CN206156748U - Chlorine dioxide gas's aerated reactor device - Google Patents
Chlorine dioxide gas's aerated reactor device Download PDFInfo
- Publication number
- CN206156748U CN206156748U CN201621175409.8U CN201621175409U CN206156748U CN 206156748 U CN206156748 U CN 206156748U CN 201621175409 U CN201621175409 U CN 201621175409U CN 206156748 U CN206156748 U CN 206156748U
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- Prior art keywords
- storehouse
- aerated reaction
- chlorine dioxide
- aerated
- aeration
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- OSVXSBDYLRYLIG-UHFFFAOYSA-N dioxidochlorine(.) Chemical compound O=Cl=O OSVXSBDYLRYLIG-UHFFFAOYSA-N 0.000 title claims abstract description 173
- 239000004155 Chlorine dioxide Substances 0.000 title claims abstract description 87
- 235000019398 chlorine dioxide Nutrition 0.000 title claims abstract description 87
- 238000005273 aeration Methods 0.000 claims abstract description 73
- 238000006243 chemical reaction Methods 0.000 claims description 199
- 239000007788 liquid Substances 0.000 claims description 27
- 238000007599 discharging Methods 0.000 claims description 21
- 239000002699 waste material Substances 0.000 claims description 13
- 239000007787 solid Substances 0.000 claims description 9
- 230000007423 decrease Effects 0.000 claims description 8
- 239000000376 reactant Substances 0.000 claims description 8
- 238000006213 oxygenation reaction Methods 0.000 claims description 7
- 238000003780 insertion Methods 0.000 claims description 4
- 230000037431 insertion Effects 0.000 claims description 4
- 239000002994 raw material Substances 0.000 abstract description 55
- 230000007613 environmental effect Effects 0.000 abstract description 7
- 238000000034 method Methods 0.000 abstract description 6
- 230000015572 biosynthetic process Effects 0.000 abstract description 5
- 238000003786 synthesis reaction Methods 0.000 abstract description 4
- 238000005516 engineering process Methods 0.000 abstract description 3
- 231100000957 no side effect Toxicity 0.000 abstract description 2
- 230000002349 favourable effect Effects 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 16
- 230000001276 controlling effect Effects 0.000 description 10
- 239000000463 material Substances 0.000 description 9
- 230000000694 effects Effects 0.000 description 7
- UKLNMMHNWFDKNT-UHFFFAOYSA-M sodium chlorite Chemical compound [Na+].[O-]Cl=O UKLNMMHNWFDKNT-UHFFFAOYSA-M 0.000 description 7
- 229960002218 sodium chlorite Drugs 0.000 description 7
- 239000000919 ceramic Substances 0.000 description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 238000002360 preparation method Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 3
- 239000000460 chlorine Substances 0.000 description 3
- 229910052801 chlorine Inorganic materials 0.000 description 3
- QBWCMBCROVPCKQ-UHFFFAOYSA-N chlorous acid Chemical compound OCl=O QBWCMBCROVPCKQ-UHFFFAOYSA-N 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 229920000728 polyester Polymers 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- XTEGARKTQYYJKE-UHFFFAOYSA-M Chlorate Chemical compound [O-]Cl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-M 0.000 description 2
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 2
- 241000790917 Dioxys <bee> Species 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- XTEGARKTQYYJKE-UHFFFAOYSA-N chloric acid Chemical compound OCl(=O)=O XTEGARKTQYYJKE-UHFFFAOYSA-N 0.000 description 2
- 229910001919 chlorite Inorganic materials 0.000 description 2
- 229910052619 chlorite group Inorganic materials 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 238000004659 sterilization and disinfection Methods 0.000 description 2
- BZSXEZOLBIJVQK-UHFFFAOYSA-N 2-methylsulfonylbenzoic acid Chemical compound CS(=O)(=O)C1=CC=CC=C1C(O)=O BZSXEZOLBIJVQK-UHFFFAOYSA-N 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000013064 chemical raw material Substances 0.000 description 1
- -1 chlorate chloroform Chemical compound 0.000 description 1
- 229940077239 chlorous acid Drugs 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 230000000284 resting effect Effects 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model is suitable for a chlorine dioxide synthesis technology's field provides a chlorine dioxide gas's aerated reactor device, including aerated reactor storehouse group, aerated reactor storehouse group includes and links to each other in order and volume degressive a plurality of aerated reactor storehouse in proper order according to the raw material handling route, all be equipped with feed inlet, discharge gate, aeration mouth and chlorine dioxide gas overfall on the aerated reactor storehouse of every, be equipped with the aeration piece that is used for quantitative aeration in the aerated reactor storehouse of every. The utility model discloses a volume that sets up is organized in degressive aerated reactor storehouse in proper order for chlorine dioxide's raw materials is carrying out the in -process of changeing, and the gaseous purity of chlorine dioxide of production is high, thereby makes chlorine dioxide no side effect in the performance efficiency produce, is favorable to the environmental protection.
