CN204017401U - A kind of ultrasonic extraction and ultrasonic evaporation and concentration integration apparatus - Google Patents
A kind of ultrasonic extraction and ultrasonic evaporation and concentration integration apparatus Download PDFInfo
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- CN204017401U CN204017401U CN201420375176.0U CN201420375176U CN204017401U CN 204017401 U CN204017401 U CN 204017401U CN 201420375176 U CN201420375176 U CN 201420375176U CN 204017401 U CN204017401 U CN 204017401U
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- storage tank
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- type evaporimeter
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Abstract
The utility model relates to a kind of ultrasonic extraction and ultrasonic evaporation and concentration integration apparatus, steam boiler water inlet is connected at water tank first filling pipe end place, steam boiler venthole connects ultrasonic type evaporimeter air intake, ultrasonic type evaporation feed liquor mouth connects preheating can discharging opening, ultrasonic type evaporimeter discharge outlet installs three-way connection, and wherein a branch road connects extract storage tank; Ultrasonic type evaporimeter steam drain is connected with separator import, separator first exports and is connected with parting liquid storage tank, separator second exports the medium entrance that to be cooled with condenser and is connected, the condenser media outlet that is cooled is connected with condensed water storage tank, condenser cooling medium inlet is connected with water tank second filling pipe end, the outlet of condenser cooling medium is connected with the import of water tank condensed water, and another branch road of ultrasonic type evaporimeter discharge outlet is connected with concentrate storage tank, and vavuum pump is arranged on the pipeline of each storage tank.The utility model have extract evenly, the advantage such as circulation rate is fast, less scaling, convenient cleaning and maintenance.
Description
Technical field
The utility model belongs to extraction and evaporation and concentration field, particularly a kind of ultrasonic extraction and ultrasonic evaporation and concentration integration apparatus.
Background technology
Ultrasonic wave, since generation, has been widely used in the fields such as food, health care and household electrical appliances, has shown as the aspects such as ultrasonic extraction, ultrasonic sterilizing, ultrasound filtration, ultrasonic cleaning.In recent years, the application of ultrasonic technique in Chinese medicine preparation extraction process receives concern and the research of Chinese scholars, and research contents is mainly the research of small scale experiments room ultrasonic extraction process.
In the extraction process of current plant chemical ingredient, be all generally adopt electrical heating, local temperature raises, and causes extraction uneven, occurs " paste tank " phenomenon.
Calandria type evaporator is common a kind of evaporation concentration equipment, and its circulation rate is lower, generally at below 0.4m/s-0.5m/s.And constantly circulate due to solution, make the solution composition in tube bank all the time close to the composition completing liquid, thus the viscosity of solution is large, boiling point is high, effective temperature difference reduces, easily produces fouling.In addition, equipment cleaning and maintenance also convenient not.Therefore, it is not serious that existing calandria type evaporator is applicable to Steaming structure, and have a small amount of crystallization and the less solution of corrosivity, the scope of application is less.
Existing extraction concentrator is generally all the form that extraction equipment separates with evaporation concentration equipment, and make whole process structure more very complicated, efficiency is low, and cost is high, and power consumption is large.
Summary of the invention
The purpose of this utility model be to provide a kind of scientific structure design rationally, extract evenly, circulation rate is fast, solution property good, less scaling, convenient cleaning and maintenance, applied widely, the simple ultrasonic extraction of technique and ultrasonic evaporation and concentration integration apparatus.
The utility model solves its technical problem and is achieved through the following technical solutions:
A kind of ultrasonic extraction and ultrasonic evaporation and concentration integration apparatus, comprise ultrasonic type evaporimeter, it is characterized in that: also comprise water tank, steam boiler, preheating can, filter, extract storage tank, separator, condenser, vavuum pump, condensed water storage tank, parting liquid storage tank and concentrate storage tank, connected the water inlet of steam boiler by the first water pump at the first filling pipe end place of described water tank, the venthole of steam boiler connects the air intake of ultrasonic type evaporimeter, the charging aperture of ultrasonic type evaporimeter is connected the discharging opening of preheating can with spinner flowmeter by centrifugal pump, the discharge outlet of ultrasonic type evaporimeter installs a three-way connection, wherein one is connected and installed the extract storage tank of filter by the branch road extracting Valve controlling, the described steam drain of ultrasonic type evaporimeter is connected with the import of separator, first outlet of separator is connected with parting liquid storage tank, second outlet of separator is connected with the cooled medium entrance of described condenser, the cooled media outlet of condenser is connected with condensed water storage tank, the cooling medium inlet of condenser is connected with the second filling pipe end of water tank by the second water pump, the cooling medium outlet of condenser is connected with the condensed water import of water tank, another branch road that ultrasonic type evaporimeter discharge outlet is provided with concentrated valve is connected with concentrate storage tank, described vavuum pump is arranged on and connects condensed water storage tank, parting liquid storage tank, on the pipeline of concentrate storage tank and extract storage tank.
