CN204107349U - Novel silicon oil emulsion reactor - Google Patents
Novel silicon oil emulsion reactor Download PDFInfo
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- CN204107349U CN204107349U CN201420572844.9U CN201420572844U CN204107349U CN 204107349 U CN204107349 U CN 204107349U CN 201420572844 U CN201420572844 U CN 201420572844U CN 204107349 U CN204107349 U CN 204107349U
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Abstract
The utility model provides novel silicon oil emulsion reactor, mainly comprise baiting valve (1), reactor external heating jacket entrance (2), anchor agitator (3), in reactor heat(ing) coil (4), reactor external heating jacket (5), reactor end socket (6), reactor manhole (7), vertical type speed reducer (change gear) (8), reactor stirring motor (9), adjustable speed high-shear emulsion machine (10), emulsification pretreatment machine shaft (11), interior heat(ing) coil gateway (12), the outlet of reactor external heating jacket (13), high-speed shearing emulsion machine stirrer paddle (14), reactor shell (15), adjustable speed high-shear emulsion machine stirring-head (16).The utility model is cooperatively interacted by the anchor agitator in reactor and adjustable speed high-shear emulsion machine, interior heat(ing) coil, reactor external heating jacket, acting in conjunction, solving existing emulsifying device can not abundant silicone oil emulsification problem, avoid that silicone oil in emulsion process solidifies, emulsification is uneven, affect the problems such as operating efficiency.
Description
Technical field
The utility model relates generally to silicone oil emulsification apparatus field, particularly relates to and has viscous silicone fluid emulsifying device.
Background technology
Silicone oil (polysiloxanes) has excellent chemical stability, heat-resisting cold resistance, weatherability, electrical insulating property, biological nature, hydrophobicity, lubricity, high refractiveness and bin stability, be widely used in various industrial trade, comprise the every field such as automobile, building, chemicals, electrical engineering and electronics industry, medical industry, paper pulp and papermaking, transport service, aerospace industry, weaving, leather, mechanical engineering, intermetallic composite coating.
Viscous silicone fluid is highly viscous fluid, due to good film-forming property, can be used for repairing the damage of hair and improves cardability, simultaneously because having the lubricating function of uniqueness, its excellent in performance as skin moisturizing agent, hair conditioner oneself generally acknowledged widely.On the other hand, silicone oil is due to its hydrophobicity, and in aqueous phase, be difficult to dispersion, then feel, fastness and elasticity are all undesirable to directly apply to fiber, can apply after therefore needing to be prepared into silicone oil emulsion.With pure silicon oil phase ratio, silicone oil emulsion not only product form has changed, and performance is also made a world of difference.It is existing own general for aspects such as cosmetics, hair products, plastic processing and textile finishings that current height glues silicone oil emulsion, and this aspect such as external building surface waterproof and leather nursing is also widely used.
The emulsification of high sticky silicone oil also exists the problems such as the wide and poor controllability of emulsification difficulty, stability of emulsion distribution of particles that is poor, emulsion always.It is oil-in-water type that usual height glues silicone oil emulsion, is convenient to association area and uses.In existing emulsification technology, conventional industrialization process is all interval emulsification, adds aqua and the emulsifying agent of a part in Autoclave, start and stir, then drop into silicone oil (oil phase), drip aqua and emulsifying agent (aqueous phase), do not stop stirring and emulsifying, last discharging.
Publication CN102961987A has the sticky silicone oil emulsification technique of serialization height and the equipment thereof of premixed: be made up of aqueous phase preparing tank, aqueous phase measuring tank, aqueous phase centrifugal pump, oil phase measuring tank, oil phase impeller pump, premixed Quimby pump, static mixer, emulsification stirred tank, circulation impeller pump and vacuum system.Emulsification stirred tank by cylindrical shell, upper cover, chuck, driving mechanism, shaft, upper strata paddle, intermediate agitation oar, end paddle, charging aperture, discharging opening, loop back head piece and vacuum orifice forms; End paddle is the oblique oar form of 45 °, four leaf, and during installation, it is 30 ~ 40mm from cylinder body bottom distance, and intermediate agitation oar is the oblique oar form of 45 °, two leaf, and upper strata paddle is two leaves, 45 ° of oblique oars, and its angle is contrary with the angle of paddle; Driving mechanism can stepless speed regulation; Described vacuum orifice is arranged on upper cover.Complex structure, bottom is stirred uneven.
