CN206881200U - A kind of multi-functional plant extracts separation integrated apparatus - Google Patents

A kind of multi-functional plant extracts separation integrated apparatus Download PDF

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Publication number
CN206881200U
CN206881200U CN201720807161.0U CN201720807161U CN206881200U CN 206881200 U CN206881200 U CN 206881200U CN 201720807161 U CN201720807161 U CN 201720807161U CN 206881200 U CN206881200 U CN 206881200U
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CN
China
Prior art keywords
extractor
integrated apparatus
functional plant
centrifuge
outlet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720807161.0U
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Chinese (zh)
Inventor
郑增辉
李交昆
曾伟民
廖创
吴晨晨
李芳�
余黄
余润兰
吴学玲
申丽
刘元东
刘学端
邱冠周
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Guangdong Guava Health Industry Co Ltd
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Guangdong Guava Health Industry Co Ltd
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Application filed by Guangdong Guava Health Industry Co Ltd filed Critical Guangdong Guava Health Industry Co Ltd
Priority to CN201720807161.0U priority Critical patent/CN206881200U/en
Application granted granted Critical
Publication of CN206881200U publication Critical patent/CN206881200U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0211Solvent extraction of solids in combination with an electric or magnetic field
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0215Solid material in other stationary receptacles
    • B01D11/0253Fluidised bed of solid materials
    • B01D11/0257Fluidised bed of solid materials using mixing mechanisms, e.g. stirrers, jets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D11/00Solvent extraction
    • B01D11/02Solvent extraction of solids
    • B01D11/0261Solvent extraction of solids comprising vibrating mechanisms, e.g. mechanical, acoustical
    • B01D11/0265Applying ultrasound

Abstract

The utility model discloses a kind of multi-functional plant to extract separation integrated apparatus, including extractor, pump, centrifuge, membrane separation device and extract solution storage bin, the discharging opening of extractor is connected by the first pipeline with the entrance of pump, the outlet of pump is connected by second pipe with the entrance of centrifuge, the outlet of centrifuge is connected by the 3rd pipeline with the entrance of membrane separation device, the outlet of membrane separation device is connected by the 4th pipeline with extract solution storage bin, and extractor is internally provided with water recirculator, supersonic generator and microwave generator.The multi-functional plant extraction separation integrated apparatus of the structure, has the advantages that extraction efficiency is high, extraction effect is good and reduces the loss of effective ingredients in plant.