Advantage of the present utility model and beneficial effect are:
1. a ultrasonic extraction and ultrasonic evaporation and concentration integration apparatus, by the extraction equipment of traditional separately work separately and evaporation concentration equipment are combined as a whole, enormously simplify technological process, the space layout of equipment is rationalized, improve extraction thickening efficiency.By the extracting method of traditional electrical heating type is designed to steam-heated method, extract and material are heated rapidly and thermally equivalent, avoid " paste tank " problem caused because of electrical heating.Due to the Pressure Drop formed between central circulating tube and heating tube inside, material circulates along with extract, material is extracted more abundant.The ultrasonic transducer of ultrasonic type evaporimeter is utilized to produce ultrasonic wave, under hyperacoustic booster action, can make to produce cavitation, mechanism, fuel factor etc. in extract to increase goods and materials molecular motion frequency, speed, produce localized hyperthermia's high pressure, increase solvent penetration power, thus improve material component leaching rate, greatly shorten extraction time and economize energy.Same ultrasonic leaching process without the need to heating, under the state that Steam Heating is closed, can be used for the extraction of heat-sensitive ingredients; In evaporation and concentration section, evaporated liquor, under hyperacoustic effect, produces ultrasonic cavitation in heating clamber, and in vaporization chamber, liquid surface produces ultrasonic atomizatio, compared with prior art, thus substantially increases disengagement area, turbulivity, Pressure Drop and steam rate of volatilization.Can make evaporated liquor at a lower temperature, complete evaporation fast in the short period.Reduce the surface tension of evaporated liquor simultaneously, reduce nucleation barrier, promote the energy exchange of solution inside, increase vaporization nucleation probability.Ultrasonic wave for fouling in heating clamber prevent and removal has a significant effect, thus increase heat transfer coefficient, liquor evaporation processes is strengthened.Higher cocnentration factor can be obtained, for thermal sensitivity weak solution material concentrated provides a comparatively suitable approach at single-effect evaporation system.
2. the utility model scientific structure design is reasonable, have extract evenly, circulation rate is fast, solution property good, less scaling, convenient cleaning and maintenance, applied widely, the simple advantage of technique, be a kind of to there is the ultrasonic extraction of higher innovation and ultrasonic evaporation and concentration integration apparatus.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model;
Fig. 2 is the structural representation of the utility model ultrasonic type evaporimeter.
Description of reference numerals:
1-preheating can, 2-centrifugal pump, 3-spinner flowmeter, 4-ultrasonic type evaporimeter, 5-separator, 6-steam boiler, 7-first water pump, 8-water tank, 9-second water pump, 10-condenser, 11-pipeline, 12-concentrates valve, 13-extracts valve, 14-filter, 15-extract storage tank, 16-concentrate storage tank, 17-parting liquid storage tank, 18-condensed water storage tank, 19-vavuum pump, the steam drain of 20-ultrasonic type evaporimeter, the charging aperture of 21-ultrasonic type evaporimeter, 22-ultrasonic transducer, the discharging opening of 23-ultrasonic type evaporimeter, the air intake of 24-ultrasonic type evaporimeter.
Detailed description of the invention
Below by specific embodiment, the utility model is described in further detail, and following examples are descriptive, is not determinate, can not limit protection domain of the present utility model with this.