Description
Technical field
The utility model belongs to the field of chlorine dioxide synthetic technology, and more particularly to a kind of aeration of chlorine dioxide is anti-
Answer device.
Background technology
Chlorine dioxide has functions that excellent disinfection eliminates the unusual smell, and is increasingly recognized by people in air sterillization application
Know and receive.Chlorine dioxide is a kind of Strong oxdiative gas, and this Strong oxdiative gas is by two or more chemical raw material (such as chlorine
Sour sodium, sodium chlorite adding citric acid or hydrochloric acid etc.) obtained by reacting in gas reaction storehouse Inner.
Although chlorine dioxide has functions that excellent disinfection eliminates the unusual smell, if purity of chlorine dioxide is not high,
The residue of such as chlorite or chlorate chloroform thing will be produced, these residues can cause chlorine dioxide playing effect
While also bring stronger side effect.Specifically, purity of chlorine dioxide is whether completely chlorine dioxide chemical energy changes
As a result embody.Purity is high, produces without chlorate and the accessory substance such as chlorite and chloroform thing, and terminal is used with regard to safety and environmental protection.
Otherwise purity is not high, and the accessory substance that it is produced will bring secondary pollution as chlorine dioxide is used, and be unfavorable for environmental protection.
However, the methods that prior art is primarily directed to chlorine dioxide generation are improved, such as acidization
Preparation method, electrochemical process preparation method, electrolysis preparation method etc.；These various preparation method researchs are how to produce
Chlorine dioxide, and lack research for how to improve purity of chlorine dioxide aspect.The generation chlorine dioxide of such as prior art
Device, there is more improvement in terms of how producing chlorine dioxide, special for the China of " CN105849036A " referring to application publication number
Sharp application documents, solve the problems, such as how continuation produces chlorine dioxide.But, for how structure of reactor makes conjunction
How reason, improve the purity of chlorine dioxide, does not refer to.
Utility model content
Main purpose of the present utility model is the aerated reaction device for providing a kind of chlorine dioxide, it is intended to solve to pass
The low problem of purity of chlorine dioxide of the generation that the aerated reaction device of system chlorine dioxide is present.
The utility model is achieved in that a kind of aerated reaction device of chlorine dioxide, including aerated reaction storehouse
Group；Aerated reaction storehouse group includes the multiple aerated reactions being sequentially connected according to Feedstock treating path and volume successively decreases successively
Storehouse；Charging aperture, discharging opening, aeration opening and chlorine dioxide overfall are equipped with the aerated reaction storehouse of each, often
It is provided with for the aeration block of quantitative aeration in the individual aerated reaction storehouse.
As optimal technical scheme of the present utility model：
Further, the aeration block is provided with connecting hole and multiple solarization air caps, the multiple solarization air cap with it is described
Connecting hole insertion.
Further, the charging aperture and the discharging opening are opened in respectively the left and right two in the aerated reaction storehouse of each
Side；The aeration opening is separately positioned on the bottom in the aerated reaction storehouse of each；The chlorine dioxide overfall difference
It is arranged on the top in the aerated reaction storehouse of each.
