CN202626102U - Chemical luminescent device - Google Patents
Chemical luminescent device Download PDFInfo
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- CN202626102U CN202626102U CN 201220069017 CN201220069017U CN202626102U CN 202626102 U CN202626102 U CN 202626102U CN 201220069017 CN201220069017 CN 201220069017 CN 201220069017 U CN201220069017 U CN 201220069017U CN 202626102 U CN202626102 U CN 202626102U
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- aluminium foil
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Abstract
The utility model discloses a chemical luminescent device. The technical scheme of the utility model is as follows: the chemical luminescent device comprises a cavity (4) surrounded by a light-transmitting deformable shell (1), wherein one or more broken chemiluminescent agent storage device(s) (6) is/ are arranged in the cavity (4); and each broken chemiluminescent agent storage device comprises a sealing bag which is made of a high polymer film, sealed with the chemiluminescent agent (5) and wrapped in an aluminium foil layer (2). According to the chemical luminescent device, the thin shell can be applied to the chemical luminescent device, so that the maximum separation protection is provided for an oxalate component and an activating agent at the same time before use; and the needed artistic effect can be provided by applying the collocation of a liquid absorption layer and a light shielding layer.
Description
Technical field
The utility model relates to a kind of chemical photic device.
Background technology
The longest structure of seeing of general commercially available chemical photic device is: the glass ampere seals a kind of chemiluminescence medicament; The another kind of chemiluminescence medicament of space sealing between variable plastic casing and the glass ampere bottle makes two kinds of medicament generation chemical reactions obtain chemoluminescences thereby break the ampere bottle during use.It is extremely sensitive to water that the use of glass ampere bottle comes from the chemiluminescence medicament some composition, and the crushability of glass ampere bottle provides a kind of good startup form to this binary reaction device in addition.But the use of glass has limited a lot of Products Development, and the product of shell class especially is because the problem that pierces through of broken glass and the development that safety-problems is hindering product form always.The another kind of chemiluminescence medicament of space sealing between plastic casing and the glass ampere bottle contains hydrogen peroxide usually in addition, and the long-time storage before using causes hydrogen peroxide from plastic casing, to ooze out and lost efficacy unavoidable.
Above-mentioned chemiluminescence medicament be by substituted-phenyl oxalate ester, fluorescent agent, peroxo-agent, catalyzer, solvent etc. constitute.We are called " barkite component " to the component that contains substituted-phenyl oxalate ester (abbreviation barkite), are called " activator " to the component that contains the peroxo-agent, and normally used peroxo-agent is a hydrogen peroxide, or carbamide peroxide.Most popular under normal conditions substituted-phenyl oxalate ester is meant two (2,4,5-three chloro-salicylic acid's n-pentyl esters) barkites (CPPO) or two (2,4,5-trichlorine Salicylate Isomyl) barkite (CIPO).Because barkite is easy to hydrolysis,, just be sealed in the composition in the glass ampere bottle usually so the barkite component is that the exhausted water of requirement is preserved usually.
The aluminum foil material of composite high-molecular material also is good exhausted water material, and the aluminum foil material of composite high-molecular material can be processed container barkite component very easily and prevent that to preserve it it is rotten.But the long immersion of the solution of barkite component can cause polymer thin-film material to separate with aluminium foil again; Final aluminium foil can be peeled away with polymeric film fully, thereby thereby causing extraneous oxidation liquid or moisture to immerse the solution that causes the barkite component from the position of peeling off lost efficacy.Should technology not be suitable for sealing the oxidation liquid that contains hydrogen peroxide more simultaneously, and, caused the whole protecting device to disintegrate because hydrogen peroxide composition wherein is more prone to cause polymkeric substance to separate with aluminum foil material, thus the loss of the hydrogen peroxide that causes or leakage.
