CN206278904U - A kind of single micro nano structure transfer device - Google Patents

A kind of single micro nano structure transfer device Download PDF

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Publication number
CN206278904U
CN206278904U CN201621241534.4U CN201621241534U CN206278904U CN 206278904 U CN206278904 U CN 206278904U CN 201621241534 U CN201621241534 U CN 201621241534U CN 206278904 U CN206278904 U CN 206278904U
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China
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micro
nano
executor
transfer
nano structure
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CN201621241534.4U
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朱瑞
徐军
刘亚琪
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Peking University
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Peking University
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Abstract

The utility model discloses a kind of single micro nano structure transfer device.Transfer device of the present utility model includes:Microscope, micro-nano executor fixed mount, micro-nano executor, transfer probe and micro-nano structure transfer substrate;There is micro-nano structure transfer substrate periodicity raised platforms and coordinate to mark, by microscope Real Time Observation and the pinpoint transfer for manipulating micro-nano executor, realizing single micro nano structure in situ;The preliminary characterization analysis to micro nano structure can be completed on micro-nano structure transfer substrate;And under microscopical home position observation, lookup in situ single micro nano structure to be transferred is marked by coordinate, and the transfer probe by micro-nano executor extracts it from micro-nano structure transfer substrate, the specified location on target substrate substrate is accurately transferred to again, and transfer positioning precision can be better than 1 micron;Using the principle of Electrostatic Absorption, in the case where the tip probe for ensureing transfer probe is cleaned, not clear impurity will not be introduced in transfer process.