Further, aerated reaction storehouse group includes the first aerated reaction storehouse, the second aerated reaction storehouse and the 3rd aeration
Reaction warehouse；The height of the charging aperture in the first aerated reaction storehouse higher than its discharging opening height, the second aerated reaction storehouse
Charging aperture height higher than its discharging opening height, the height of the charging aperture in the 3rd aerated reaction storehouse is higher than its discharging opening
Height.
Further, the volume in the first aerated reaction storehouse, the second aerated reaction storehouse and the 3rd aerated reaction storehouse
Lapse rate is set to 0.5 times.
Further, the first aerated reaction storehouse, the second aerated reaction storehouse and the 3rd aerated reaction storehouse are integrated in
In one housing.
Further, the total amount of reactant liquor in the group of the aerated reaction storehouse is set to 169 with the ratio of aeration total amount：1.
Further, aerated reaction storehouse group is provided with the temperature control for controlling the environment temperature of aerated reaction storehouse group
Part.
Further, aerated reaction storehouse group is also associated with the pneumatic flow for controlling in the group of the aerated reaction storehouse
Reaction controlling storehouse；The reaction controlling storehouse includes the oxygenation air pump for producing tolerance and is connected with the oxygenation air pump
Multiple pneumatic flow meters, the pneumatic flow meter of each is correspondingly connected with the aeration block of each.
Further, aerated reaction storehouse group is connected with for the waste trap of separating treatment waste liquid.
The aerated reaction device of the chlorine dioxide that the utility model is provided, by making a generation chlorine dioxide
The synthesizer of body, in synthesis, raw material passes through the aerated reaction storehouse that charging aperture successively decreases successively into volume to chlorine dioxide
Group carries out multi-stage aeration reaction so that the generating process interlink function in the group of aerated reaction storehouse, and then the raw material of chlorine dioxide exists
During being converted, reaction more fully, make generation chlorine dioxide purity reach it is high so that chlorine dioxide
It is free from side effects generation while effect is played, is conducive to environmental protection.
Description of the drawings
Fig. 1 is the structural representation of the aerated reaction device of the chlorine dioxide that the utility model embodiment is provided；
Fig. 2 is that the stereochemical structure of the aerated reaction device of the chlorine dioxide that the utility model embodiment is provided is illustrated
Figure.
In figure：1- housings, 11- raw material premix conjunction storehouse, 111- material inlets, 112- liquid outlets, 12- aerated reactions storehouse group,
The first aerated reactions of 121- storehouse, 1211- downtake pipes, 1212- charging apertures, the second aerated reactions of 122- storehouse, 1221- second rows
Tracheae, the aerated reaction storehouses of 123- the 3rd, the blast pipes of 1231- the 3rd, 1232- discharging openings, 1233- aeration openings, 1234- chlorine dioxide
Gas overflowing mouth, 124- aeration blocks, 125- chlorine dioxide exhaust mains, 13- reaction controllings storehouse, 131- oxygenation air pumps, 132- gas
Pressure type flowmeter, 14- ceramics temperature control plates, 141- temperature control plate power ports, 15- waste traps, 151- waste discharge liquid pipes.
Specific embodiment
In order that the purpose of this utility model, technical scheme and advantage become more apparent, below in conjunction with accompanying drawing and enforcement
Example, is further elaborated to the utility model.It should be appreciated that specific embodiment described herein is only to explain this
Utility model, is not used to limit the utility model.
It should be noted that when element is referred to as " being fixed on " or " being arranged at " another element, it can be directly another
On one element or it is connected on another element.When an element is referred to as " being connected to " another element, it can be with
It is directly to another element or is indirectly connected to another element.
The utility model provides a kind of aerated reaction device of chlorine dioxide, by arranging according to Feedstock treating road
The aerated reaction storehouse group 12 that footpath is sequentially connected and volume successively decreases successively, so that the chlorine dioxide purity for producing is high, so as to
Make chlorine dioxide have no side effect generation while effect is played, be conducive to environmental protection.