Summary of the invention
The purpose of the utility model is that a kind of chemical photic device will be provided, and it has avoided the use of glass ampere, has improved the safety in utilization of device.Simultaneously well isolated barkite component and activator, reduced of the influence of their influence and external environments each other them.The technical scheme of taking for the purpose that reaches the utility model comprises; The cavity 4 that surrounds by the shell 1 of variable light transmission shape; Have in the cavity 4 one or more can broken chemiluminescence medicament storage device 6, can broken chemiluminescence medicament storage device 6 comprise being wrapped in the air-tight pouch 3 that the high molecular polymer films that are sealed with chemiluminescence medicament 5 in the aluminium foil layer 2 are processed.
In the above-mentioned chemical photic device, in the described cavity 4 chemiluminescence medicament 5 is housed, described chemiluminescence medicament 5 is barkite component 5-A or activator 5-B.
In the above-mentioned chemical photic device, described shell 1 is processed by film or thin plate material, and its thickness is between 0.04mm-2mm; Its material can be Vilaterm or Vestolen PP 7052 or nylon or SE or polyethylene terephthalate or PVAC polyvinylalcohol or polyvinylidene chloride or high-barrier MA-PVDC or ethylene/vinyl alcohol copolymer EVOH or gather naphthalene ester PEN, or two or more bilayer to the multiwalled matrix material in these materials.
In the above-mentioned chemical photic device, liquid-adsorption layer or and light-shielding layer are housed in the described cavity 4.
In the above-mentioned chemical photic device, the cavity that said cavity 4 inside are vacuumized.
In the above-mentioned chemical photic device; Described air-tight pouch 3, its material can be perfluoroethylene third rare (FEP) or Meltability polytetrafluorethyletubular (PFA) or Vestolen PP 7052 (PP) or Vilaterm (PE) or SE (PVC) or polyester (PET) or polyvinylidene chloride (PVDC) or high-barrier MA-PVDC; The thickness of described high molecular polymer film is between 0.0001mm-0.3mm; Described aluminium foil layer 2 is made up of one or more layers aluminium foil, each layer aluminium foil by one or many open the aluminium foils parcel and form, the thickness of every or every layer aluminium foil is between 0.001mm-0.2mm; Described aluminium foil layer 2 is exposed to extraneous limit quilt other part backfin one or many formation backfin seal area 10 with its contacted aluminium foil.
In the above-mentioned chemical photic device, the described all or part of sealer coat that is provided with of outside surface that can broken chemiluminescence medicament storage device 6, this sealer coat obtains through aluminium foil layer partly or entirely impregnated in the liquid curable sealing material; Described sealing material is curable liquid macromolecule resin material or wax or sticker, and its cure states is breakable;
Described outer surface part that can broken chemiluminescence medicament storage device 6 impregnated in the liquid curable sealing material; Be meant and be exposed to extraneous aluminium foil limit backfin one or many formation backfin seal area 10 together; Sealing material obtains sealer coat thereby this backfin place is impregnated in curable liquid, makes the backfin slit sealed by sealing material.
In the above-mentioned chemical photic device, described coated outside that can broken chemiluminescence medicament storage device 6 has nonocclusive high molecular polymer film.
In the above-mentioned chemical photic device; Can be crushed from shell 1 external application pressure or pierced through or cut by broken chemiluminescence medicament storage device 6 in the described cavity 4 by the sharp-pointed or sharp object in the cavity 4, thus the chemiluminescence medicament 5 of its seal inside is discharged in the printing opacity cavity 4.
In the above-mentioned chemical photic device, the capsule 3 that described high molecular polymer film is processed is provided with into Kai Qu; This enters out the district can be thin zone that pre-treatment goes out on the air-tight pouch 3 or the indentation that does not penetrate; Or the fusion potted line that is easier to be opened that when the thermofussion welding edge, obtains through suitable heat sealed time and heat-seal temperature and pressure, or the concavo-convex sealing groove that matches is welded on the seal that the internal surface of film forms.
The chemical photic device of the utility model does not use glass ampere bottle; Make the shell shell can be applied in the chemical photic device; To barkite component and activator maximum isolating and protecting is provided before use simultaneously, but also can have used liquid-adsorption layer or needed artistic effect is provided with the collocation of light-shielding layer.
