CN205517697U - Horizontal reactor - Google Patents

Horizontal reactor Download PDF

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Publication number
CN205517697U
CN205517697U CN201620034061.4U CN201620034061U CN205517697U CN 205517697 U CN205517697 U CN 205517697U CN 201620034061 U CN201620034061 U CN 201620034061U CN 205517697 U CN205517697 U CN 205517697U
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China
Prior art keywords
water conservancy
conservancy diversion
horizontal reactor
reative cell
dividing plate
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Expired - Fee Related
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CN201620034061.4U
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Chinese (zh)
Inventor
艾秋红
罗和安
黄荣辉
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Xiangtan University
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Xiangtan University
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Abstract

The utility model provides a horizontal reactor. Horizontal reactor is including the casing, feed inlet, discharge gate and a plurality of baffle that have accommodating space. The feed inlet with the discharge gate is located respectively the both ends of casing, it is a plurality of baffle perpendicular to material is followed the feed inlet extremely the flow direction of discharge gate sets up at the interval in proper order, and is a plurality of the baffle will accommodating space separates for a plurality of reacting chambers, the shape of baffle size with the shape size phase -match of casing cross section, every a plurality of water conservancy diversion through -hole has been seted up on the baffle, the water conservancy diversion through -hole is followed the degree of depth direction distribution of material in the reacting chamber. The utility model provides a horizontal reactor, loading and unloading capacity is high, and can stop reactant back mixing phenomenon.