Publication 201220003338.9 silicone oil emulsification agitating device: cylinder lateral wall is provided with handle, cylindrical shell bottom is installed with road wheel, shaft is provided with above cylindrical shell, shaft is lifted on above cylindrical shell by fixed pulley, suspension ring and lifting rope, the lower end of shaft is installed with agitator, agitator includes two fixed disks, be installed with several teeter column, and shaft is driven between two fixed disks by motor.Suspension ring are provided with the stay cord of mobile shaft.Be not suitable for viscous silicone fluid emulsification mixing.
Utility model content
The purpose of this utility model is the deficiency in order to make up prior art, provide novel silicon oil emulsion reactor, solving existing emulsifying device can not abundant silicone oil emulsification problem, avoids that silicone oil in emulsion process solidifies, emulsification is uneven, affects the problems such as operating efficiency.
The utility model is achieved through the following technical solutions:
Novel silicon oil emulsion reactor, comprise baiting valve (1), reactor external heating jacket entrance (2), anchor agitator (3), in reactor heat(ing) coil (4), reactor external heating jacket (5), reactor end socket (6), reactor manhole (7), vertical type speed reducer (change gear) (8), reactor stirring motor (9), adjustable speed high-shear emulsion machine (10), emulsification pretreatment machine shaft (11), interior heat(ing) coil gateway (12), the outlet of reactor external heating jacket (13), high-speed shearing emulsion machine stirrer paddle (14), reactor shell (15), adjustable speed high-shear emulsion machine stirring-head (16).
Described novel silicon oil emulsion reactor is normal pressure reactor.Reactor is stainless steel reactor, or glass lined reaction vessel, or carbon steel lining fiberglass reactor.
In described novel silicon oil emulsion reactor, (4) heat(ing) coil is stainless steel tube, or carbon steel pipe; Interior heat(ing) coil (4) gateway from the preformed hole turnover (6) of stainless steel reactor end socket, or processing reactor cylindrical shell (15) time reserved.
(10) rotating speed per minute is between 0-18000 for the adjustable speed high-shear emulsion machine of described novel silicon oil emulsion reactor, and (16) (11) emulsification pretreatment machine shaft be 304 stainless steels with adjustable speed high-shear emulsion machine stirring-head.
(14) (11) the adjustable speed high-shear emulsion machine shaft (10) of described novel silicon oil emulsion reactor increase layer 2-3 impeller type stirring blade leaf.
(10) the adjustable speed high-shear emulsion machine of described novel silicon oil emulsion reactor is vertically arranged in stainless steel reactor end socket horizontal DN80 preformed hole (6), and (14) shaft (11) bottom is designed with layer 2-3 impeller type stirring blade leaf.Silicone oil emulsification reactor operation principle is: the anchor formula of reactor stirs rotating speed per minute generally between 50-130, undesirable to the stirring and mixing effect of high-viscosity material; By to increase in reactor heat(ing) coil (4) with adjustable speed high-shear emulsion machine (9), speed governing high-shear emulsion machine rotating speed per minute, generally between 0-18000, speeds programming rate on the one hand, reduces material viscosity; (14) stirred with anchor formula by increase layer 2-3 impeller type stirring blade leaf on the other hand and cooperatively interact, then by adjustable speed high-shear emulsion machine (10) to the acting in conjunction that high-viscosity material high shear is stirred, reach the fully emulsified reaction of silicone oil; In process, hand labor intensity is little, time saving and energy saving, improves operating efficiency.
The utility model has the advantages that:
The utility model reasonable in design, easy to install, ensure that in emulsion process, silica gel can not solidify or emulsification uneven, it is uniformly mixed fully, meet the requirement of emulsion process, and by increase in reactor heat(ing) coil (4) with adjustable speed high-shear emulsion machine (9), make workman's labor intensity little, time saving and energy saving, improve operating efficiency.