Description of drawings
Fig. 1 is the structure cross-sectional schematic of this device;
Fig. 2 be can broken chemiluminescence medicament storage device structural representation;
Fig. 3 establishes the structural representation of the chemical photic device with pattern display function of liquid-adsorption layer and light shield layer in being;
Fig. 4 is the STRUCTURE DECOMPOSITION synoptic diagram of Fig. 3.
Embodiment
As shown in Figure 1; 1 is shell; Shell 1 is that the deformable thickness by a printing opacity is that the acrylic sheet material of 0.65mm is processed; Periphery through the melting welding acrylic sheet forms hermetic cavity body 4, and in cavity 4, being equipped with one can broken chemiluminescence medicament storage device 6, and the air-tight pouch of can broken chemiluminescence medicament storage device 6 being processed by the high molecular polymer film that is sealed with chemiluminescence medicament of aluminium foil layer 2 parcels 3 (hereinafter to be referred as capsule 3) constitutes.The material of capsule 3 can be perfluoroethylene third rare (FEP) or Meltability polytetrafluorethyletubular (PFA) or Vestolen PP 7052 (PP) or Vilaterm (PE) or SE (PVC) or polyester (PET) or polyvinylidene chloride (PVDC) or high-barrier MA-PVDC; The thickness of described high molecular polymer film between 0.0001mm-0.3mm, preferred 0.01mm-0.1mm.What select for use in the present embodiment is the capsule 3 that the polyvinylidene film weld all around periphery of 0.03mm thickness is processed.Usually, chemiluminescence medicament is meant barkite component 5-A or activator 5-B.In the middle of present embodiment, sealing is the liquid that contains the component 5-A of barkite in the capsule 3, and that sealing is activator 5-B in cavity 4, and activator 5-B can be that liquid also can be solid, for example carbamide peroxide.
The material of shell 1 can also be a thin-film material, the thickness of material between 0.04mm-2mm, preferred 0.06mm-0.8mm; Its material can also be Vilaterm or Vestolen PP 7052 or nylon or SE or polyethylene terephthalate or PVAC polyvinylalcohol or polyvinylidene chloride or high-barrier MA-PVDC or ethylene/vinyl alcohol copolymer EVOH or gather naphthalene ester PEN, or two or more bilayer to the multiwalled matrix material in these materials.Cavity 4 can also have openable opening, can be discharged to shell 1 outside with mixing the luminous liquid in back.
When producing; We are sealed in barkite component 5-A in the capsule 3 earlier, use then thickness as the aluminium foil of 0.02mm closely winding up form aluminium foil layer 2 in the outside of capsule 3, the aluminium foil area of use is greater than the shared area of capsule 3; The aluminium foil that exceeds capsule 3 will compress each other closely; And to the backfin and compress (as shown in Figure 2) repeatedly of the edge of aluminium foil be formed backfin seal area 10, aluminium foil layer 2 plays the effect that is isolated in capsule 3 and the external environment that makes.
In the middle of actual production, we can adopt laminated aluminium foil that capsule 3 is wrapped up, and make aluminium foil layer 2 sealings more reliable.The multiwalled parcel can be that an aluminium foil carries out the multiwalled winding up to capsule 3, also can be that many aluminium foil repeatedly encases capsule 3.No matter be multilayer winding up or many parcels, each layer or each are opened the edge of aluminium foil preferably will reserve the backfin sealing that suitable area is used for outermost edge.The thickness of each layer aluminium foil layer 2 can be 0.001mm-0.2mm.The aluminum foil material thickness that present embodiment is used is at 0.06mm.The scope of preferred aluminum foil thickness is between the 0.006mm-0.09mm.
In use; Only need in the cavity 4 of this chemical photic device shell 1 in device, exert pressure; Aluminium foil layer 2 also deforms, and squeeze is passed to capsule 3, and the film of capsule 3 breaks under pressure; Simultaneously aluminium foil layer 2 also the backfin seal area 10 at the edge of deformation fracture or aluminium foil layer 2 outwards squeezed moving strength and open by inner; The chemiluminescence medicament of liquid flows out can broken chemiluminescence medicament storage device 6, component 5-A that contain barkite in the capsule 3 is flow in the cavity 4 mix with activator 5-B, thereby obtain chemoluminescence.