Description

A kind of single micro nano structure transfer device
Technical field
The utility model is related to the pinpoint transfer techniques of single micro nano structure, and in particular to a kind of single micro-nano Structure transfer device.
Background technology
Material and structure under micro-nano-scale be widely used in because of its unique physical and chemical performance information, the energy, The fields such as environment, life science and chemical industry, and increasingly show potential application value.Ground in micro Nano material and structure In studying carefully, generally require to observe and measure the physicochemical characteristics of single structure, such as single-root carbon nano-tube or semiconductor nanowires Electrons transport property, to explore its application in microelectronic component, the optical characteristics of single metal nano flake for another example, with Explore its application in the environment or biology sensor based on optical characteristics, and the single nanostructured with special shape Electron microscope phenetic analysis etc..Additionally, cannot be solved in the research and application of current material and device under macro-scale The problem in science or technical barrier released are also required to find principle or solution under micro/nano-scale, it is therefore desirable to by macroscopic material With device fabrication to micro-nano-scale, then it is conducted a research by microscopic sdIBM-2+2q.p.approach detection mode.
In the processing preparation process of micro Nano material and structure, often numerous structures are mixed, such as useization Learn vapour deposition process and prepare nano wire or solution methods growth nano particle, gather generally in the substrate or solution of mm-scale Ten hundreds of micro-nano materials and structure, and cannot be transferred out of single structure carries out microstructure and properties observation;In addition, After material devices under macro-scale are machined into micro/nano-scale, also generally needing to transfer them to ground in observation instrument Study carefully.The usual use of transfer currently for single micro nano structure is diluted dispersion in the solution, then by solution titration in institute The method on substrate is needed, this disposable batch transfer method cannot be accomplished to be pinpointed for specific micro nano structure first Transfer, the research that the fixed position needed for can only be selected from the micro nano structure being randomly dispersed on a large scale on substrate is right As, secondly, it is impossible to accomplish to carry out secondary transferring for single micro nano structure interested, once micro nano structure is adsorbed to lining On bottom, will be unable to take out again be transferred to carries out other phenetic analysis or processing on other substrate, and the 3rd, the method is easily turning Not clear impurity is introduced during shifting.
Utility model content
In order to the pinpoint for realizing single micro nano structure is shifted, the utility model provides a kind of single micro nano structure Transfer device, the pinpoint transfer of micro nano structure is realized by cleverly designing.
Single micro nano structure transfer device of the present utility model includes:Microscope, micro-nano executor fixed mount, micro-nano behaviour Vertical device, transfer probe and micro-nano structure transfer substrate;Wherein, micro-nano executor fixed mount is rigidly fixed on microscope; Micro-nano executor is rigidly attached on micro-nano executor fixed mount;Transfer probe is arranged on the top of micro-nano executor;Micro-nano knot What structure transfer substrate position was fixed is placed on microscopical sample stage, vacantly carries to be transferred on micro-nano structure transfer substrate Micro nano structure;Micro-nano structure transfer substrate includes substrate, periodic raised platforms and coordinate mark, in surfacing Periodic raised platforms and coordinate mark are formed by micro-nano technology on substrate, coordinate is labeled as on the surface of substrate according to solid The regular label of determining deviation periodic arrangement, forms groove, the point of the width more than transfer probe of groove between raised platforms The width at end.
There is a size for dimension more than 5 μm in single micro nano structure requirement to be transferred, such as quasi- one-dimensional nano line , more than 5 μm, certain length of side of quasi- two-dimensional nano thin slice is more than 5 μm for length;For the micro-nano with a dimension more than raised platforms Rice structure a, part is located in raised platforms, and another part is suspended on the groove between raised platforms.
Microscope uses light microscope, or electron microscope;Microscope includes microscope body, sample stage, object lens With imaging display system;Wherein, microscope body includes mechanical cover, imaging optical path and illuminator;Sample stage, object lens and into As display system is connected to microscope body, sample stage is relative with object lens;Sample stage has horizontal two-dimension position adjustments, height Regulation and rotation regulatory function;The enlargement ratio of object lens is adjustable, and microscope entirety enlargement ratio is up to or more than 2000 ~10000 times, the operating distance of object lens is more than 10mm;Imaging display system is a computer, it is desirable to which it is high to be imaged the speed of response, For example during 500,000 pixel of imaging resolution, frame per second is per second more than 60 frames.
