CN205730453U - For extracting the reflux, extract, device of hypolipidemic activity material from alura fine horse Fructus Jujubae - Google Patents
For extracting the reflux, extract, device of hypolipidemic activity material from alura fine horse Fructus Jujubae Download PDFInfo
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- CN205730453U CN205730453U CN201620713674.0U CN201620713674U CN205730453U CN 205730453 U CN205730453 U CN 205730453U CN 201620713674 U CN201620713674 U CN 201620713674U CN 205730453 U CN205730453 U CN 205730453U
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Abstract
This utility model discloses a kind of reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae, including magnetic stirring apparatus, electric jacket, flask, extraction mechanism and spherical condensation tube, described extraction mechanism includes top connection, lower contact, extract end cylinder and extract cylinder, described top connection includes the first airway and the first gas-liquid flow siphunculus, the gas outlet of described first airway is located on the sidewall of described first gas-liquid flow siphunculus and is connected with described first gas-liquid flow siphunculus fluid communication, described lower contact includes the second airway, catheter and the second gas-liquid flow siphunculus, the air inlet of described second airway is located on the sidewall of described second gas-liquid flow siphunculus and is connected with described second gas-liquid flow siphunculus fluid communication, the liquid outlet of described catheter is located on the sidewall of described second gas-liquid flow siphunculus.This utility model extraction rate is fast and saves Extraction solvent, utilizes grading extraction, makes full use of the Extraction solvent of backflow, forms multilamellar and extracts, improves extraction rate.
Description
Technical field
This utility model relates to chemical experiment field, more particularly, to one for extracting fall from alura fine horse Fructus Jujubae
The reflux, extract, device of blood fat active substance.
Background technology
In to alura fine horse Fructus Jujubae hypolipidemic activity material extraction and measure during, need with ethanol fresh and dry
Alura fine horse Fructus Jujubae processed extracts.Need to be extracted by the material dissolving in ethanol as much as possible, to keep away during extracting
The residual quantity exempting from these materials affects the research of the hypolipidemic activity to other materials.And existing reflux, extract, device not only extracts
Speed is slow, and during extracting, solvent usage amount is bigger.
Utility model content
Because in this, this utility model purpose be that provide a kind of extraction rate fast and save Extraction solvent for
From alura fine horse Fructus Jujubae, extract the reflux, extract, device of hypolipidemic activity material, utilize grading extraction, the Extraction solvent to backflow
Make full use of, form multilamellar and extract, improve extraction rate.
For reaching above-mentioned purpose, this utility model uses following technical proposals: for extracting fall blood from alura fine horse Fructus Jujubae
The reflux, extract, device of fat active substance, including magnetic stirring apparatus, electric jacket, flask, extraction mechanism and spherical condensation tube, described
Extraction mechanism includes cylinder at the bottom of top connection, lower contact, extraction and extracts cylinder, and described top connection includes the first airway and the first gas-liquid
Runner pipe, the gas outlet of described first airway be located on the sidewall of described first gas-liquid flow siphunculus and with described first gas-liquid flow
Siphunculus fluid communication connects, and described lower contact includes the second airway, catheter and the second gas-liquid flow siphunculus, described second inducing QI
The air inlet of pipe is located on the sidewall of described second gas-liquid flow siphunculus and is connected with described second gas-liquid flow siphunculus fluid communication, institute
The liquid outlet stating catheter is located on the sidewall of described second gas-liquid flow siphunculus, and the sidewall of cylinder at the bottom of described extraction is provided with liquid and returns
Stream siphon, the described liquid siphonal liquid outlet of backflow is connected with the inlet fluid communication of described catheter, described extraction
It is equipped with filter opening at the bottom of the cylinder of end cylinder and at the bottom of the cylinder of described extraction cylinder;The inlet end of described spherical condensation tube and described first gas-liquid flow
The outlet side fluid communication of siphunculus is tightly connected, the liquid outlet of described first gas-liquid flow siphunculus and the liquid feeding end stream of described extraction cylinder
Body conducting is tightly connected, and at the bottom of the liquid outlet of described extraction cylinder and described extraction, the liquid feeding end fluid communication of cylinder is tightly connected, described
The liquid feeding end fluid communication of the liquid outlet and described second gas-liquid flow siphunculus that extract end cylinder is tightly connected, described second gas-liquid circulation
The liquid outlet of pipe is tightly connected with the bottleneck fluid communication of described flask, and described flask is located in described electric jacket, described electric heating
It is mounted on described magnetic stirring apparatus;It is provided with magnet rotor in described flask;The air inlet of described first airway and described the
The gas outlet fluid communication of two airways is tightly connected.