Description

Horizontal reactor
Technical field
This utility model relates to technical field of chemical, is specifically related to a kind of horizontal reactor.
Background technology
At chemical technology field, horizontal reactor is used for liquid-liquid phase or liquid-solid phase reaction.Existing Having in technology, reactor is designed to multistage reactor more, and reactant is through multi-stage reaction chamber step by step React, form tandem reaction sequence, it is achieved improve the purpose of reactor production capacity.
In correlation technique, horizontal reactor uses polylith overflow plate to be separated into by reactor multiple Reative cell, the material of upper level reative cell reacts to next stage through the top overflow of described overflow plate Room, forms flow reactor.But, in the course of the work, every grade is anti-for described multistage reactor Answering the liquid level in room to need to reach the extreme higher position of described overflow plate, material could pass through overflow plate Overflow, to next stage reative cell, does not i.e. arrive described overflow plate when the liquid level of upper level reative cell During extreme higher position, the reactionless thing of subordinate's reative cell, so that the reaction volume in reative cell at different levels Uneven, reative cells at different levels are not fully used;And the top of described overflow plate is with described The roof of reactor has certain spacing, thus limits the reaction volume in each reative cell, Affect the production capacity of reactor.Meanwhile, all reach described when the liquid level of adjacent two-stage reaction room During the extreme higher position of overflow plate, it is easily generated the phenomenon of the material back-mixing of next stage reative cell, thus Affect the concentration distribution during material reaction and Temperature Distribution, affect product qualities.
Therefore, it is necessary to provide a kind of new horizontal reactor to solve above-mentioned technical problem.
Utility model content
The purpose of this utility model is to overcome above-mentioned technical problem, it is provided that a kind of can raising produces energy Power, and the horizontal reactor of reactant air-teturning mixed phenomenon can be stopped.
The technical solution of the utility model is as follows:
A kind of horizontal reactor, including have the housing of receiving space, charging aperture, discharging opening and Multiple dividing plates.Described charging aperture and described discharging opening are respectively arranged on the two ends of described housing, multiple Described divider upright in material along described charging aperture to described discharging opening flow direction successively between Every setting, described receiving space is divided into multiple reative cell, described dividing plate by multiple described dividing plates The shape size of shape size and described housing cross-sectional match, each described dividing plate is opened It is provided with several water conservancy diversion through holes, described water conservancy diversion through hole depth direction of material along described reative cell Distribution.
Preferably, the percent opening of the described water conservancy diversion through hole on each described dividing plate is 0.01%-10%.
Preferably, along the bottom of described reative cell to top-direction, adjacent two described water conservancy diversion lead to The spacing in hole is the 1/20-1/5 of described divider height.
Preferably, described horizontal reactor also includes multiple agitating device, each described reative cell It is correspondingly arranged a described agitating device.
Preferably, the quantity of described reative cell is 2-8.
Compared with correlation technique, the horizontal reactor that this utility model provides, have the most useful Effect:
One, by arranging multiple dividing plate in described horizontal reactor, by described horizontal reactor Being divided into multiple reative cell, the shape size of described dividing plate is big with the cross sectional shape of described reative cell Little match, make the housing that reaction compartment is described horizontal reactor of each reative cell with described Dividing plate encloses the whole space of formation, and compared with correlation technique, this reaction compartment increases, thus The reaction volume in each reative cell can be increased, improve the production capacity in each reative cell.Institute State and on dividing plate, offer several water conservancy diversion through holes, described refluence through hole material along described reative cell Depth direction is distributed, when in described reative cell, the liquid level arrival of material is provided with described water conservancy diversion through hole During position, material flows through next stage reative cell through described water conservancy diversion through hole, after multi-stage reaction chamber by Described discharging opening is discharged, and obtains product.By arranging multiple institute at the longitudinal direction of described dividing plate State water conservancy diversion through hole, make material fill each reative cell in the short period of time, and make each reative cell Interior material liquid level maintains an equal level, and improves the utilization ratio of each reative cell, and shortens the product of product Go out the time, improve the production capacity of described horizontal multi-stage reactor.
Two, material is flowed to discharging opening by charging aperture is to be led to by the water conservancy diversion on each described dividing plate Hole stream realizes, and described reaction of high order indoor are in barotropic state, makes to enter described in material edge all the time Material mouth flows to the direction of described discharging opening, thus can stop the phenomenon of material back-mixing, improves and produces The quality of thing.
Accompanying drawing explanation
Fig. 1 is the structural representation of this utility model horizontal reactor;
Fig. 2 is the structural representation of the embodiment one of horizontal reactor median septum shown in Fig. 1;
Fig. 3 is the structural representation of the embodiment two of horizontal reactor median septum shown in Fig. 1;
Fig. 4 is the structural representation of the embodiment three of horizontal reactor median septum shown in Fig. 1.
Detailed description of the invention
Below in conjunction with drawings and embodiments, the utility model is described in further detail.
Embodiment one
Refer to Fig. 1, for the structural representation of this utility model horizontal reactor.Described horizontal Reactor 1 includes having the housing 11 of receiving space (non-label), charging aperture 12, discharging Mouth 13, multiple dividing plate 14 and agitating device 15.Described charging aperture 12 and described discharging opening 13 Being located at the two ends of described housing 11, described charging aperture 11 is described for being delivered to by reaction mass In housing 11, described discharging opening 13 is for exporting reacted product.Multiple described dividing plates 14 be perpendicular to material along described charging aperture 12 to the flow direction of described discharging opening 13 successively between In the receiving space being located at described housing 11.Described agitating device 15 is used for stirring material, Make reactant mix homogeneously, improve reaction efficiency.