Micro-nano executor includes coarse adjustment executor and fine tuning executor;Wherein, coarse adjustment executor passes through pinion and rack Or Damping sliding rail mechanism carries out three-dimensional position regulation, inclination angle, pivot angle and rotation regulation are carried out by bearing locking mechanism;Coarse adjustment Executor includes coarse adjustment fixing device for installing, coarse position governor motion and coarse adjustment drive link, and coarse adjustment fixing device for installing is fixed On micro-nano executor fixed mount, coarse position governor motion is installed on coarse adjustment fixing device for installing, in coarse position The top of governor motion is rigidly connected coarse adjustment drive link;Fine tuning executor realizes fine three by piezoelectric ceramics or hydraulic mechanism Dimension position adjustments, can reach the position adjustments resolution ratio better than 0.1 micron;Fine tuning executor includes that fixed dress is installed in fine tuning Put, fine tuning position adjusting mechanism, controller and fine tuning drive link, fine tuning is set on the top of coarse adjustment drive link fixed dress is installed Put;Fine tuning position adjusting mechanism is set on fine tuning fixing device for installing, and fine tuning position adjusting mechanism passes through conductor cable or liquid Pressure pipe is connected to controller, is rigidly connected fine tuning drive link on the top of fine tuning position adjusting mechanism.
Transfer probe includes three-dimensional locking mechanism of rotating shaft, probe fix bar and tip probe;Wherein, three-dimensional rotating shaft locking machine Structure is rigidly attached at the top of the fine tuning drive link of the fine tuning executor of micro-nano executor;Installed on three-dimensional locking mechanism of rotating shaft Probe fix bar;It is rigidly connected tip probe on the top of probe fix bar;Under the drive of micro-nano executor, probe energy is shifted Enough carry out position adjustments;Probe fix bar is rigidly connected tip probe and micro-nano executor, and locks machine by three-dimensional rotating shaft Structure can adjust probe fix bar with the angle between the drive link of the fine tuning executor of micro-nano executor;The tip of tip probe Diameter is less than 0.5 micron, is bonded what is shifted in single micro nano structure transfer process by the Electrostatic Absorption effect at tip Single micro nano structure.
Micro-nano structure transfer substrate includes substrate, periodic raised platforms and coordinate mark;Cutting is needed according to experiment The size of substrate;The periodicity raised platforms of substrate surface are shaped as square or circle, size between 5~10 microns, Between 1~3 micron, the spacing of adjacent protrusion platform is the width of groove between 1~3 micron to height;The table of raised platforms Face is polished surface, and flatness is less than 1 nanometer;Coordinate marks the position to each raised platforms on micro-nano structure transfer substrate It is accurately positioned.
Advantage of the present utility model:
The utility model dexterously devises the micro-nano structure transfer substrate marked with periodicity raised platforms and coordinate, By microscope Real Time Observation and the pinpoint transfer for manipulating micro-nano executor, realizing single micro nano structure in situ;One Aspect, micro-nano structure transfer substrate, can be complete on micro-nano structure transfer substrate used as the substrate base for carrying micro nano structure The preliminary characterization analysis of paired micro nano structure;On the other hand, under microscopical home position observation, by micro-nano structure transfer base Single micro nano structure to be transferred is searched in coordinate mark original position on piece, and can be incited somebody to action by the transfer probe of micro-nano executor It is extracted from micro-nano structure transfer substrate, then is accurately transferred to the specified location on target substrate substrate, transfer positioning Precision can be better than 1 micron;Additionally, transfer method of the present utility model employs the principle of Electrostatic Absorption, ensureing transfer spy In the case that the tip probe of pin is cleaned, not clear impurity will not be introduced in micro nano structure transfer process.
Brief description of the drawings
Fig. 1 is the dimensional structure diagram of one embodiment of single micro nano structure transfer device of the present utility model;
Fig. 2 is the micro-nano structure transfer substrate of one embodiment of single micro nano structure transfer device of the present utility model Schematic diagram;
Fig. 3 is the micro-nano structure transfer substrate of one embodiment of single micro nano structure transfer device of the present utility model On coordinate mark schematic diagram;
The flow chart of the transfer method of Fig. 4 single micro nano structures of the present utility model, wherein, (A) and (B) is visited for transfer Schematic diagram in the groove that the tip of the tip probe of pin enters below single micro nano structure overhanging portion, (C) is above to carry point Head probe drives the schematic diagram of the raised platforms of the single upward out micro-nano structure transfer substrate of micro nano structure, and (D) is single Micro nano structure adsorbs the sophisticated schematic diagram in tip probe by Electrostatic Absorption effect, and (E) is to reduce sample stage height extremely The micro-nano structure transfer substrate fixed on sample stage will not contact the schematic diagram of the tip probe of transfer probe, and (F) is rising Sample stage makes microscope imaging focus on the schematic diagram on the surface of the target substrate substrate of micro nano structure to be received, and (G) is drop The height of low tip probe causes that single micro nano structure is contacted to the schematic diagram on the surface of target substrate substrate, and (H) is tip Remove the schematic diagram of the single micro nano structure for being shifted in the tip of probe.
Specific embodiment
Below in conjunction with the accompanying drawings, the utility model is described further by embodiment.
As shown in figure 1, the single micro nano structure transfer device of the present embodiment includes:Microscope, micro-nano executor are fixed Frame 5, micro-nano executor, transfer probe and micro-nano structure transfer substrate 4.
Microscope includes microscope body 11, sample stage 12, object lens 13 and imaging display system 14;Wherein, microscope master Body 11 includes mechanical cover, imaging optical path and illuminator;Sample stage 12, object lens 13 and imaging display system are connected to micro- Mirror main body, sample stage 12 is relative with object lens 13;Micro-nano executor fixed mount 5 is rigidly fixed and is attached on microscope body 11.