The above-mentioned reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae, in described extraction cylinder and
It is equipped with filter course in cylinder at the bottom of described extraction.
The above-mentioned reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae, described filter course is de-
Fat cotton layer.
The above-mentioned reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae, described spherical condensation tube
Inlet end be provided in the described first gas-liquid flow siphunculus of described first gas-liquid flow siphunculus outlet side, close on described first gas
The inwall of the described first gas-liquid flow siphunculus of liquid stream siphunculus gas outlet is provided with the first frosted layer, described first frosted layer and described
The frosted layer of spherical condensation tube inlet end is tightly connected.
The above-mentioned reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae, described first gas-liquid flow
Siphunculus liquid outlet is located in the liquid feeding end of described extraction cylinder, closes on described first gas-liquid of described first gas-liquid flow siphunculus liquid outlet
The outer wall of runner pipe is provided with the second frosted layer;The described extraction cylinder inwall closing on described extraction cylinder liquid feeding end is provided with the 3rd mill
Layer of sand, described second frosted layer and described 3rd frosted layer are tightly connected.
The above-mentioned reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae, going out of described extraction cylinder
Liquid mouth is located in the liquid feeding end of cylinder at the bottom of described extraction, and the outer wall of the described extraction cylinder closing on described extraction cylinder liquid outlet is provided with
Four frosted layers;Close on the inwall of cylinder at the bottom of the described extraction of the inlet of cylinder at the bottom of described extraction and be provided with the 5th frosted layer, described
Four frosted layers are tightly connected with described 5th frosted layer.
The above-mentioned reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae, cylinder at the bottom of described extraction
Liquid outlet is located in the liquid feeding end of described second gas-liquid flow siphunculus, closes on cylinder at the bottom of the described extraction of the liquid outlet of cylinder at the bottom of described extraction
Outer wall be provided with the 6th frosted layer, close on the inwall of the described second gas-liquid flow siphunculus of described second gas-liquid flow siphunculus inlet
Being provided with the 7th frosted layer, described 6th frosted layer is tightly connected with described 7th frosted layer.
The above-mentioned reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae, described second gas-liquid flow
The liquid outlet of siphunculus is located in the bottleneck of described flask, closes on described second gas-liquid of the liquid outlet of described second gas-liquid flow siphunculus
The outer wall of runner pipe is provided with the 8th frosted layer, and described 8th frosted layer is tightly connected with the frosted layer of described flask bottleneck.
The beneficial effects of the utility model are as follows:
1. this utility model uses multilamellar reflux, extract, is possible not only to improve extraction rate, also helps minimizing and extracts molten
The usage amount of agent.
2. this utility model utilizes multilamellar reflux, extract, is conducive to carrying out fully for dissolving in the material in Extraction solvent
Extract.
Accompanying drawing explanation
Fig. 1 is that this utility model is for extracting the knot of the reflux, extract, device of hypolipidemic activity material from alura fine horse Fructus Jujubae
Structure schematic diagram;
Fig. 2 is that this utility model is for extracting the reflux, extract, device of hypolipidemic activity material from alura fine horse Fructus Jujubae
The structural representation of joint;
Fig. 3 is that this utility model is for extracting carrying of the reflux, extract, device of hypolipidemic activity material from alura fine horse Fructus Jujubae
Take the structural representation of cylinder;
Fig. 4 is that this utility model is for extracting carrying of the reflux, extract, device of hypolipidemic activity material from alura fine horse Fructus Jujubae
Take the structural representation of end cylinder;
Fig. 5 is that this utility model is under the reflux, extract, device extracting hypolipidemic activity material from alura fine horse Fructus Jujubae
The structural representation of joint.
In figure: 1-magnetic stirring apparatus;2-electric jacket;3-flask;4-lower contact;5-extracts end cylinder;6-extracts cylinder;Connect on 7-
Head;8-spherical condensation tube;9-the second airway;10-the first airway;11-catheter;12-liquid backflow siphon;13-
One gas-liquid flow siphunculus;14-the first frosted layer;15-the second frosted layer;16-the 3rd frosted layer;17-the 4th frosted layer;18-filter opening;
19-the 5th frosted layer;20-the 6th frosted layer;21-the second gas-liquid flow siphunculus;22-the 7th frosted layer;23-the 8th frosted layer;24-
Filter course.