Refer to accompanying drawing 1 and Fig. 2, the aerated reaction device of the chlorine dioxide, including aerated reaction storehouse group 12；Aeration
Reaction warehouse group 12 includes the multiple aerated reaction storehouses being sequentially connected according to Feedstock treating path and volume successively decreases successively；The exposure of each
Charging aperture 1212, discharging opening 1232, aeration opening 1233 and chlorine dioxide overfall 1234 are equipped with solid/liquid/gas reactions storehouse, often
The aeration block 124 for quantitative aeration is provided with individual aerated reaction storehouse.
The aerated reaction device of the chlorine dioxide that the utility model embodiment is provided, by making a generation dioxy
Change the synthesizer of chlorine body, in synthesis, raw material passes through the exposure that charging aperture 111 successively decreases successively into volume to chlorine dioxide
Solid/liquid/gas reactions storehouse group 12 carries out multi-stage aeration reaction so that the generating process interlink function in aerated reaction storehouse group 12, and then dioxy
Change the raw material of chlorine during being converted, reaction more fully, make generation chlorine dioxide purity reach it is high, from
And make chlorine dioxide be free from side effects generation while effect is played, be conducive to environmental protection.
Additionally, it is preferable that storehouse 11 can also be closed by arranging raw material premix, allowed in chlorine dioxide before synthesis
Raw material first closes mixing in storehouse 11 in raw material premix, and mixed raw material enters back into aerated reaction storehouse group 12, and to carry out multi-stage aeration anti-
Should, further help in that chlorine dioxide precursor reactant is more abundant, to improve the purity of chlorine dioxide.
Further, for the ease of the raw material after premixing from the overflow of liquid outlet 112 to the first aerated reaction storehouse 121 in,
Meanwhile, mixed raw material carries out the multi-stage aeration reaction of ladder ground into aerated reaction storehouse group 12, contributes to overall generating process
Interlink function, to improve the purity of chlorine dioxide, aerated reaction storehouse includes being sequentially connected and volume successively decreases successively first
Aerated reaction storehouse 121, the second aerated reaction storehouse 122 and the 3rd aerated reaction storehouse 123；The charging aperture in the first aerated reaction storehouse 121
1212 liquid outlets 112 for closing storehouse 11 with raw material premix are connected, and raw material premix are closed the height of the liquid outlet 112 in storehouse 11 and exposed higher than first
The height of the charging aperture 1212 in solid/liquid/gas reactions storehouse 121.
Additionally, height of the height of the charging aperture 1212 in the first aerated reaction storehouse 121 higher than its discharging opening 1232, second exposes
The height of the charging aperture 1212 in solid/liquid/gas reactions storehouse 122 higher than its discharging opening 1232 height, the charging aperture in the 3rd aerated reaction storehouse 123
Height of 1212 height higher than its discharging opening 1232, it is preferable that difference in height is located between 0.3～0.6cm, in order to form original
Natural inflow of the material from a upper aerated reaction storehouse to next aerated reaction storehouse.
Preferably, charging aperture 1212 and discharging opening 1232 are opened in respectively the left and right sides in the aerated reaction storehouse of each；Expose
Gas port 1233 is separately positioned on the bottom in the aerated reaction storehouse of each；Chlorine dioxide overfall 1234 is separately positioned on each
Aerated reaction storehouse top.Specifically, in the present embodiment, aeration opening 1233 be separately positioned on the first aerated reaction storehouse 121,
Two aerated reaction storehouses 122 and the bottom in the 3rd aerated reaction storehouse 123.Charging aperture 1212, discharging opening 1232 are separately positioned on first
The middle and lower part in aerated reaction storehouse 121, the second aerated reaction storehouse 122 and the 3rd aerated reaction storehouse 123, charging aperture 1212 and discharging opening
1232 left and right two for being opened in the first aerated reaction storehouse 121, the second aerated reaction storehouse 122 and the 3rd aerated reaction storehouse 123 respectively
Side.Chlorine dioxide overfall 1234 is separately positioned on the first aerated reaction storehouse 121, the second aerated reaction storehouse 122 and the 3rd
The top in aerated reaction storehouse 123.It should be noted that, to put it more simply, the first aerated reaction storehouse 121, the second aeration of the present embodiment
Reaction warehouse 122, the charging aperture 1212 in the 3rd aerated reaction storehouse 123, discharging opening 1232, aeration opening 1233 and chlorine dioxide
Overfall 1234 can be indicated using same label, not make differentiation in addition.