Because this device in use, chemiluminescence reaction can produce portion gas, influences this device effect in use, and we can vacuumize processing in cavity 4 inside to this device when producing.
Like Fig. 3, shown in Figure 4; 1 is the shell that composite film material that the outer polyester PET total thickness of inner layer polyethylene of a printing opacity is 0.2mm is processed; Shell 1 weld all around contoured becomes cavity 4; 6 is can broken chemiluminescence medicament storage device, can comprise the capsule that is sealed with chemiluminescence medicament 3 by aluminium foil layer 2 parcels by broken chemiluminescence medicament storage device 6.In the middle of present embodiment, component 5-A and the activator 5-B that we will contain barkite is sealed in two respectively by 3 li in the capsule of aluminium foil layer 2 parcels, and processing two independently can broken chemiluminescence medicament storage device 6.7 is image device, and 8 is the pierced pattern that on image device, is provided with.In the middle of present embodiment, image device 7 is two thin plates of engraving the pentagram pattern, and the material of thin plate is the light-shielding layer that macromolecular material or light-proof materials such as paper or aluminium foil are processed.Between cavity 4 inherent these two image devices 7 liquid-adsorption layer 9 is housed also.The material of liquid-adsorption layer 9 can be polypropylene non-woven fabric or paper.In use, divide don't push broken two can broken chemiluminescence medicament storage device 6, let the component 5-A that contains barkite flow in the cavity 4 and be adsorbed on back mixing on the liquid-adsorption layer 9 with activator 5-B, the blended soup promptly produces chemoluminescence.Because image device 7 is processed by light-proof material; And on this lighttight material, engraved out star-like shape; And the liquid-adsorption layer 9 that has adsorbed luminescent solution is set between these the two lighttight image devices 7, makes chemoluminescence to come out from star-like pierced pattern 8 irradiations.
We can also adopt PP SHEET FOR OPP TAPE (being the BOPP film) composite polyethylene (PE) film that is printed with multi color pattern as image device 7.Like this, in use, the pattern on the image device 7 will be bright by the illumination that chemiluminescent fluid is sent, and its pattern will be by coming out to the surface emitting of shell 1 in the cavity 4.Described printed layers can be on the interlayer face of two-layer matrix material.
For improve can broken chemiluminescence medicament storage device 6 stopping property; Make capsule 3 more effectively with can broken chemiluminescence medicament storage device 6 external environments in moisture isolated; We can be with can broken chemiluminescence medicament storage device 6 or backfin seal area 10 places of aluminium foil layer 2 dipping sealing material; Like paraffin, lower molecular weight PE, epoxy resin, high-consistency petroleum base railway grease, silicon wax, polyurethane adhesive etc. all is operable sealing material, and these sealing materials must fragmentation under external force after curing.When for example producing; Can the broken chemiluminescence medicament storage device 6 whole waxes of putting into thawing; Promptly let liquid wax the slit of backfin seal area 10 filled and the surface of whole aluminium foil layer 2 is covered; Can take out under the placement normal temperature by broken chemiluminescence medicament storage device 6 then, make the wax of aluminium foil layer 2 surfaces and backfin seal area 10 solidify to form sealer coat.Also can be only backfin seal area 10 places that can broken chemiluminescence medicament storage device 6 be immersed in and fill its slit of sealing in the fused wax liquid.Because solidified wax is broken easily, can not influence the release of inner chemiluminescence medicament.
Outside that can broken chemiluminescence medicament storage device 6 can be enclosed with nonocclusive high molecular polymer film, punctures film shell 1 with the wedge angle of avoiding aluminium foil layer backfin seal area 10 to form.Also can be wrapped in the outside of aluminium foil layer 2 with the mode of thermal contraction casing tube, but for the liquid after the device fragmentation can be flowed out, so wrap must leave slit or opening.
In the above-mentioned chemical photic device; In the described cavity 4 sharp-pointed or sharp objects can be housed; Piercing through or cut when being used for from shell 1 external application pressure pressing can broken chemiluminescence medicament storage device 6, thereby the chemiluminescence medicament 5 of its seal inside is discharged in the printing opacity cavity 4.
