CN202526939U - Resin elution tank - Google Patents

Resin elution tank Download PDF

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Publication number
CN202526939U
CN202526939U CN2012201128884U CN201220112888U CN202526939U CN 202526939 U CN202526939 U CN 202526939U CN 2012201128884 U CN2012201128884 U CN 2012201128884U CN 201220112888 U CN201220112888 U CN 201220112888U CN 202526939 U CN202526939 U CN 202526939U
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CN
China
Prior art keywords
resin
inner barrel
heat exchange
outer sleeve
tank body
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2012201128884U
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Chinese (zh)
Inventor
花瑞华
潘为群
徐浩龙
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HANGZHOU LONGYANG BIOTECHNOLOGY CO Ltd
Original Assignee
HANGZHOU LONGYANG BIOTECHNOLOGY CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Priority to CN2012201128884U priority Critical patent/CN202526939U/en
Application granted granted Critical
Publication of CN202526939U publication Critical patent/CN202526939U/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model provides a resin elution tank which comprises a closed barrel-type tank body, wherein a material inlet hole, a material outlet hole, a liquid inlet hole and a liquid outlet are formed in the tank body, and a temperature probe is arranged on the tank body; the tank body is of a two-layer clamping sleeve type structure and comprises an inner barrel body and a heat exchange outer sleeve body; the heat exchange outer sleeve body is of a hollow structure; a temperature conduction medium is arranged in the heat exchange outer sleeve body; the heat exchange outer sleeve body is attached to and wrap the outer side face of the inner barrel body; a resin separation screen is arranged in the tank body in an inclination manner; and the relatively low end of the resin separation screen and the material outlet hole are positioned at the same level. The resin elution tank has a temperature control function and can quickly and precisely reach a temperature value required by the process; and eluted resin can be taken out conveniently.