Specifically, material inlet 111 could be arranged to two, in order to the raw material by chlorine dioxide is produced respectively by not
Same material inlet 111 imports to raw material premix and closes in storehouse 11.Refinement ground, one of which is led by the first material inlet 111
Enter to raw material premix and close in storehouse 11, another by the raw material of generation chlorine dioxide is imported to by the second material inlet 111
Raw material premix are closed in storehouse 11.
Additionally, it should be noted that, the aerated reaction storehouse group 12 of the utility model embodiment is preferably arranged to three, i.e., suitable
The first aerated reaction storehouse 121, the second aerated reaction storehouse 122 and the 3rd aerated reaction storehouse 123 that secondary connected and volume successively decreases successively.
It is to be appreciated that the first aerated reaction storehouse 121, the second aerated reaction storehouse 122 and the 3rd aerated reaction storehouse 123 are mutually passed through for three
Logical ladder aerated reaction storehouse.Aerated reaction storehouse group 12 includes but is not limited to three aerated reaction storehouses, can be anti-in three aerations
Answering increases the quantity in aerated reaction storehouse on storehouse, in order to the raw material after premixing to be carried out step aeration stripping more than three-level.
In addition it is also possible to be set in the parameter of the relation existed according to three aerated reaction storehouses, parameter is zoomed in or out in proportion,
To meet the different changes to chlorine dioxide demand.
Specifically, the first aerated reaction storehouse 121, the second aerated reaction storehouse 122 and the 3rd aerated reaction storehouse 123 are both designed as
The cylindrical shape of high polyester PVC materials, in order to the raw material after premixing is carried out into three-level step aeration stripping.First aeration is anti-
Storehouse 121 is answered to connect downtake pipe 1211, the connection of the second aerated reaction storehouse 122 second exhaust pipe 1221, the 3rd aerated reaction storehouse
123 the 3rd blast pipes 1231 of connection, downtake pipe 1211, the blast pipe 1231 of second exhaust pipe 1221 and the 3rd are collected to one
To working space on chlorine dioxide exhaust main 125, in order to output after chlorine dioxide is collected.
Further, it is contemplated that raw material premix close the volume of storehouse 11 size, determine raw material enter ratio, enter amount with
And the time speed for entering, meanwhile, the time of the purity of the output of chlorine dioxide and Raw Material Blending Ratio and raw material reaction and
There is direct relation with aeration storage capacity etc., therefore, in order that raw material reacts more fully in rear end step aerated reaction storehouse, enter
And the output for having chlorine dioxide with high purity is caused, raw material premix are closed the volume in storehouse 11 and are set with the total measurement (volume) ratio of aerated reaction storehouse group 12
For 1：13.6；The volume lapse rate in the first aerated reaction storehouse 121, the second aerated reaction storehouse 122 and the 3rd aerated reaction storehouse 123 sets
For 0.5 times.Preferably, the volumetric ratio of volume and the first aerated reaction storehouse 121 that raw material premix close storehouse 11 is set to 1：5, raw material is pre-
The volumetric ratio in the volume of mixing bunker 11 and the second aerated reaction storehouse 122 is set to 1：4.5, raw material premix close the volume and the 3rd in storehouse 11
The volumetric ratio in aerated reaction storehouse 123 is set to 1：4.0.