The quantity of described dividing plate 14 is 1-7, accordingly, the collecting of described housing 11 is empty Between be separated to form 2-8 reative cell 111, multiple described reative cells 111 make described horizontal reacting Device 1 forms flow reactor.
It should be noted that the quantity of described dividing plate 14 is not limited to 1-7, other dividing plate Being included in protection domain of the present utility model of quantity equivalent.
Referring again to Fig. 2, for the structure of the embodiment one of horizontal reactor median septum shown in Fig. 1 Schematic diagram.The shape size phase of the shape size of described dividing plate 14 and described housing 11 cross section Coupling, after installing described dividing plate 14, the inwall of described dividing plate 14 and described housing 11 is continuously Gap, the reaction compartment making each described reative cell 111 is described housing 11 and described dividing plate 14 Enclosing the whole space of formation, the reaction compartment of formation increases, thus can increase each reative cell Interior reaction volume, improves the production capacity in each reative cell.
Several water conservancy diversion through holes 141, described water conservancy diversion through hole is offered on each described dividing plate 14 141 run through described dividing plate 14 along the flow direction of material is arranged, and described water conservancy diversion through hole 141 The depth direction distribution of material along described reative cell 111, the most described water conservancy diversion through hole 141 is longitudinally Distribution, makes the most corresponding different liquid level of described water conservancy diversion through hole 141.When described reative cell When material liquid level in 111 reaches described water conservancy diversion through hole 141 position of extreme lower position, material warp The described water conservancy diversion through hole 141 of this position flow to next stage reative cell.Material is in the short period of time It is distributed in multiple described reative cell 111, and makes the material liquid level in each described reative cell 111 hold It is flat, so that the reaction compartment of described each reative cell 111 is utilized effectively.
The percent opening of the described water conservancy diversion through hole 141 on each described dividing plate 14 is 0.01%-10%, On the one hand the material in reative cell 111 described in upper level is made to be circulated to smoothly described in next stage anti- Answering room, if the percent opening of described water conservancy diversion through hole 141 is less, material is at reative cell described in upper level Pile up in 111, thus affect powder feeding efficiency, reduce the production capacity of described horizontal reactor 1; On the other hand, the material liquid level in rational circulation area makes described reative cell 111 maintains relatively High and rational level, is further ensured that the utilization ratio of described reative cell 111.
Along the bottom of described reative cell 111 to top-direction, two adjacent described water conservancy diversion through holes 141 spaced sets, the most described water conservancy diversion through hole 141 is uniformly opened on described dividing plate 14.
On each described dividing plate 14, along the bottom of described reative cell 111 to top-direction, phase The spacing of two adjacent described water conservancy diversion through holes 141 is the 1/20-1/5 of described dividing plate 14 height, logical Cross the spacing designing neighbouring two described water conservancy diversion through hole 141, be further ensured that described reative cell Material liquid level in 111.Wherein, the spacing of two adjacent described water conservancy diversion through holes 141 is two The spacing of the centrage of individual described water conservancy diversion through hole 141.
It should be noted that described water conservancy diversion through hole 141 can be in a column distribution, it is also possible in many Column distribution, as long as the differing heights of described dividing plate longitudinal direction is distributed described water conservancy diversion through hole 141 ?.
Corresponding, the quantity of described agitating device 15 is equal with the quantity of described reative cell 111, It is respectively arranged in each described reative cell 111, for reaction mass is stirred, improves anti- Answer the reaction efficiency of thing.
Embodiment two
The described horizontal reactor structure of present embodiment is essentially identical with embodiment one, difference It is the distribution of water conservancy diversion through hole described in described dividing plate.Diaphragm structure to present embodiment below It is described in detail.
Referring again to Fig. 3, for the structure of the embodiment two of horizontal reactor median septum shown in Fig. 1 Schematic diagram.Several water conservancy diversion through holes 241, described water conservancy diversion is offered on each described dividing plate 24 The depth direction distribution of through hole 241 material along described reative cell 111, the most described water conservancy diversion through hole 241 the most corresponding different liquid levels.Described water conservancy diversion through hole on each described dividing plate 24 The percent opening of 241 is 0.01%-10%.
Along the bottom of described reative cell 111 to top-direction, two adjacent described water conservancy diversion through holes The spacing of 241 is gradually reduced, and the most described water conservancy diversion through hole 241 is positioned at bottom described dividing plate 24 Open cell content is less than the open cell content at top, it is ensured that material liquid level maintains higher level;Meanwhile, Open cell content at top increases, and can increase the material circulation at top, thus avoid described instead Room 111 panful is answered to have to use the mode reducing inlet amount to adjust the condition of production.
On each described dividing plate 24, along the bottom of described reative cell 111 to top-direction, phase The spacing of two adjacent described water conservancy diversion through holes 241 is the 1/20-1/5 of described dividing plate 24 height, logical Cross the spacing designing neighbouring two described water conservancy diversion through hole 241, be further ensured that described reative cell Material liquid level in 111.Wherein, the spacing of two adjacent described water conservancy diversion through holes 241 is two The spacing of the centrage of individual described water conservancy diversion through hole 241.
Described water conservancy diversion through hole 241 is preferably circular, reduces circulation because circular configuration periphery is smooth Resistance, in addition, the shape of described water conservancy diversion through hole 241 can also be square, rhombus, ladder Shape, star or other are irregularly shaped.
Embodiment three
The described horizontal reactor structure of present embodiment is essentially identical with embodiment one, difference It is the distribution of water conservancy diversion through hole described in described dividing plate.Diaphragm structure to present embodiment below It is described in detail.