Description

A kind of multi-functional plant extracts separation integrated apparatus
Technical field
It the utility model is related to a kind of multi-functional plant extraction separation integrated apparatus.
Background technology
Active skull cap components in plant have broad application prospects in fields such as medicine, food, chemical industry.Improve plant The recovery rate of active ingredient, shorten process cycle, reduce energy consumption, be always the emphasis of plant extract research.Traditional carries Taking technique equipment continues to use the extractor of jacket type, is gradually heating to Extracting temperature by the way of jacket steam or heating water bath more (such as 100 DEG C of water extraction), the soluble constituents after holding certain time in plant are gradually extracted into solvent.It is however, this Traditional extraction equipment, which does not only exist equipment processing difficulties, manufacturing cost height while extraction process, to be needed to be heated at high temperature, and is expended big The heat energy of amount, causes production cost to raise, and production efficiency reduces.In addition, in high temperature environments, the active ingredient in plant is easy Destroyed, it is difficult to targetedly extract certain active ingredient.In current green low-carbon economy and efficiently quick high-volume is raw In the case that production increasingly protrudes, this traditional production equipment and mode obviously lack the market competitiveness.
Ultrasonic wave-microwave radiation exaraction is extractive technique emerging in recent years.When ultrasonic wave-microwave is propagated in media as well When, because ultrasonic wave-microwave interacts with medium, so as to produce a series of effect of mechanics, calorifics, electromagnetism.Grind Study carefully and show, ultrasonic wave can make plant cell wall produce hole, be advantageous to the dissolution of the target compound in cell, can promote Mass transport process.In addition, ultrasonic wave can also reduce raw meal particle size, so as to increase the contact area of material and solvent, be advantageous to mesh Mark the extraction of compound.Microwave by intracellular polar water molecules or can be extracted material absorbing and produce amount of heat, make thin Intracellular temperature rises rapidly, and pressure caused by water vapor can break through cell membrane and cell membrane, forms larger mass transfer channel, from And promote the extraction of target compound.
That announces in recent years, which is related to the equipment that microwave or ultrasonic assistant extract, is mainly:(1) merely using microwave or Extracted using ultrasonic assistant merely, its extraction efficiency is limited;(2) ultrasonic wave-Microwave Extraction device is placed in simultaneously closed Formula high pressure extraction tank and open atmospheric extraction device.The former is fine to the intensity and sealing requirements for extracting tank material, safe Property is poor, not easy-to-search failure and maintenance and expensive.The latter tends not to the heat and regulation extraction temperature inside control device Degree, some thermal instability target compounds may be caused to degrade when temperature is too high.In addition, in the prior art, vegetable active into The extraction and separation divided is all independent separate operation.The mode filtered again with filter screen (filter cloth) after extraction carries out filtering point From because the reduction of extract solution temperature easily causes filter net jam, plant residue residual, separation is not thorough, need to repeatedly change filter screen Deng, the purpose of simplified technique can not be reached, be unfavorable for industrialized production.
Utility model content
In view of this, the purpose of this utility model is to provide a kind of multi-functional plant extraction separation integrated apparatus, solves Above mentioned problem.
The utility model is solved the above problems by following technological means:A kind of multi-functional plant extraction isolation integral dress Put, including extractor, pump, centrifuge, membrane separation device and extract solution storage bin, the discharging opening of extractor pass through the first pipeline Connected with the entrance of pump, the outlet of pump is connected by second pipe with the entrance of centrifuge, and the outlet of centrifuge passes through the 3rd pipe Road is connected with the entrance of membrane separation device, and the outlet of membrane separation device is connected by the 4th pipeline with extract solution storage bin, extraction Tank is internally provided with water recirculator, supersonic generator and microwave generator.
Further, it is provided with stirring structure on the extractor.
Further, the stirring structure include being centrally positioned in motor at the top of extractor, by motor-driven rotation and The agitating shaft stretched into extractor and the agitating paddle being distributed on agitating shaft.
Further, in addition to controller, the pump, centrifuge, membrane separation device, water recirculator, ultrasonic wave occur Device, microwave generator and motor control with controller connect respectively.
Further, in addition to condensation reflux device, the entry and exit of the condensation reflux device connect with extractor respectively.
Further, thermometer and liquid level gauge are provided with the extractor.
Further, the exit of the pump is connected with threeway, and the one outlet of threeway passes through second pipe and centrifuge Entrance is connected, and another outlet of threeway is connected by return duct with extractor.
Further, in addition to return duct the sealant supplement cylinder connected.
Further, the extractor open top, top cover is provided with opening.
The beneficial effects of the utility model:
1. employing no chuck microwave heating arrangement substitutes conventional vapor or water-bath chuck heating arrangement, equipment system is reduced This is caused, while the energy consumption reduced.Extractor use simultaneously can open lid mode, and easily maintenance and maintenance, reduce maintenance Cost.
2. installing supersonic generator and microwave generator simultaneously in extractor, the cavitation effect of ultrasonic wave is taken full advantage of Should be with mechanism and the rapid and uniform heating of microwave the characteristics of, extraction time is greatly shortened, improve production yield.Meanwhile Stirring structure is installed on extractor, is used cooperatively jointly with supersonic generator and microwave generator so that material is with surpassing Sound wave and microwave reaction are more uniformly distributed, and enhance extraction effect.