The setting relation that raw material premix close storehouse 11 and the volume of aerated reaction storehouse group 12 is illustrated below, referring to table 1.Tool
Body ground, premixing storage capacity and the total measurement (volume) ratio of aerated reaction storehouse group 12 are 1：13.6 times, each step aeration storage capacity lapse rate is
0.5 times.The volumetric ratio of volume and the first aerated reaction storehouse 121 that raw material premix close storehouse 11 is set to 1：5, raw material premix close storehouse 11
The volumetric ratio in volume and the second aerated reaction storehouse 122 is set to 1：4.5, raw material premix close the volume in storehouse 11 and the 3rd aerated reaction storehouse
123 volumetric ratio is set to 1：4.0.
Table 1
Because we abide by this volume fraction relation of Xun, so that chlorine dioxide produces purity height.
Further, in the present embodiment, in being raw material in sodium chlorate or sodium chlorite adding citric acid or hydrochloric acid, we select
Sodium chlorite and hydrochloric acid obtain chlorine dioxide for raw material, and its reaction equation is：
2ClO2+H2O-HClO2+HClO3
According to reaction equation, select to add hydrochloric acid to go out chlorine dioxide as raw material reaction with sodium chlorite, set sodium chlorite
Concentration is 7～10%, chooses a concentration point；Concentration of hydrochloric acid is set as 6～9%, a concentration point is chosen, sodium chlorite is set
Solution reaction amount is 75ml/H, set hydrochloric acid solution quantitative response amount draw as 82.5ml/H, then react after chlorine dioxide in theory
Yield should be in more than 5000mg/H.By setting when material concentration and consumption, abide by raw material premixing storehouse 11 in Xun tables 1 and hold
The setting relation of product and the step aeration storage capacity of insertion, then the yield of chlorine dioxide is 5100mg, has reached theoretical quantum of output.
Additionally, in order to further be set by the total amount and the relation of aeration total amount of the reactant liquor in aerated reaction storehouse group 12
It is fixed so that raw material reacts more fully in the group of aeration storehouse, and then cause the output for having chlorine dioxide with high purity, aerated reaction storehouse group
The total amount of the reactant liquor in 12 is set to 169 with the ratio of aeration total amount：1.
Hereinafter citing is set for the total amount of the reactant liquor in aerated reaction storehouse group 12 and the relation of aeration total amount, referring to
Table 2.
Table 2
Take in table 21 citing and further illustrate the total amount of reactant liquor and the setting relation of aeration total amount：Still chlorous acid is taken
Sodium and hydrochloric acid are described as follows as chlorine dioxide reaction raw material：
Its reaction equation is：
2ClO2+H2O-HClo2+HClO3
Sodium chlorite and hydrochloric acid as liquid charging stock premixing after → overflow into and carry out aeration in the first aerated reaction storehouse 121
The volume of liquid storage is that the aeration tolerance of 169.60ml → needs should be maintained in the first aerated reaction storehouse 121 of stripping → now
1.0L/min。
When the raw material of aeration storehouse 1 is overflowed to 169.60ml → raw material overflows into and continues in the second aerated reaction storehouse 122 automatically
The volume of liquid storage is that the aeration tolerance of 141.30ml → needs should be maintained in the second aerated reaction storehouse 122 of aeration stripping → now
0.83L/min。
When the raw material of aeration storehouse 2 is overflowed to 141.30ml → raw material overflows into and continues in the 3rd aerated reaction storehouse 123 automatically
The volume of the liquid storage of the 3rd aerated reaction storehouse 123 of aeration stripping → now is that the aeration tolerance of 113.1ml → needs should be maintained at
0.67L/min。
In above three-level step aeration, each aerated reaction storehouse upper end is designed with chlorine dioxide overfall 1234,
The chlorine dioxide that aeration stripping goes out is facilitated to overflow.Amount further by the reactant liquor in each of the above aerated reaction storehouse is total with aeration
The relation setting of amount, according to this relation step aeration stripping is set for, anti-in order to the aeration in this chlorine dioxide
Answer acquisition chlorine dioxide with high purity gas in device.