Referring again to Fig. 4, for the structure of the embodiment three of horizontal reactor median septum shown in Fig. 1 Schematic diagram.As a example by continuous three described dividing plates, along the flow direction of material, described in three every Plate is represented sequentially as 34a, 34b, 34c, and each described dividing plate 34a, 34b, 34c are upper respectively Offer several water conservancy diversion through holes, be expressed as 341a, 341b, 341c.
Described water conservancy diversion through hole 341a, 341b, 341c material along described reative cell 111 respectively Depth direction distribution.The upper corresponding described water conservancy diversion of each described dividing plate 34a, 34b, 34c leads to The percent opening of hole 341a, 341b and 341c is 0.01%-10%.
Described water conservancy diversion through hole 341a on adjacent two described dividing plate 34a, 34b, 34c, 341b, 341c be cross-flow distribution, the most described water conservancy diversion through hole 341a, 341b be cross-flow distribution, described in lead Opening 341b, 341c are cross-flow distribution.Concrete structure is: the institute on described dividing plate 34a State water conservancy diversion through hole 341a and be distributed in the position that the center line of described dividing plate 34a keeps left, described dividing plate Described water conservancy diversion through hole 341b on 34b is distributed in the midline position of described dividing plate 34b, described The center line that described water conservancy diversion through hole 341c on dividing plate 34c is distributed in described dividing plate 34c is kept right Position.Described water conservancy diversion through hole 341a on the most adjacent two described dividing plate 34a, 34b, 34c, 341b, 341c anon-normal is to setting.The center line of described dividing plate 34a, 34b, 34c is along described reaction The bottom of room 111 is arranged to top-direction, for the line of symmetry of described dividing plate 34a, 34b, 34c.
It should be noted that the upper correspondence of continuous three described dividing plate 34a, 34b, 34c is described The position of water conservancy diversion through hole 341a, 341b, 341c is not limited to this, it is possible to realize adjacent two Individual described dividing plate 34a, 34b, 34c upper corresponding described water conservancy diversion through hole 341a, 341b, 341c In cross-flow, the mode of distribution is all contained in protection domain of the present utility model.
By making the upper corresponding described water conservancy diversion through hole of adjacent two described dividing plate 34a, 34b, 34c 341a, 341b, 341c are cross-flow distribution, can increase material stream in described reative cell 111 Path, thus material mixability in reative cell 111 can be improved, thus improve reaction Efficiency.
Along the bottom of described reative cell 111 to top-direction, each described dividing plate 34a, 34b, Upper corresponding described water conservancy diversion through hole 341a, 341b, 341c spaced set of 34c, i.e. described in lead Opening 341a, 341b, 341c are uniformly opened in described dividing plate 34a, 34b, 34c of correspondence On.
It should be noted that adjacent two described water conservancy diversion through holes are not limited to spaced set, phase The spacing of two adjacent described water conservancy diversion through holes can use the set-up mode in embodiment two, the most adjacent The spacing of two described water conservancy diversion through holes be gradually reduced, make described water conservancy diversion through hole be positioned at described dividing plate The open cell content of bottom is less than the open cell content at top.
Along the bottom of described reative cell 111 to top-direction, two institutes adjacent on each dividing plate State the spacing of water conservancy diversion through hole 341a, 341b, 341c be corresponding described dividing plate 34a, 34b, The 1/20-1/5 of 34c height, by designing the spacing of two neighbouring described water conservancy diversion through holes, enters One step ensures the material liquid level in described reative cell 111.
The horizontal reactor 1 that this utility model provides can be used for liquid--liquid reaction or solid-liquid is contrary Should.
Compared with correlation technique, the horizontal reactor that this utility model provides, have the most useful Effect:
One, by arranging multiple dividing plate in described horizontal reactor, by described horizontal reactor Being divided into multiple reative cell, the shape size of described dividing plate is big with the cross sectional shape of described reative cell Little match, make the housing that reaction compartment is described horizontal reactor of each reative cell with described Dividing plate encloses the whole space of formation, and compared with correlation technique, this reaction compartment increases, thus The reaction volume in each reative cell can be increased, improve the production capacity in each reative cell.Institute State and on dividing plate, offer several water conservancy diversion through holes, described refluence through hole material along described reative cell Depth direction is distributed, when in described reative cell, the liquid level arrival of material is provided with described water conservancy diversion through hole During position, material flows through next stage reative cell through described water conservancy diversion through hole, after multi-stage reaction chamber by Described discharging opening is discharged, and obtains product.By arranging multiple institute at the longitudinal direction of described dividing plate State water conservancy diversion through hole, make material fill each reative cell in the short period of time, and make each reative cell Interior material liquid level maintains an equal level, and improves the utilization ratio of each reative cell, and shortens the product of product Go out the time, improve the production capacity of described horizontal multi-stage reactor.
Two, material is flowed to discharging opening by charging aperture is to be led to by the water conservancy diversion on each described dividing plate Hole stream realizes, and described reaction of high order indoor are in barotropic state, makes to enter described in material edge all the time Material mouth flows to the direction of described discharging opening, thus can stop the phenomenon of material back-mixing, improves and produces The quality of thing.
The horizontal reactor of this utility model offer and horizontal reactor of the prior art are provided Carry out contrast test, when the housing of described horizontal reactor has the receiving space of equivalent, and use In the case of in same substance reaction, reaction, each parameter is identical, it is sleeping that this utility model provides The production capacity of formula reactor, compared to being prior art, improves 20-40%.
The foregoing is only embodiment of the present utility model, not thereby limit of the present utility model The scope of the claims, every equivalent structure utilizing this utility model description and accompanying drawing content to be made or Equivalence flow process conversion, or directly or indirectly it is used in other relevant technical field, the most in like manner wrap Include in scope of patent protection of the present utility model.