The capsule 3 that above-mentioned high molecular polymer film is processed is provided with into Kai Qu.Can be thin zone that pre-treatment goes out on the air-tight pouch 3 or the indentation that does not penetrate; Or the fusion potted line that is easier to be opened that when the thermofussion welding edge, obtains through suitable heat sealed time and heat-seal temperature and pressure, or the concavo-convex sealing groove that matches is welded on the seal that the internal surface of film forms.
The above only is the preferred implementation of the utility model; Should be understood that; For those skilled in the art; Under the prerequisite that does not break away from the utility model know-why, can also make some improvement and retouching, these improvement and retouching also should be regarded as the protection domain of the utility model
Claims (16)
1. chemical photic device; It is characterized in that; Comprise the cavity (4) that the shell (1) by variable light transmission shape surrounds; Have in this cavity (4) one or more can broken chemiluminescence medicament storage device (6), can broken chemiluminescence medicament storage device (6) comprise being wrapped in the air-tight pouch (3) that the high molecular polymer film that is sealed with chemiluminescence medicament (5) in the aluminium foil layer (2) is processed.
2. chemical photic device according to claim 1 is characterized in that, chemiluminescence medicament (5) is housed in the described cavity (4), and described chemiluminescence medicament (5) is barkite component 5-A or activator 5-B.
3. chemical photic device according to claim 1 is characterized in that, described shell (1) is processed by film or thin plate material, and its thickness is between 0.04mm-2mm; Its material can be Vilaterm or Vestolen PP 7052 or nylon or SE or polyethylene terephthalate or PVAC polyvinylalcohol or polyvinylidene chloride or high-barrier MA-PVDC or ethylene/vinyl alcohol copolymer EVOH or gather naphthalene ester PEN, or two or more bilayer to the multiwalled matrix material in these materials.
4. according to claim 1 or 2 or 3 described chemical photic devices, it is characterized in that, liquid-adsorption layer or and light-shielding layer are housed in the described cavity (4).
5. according to claim 1 or 2 or 3 described chemical photic devices, it is characterized in that the cavity that said cavity (4) inside is vacuumized.
6. according to claim 1 or 2 or 3 described chemical photic devices; It is characterized in that the material of described air-tight pouch (3) can be perfluoroethylene third rare (FEP) or Meltability polytetrafluorethyletubular (PFA) or Vestolen PP 7052 (PP) or Vilaterm (PE) or SE (PVC) or polyester (PET) or polyvinylidene chloride (PVDC) or high-barrier MA-PVDC; The thickness of described high molecular polymer film is between 0.0001mm-0.3mm; Described aluminium foil layer (2) is made up of one or more layers aluminium foil, each layer aluminium foil by one or many open the aluminium foils parcel and form, the thickness of every or every layer aluminium foil is between 0.001mm-0.2mm; Described aluminium foil layer (2) is exposed to extraneous limit quilt other part backfin one or many formation backfin seal area (10) with its contacted aluminium foil.
7. according to claim 1 or 2 or 3 described chemical photic devices; It is characterized in that; The described all or part of sealer coat that is provided with of outside surface that can broken chemiluminescence medicament storage device (6), this sealer coat obtains through aluminium foil layer partly or entirely impregnated in the liquid curable sealing material; Described sealing material is curable liquid macromolecule resin material or wax or sticker, and its cure states is breakable;
Described outer surface part that can broken chemiluminescence medicament storage device (6) impregnated in the liquid curable sealing material; Be meant and be exposed to extraneous aluminium foil limit quilt other part backfin one or many with its contacted aluminium foil; Sealing material obtains sealer coat thereby this backfin place is impregnated in curable liquid, makes the backfin slit sealed by sealing material.
8. according to claim 1 or 2 or 3 described chemical photic devices, it is characterized in that described coated outside that can broken chemiluminescence medicament storage device (6) has nonocclusive high molecular polymer film.
9. chemical photic device according to claim 6 is characterized in that, described coated outside that can broken chemiluminescence medicament storage device (6) has nonocclusive high molecular polymer film.
10. chemical photic device according to claim 7 is characterized in that, described coated outside that can broken chemiluminescence medicament storage device (6) has nonocclusive high molecular polymer film.