Accompanying drawing explanation
accompanying drawing 1for the utility model structural representation, in figure, critical piece title is as follows:
(1) baiting valve, (2) reactor external heating jacket entrance, (3) anchor agitator, (4) heat(ing) coil in reactor, (5) reactor external heating jacket, (6) reactor end socket, (7) reactor manhole, (8) vertical type speed reducer (change gear), (9) reactor stirring motor, (10) adjustable speed high-shear emulsion machine, (11) emulsification pretreatment machine shaft, (12) interior heat(ing) coil gateway, (13) reactor external heating jacket outlet, (14) high-speed shearing emulsion machine stirrer paddle, (15) reactor shell, (16) adjustable speed high-shear emulsion machine stirring-head.
Detailed description of the invention
See accompanying drawing 1, novel silicon oil emulsion reactor comprise baiting valve (1), reactor external heating jacket entrance (2), anchor agitator (3), in reactor heat(ing) coil (4), reactor external heating jacket (5), reactor end socket (6), reactor manhole (7), vertical type speed reducer (change gear) (8), reactor stirring motor (9), adjustable speed high-shear emulsion machine (10), emulsification pretreatment machine shaft (11), interior heat(ing) coil gateway (12), the outlet of reactor external heating jacket (13), high-speed shearing emulsion machine stirrer paddle (14), reactor shell (15), adjustable speed high-shear emulsion machine stirring-head (16).
Described novel silicon oil emulsion reactor is 1000 liter of 304 stainless steel normal pressure reactor.
In described novel silicon oil emulsion reactor, (4) heat(ing) coil is DN20 stainless steel tube, interior heat(ing) coil (4) gateway from stainless steel reactor end socket (6) DN50 preformed hole turnover.
(10) rotating speed per minute is between 0-18000 for the adjustable speed high-shear emulsion machine of described novel silicon oil emulsion reactor, and (16) (11) emulsification pretreatment machine shaft be 304 stainless steels with adjustable speed high-shear emulsion machine stirring-head.
(10) the adjustable speed high-shear emulsion machine of described novel silicon oil emulsion reactor is vertically arranged in stainless steel reactor end socket horizontal DN80 preformed hole (6), and (14) shaft (11) bottom is designed with layer 2-3 impeller type stirring blade leaf.
Claims (5)
1. novel silicon oil emulsion reactor, is characterized in that: comprise baiting valve (1), reactor external heating jacket entrance (2), anchor agitator (3), in reactor heat(ing) coil (4), reactor external heating jacket (5), reactor end socket (6), reactor manhole (7), vertical type speed reducer (change gear) (8), reactor stirring motor (9), adjustable speed high-shear emulsion machine (10), emulsification pretreatment machine shaft (11), interior heat(ing) coil gateway (12), the outlet of reactor external heating jacket (13), high-speed shearing emulsion machine stirrer paddle (14), reactor shell (15), adjustable speed high-shear emulsion machine stirring-head (16).
2. novel silicon oil emulsion reactor according to claim 1, is characterized in that: reactor is stainless steel reactor, or glass lined reaction vessel, or carbon steel lining fiberglass reactor.
3. novel silicon oil emulsion reactor according to claim 1, is characterized in that: (4) interior heat(ing) coil is stainless steel tube, or carbon steel pipe; Interior heat(ing) coil (4) gateway from the preformed hole turnover (6) of reactor end socket, or processing reactor cylindrical shell (15) time reserved.
4. novel silicon oil emulsion reactor according to claim 1, it is characterized in that: adjustable speed high-shear emulsion machine (10) rotating speed per minute between 0-18000, emulsification pretreatment machine shaft (11) with adjustable speed high-shear emulsion machine stirring-head (16) material be 304 stainless steels.
5. novel silicon oil emulsion reactor according to claim 1, is characterized in that: (14) (11) adjustable speed high-shear emulsion machine shaft (10) increase layer 2-3 impeller type stirring blade leaf.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201420572844.9U CN204107349U (en) | 2014-10-06 | 2014-10-06 | Novel silicon oil emulsion reactor |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201420572844.9U CN204107349U (en) | 2014-10-06 | 2014-10-06 | Novel silicon oil emulsion reactor |
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CN204107349U true CN204107349U (en) | 2015-01-21 |
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CN201420572844.9U Active CN204107349U (en) | 2014-10-06 | 2014-10-06 | Novel silicon oil emulsion reactor |
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CN (1) | CN204107349U (en) |
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2014
- 2014-10-06 CN CN201420572844.9U patent/CN204107349U/en active Active
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