse of cylinder lumen and flow-stopping plate is equipped with liquid pass hole.
The liquid pass hole is located at the top of flow-stopping plate.
The width direction of the flow-stopping plate and inner cylinder it is radially consistent, it includes polylith flow-stopping plate that the flow-stopping plate, which is divided into every group,
It is multigroup, with group flow-stopping plate width direction by it is same it is radial be arranged, multigroup flow-stopping plate ring cloth setting, to by cylinder lumen
It is separated into multiple standing areas.
The utility model can realize the two-phase mixtures liquid into inner cylinder centre during inner cylinder circuitous flow
It is layered, supernatant liquid is flowed out from upper leakage fluid dram, and lower liquid is flowed out from lower leakage fluid dram, that is to say, that the utility model can
It realizes being layered when entering for two-phase mixtures liquid, the separation two-phase mixtures liquid of serialization can be shown, be conducive to postorder continuous
Change is handled, and is easy to implement continuous production, and two-phase liquid separating rate is fast, good separating effect.In addition, the utility model is only
It is made of two core components of tank body and inner cylinder, thus structure is very simple.
Description of the drawings
Specific embodiment of the present utility model is described in further detail below in conjunction with the accompanying drawings：
Fig. 1 is the principle schematic diagram of the utility model；
Fig. 2 is the sectional view of line A-A in Fig. 1.
Specific implementation mode
Referring to Figures 1 and 2, two-phase mixtures liquid separating appts include tank body 1, and 1 top of tank body is equipped with sealing cover 2, tank body 1
Bottom wall in the low skewed setting in the high other side in side, 1 side wall of tank body is equipped with slag-drip opening 8, and slag-drip opening 8 is close to tank body bottom wall
Downside is arranged.Lower leakage fluid dram 7 of the position in upper upper leakage fluid dram 6 and position under, upper leakage fluid dram 6 are additionally provided on 1 side wall of tank body
For the small liquid discharge of proportion, lower leakage fluid dram 7 is discharged for heavy liquid；For the ease of observing the interface of two-phase liquid,
Observation window 9 is equipped on 1 side wall of tank body.The inner cylinder 3 being connected to vertically on 1 bottom wall of tank body is equipped in tank body 1, for the ease of tearing open
Dress, inner cylinder 3 are connected in a manner of inserting on tank body bottom wall, i.e., the bottom wall of tank body 1 is equipped with corresponding to 3 cross-sectional shape of inner cylinder
Slot, the inner cylinder 3 is inserted into slot, and the upper end of inner cylinder 3 is usually concordant with the upper end of tank body 1, can also be slightly below tank
The upper end of body 1.With reference to Fig. 2, the inner cylinder 3 has cylinder lumen 4 helically linear under vertical view state, and 3 side of inner cylinder sets side
Opening 13, cylinder lumen 4 is connected to by side opening 13 with tank inner chamber, is connected with and is stretched into cylinder lumen 4 on the sealing cover 2
The inlet tube 5 of center portion position, inlet tube 5 preferably extend into the lower position of cylinder lumen 4, to reduce liquid into fashionable impact.
By there are many settings of cylinder lumen 4 of inner cylinder 3 helically the mode possibility of threadiness, but most plain mode is no more than
Using following manner：I.e. inner cylinder 3 has a plank to be made, and outside from coil to coil is curled up since one side of plank, after the completion of curling up
With regard to forming inner cylinder 3, side opening 13 and helically linear cylinder lumen 4 are also just formed during curling up plank and forming inner cylinder
, Fig. 2 shows the transverse shapes of inner cylinder 3 made of being curled up by plank.
After two-phase mixtures liquid enters 4 centre of cylinder lumen, tank inner chamber can be flowed into through circuitous flow, in order into
One step slows down two-phase mixtures liquid and is easy to implement in the flowing velocity of cylinder lumen 4 to be layered in flow process, can be in cylinder
Several pieces of flow-stopping plates 11 for slowing down flow rate of liquid are set in chamber 4, the flow-stopping plate 11 is connected on the wall surface of cylinder lumen, described
Flow-stopping plate short transverse is consistent with the short transverse of cylinder lumen 4,11 lower end of the flow-stopping plate contacts with tank body bottom wall, upper end most
It is good concordant with 3 upper end of inner cylinder.The flow-stopping plate 11 is equipped with multiple liquid pass holes 12, in order to further slow down liquid in cylinder lumen
4 flow velocity, the liquid pass hole 12 are located at the top of the flow-stopping plate 11.Following arrangement side may be used in several pieces of flow-stopping plates 11
The width direction of the flow-stopping plate 11 is set as radially consistent with inner cylinder 3, several pieces of flow-stopping plates 11 are divided by formula with reference to Fig. 2
Multigroup, every group includes polylith flow-stopping plate 11, and the width direction with the flow-stopping plate 11 of group is arranged by same radial direction, multigroup flow-stopping plate ring
Cloth is arranged, to which cylinder lumen 4 is separated into multiple standing areas；Each standing area's volume is answered essentially identical；Above-mentioned set-up mode
The intensity of inner cylinder 3 can be improved, and it is not in excessive fluctuation that liquid, which may be implemented, in the flowing of cylinder lumen 4, be conducive to divide
Layer.