11. according to claim 1 or 2 or 3 described chemical photic devices; It is characterized in that; Can be crushed from shell (1) external application pressure or pierced through or cut by broken chemiluminescence medicament storage device (6) in the described cavity (4) by the sharp-pointed or sharp object in the cavity (4), thus the chemiluminescence medicament (5) of its seal inside is discharged in the printing opacity cavity (4).
12. chemical photic device according to claim 6; It is characterized in that; Can be crushed from shell (1) external application pressure or pierced through or cut by broken chemiluminescence medicament storage device (6) in the described cavity (4) by the sharp-pointed or sharp object in the cavity (4), thus the chemiluminescence medicament (5) of its seal inside is discharged in the printing opacity cavity (4).
13. chemical photic device according to claim 7; It is characterized in that; Can be crushed from shell (1) external application pressure or pierced through or cut by broken chemiluminescence medicament storage device (6) in the described cavity (4) by the sharp-pointed or sharp object in the cavity (4), thus the chemiluminescence medicament (5) of its seal inside is discharged in the printing opacity cavity (4).
14., it is characterized in that the capsule (3) that described high molecular polymer film is processed is provided with into Kai Qu according to claim 1 or 2 or 3 described chemical photic devices; This enters out the district can be thin zone that pre-treatment goes out on the air-tight pouch (3) or the indentation that does not penetrate; Or the fusion potted line that is easier to be opened that when the thermofussion welding edge, obtains through suitable heat sealed time and heat-seal temperature and pressure, or the concavo-convex sealing groove that matches is welded on the seal that the internal surface of film forms.
15. chemical photic device according to claim 6 is characterized in that, the capsule (3) that described high molecular polymer film is processed is provided with into Kai Qu; This enters out the district can be thin zone that pre-treatment goes out on the air-tight pouch (3) or the indentation that does not penetrate; Or the fusion potted line that is easier to be opened that when the thermofussion welding edge, obtains through suitable heat sealed time and heat-seal temperature and pressure, or the concavo-convex sealing groove that matches is welded on the seal that the internal surface of film forms.
16. chemical photic device according to claim 7 is characterized in that, the capsule (3) that described high molecular polymer film is processed is provided with into Kai Qu; This enters out the district can be thin zone that pre-treatment goes out on the air-tight pouch (3) or the indentation that does not penetrate; Or the fusion potted line that is easier to be opened that when the thermofussion welding edge, obtains through suitable heat sealed time and heat-seal temperature and pressure, or the concavo-convex sealing groove that matches is welded on the seal that the internal surface of film forms.
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220069017 CN202626102U (en) | 2012-02-27 | 2012-02-27 | Chemical luminescent device |
| US14/118,164 US9488319B2 (en) | 2011-05-17 | 2012-05-16 | Film chemiluminescent device |
| PCT/CN2012/000676 WO2012155537A1 (en) | 2011-05-17 | 2012-05-16 | A film chemiluminescent device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201220069017 CN202626102U (en) | 2012-02-27 | 2012-02-27 | Chemical luminescent device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN202626102U true CN202626102U (en) | 2012-12-26 |
Family
ID=47379322
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201220069017 Expired - Lifetime CN202626102U (en) | 2011-05-17 | 2012-02-27 | Chemical luminescent device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN202626102U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108343847A (en) * | 2017-01-23 | 2018-07-31 | 北京文海阳工贸有限责任公司 | A kind of chemical photic device |
-
2012
- 2012-02-27 CN CN 201220069017 patent/CN202626102U/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108343847A (en) * | 2017-01-23 | 2018-07-31 | 北京文海阳工贸有限责任公司 | A kind of chemical photic device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20170511 Address after: 102205 Beijing City West Village Ma Changping District Yangfang town northwest of Haiyang Jingwen trade limited liability company Patentee after: BEIJING WENHAIYANG INDUSTRY AND TRADE CO., LTD. Address before: 102205 Beijing City, Changping District Beijing paper company Haiyang Yangfang town Patentee before: Jin Chaoyang |
|
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20121226 |