Detailed description of the invention
In order to be illustrated more clearly that this utility model, below in conjunction with preferred embodiments and drawings, this utility model is done into one
The explanation of step.Parts similar in accompanying drawing are indicated with identical reference.It will be appreciated by those skilled in the art that following
Specifically described content is illustrative and be not restrictive, and should not limit protection domain of the present utility model with this.
As it is shown in figure 1, this utility model is for extracting the reflux, extract, dress of hypolipidemic activity material from alura fine horse Fructus Jujubae
Put, including magnetic stirring apparatus 1, electric jacket 2, flask 3, extraction mechanism and spherical condensation tube 8.Wherein, as it is shown in figure 1, described in carry
Taking mechanism to include top connection 7, lower contact 4, extract end cylinder 5 and extract cylinder 6, described top connection 7 includes the first airway 10 and the
One gas-liquid flow siphunculus 13, the gas outlet of described first airway 10 be located on the sidewall of described first gas-liquid flow siphunculus 13 and with institute
Stating the first gas-liquid flow siphunculus 13 fluid communication to connect, described lower contact 4 includes the second airway 9, catheter 11 and the second gas-liquid
Runner pipe 21, the air inlet of described second airway 9 is located on the sidewall of described second gas-liquid flow siphunculus 21 and with described second
Gas-liquid flow siphunculus 21 fluid communication connects, and the liquid outlet of described catheter 11 is located at the sidewall of described second gas-liquid flow siphunculus 21
On, the sidewall of cylinder 5 at the bottom of described extraction is provided with liquid backflow siphon 12, the liquid outlet of described liquid backflow siphon 12 and institute
The inlet fluid communication stating catheter 11 connects, as shown in Figure 3 and Figure 4, at the bottom of the cylinder of cylinder 5 at the bottom of described extraction and described extraction cylinder
Filter opening 18 it is equipped with at the bottom of the cylinder of 6.
As it is shown in figure 1, the outlet side fluid of the inlet end of described spherical condensation tube 8 and described first gas-liquid flow siphunculus 13 is led
Leading to and be tightly connected, the liquid outlet of described first gas-liquid flow siphunculus 13 is tightly connected with the liquid feeding end fluid communication of described extraction cylinder 6,
At the bottom of the liquid outlet of described extraction cylinder 6 and described extraction, the liquid feeding end fluid communication of cylinder 5 is tightly connected, and at the bottom of described extraction, cylinder 5 goes out
Liquid end is tightly connected with the liquid feeding end fluid communication of described second gas-liquid flow siphunculus 21, described second gas-liquid flow siphunculus 21 go out liquid
Holding the bottleneck fluid communication with described flask 3 to be tightly connected, described flask 3 is located in described electric jacket 2, and described electric jacket 2 is put
On described magnetic stirring apparatus 1, in described flask 3, it is provided with magnet rotor;The air inlet of described first airway 10 and described the
The gas outlet fluid communication of two airways 9 is tightly connected.
Wherein, as illustrated in fig. 1 and 2, the inlet end of described spherical condensation tube 8 is provided at described first gas-liquid flow siphunculus 13
In the described first gas-liquid flow siphunculus 13 of outlet side, close on described first gas-liquid flow of described first gas-liquid flow siphunculus 13 gas outlet
The inwall of siphunculus 13 is provided with the first frosted layer 14, described first frosted layer 14 and the frosted of described spherical condensation tube 8 inlet end
Layer is tightly connected;As shown in Figures 1 to 3, described first gas-liquid flow siphunculus 13 liquid outlet is located in the liquid feeding end of described extraction cylinder 6,
The outer wall of the described first gas-liquid flow siphunculus 13 closing on described first gas-liquid flow siphunculus 13 liquid outlet is provided with the second frosted layer 15;
Described extraction cylinder 6 inwall closing on described extraction cylinder 6 liquid feeding end is provided with the 3rd frosted layer 16, described second frosted layer 15 and institute
State the 3rd frosted layer 16 to be tightly connected;Shown in as shown in Figure 1, Figure 3 and Figure 4, the liquid outlet of described extraction cylinder 6 is located at cylinder at the bottom of described extraction
In the liquid feeding end of 5, the outer wall of the described extraction cylinder 6 closing on described extraction cylinder 6 liquid outlet is provided with the 4th frosted layer 17;Close on institute
State the inwall of cylinder 5 at the bottom of the described extraction of the inlet extracting end cylinder 5 and be provided with the 5th frosted layer 19, described 4th frosted layer 17 with
Described 5th frosted layer 19 is tightly connected;As shown in Figure 1, Figure 4 and Figure 5, the liquid outlet of cylinder 5 at the bottom of described extraction is located at described second
In the liquid feeding end of gas-liquid flow siphunculus 21, close on the outer wall of cylinder 5 at the bottom of the described extraction of the liquid outlet of cylinder 5 at the bottom of described extraction and be provided with
Six frosted layers 20, the inwall of the described second gas-liquid flow siphunculus 21 closing on described second gas-liquid flow siphunculus 21 inlet is provided with
Seven frosted layers 22, described 6th frosted layer 20 is tightly connected with described 7th frosted layer 22;As shown in Figure 1 and Figure 5, described second
The liquid outlet of gas-liquid flow siphunculus 21 is located in the bottleneck of described flask 3, closes on the liquid outlet of described second gas-liquid flow siphunculus 21
The outer wall of described second gas-liquid flow siphunculus 21 is provided with the 8th frosted layer 23, described 8th frosted layer 23 and described flask 3 bottleneck
Frosted layer be tightly connected.In order to improve sealing, vaseline can be coated in the place of two frosted layer joints.