3. being provided with water recirculator in extractor, the effect to cool immediately can be achieved, adjust carrying in extractor Temperature is taken, avoids destruction of the high temperature to thermal activity material in extractor.
4. being provided with the centrifuge of separation of solid and liquid in extraction equipment rear end, on the one hand plant extract residue can be carried out at dehydration Reason, in case follow-up comprehensive utilization, on the other hand, can make extract solution flow through membrane separation device in a heated state, be not easily blocked, and Speed is fast, reduces the loss of effective ingredients in plant.
5. extraction separator of the present utility model, extracting and developing step is combined, simplifies technique, is shortened Time, industrialization, scale extraction production can be achieved.
Brief description of the drawings
The utility model is further described with reference to the accompanying drawings and examples.
Fig. 1 is structural representation of the present utility model.
Embodiment
The utility model is described in detail below with reference to accompanying drawing, as shown in Figure 1:The utility model provides one kind Multi-functional plant extracts separation integrated apparatus, including extractor 1, pump 19, centrifuge 16, membrane separation device 17 and extract solution Storage bin 18, the extractor open top, opening is provided with top cover 4, charging aperture 5 is provided with the top cover, extract Pot sidewall is provided with solvent inlet, thermometer 11 and liquid level gauge 12, and close to extractor top layout, thermometer is used to survey thermometer The temperature of extract solution is measured, liquid level gauge connects with extraction top tank structure, and extraction pot bottom is provided with discharging opening 6, the discharging opening of extractor Connected by the first pipeline with the entrance of pump, the outlet of pump is connected by second pipe with the entrance of centrifuge, and centrifuge goes out Mouth is connected by the 3rd pipeline with the entrance of membrane separation device, and the outlet of membrane separation device passes through the 4th pipeline and extract solution stores Case connects, and extractor is internally provided with water recirculator 13, supersonic generator 2 and microwave generator 3, extractor side Wall is provided with the cooling water inlet connected with water recirculator and coolant outlet, and microwave generator is arranged on the interior of extractor Both sides among side, supersonic generator are arranged on the bottom of extractor, and the centrifuge is horizontal centrifuge, for ease of to extraction The flowing of liquid is controlled, it may be considered that valve 20 is set on the first pipeline, second pipe and the 3rd pipeline.Using the knot The plant extract separation integrated apparatus of structure, has the following advantages that:1. employ the heating of no chuck microwave substitute conventional vapor or Water-bath chuck heating arrangement, reduce equipment manufacturing costs, while the energy consumption reduced.Extractor use simultaneously can open lid side Formula, easily maintenance and maintenance, reduce maintenance cost;2. supersonic generator is installed simultaneously in extractor and microwave occurs Device, the characteristics of taking full advantage of the cavitation effect and mechanism and the rapid and uniform heating of microwave of ultrasonic wave, greatly shorten and carry The time is taken, improves production yield;3. being provided with water recirculator in extractor, the effect to cool immediately, regulation can be achieved Extracting temperature in extractor, avoid destruction of the high temperature to thermal activity material in extractor;4. set in extraction equipment rear end There is the centrifuge of separation of solid and liquid, on the one hand plant extract residue can be subjected to dewater treatment, in case follow-up comprehensive utilization, the opposing party Face, extract solution can be made to flow through membrane separation device in a heated state, be not easily blocked, and speed is fast, reduces effective ingredients in plant Loss;5. extraction separator of the present utility model, extracting and developing step is combined, simplifies technique, when shortening Between, industrialization, scale extraction production can be achieved.
As the further improvement to above-mentioned technical proposal, stirring structure, the stirring knot are provided with the extractor Structure includes being centrally positioned in motor 7 at the top of extractor, by motor-driven rotation and the agitating shaft 8 stretched into extractor and The agitating paddle 9 being distributed on agitating shaft.Stirring structure is installed on extractor, with supersonic generator and microwave generator It is used cooperatively jointly so that material is more uniformly distributed with ultrasonic wave and microwave reaction, enhances extraction effect.
As the further improvement to above-mentioned technical proposal, in addition to controller 15, the pump, centrifuge, UF membrane dress Put, water recirculator, supersonic generator, microwave generator and motor control with controller connect respectively.Pass through control Device cooperates between controlling each component, improves the convenience of operation.
As the further improvement to above-mentioned technical proposal, in addition to condensation reflux device 10, the going out of the condensation reflux device, Entrance connects with extractor respectively.
As the further improvement to above-mentioned technical proposal, the exit of the pump is connected with threeway, and one of threeway goes out Mouth is connected by second pipe with the entrance of centrifuge, and another outlet of threeway is connected by return duct with extractor, is also wrapped The sealant supplement cylinder 14 connected with return duct is included, valve is also equipped with return duct.The circulation for the being arranged to extract solution extraction of return duct Provide feasibility.
Finally illustrate, above example is only unrestricted to illustrate the technical solution of the utility model, although ginseng The utility model is described in detail according to preferred embodiment, it will be understood by those within the art that, can be to this The technical scheme of utility model is modified or equivalent substitution, without departing from the objective and model of technical solutions of the utility model Enclose, it all should cover among right of the present utility model.