A kind of ultrasonic extraction and ultrasonic evaporation and concentration integration apparatus, comprise ultrasonic type evaporimeter 4, its innovation is: also comprise water tank 8, steam boiler 6, preheating can 1, filter 14, extract storage tank 15, separator 5, condenser 10, vavuum pump 19, condensed water storage tank 18, parting liquid storage tank 17 and concentrate storage tank 16, connected the water inlet of steam boiler by the first water pump 7 at the first filling pipe end place of described water tank, the venthole of steam boiler connects the air intake 24 of ultrasonic type evaporimeter, the charging aperture 21 of ultrasonic type evaporimeter is connected the discharging opening of preheating can by centrifugal pump 2 and spinner flowmeter 3, a three-way connection is installed at discharging opening 23 place of ultrasonic type evaporimeter, wherein one by the extract storage tank extracting the branch road that controls of valve 13 and be connected and installed filter, the steam drain 20 of described ultrasonic type evaporimeter is connected with the import of separator, first outlet of separator is connected with parting liquid storage tank, second outlet of separator is connected with the cooled medium entrance of described condenser, the cooled media outlet of condenser is connected with condensed water storage tank, the cooling medium inlet of condenser is connected with the second filling pipe end of water tank by the second water pump 9, the cooling medium outlet of condenser is connected with the condensed water import of water tank, another branch road that ultrasonic type evaporimeter discharge outlet is provided with concentrated valve 12 is connected with concentrate storage tank, described vavuum pump is arranged on and connects condensed water storage tank, parting liquid storage tank, on the pipeline 11 of concentrate storage tank and extract storage tank.
Described ultrasonic type evaporimeter is by lower tube box, shell, shell and the ultrasonic transducer 22 of upper tube box composition are formed, upper perforated plate is welded in shell, lower perforated plate, install between upper perforated plate with lower perforated plate and be fixedly connected with one group of heat exchanger tube, central circulating tube is fixedly mounted with at the medium position of this group of heat exchanger tube, shell arranges air intake, shell arranges the charging aperture being positioned at central circulating tube top, the top of upper tube box is shaped with steam drain, the bottom of lower tube box is shaped with discharging opening, a support is fixedly mounted with in lower tube box, this support is installed with the ultrasonic transducer be made up of one group of compound bar PZT (piezoelectric transducer).
Operation principle of the present utility model:
This technique generally can be divided into Liang Ge workshop section: ultrasonic extraction section and ultrasonic evaporation and concentration section.
Ultrasonic extraction section: 1. to water filling in water tank to liquid level face, opens the first water pump to water delivery in steam boiler, starts steam boiler; 2. material is put into preheating can, and be heated to temperature required rear unlatching centrifugal pump, be fed to ultrasonic type evaporimeter; 3. start ultrasonic type evaporimeter, utilize ultrasonic wave to carry out assisted extraction; 4. to be extracted complete, open and extract valve, make material and extract enter filter and filter, collect extract afterwards to extract storage tank.
As material need repeatedly extract, the material in filter need be taken out and repeat step 1 to 3.
If for the extraction of heat-sensitive ingredients, change, directly from step 2 for avoiding the drug ingedient structure caused by heating factors.
Ultrasonic evaporation and concentration section: 1. to water filling in water tank to liquid level face, opens the first water pump to water delivery in steam boiler, starts steam boiler; 2. open vavuum pump and the second water pump, open the valve at each storage tank upper feeding mouth place simultaneously, make whole system be in required vacuum state; 3. the extract in collection extract storage tank enters preheating can and carries out preheating, and open the valve of steam boiler, make steam preheating ultrasonic type evaporimeter, liquid temp to be extracted reaches required preheat temperature simultaneously, starts charging; 4. separator is cyclone separator, it is for being separated the solid material be mixed in steam, steam generates cooling water by condenser and is stored in condensed water storage tank, the material storing be mingled with is in parting liquid storage tank, to be concentratedly to complete, open concentrated valve, collect concentrate in concentrate storage tank.
As needed repeatedly evaporation and concentration, the concentrate in concentrate storage tank need be re-injected in preheating can, repeating 1 to 4 steps, until concentrate reaches necessary requirement.
Although disclose embodiment of the present utility model and accompanying drawing for the purpose of illustration, but it will be appreciated by those skilled in the art that: in the spirit and scope not departing from the utility model and claims, various replacement, change and amendment are all possible, therefore, scope of the present utility model is not limited to the content disclosed in embodiment and accompanying drawing.