Additionally, referring to table 3, the speed that control material rate is entered in aerated reaction storehouse group 12 with raw material can also be passed through,
Further improve the purity of chlorine dioxide.Specifically, the speed speed that raw material is entered in aerated reaction storehouse group 12, has referred to
How many raw materials how long, in aerated reaction storehouse group 12 reacted and by complete aeration stripping by interior resting on.
Table 3
Further, the upper end in raw material premix conjunction storehouse 11 is provided with and enter for air and cause raw material premix to close formation in storehouse 11
The pore of air pressure.A pore is opened up by closing the upper end in storehouse 11 in raw material premix, is entered for air, it is empty in storehouse to be formed
Atmospheric pressure, after facilitating raw material premix to close, can be flowed into the first aerated reaction storehouse 121 under gas pressure from liquid outlet 112
It is interior.
Further, raw material premix close storehouse 11 and aerated reaction storehouse group 12 is integrated in a housing 1, specifically, Ke Yiyou
The high polyester PVC board of one fixed dimension is fabricated to a cubic box with closure cap, anti-in order to carry out aeration stripping
Should.Further, aerated reaction storehouse group 12 is provided with the temperature control part for controlling the environment temperature of aerated reaction storehouse group 12, preferably
Ground, temperature control part is set to ceramic temperature control plate 14.Preferably, the ceramic temperature control plate 14 in this enforcement is set to three, the ceramics of three
Temperature control plate 14 is contacted by electric power connection line, and temperature control plate power port 141 is provided with housing 1, and the ceramic temperature control plate 14 of three is same
The temperature control plate power port 141 of setting is connected, with ensure three aerated reaction storehouses environment temperature within the specific limits.Preferably,
Ceramic temperature control plate 14 controls environment temperature at 10～20 degree.
Further, aerated reaction storehouse group 12 is also associated with for controlling the anti-of the pneumatic flow in aerated reaction storehouse group 12
Storehouse 13 should be controlled；Reaction controlling storehouse 13 includes the oxygenation air pump 131 for producing tolerance and many with what oxygenation air pump 131 was connected
Individual pneumatic flow meter 132, the pneumatic flow meter 132 of each is correspondingly connected with the aeration block 124 of each.It should be noted that, expose
Air parcel 124 can adopt existing conventional techniques.Preferably, aeration block 124 is provided with connecting hole and multiple solarization air caps, multiple
Solarization air cap and connecting hole insertion.Specifically, aeration block 124 adopts the dilute aeration block 124 of polyester tetrafluoro, on the aeration block 124 before
Afterwards the intensive solarization air cap in left and right, at the middle part of aeration block 124 connection circular hole is provided with, and the aeration block 124 of each is used for the air pressure of each
Flowmeter 132 is connected, so that the aeration block 124 of each carries out quantitative aeration in different aerated reaction storehouses.Additionally, air pressure
Flowmeter 132 can adopt existing conventional techniques, specifically, connecting circular tube and the aeration of each that pneumatic flow meter 132 is arranged
The connection circular hole of block 124 is communicated, in order to make different aerated reaction storehouses reach different tolerance.In addition, solarization air cap can be with Jing
Cross laser to get, the intensive amount of the solarization air cap got by laser is while disclosure satisfy that aeration, so that the aeration of each
Aerosol aeration state is in reaction warehouse.
Further, aerated reaction storehouse group 12 is connected with the waste trap 15 for separating treatment waste liquid.Waste liquid is separated
Device 15 is connected by waste discharge liquid pipe 151 with the discharging opening 1232 in the 3rd aerated reaction storehouse 123.Specifically, waste discharge liquid pipe 151 can be with
U-shaped discharging tube is designed as, in order to by carrying out the waste liquid of reception after separating treatment, to be transported to waste liquid outlet, further have
Beneficial to environmental protection.
It should be noted that, in the present embodiment, aerated reaction storehouse group 12, raw material premix is closed into storehouse 11 and reaction controlling storehouse 13 is equal
In being placed in same housing 1, specifically, housing 1 includes a device storehouse and No. two device storehouses, and aerated reaction storehouse group 12 is placed in
In a number device storehouse, raw material premix close storehouse 11 and reaction controlling storehouse 13 is placed in No. two device storehouses.