In order to avoid alura fine horse Fructus Jujubae tiny Fructus Jujubae block falls into described flask 3 from filter opening 18, in the present embodiment, carry described
Being equipped with filter course 24 in taking cylinder 6 and in cylinder 5 at the bottom of described extraction, described filter course 24 is degreasing cotton layer.
In the present embodiment, at the bottom of described extraction, between cylinder 5 and described top connection 7, it is being provided with two described extraction cylinders 6, wherein,
Being smaller in size than of described extraction cylinder 6 above is positioned at the described extraction cylinder 6 of lower section.
Utilize this utility model attempt from alura fine horse Fructus Jujubae hypolipidemic activity material time, in described flask 3 add second
Alcohol, is then respectively put into the alura fine horse Fructus Jujubae of broken shape in cylinder 5 at the bottom of described extraction cylinder 6 and described extraction, and in described extraction
Add a small amount of ethanol in end cylinder, then according to build this utility model shown in Fig. 1, be next turned on described spherical condensation tube 8 and cool down
Recirculated water, open described magnetic stirring apparatus 1 and the power supply of described electric jacket 2.Utilize the multistage extraction of multilamellar drip washing
Mode can be effectively improved the extraction rate of the material dissolving in ethanol in alura fine horse Fructus Jujubae, saves experimental period.
Above-described embodiment of the present utility model is only for clearly demonstrating this utility model example, and is not
Restriction to embodiment of the present utility model, for those of ordinary skill in the field, on the basis of described above
On can also make other changes in different forms, cannot all of embodiment be given exhaustive here, every genus
Obviously changed in what the technical solution of the utility model extended out or change still in protection model of the present utility model
The row enclosed.
Claims (8)
1. for extracting the reflux, extract, device of hypolipidemic activity material from alura fine horse Fructus Jujubae, it is characterised in that include magnetic force
Agitator (1), electric jacket (2), flask (3), extraction mechanism and spherical condensation tube (8), described extraction mechanism includes top connection
(7), lower contact (4), extract end cylinder (5) and extraction cylinder (6), described top connection (7) includes the first airway (10) and the first gas
Liquid stream siphunculus (13), the gas outlet of described first airway (10) be located on the sidewall of described first gas-liquid flow siphunculus (13) and with
Described first gas-liquid flow siphunculus (13) fluid communication connects, and described lower contact (4) includes the second airway (9), catheter (11)
With the second gas-liquid flow siphunculus (21), the air inlet of described second airway (9) is located at the side of described second gas-liquid flow siphunculus (21)
Being connected on wall and with described second gas-liquid flow siphunculus (21) fluid communication, the liquid outlet of described catheter (11) is located at described second
On the sidewall of gas-liquid flow siphunculus (21), the sidewall of cylinder (5) at the bottom of described extraction is provided with liquid backflow siphon (12), described liquid
The liquid outlet of backflow siphon (12) is connected with the inlet fluid communication of described catheter catheter (11), cylinder at the bottom of described extraction
(5) filter opening (18) it is equipped with at the bottom of cylinder and at the bottom of the cylinder of described extraction cylinder (6);The inlet end of described spherical condensation tube (8) is with described
The outlet side fluid communication of the first gas-liquid flow siphunculus (13) is tightly connected, the liquid outlet of described first gas-liquid flow siphunculus (13) and institute
The liquid feeding end fluid communication stating extraction cylinder (6) is tightly connected, cylinder (5) at the bottom of the liquid outlet of described extraction cylinder (6) and described extraction
Liquid feeding end fluid communication is tightly connected, the liquid outlet of cylinder (5) at the bottom of described extraction and the feed liquor of described second gas-liquid flow siphunculus (21)
End fluid communication is tightly connected, the liquid outlet of described second gas-liquid flow siphunculus (21) and the bottleneck fluid communication of described flask (3)
Being tightly connected, described flask (3) is located in described electric jacket (2), and described electric jacket (2) is placed on described magnetic stirring apparatus (1),
Described flask is provided with magnet rotor in (3);The air inlet of described first airway (10) is given vent to anger with described second airway (9)
Mouth fluid communication is tightly connected.
Reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae the most according to claim 1,
It is characterized in that, in described extraction cylinder (6) and in cylinder (5) at the bottom of described extraction, be equipped with filter course (24).
Reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae the most according to claim 2,
It is characterized in that, described filter course (24) is degreasing cotton layer.
4. according to arbitrary described the carrying for the backflow of extraction hypolipidemic activity material from alura fine horse Fructus Jujubae of claims 1 to 3
Fetching is put, it is characterised in that the inlet end of described spherical condensation tube (8) is provided at described first gas-liquid flow siphunculus (13) and gives vent to anger
In the described first gas-liquid flow siphunculus (13) of end, close on described first gas-liquid flow of described first gas-liquid flow siphunculus (13) gas outlet
The inwall of siphunculus (13) is provided with the first frosted layer (14), described first frosted layer (14) and described spherical condensation tube (8) air inlet
The frosted layer of end is tightly connected.
Reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae the most according to claim 4,
It is characterized in that, described first gas-liquid flow siphunculus (13) liquid outlet is located in the liquid feeding end of described extraction cylinder (6), closes on described
The outer wall of the described first gas-liquid flow siphunculus (13) of one gas-liquid flow siphunculus (13) liquid outlet is provided with the second frosted layer (15);Close on
Described extraction cylinder (6) inwall of described extraction cylinder (6) liquid feeding end is provided with the 3rd frosted layer (16) layer, described second frosted layer
(15) it is tightly connected with described 3rd frosted layer (16) layer.
Reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae the most according to claim 5,
It is characterized in that, the liquid outlet of described extraction cylinder (6) is located in the liquid feeding end of cylinder (5) at the bottom of described extraction, closes on described extraction cylinder
(6) outer wall of the described extraction cylinder (6) of liquid outlet is provided with the 4th frosted layer (17) layer;Close on entering of cylinder (5) at the bottom of described extraction
The inwall of cylinder (5) at the bottom of the described extraction of liquid mouth is provided with the 5th frosted layer (19), described 4th frosted layer (17) layer and described the
Five frosted layers (19) are tightly connected.
Reflux, extract, device for extracting hypolipidemic activity material from alura fine horse Fructus Jujubae the most according to claim 6,
It is characterized in that, the liquid outlet of cylinder (5) at the bottom of described extraction is located in the liquid feeding end of described second gas-liquid flow siphunculus (21), closes on institute
State the outer wall of cylinder (5) at the bottom of the described extraction of the liquid outlet extracting end cylinder (5) and be provided with the 6th frosted layer (20), close on described second
The inwall of the described second gas-liquid flow siphunculus (21) of gas-liquid flow siphunculus (21) inlet is provided with the 7th frosted layer (22), and described
Six frosted layers (20) are tightly connected with described 7th frosted layer (22).
8. according to arbitrary described the carrying for the backflow of extraction hypolipidemic activity material from alura fine horse Fructus Jujubae of claim 5~7
Fetching is put, it is characterised in that the liquid outlet of described second gas-liquid flow siphunculus (21) is located in the bottleneck of described flask (3), closes on
The outer wall of the described second gas-liquid flow siphunculus (21) of the liquid outlet of described second gas-liquid flow siphunculus (21) is provided with the 8th frosted layer
(23), described 8th frosted layer (23) is tightly connected with the frosted layer of described flask (3) bottleneck.
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Cited By (1)
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CN108579123A (en) * | 2018-04-08 | 2018-09-28 | 太极集团四川南充制药有限公司 | The method for extracting liposoluble constituent with solvent recovery integrated apparatus using fat-soluble ingredient cycle extraction |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108579123A (en) * | 2018-04-08 | 2018-09-28 | 太极集团四川南充制药有限公司 | The method for extracting liposoluble constituent with solvent recovery integrated apparatus using fat-soluble ingredient cycle extraction |
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Granted publication date: 20161130 Termination date: 20170707 |