Micro-nano executor includes coarse adjustment executor 21 and fine tuning executor 22;Wherein, coarse adjustment executor 21 is pacified including coarse adjustment Dress fixing device 211, coarse position governor motion 212 and coarse adjustment drive link 213, coarse adjustment fixing device for installing 211 are fixedly mounted On micro-nano executor fixed mount 5, coarse position governor motion 212 is installed on coarse adjustment fixing device for installing 211, in coarse adjustment position The top for putting governor motion 212 is rigidly connected coarse adjustment drive link 213;Fine tuning executor 22 include fine tuning fixing device for installing 221, Fine tuning position adjusting mechanism 222, controller 223 and fine tuning drive link 224, fine tuning peace is set on the top of coarse adjustment drive link 213 Dress fixing device 221;Fine tuning position adjusting mechanism 222, fine tuning position adjusting mechanism are set on fine tuning fixing device for installing 221 222 are connected to controller 223 by conductor cable or hydraulic tube, are rigidly connected carefully on the top of fine tuning position adjusting mechanism 222 Adjust drive link 224.Fine tuning position adjusting mechanism 222 is manipulated in tri- movements in direction of X, Y and Z by controller 223.
Transfer probe includes three-dimensional locking mechanism of rotating shaft 31, probe fix bar 32 and tip probe 33;Wherein, three-dimensional rotating shaft Retaining mechanism 31 is rigidly attached at the top of the fine tuning drive link 224 of the fine tuning executor of micro-nano executor;In three-dimensional spindle lock Probe fix bar 32 is installed in tight mechanism 31;It is rigidly connected tip probe 33 on the top of probe fix bar 32.
As shown in Fig. 2 micro-nano structure transfer substrate 4 includes substrate 41, periodic raised platforms 42 and coordinate mark 44; Periodic raised platforms 42 and coordinate mark 44, raised platforms 42 are formed by micro-nano technology on the substrate 41 of surfacing Between formed groove 43.As shown in figure 3, coordinate mark 44 is have rule according to constant spacing periodic arrangement on the surface of substrate Rule label, to mark the accurate location of periodic raised platforms 42.
The transfer method of the single micro nano structure of the present embodiment, comprises the following steps:
1) micro nano structure is transferred on micro-nano structure transfer substrate:
Volatile non-corrosiveness solution containing micro nano structure is titrated on micro-nano structure transfer substrate;
2) by microscope Real Time Observation and mobile example platform, according to the coordinate mark on micro-nano structure transfer substrate, seek The position of micro nano structure to be transferred is found, micro nano structure to be transferred is moved to field of microscope center;
3) microscope Real Time Observation, is moved to microscopical by the coarse adjustment executor manipulation transfer probe of micro-nano executor Between object lens and sample stage, then the tip of the tip probe of the fine tuning executor control transfer probe for passing through micro-nano executor enters In groove below the overhanging portion of single micro nano structure 5, shown in such as Fig. 4 (A) and (B);
4) tip probe is controlled to be lifted up by the fine tuning executor of micro-nano executor so that the tip of tip probe exists Contacted in uphill process to single micro nano structure bottom, tip probe is carried in continuation, drive single micro nano structure to move upwards It is dynamic, the raised platforms of micro-nano structure transfer substrate are then left, shown in such as Fig. 4 (C);
5) when single micro nano structure completely disengages from raised platforms, single micro nano structure 5 passes through Electrostatic Absorption effect Absorption is at the tip of tip probe, and such as Fig. 4 (D) is shown;
6) further after the height of lifting tip probe, keep the tip of tip probe single micro-nano with Electrostatic Absorption Structure is maintained in the microscopical visual field in existing position, and now microscope imaging focuses on micro-nano structure transfer substrate table The surface of the periodic raised platforms in face, the tip of tip probe and the single micro nano structure of Electrostatic Absorption are regarded in microscope Yezhong is presented blurred picture;
7) microscopical sample stage is controlled, sample stage height is reduced first to safe altitude, safe altitude refers to work as sample In two dimensional surface during mobile example platform, the micro-nano structure transfer substrate fixed on sample stage will not contact transfer probe to platform Shown in tip probe, such as Fig. 4 (E), micro-nano structure transfer substrate is removed, then by the target substrate substrate of micro nano structure to be received 6 are moved in the middle of the microscopical visual field, slowly rise sample stage, microscope imaging is focused on the mesh of micro nano structure to be received The surface of substrate base is marked, shown in such as Fig. 4 (F);
8) according to absorption tip probe tip on single micro nano structure azimuth vernier adjusting sample stage position and Direction, under microscope high power imaging, point is adjusted to by the particular location of micro nano structure to be received on target substrate substrate 6 The tip of head probe and the single micro nano structure of Electrostatic Absorption under the microscope at the position of blurred picture;
9) the slow height for reducing tip probe is controlled by the fine tuning executor of micro-nano executor so that single micro-nano Form touch shown in such as Fig. 4 (G), and is adsorbed on the surface of target substrate substrate to the surface of target substrate substrate 6, then will The single micro nano structure for being shifted is removed at the tip of tip probe, shown in such as Fig. 4 (H), completes turning for single micro nano structure 5 Move past journey.
It is finally noted that, the purpose for publicizing and implementing mode is that help further understands the utility model, but It will be appreciated by those skilled in the art that:Do not departing from the utility model and appended spirit and scope by the claims, respectively It is all possible to plant substitutions and modifications.Therefore, the utility model should not be limited to embodiment disclosure of that, the utility model Claimed scope is defined by the scope that claims are defined.