Claims (5)

1. a horizontal reactor, including having the housing of receiving space, charging aperture and discharging opening, Described charging aperture and described discharging opening are respectively arranged on the two ends of described housing, it is characterised in that described Horizontal reactor also includes multiple dividing plate, and multiple described divider upright are in material along described charging aperture extremely The flow direction of described discharging opening is spaced setting successively, and described receiving space is divided by multiple described dividing plates It is divided into multiple reative cell, the shape size phase of the shape size of described dividing plate and described housing cross-sectional Coupling, each described dividing plate offers several water conservancy diversion through holes, described water conservancy diversion through hole along described instead Answer the depth direction distribution of indoor material.
Horizontal reactor the most according to claim 1, it is characterised in that each described every The percent opening of the described water conservancy diversion through hole on plate is 0.01%-10%.
Horizontal reactor the most according to claim 1, it is characterised in that along described reaction The bottom of room is to top-direction, and the spacing of adjacent two described water conservancy diversion through holes is described divider height 1/20-1/5。
Horizontal reactor the most as claimed in any of claims 1 to 3, its feature exists In, described horizontal reactor also includes that multiple agitating device, each described reative cell are correspondingly arranged one Individual described agitating device.
Horizontal reactor the most as claimed in any of claims 1 to 3, its feature exists In, the quantity of described reative cell is 2-8.
CN201620034061.4U 2016-01-14 2016-01-14 Horizontal reactor Expired - Fee Related CN205517697U (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105664820A (en) * 2016-01-14 2016-06-15 湘潭大学 Horizontal reactor
CN110628471A (en) * 2019-10-18 2019-12-31 湖州联创环保科技有限公司 Horizontal pipe stepped liquid phase continuous reaction device suitable for preparing biodiesel by biological enzyme method
CN113209923A (en) * 2021-04-22 2021-08-06 江苏百赛飞生物科技有限公司 Device for effectively removing heat discharged in mixing process

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105664820A (en) * 2016-01-14 2016-06-15 湘潭大学 Horizontal reactor
CN110628471A (en) * 2019-10-18 2019-12-31 湖州联创环保科技有限公司 Horizontal pipe stepped liquid phase continuous reaction device suitable for preparing biodiesel by biological enzyme method
CN113209923A (en) * 2021-04-22 2021-08-06 江苏百赛飞生物科技有限公司 Device for effectively removing heat discharged in mixing process

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Granted publication date: 20160831

Termination date: 20210114