Cylinder lumen 4 is actually divided into multiple standing chambers by the setting of flow-stopping plate 11, and two-phase mixtures liquid is from feed liquor
Pipe 5 enters after cylinder lumen 4 along helically linear 4 circuitous flow of cylinder lumen, after flow-stopping plate 11 is encountered in flow process
Liquid can be increased slowly, and then from 12 overflow of liquid pass hole to next standing chamber, such two-phase mixtures liquid is in cylinder lumen 4
During circuitous flow is until flow into tank inner chamber, multiple stratification for standing chamber can be passed through, can get preferable point
From effect and higher separative efficiency.The supernatant liquid of the two-phase liquid of layering is flowed out by upper leakage fluid dram 6, lower liquid passes through
Lower leakage fluid dram 7 flows out, and for the ease of adjusting the height and position of layering interfaces, is connected with hose 10 on lower leakage fluid dram 7, passes through change
The outlet height of hose 10 can adjust the outflow height of the liquid flowed out from lower leakage fluid dram, exist so as to adjust two-phase liquid
The height and position of layering interfaces in tank body.
Claims (9)
1. a kind of two-phase mixtures liquid separating appts, it is characterised in that including being equipped with sealing cover（2）Tank body（1）Be located at tank
Body（1）It is interior and be connected to tank body vertically（1）Inner cylinder on bottom wall（3）；The inner cylinder（3）With helically linear under vertical view state
Cylinder lumen（4）, the sealing cover（2）On be connected with and stretch into cylinder lumen（4）The inlet tube in centre（5）, the cylinder
Intracoelomic cavity（4）By being located at inner cylinder（3）The side opening of side is connected to tank inner chamber, to make to enter inner cavity（4）Centre
Liquid in cylinder lumen（4）Tank inner chamber can be flowed into after interior circuitous flow through side opening；Tank body（1）It is equipped with small for proportion
The upper leakage fluid dram of liquid discharge（6）With the lower leakage fluid dram for the discharge of heavy liquid（7）.
2. two-phase mixtures liquid separating appts according to claim 1, it is characterised in that the tank body（1）Bottom wall on
It is equipped with and inner cylinder（3）The corresponding slot of cross-sectional shape, the inner cylinder（3）It is inserted into slot.
3. two-phase mixtures liquid separating appts according to claim 1, it is characterised in that the tank body（1）Bottom wall be in
The low skewed setting in the high other side in side, tank body（1）Side wall is equipped with the slag-drip opening close to tank body bottom wall downside setting（8）.
4. two-phase mixtures liquid separating appts according to claim 1, it is characterised in that the tank body（1）It is set on side wall
It is useful for the observation window of observation liquid interface（9）.
5. two-phase mixtures liquid separating appts according to claim 1, it is characterised in that the lower leakage fluid dram（7）Upper company
It is connected to hose（10）, in order to adjust the outflow height of the liquid flowed out from lower leakage fluid dram.
6. the two-phase mixtures liquid separating appts according to any claim in claim 1-5, it is characterised in that described
Inner cylinder（3）For made of plank and since one side of plank outside from coil to coil curl up the cylinder to be formed, in the cylinder
Chamber（4）It is formed during plank curls up to form inner cylinder with side opening.
7. two-phase mixtures liquid separating appts according to claim 6, it is characterised in that the cylinder lumen（4）Inside set
There are several pieces to be used to slow down flow rate of liquid and be connected to cylinder lumen（4）Flow-stopping plate on wall surface（11）, the flow-stopping plate height
Direction and cylinder lumen（4）Short transverse is consistent and flow-stopping plate（11）It is equipped with liquid pass hole（12）.
8. two-phase mixtures liquid separating appts according to claim 7, it is characterised in that the liquid pass hole（12）It is located at gear
Flowing plate（11）Top.
9. two-phase mixtures liquid separating appts according to claim 7 or 8, it is characterised in that the flow-stopping plate（11）'s
Width direction and inner cylinder（3）Radially consistent, the flow-stopping plate（11）It includes polylith flow-stopping plate to be divided into every group（11）It is multigroup, together
The flow-stopping plate of group（11）Width direction by it is same it is radial be arranged, multigroup flow-stopping plate ring cloth setting, to by cylinder lumen（4）Point
It is divided into multiple standing areas.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721906668.8U CN207950754U (en) | 2017-12-30 | 2017-12-30 | Two-phase mixtures liquid separating appts |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721906668.8U CN207950754U (en) | 2017-12-30 | 2017-12-30 | Two-phase mixtures liquid separating appts |
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| Publication Number | Publication Date |
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| CN207950754U true CN207950754U (en) | 2018-10-12 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201721906668.8U Active CN207950754U (en) | 2017-12-30 | 2017-12-30 | Two-phase mixtures liquid separating appts |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107837564A (en) * | 2017-12-30 | 2018-03-27 | 山东天化学股份有限公司 | Two-phase mixtures liquid separating appts |
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2017
- 2017-12-30 CN CN201721906668.8U patent/CN207950754U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107837564A (en) * | 2017-12-30 | 2018-03-27 | 山东天化学股份有限公司 | Two-phase mixtures liquid separating appts |
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