Claims (9)

1. a kind of multi-functional plant extracts separation integrated apparatus, it is characterised in that:Including extractor, pump, centrifuge, UF membrane Device and extract solution storage bin, the discharging opening of extractor are connected by the first pipeline with the entrance of pump, and the outlet of pump passes through Two pipelines are connected with the entrance of centrifuge, and the outlet of centrifuge is connected by the 3rd pipeline with the entrance of membrane separation device, film point Outlet from device is connected by the 4th pipeline with extract solution storage bin, and extractor is internally provided with water recirculator, surpassed Sonic generator and microwave generator.
2. multi-functional plant according to claim 1 extracts separation integrated apparatus, it is characterised in that:On the extractor It is provided with stirring structure.
3. multi-functional plant according to claim 2 extracts separation integrated apparatus, it is characterised in that:The stirring structure Including being centrally positioned in motor at the top of extractor, by motor-driven rotation and the agitating shaft stretched into extractor and distribution Agitating paddle on agitating shaft.
4. multi-functional plant according to claim 3 extracts separation integrated apparatus, it is characterised in that:Also include control Device, the pump, centrifuge, membrane separation device, water recirculator, supersonic generator, microwave generator and motor difference Control and connect with controller.
5. multi-functional plant according to claim 1 extracts separation integrated apparatus, it is characterised in that:Also include condensing back Device is flowed, the entry and exit of the condensation reflux device connect with extractor respectively.
6. multi-functional plant according to claim 1 extracts separation integrated apparatus, it is characterised in that:On the extractor It is provided with thermometer and liquid level gauge.
7. multi-functional plant according to claim 1 extracts separation integrated apparatus, it is characterised in that:The outlet of the pump Place is connected with threeway, and the one outlet of threeway is connected by second pipe with the entrance of centrifuge, and another outlet of threeway is logical Return duct is crossed to connect with extractor.
8. multi-functional plant according to claim 7 extracts separation integrated apparatus, it is characterised in that:Also include and backflow The sealant supplement cylinder of pipe connection.
9. the multi-functional plant extraction separation integrated apparatus according to claim 1-8 any one, it is characterised in that:Institute Extractor open top is stated, opening is provided with top cover.
CN201720807161.0U 2017-07-05 2017-07-05 A kind of multi-functional plant extracts separation integrated apparatus Expired - Fee Related CN206881200U (en)

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Application Number Priority Date Filing Date Title
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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108568138A (en) * 2018-07-09 2018-09-25 山东端信堂大禹药业有限公司 A kind of device and its extracting method extracting tanshinone compound from Radix Salviae Miltiorrhizae
CN108607234A (en) * 2018-04-04 2018-10-02 俞潺潺 A kind of traditional Chinese medicine extraction device
CN111849622A (en) * 2020-08-13 2020-10-30 河南省农业科学院 Biphase leaching automation device for flavor seasoning oil
CN112535953A (en) * 2019-09-21 2021-03-23 龙岩市瑞泽环保科技有限公司 Membrane classification and separation process for plant extraction industry
IT202000023539A1 (en) * 2020-10-06 2022-04-06 Packtin S R L EXTRACTION PLANT
TWI831481B (en) * 2022-11-22 2024-02-01 國立屏東科技大學 Extraction system and preparation method of plant milk powder

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108607234A (en) * 2018-04-04 2018-10-02 俞潺潺 A kind of traditional Chinese medicine extraction device
CN108568138A (en) * 2018-07-09 2018-09-25 山东端信堂大禹药业有限公司 A kind of device and its extracting method extracting tanshinone compound from Radix Salviae Miltiorrhizae
CN112535953A (en) * 2019-09-21 2021-03-23 龙岩市瑞泽环保科技有限公司 Membrane classification and separation process for plant extraction industry
CN111849622A (en) * 2020-08-13 2020-10-30 河南省农业科学院 Biphase leaching automation device for flavor seasoning oil
CN111849622B (en) * 2020-08-13 2023-07-04 河南省农业科学院 Automatic biphase leaching device for flavored seasoning oil
IT202000023539A1 (en) * 2020-10-06 2022-04-06 Packtin S R L EXTRACTION PLANT
WO2022074467A1 (en) * 2020-10-06 2022-04-14 Packtin S.R.L. Extraction system
TWI831481B (en) * 2022-11-22 2024-02-01 國立屏東科技大學 Extraction system and preparation method of plant milk powder

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CF01 Termination of patent right due to non-payment of annual fee

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