Claims (8)

1. a kind of single micro nano structure transfer device, it is characterised in that the transfer device includes:Microscope, micro-nano are manipulated Device fixed mount, micro-nano executor, transfer probe and micro-nano structure transfer substrate;Wherein, the micro-nano executor fixed mount rigidity It is fixedly mounted on microscope;The micro-nano executor is rigidly attached on micro-nano executor fixed mount;The transfer probe peace Mounted in the top of micro-nano executor;What the micro-nano structure transfer substrate position was fixed is placed on microscopical sample stage, Micro nano structure to be transferred is vacantly carried on micro-nano structure transfer substrate;The micro-nano structure transfer substrate includes substrate, week Phase property raised platforms and coordinate mark, on the substrate of surfacing by micro-nano technology formed periodic raised platforms and Coordinate is marked, and the coordinate is labeled as the regular label according to constant spacing periodic arrangement on the surface of substrate, and projection is flat Groove, the sophisticated width of the width more than transfer probe of the groove are formed between platform.
2. transfer device as claimed in claim 1, it is characterised in that the microscope uses light microscope, or electronics Microscope;The microscope includes microscope body, sample stage, object lens and imaging display system;Wherein, microscope body includes Mechanical cover, imaging optical path and illuminator;Sample stage, object lens and imaging display system are connected to microscope body, sample Platform is relative with object lens;There are sample stage horizontal two-dimension position adjustments, height to adjust and rotation regulatory function;The times magnification of object lens Rate is adjustable, and microscope entirety enlargement ratio is up to or more than 2000~10000 times, and the operating distance of object lens is more than 10mm; Imaging display system is a computer.
3. transfer device as claimed in claim 1, it is characterised in that the micro-nano executor includes coarse adjustment executor and fine tuning Executor;Wherein, coarse adjustment executor carries out three-dimensional position regulation by pinion and rack or Damping sliding rail mechanism, by axle Holding retaining mechanism carries out inclination angle, pivot angle and rotation regulation;Coarse adjustment executor includes that coarse adjustment fixing device for installing, coarse position are adjusted Mechanism and coarse adjustment drive link, coarse adjustment fixing device for installing are fixedly mounted on micro-nano executor fixed mount, are installed in coarse adjustment and fixed Coarse position governor motion is installed on device, is rigidly connected coarse adjustment drive link on the top of coarse position governor motion;Fine tuning is grasped Vertical device realizes that fine three-dimensional position is adjusted by piezoelectric ceramics or hydraulic mechanism, and position adjustments resolution ratio is more than 0.1 micron;Carefully Adjusting executor includes fine tuning fixing device for installing, fine tuning position adjusting mechanism, controller and fine tuning drive link, in coarse adjustment drive link Top set fine tuning fixing device for installing;Fine tuning position adjusting mechanism, fine tuning position are set on fine tuning fixing device for installing Governor motion is connected to controller by conductor cable or hydraulic tube, is rigidly connected fine tuning on the top of fine tuning position adjusting mechanism Drive link.
4. transfer device as claimed in claim 1, it is characterised in that the transfer probe include three-dimensional locking mechanism of rotating shaft, Probe fix bar and tip probe;Wherein, three-dimensional locking mechanism of rotating shaft is rigidly attached at the top of micro-nano executor;Turn in three-dimensional Probe fix bar is installed on shaft locking mechanism;It is rigidly connected tip probe on the top of probe fix bar;In micro-nano executor Under drive, transfer probe can carry out position adjustments;Probe fix bar is rigidly connected tip probe and micro-nano executor, and leads to Crossing three-dimensional locking mechanism of rotating shaft can adjust probe fix bar with the angle between the drive link of the fine tuning executor of micro-nano executor Degree.
5. transfer device as claimed in claim 4, it is characterised in that the tip diameter of the tip probe is less than 0.5 micron, The single micro nano structure for being shifted is bonded in single micro nano structure transfer process by the Electrostatic Absorption effect at tip.
6. transfer device as claimed in claim 1, it is characterised in that the shape of the periodicity raised platforms in the micro-nano structure Shape is square or circle, and between 5~10 microns, highly between 1~3 micron, the spacing of adjacent protrusion platform is size The width of groove is between 1~3 micron.
7. transfer device as claimed in claim 6, it is characterised in that the surface of the raised platforms is polished surface, smooth Degree is less than 1 nanometer.
8. transfer device as claimed in claim 1, it is characterised in that the single micro nano structure to be transferred has The size of dimension is more than 5 μm;For the micro nano structure with a dimension more than raised platforms, a part is located at raised platforms On, another part is suspended on the groove between raised platforms.
CN201621241534.4U 2016-11-18 2016-11-18 A kind of single micro nano structure transfer device Withdrawn - After Issue CN206278904U (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106430084A (en) * 2016-11-18 2017-02-22 北京大学 Single micro/nano structure transferring device and single micro/nano structure transferring method
CN111261473A (en) * 2020-03-31 2020-06-09 中山大学 Method for manufacturing single one-dimensional nano-structure field emission cold cathode

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106430084A (en) * 2016-11-18 2017-02-22 北京大学 Single micro/nano structure transferring device and single micro/nano structure transferring method
CN106430084B (en) * 2016-11-18 2017-12-01 北京大学 A kind of single micro nano structure transfer device and its transfer method
CN111261473A (en) * 2020-03-31 2020-06-09 中山大学 Method for manufacturing single one-dimensional nano-structure field emission cold cathode

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