Preferred embodiment of the present utility model is these are only, it is all in this practicality not to limit the utility model
Any modification, equivalent or improvement made within new spirit and principle etc., should be included in guarantor of the present utility model
Within the scope of shield.
Claims (10)
1. the aerated reaction device of a kind of chlorine dioxide, it is characterised in that including aerated reaction storehouse group；The aerated reaction
Storehouse group includes the multiple aerated reaction storehouses being sequentially connected according to Feedstock treating path and volume successively decreases successively；The aeration of each
Charging aperture, discharging opening, aeration opening and chlorine dioxide overfall are equipped with reaction warehouse, the aerated reaction storehouse of each
Inside it is provided with for the aeration block of quantitative aeration.
2. the aerated reaction device of chlorine dioxide as claimed in claim 1, it is characterised in that the aeration block is provided with
Connecting hole and multiple solarization air caps, the multiple solarization air cap and the connecting hole insertion.
3. the aerated reaction device of chlorine dioxide as claimed in claim 1, it is characterised in that the charging aperture and described
Discharging opening is opened in respectively the left and right sides in the aerated reaction storehouse of each；The aeration opening is separately positioned on the described of each
The bottom in aerated reaction storehouse；The chlorine dioxide overfall is separately positioned on the top in the aerated reaction storehouse of each.
4. the aerated reaction device of chlorine dioxide as claimed in claim 3, it is characterised in that aerated reaction storehouse group
Including the first aerated reaction storehouse, the second aerated reaction storehouse and the 3rd aerated reaction storehouse；The charging aperture in the first aerated reaction storehouse
Height higher than its discharging opening height, the height of the charging aperture in the second aerated reaction storehouse higher than its discharging opening height,
Height of the height of the charging aperture in the 3rd aerated reaction storehouse higher than its discharging opening.
5. the aerated reaction device of chlorine dioxide as claimed in claim 4, it is characterised in that first aerated reaction
The volume lapse rate in storehouse, the second aerated reaction storehouse and the 3rd aerated reaction storehouse is set to 0.5 times.
6. the aerated reaction device of the chlorine dioxide as described in any one of claim 4, it is characterised in that described first exposes
Solid/liquid/gas reactions storehouse, the second aerated reaction storehouse and the 3rd aerated reaction storehouse are integrated in a housing.
7. the aerated reaction device of the chlorine dioxide as described in any one of claim 1～6, it is characterised in that the exposure
The total amount of the reactant liquor in the group of solid/liquid/gas reactions storehouse is set to 169 with the ratio of aeration total amount：1.
8. the aerated reaction device of the chlorine dioxide as described in any one of claim 1～6, it is characterised in that the exposure
Solid/liquid/gas reactions storehouse group is provided with the temperature control part for controlling the environment temperature of aerated reaction storehouse group.
9. the aerated reaction device of the chlorine dioxide as described in any one of claim 1～6, it is characterised in that the exposure
Solid/liquid/gas reactions storehouse group is also associated with the reaction controlling storehouse for controlling the pneumatic flow in the group of the aerated reaction storehouse；The reaction control
Storehouse processed include the oxygenation air pump by producing tolerance and multiple pneumatic flows for being connected with the oxygenation air pump based on, the institute of each
State pneumatic flow meter to be correspondingly connected with the aeration block of each.
10. the aerated reaction device of the chlorine dioxide as described in any one of claim 1～6, it is characterised in that the exposure
Solid/liquid/gas reactions storehouse group is connected with for the waste trap of separating treatment waste liquid.
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| CN201621175409.8U CN206156748U (en) | 2016-10-26 | 2016-10-26 | Chlorine dioxide gas's aerated reactor device |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106365121A (en) * | 2016-10-26 | 2017-02-01 | 吴予奇 | Aeration reaction device of chlorine dioxide gas |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106365121A (en) * | 2016-10-26 | 2017-02-01 | 吴予奇 | Aeration reaction device of chlorine dioxide gas |
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