Claims (1)
1. a ultrasonic extraction and ultrasonic evaporation and concentration integration apparatus, comprise ultrasonic type evaporimeter, it is characterized in that: also comprise water tank, steam boiler, preheating can, filter, extract storage tank, separator, condenser, vavuum pump, condensed water storage tank, parting liquid storage tank and concentrate storage tank, connected the water inlet of steam boiler by the first water pump at the first filling pipe end place of described water tank, the venthole of steam boiler connects the air intake of ultrasonic type evaporimeter, the charging aperture of ultrasonic type evaporimeter is connected the discharging opening of preheating can with spinner flowmeter by centrifugal pump, the discharge outlet of ultrasonic type evaporimeter installs a three-way connection, wherein one is connected and installed the extract storage tank of filter by the branch road extracting Valve controlling, the described steam drain of ultrasonic type evaporimeter is connected with the import of separator, first outlet of separator is connected with parting liquid storage tank, second outlet of separator is connected with the cooled medium entrance of described condenser, the cooled media outlet of condenser is connected with condensed water storage tank, the cooling medium inlet of condenser is connected with the second filling pipe end of water tank by the second water pump, the cooling medium outlet of condenser is connected with the condensed water import of water tank, another branch road that ultrasonic type evaporimeter discharge outlet is provided with concentrated valve is connected with concentrate storage tank, described vavuum pump is arranged on and connects condensed water storage tank, parting liquid storage tank, on the pipeline of concentrate storage tank and extract storage tank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420375176.0U CN204017401U (en) | 2014-07-08 | 2014-07-08 | A kind of ultrasonic extraction and ultrasonic evaporation and concentration integration apparatus |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201420375176.0U CN204017401U (en) | 2014-07-08 | 2014-07-08 | A kind of ultrasonic extraction and ultrasonic evaporation and concentration integration apparatus |
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| CN204017401U true CN204017401U (en) | 2014-12-17 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201420375176.0U Withdrawn - After Issue CN204017401U (en) | 2014-07-08 | 2014-07-08 | A kind of ultrasonic extraction and ultrasonic evaporation and concentration integration apparatus |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104138670A (en) * | 2014-07-08 | 2014-11-12 | 四川理工学院 | Process for extracting and concentrating total flavone in hawthorn |
| CN105060602A (en) * | 2015-09-17 | 2015-11-18 | 天津科技大学 | Industrial wastewater ultrasonic cooperative treatment and ultrasonic evaporative crystallization integrated technology and device |
| CN108682271A (en) * | 2018-05-08 | 2018-10-19 | 河南莱帕克化工设备制造有限公司 | Multiple-effect evaporation and crystallization production practice instructional device |
-
2014
- 2014-07-08 CN CN201420375176.0U patent/CN204017401U/en not_active Withdrawn - After Issue
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104138670A (en) * | 2014-07-08 | 2014-11-12 | 四川理工学院 | Process for extracting and concentrating total flavone in hawthorn |
| CN104138670B (en) * | 2014-07-08 | 2016-02-03 | 四川理工学院 | A kind of extraction concentration technique of hawthorn fruit total flavone |
| CN105060602A (en) * | 2015-09-17 | 2015-11-18 | 天津科技大学 | Industrial wastewater ultrasonic cooperative treatment and ultrasonic evaporative crystallization integrated technology and device |
| CN105060602B (en) * | 2015-09-17 | 2017-05-24 | 天津科技大学 | Industrial wastewater ultrasonic cooperative treatment and ultrasonic evaporative crystallization integrated technology and device |
| CN108682271A (en) * | 2018-05-08 | 2018-10-19 | 河南莱帕克化工设备制造有限公司 | Multiple-effect evaporation and crystallization production practice instructional device |
| CN108682271B (en) * | 2018-05-08 | 2023-12-19 | 河南莱帕克化工设备制造有限公司 | Practical training teaching device for multi-effect evaporation and crystallization production |
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| Date | Code | Title | Description |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| AV01 | Patent right actively abandoned |
Granted publication date: 20141217 Effective date of abandoning: 20160203 |
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| C25 | Abandonment of patent right or utility model to avoid double patenting |