Description

A kind of resin elution jar
Technical field
The utility model relates to a kind of pharmaceutical manufacturing equipment, and more particularly, it relates to a kind of resin elution jar that is used for heparin production process wash-out operation.
Background technology
Heparin is the anticoagulant of extensive use clinically at present; Along with the raising of social life level and the development of medicinal career; The demand of heparin is growing, and each pharmaceutical equipment manufacturing enterprise is also updating properties of product, to satisfy the requirement of market to heparin output and quality.But the resin elution jar structure function that is used for heparin production at present is all fairly simple, and the screen cloth that is used for barrier resin is arranged on the liquid outlet place, when liquid level reduces gradually; During the resin bulk deposition; Resin can hinder soup to be passed through, and causes that the soup rate of outflow is slow, flow is little, influences production efficiency; The technology regulation and control are cumbersome, do not possess heating or cooling device, and technological temperature is wayward.Mostly the device fabrication material is plastics or ordinary metallic material in addition, is prone to corrosion fast under the high salinity condition of wash-out operation, is not durable.Notification number is that the utility model of CN100336656C discloses a kind of injection device that is used for resin transfer moulding technology on September 12nd, 2007; It comprises source of the gas, vavuum pump, resin container, conveyance conduit and die device; In the said resin container agitator is arranged, have on the cover can external source of the gas valve, sprue and the interface that can be connected with vavuum pump; Resin container is logical through a termination of output switch and conveyance conduit, and the other end of conveyance conduit has the die device connection of steam vent through input switch and end face; Described resin container and conveyance conduit outsourcing oil bath heating system; The oil bath heating system is connected with the oil bath circulating pump.Injection device of the present invention adopts the constant voltage method for implanting, does not receive the restriction of bi-component mixed proportion scope, wide adaptability; Easy to use, equipment is simple, and cost reduces; Have the flexibility function, but use occasion of the present invention and technological requirement and be not suitable for the wash-out operation that heparin is produced.
The utility model content
Simple in order to overcome the wash-out functions of the equipments that existing heparin produces, technology regulation and control trouble, equipment and materials is prone to the deficiency of corrosion fast, and the utility model provides the resin elution jar that a kind of structure is provided with rationally, function is more complete, durable.
The technical scheme of the utility model is: a kind of resin elution jar, comprise closed tubular tank body, and said tank body is provided with charging hole, discharge opening, inlet opening, liquid outlet and temp probe; Said tank body is a double-jacket formula structure; Comprise inner barrel and heat exchange outer sleeve body, the heat exchange outer sleeve body is a hollow structure, in be provided with and lead warm medium; The heat exchange outer sleeve body is fitted and is surrounded on the lateral surface of inner barrel; Be provided with the resin isolation screen cloth in the said tank body, the resin isolation screen cloth is obliquely installed, and its a lower end and discharge opening is in sustained height.The heat exchange outer sleeve body can provide all temps to inner barrel heating or cooling, makes the temperature of wash-out operation reach the optimum value of technological requirement quickly and accurately.In addition, the heat exchange outer sleeve body makes this resin elution jar possess function of temperature control, is convenient to carry out the exploration and the Parameter Optimization experiment of new technology.Resin isolation screen cloth and liquid outlet remain with a segment distance, and resin is stopped on the resin isolation screen cloth, and the liquid outlet place remains unimpeded like this.After the soup emptying, when taking out resin, only need open discharge opening and make resin the resin isolation screen cloth rolls out and gets final product in deadweight effect lower edge with recycling.
As preferably, the inwall of inner barrel is provided with the Teflon sheath.The wash-out operation is carried out in high salinity salt solution, and the Teflon sheath can effectively protect the inwall of inner barrel to make it the corrosion of anti-salt solution.
As preferably, be provided with coil pipe in the heat exchange outer sleeve body, coil pipe is around inner barrel shape setting in the shape of a spiral.Coil pipe is the circulation passage of heating agent or refrigerant, and coil pipe has longer path, so leading warm medium and can fully contact raising temperature adjusting speed in heating agent or refrigerant in the coil pipe and the heat exchange outer sleeve body.
As preferably, the material of tank body is a stainless steel.Stainless steel intensity is high, and corrosion-resistant, the tank body of processing is durable, and elegant in appearance.
As preferably, the resin isolation screen cloth is a double-decker, comprises silk screen and orifice plate, and silk screen is fixed on the orifice plate end face.This double-deck resin isolation screen cloth can filter soup, and higher weight capacity is arranged again, can bear the weight of the resin particle of accumulation.
As preferably; The top of inner barrel is provided with the motor that is connected with inner barrel, and motor output end is connected with decelerator, and the decelerator output is connected with the agitator axostylus axostyle; The agitator axostylus axostyle is along the axis setting of inner barrel, and the middle part and the bottom of agitator axostylus axostyle are respectively equipped with stirring vane.Stirring vane can stir salt solution under motor-driven, make liquid flow, accelerates elution process, thereby enhances productivity.
As preferably, be equipped with mozzle on the port of inlet opening and liquid outlet.Mozzle can and conflux the directed drainage of liquid, annotates like this and to collect liquid all very convenient, and is beneficial to the clean and tidy health that surrounding environment is is respectively imported and exported in maintenance.
The beneficial effect of the utility model is:
The structure setting is more reasonable, and function is more.The utility model is provided with the resin isolation screen cloth of double-jacket formula structure and inclination, can fast accurately carry out Separation of Solid and Liquid, and the wash-out operation is carried out under optimum process condition, and operation can reclaim resin again after accomplishing easily.
Description of drawings
Fig. 1 is a kind of structural representation of the utility model;
Fig. 2 is a kind of vertical view of tank body in the utility model.
Among the figure, 1-inner barrel, 2-heat exchange outer sleeve body, 3-resin isolation screen cloth, 4-charging hole; The 5-discharge opening, 6-inlet opening, 7-liquid outlet, 8-temp probe, 9-motor; The 10-decelerator, 11-agitator axostylus axostyle, 12-stirring vane, 13-coil pipe; 14-steam-out (SO) inlet, the 15-condensed water discharge outlet, 16-heat-conductive water filler, the 17-heat-conductive water changes the mouth of a river.
The specific embodiment
Below in conjunction with the accompanying drawing specific embodiment the utility model is described further.
Embodiment:
As depicted in figs. 1 and 2; A kind of resin elution jar comprises closed tubular tank body, and said tank body top is provided with charging hole 4, the perfusion salt solution that supplies resin to get into and cleans the inlet opening 6 with clear water; Said tank base minimum point is provided with discharges the liquid outlet 7 that soup is used; Said tank base locates to be provided with the discharge opening 5 that takes out resin behind the wash-out on the upper side, and said tank body is a double-jacket formula structure, comprises inner barrel 1 and heat exchange outer sleeve body 2; The inwall of inner barrel 1 is provided with the Teflon sheath, and inner barrel 1 top is equipped with the temp probe 8 that stretches into inner barrel 1 depths temperature when surveying that the wash-out operation is carried out in the inner barrel 1; Heat exchange outer sleeve body 2 is a hollow structure, and inner is heat-conducting medium with water, and heat exchange outer sleeve body 2 is fitted and surrounded on the lateral surface of inner barrel 1; Heat exchange outer sleeve body 2 tops are provided with heat-conductive water filler 16, and heat exchange outer sleeve body 2 tops are provided with heat-conductive water and change the mouth of a river 17, are provided with coil pipe 13 in the heat exchange outer sleeve body 2; Coil pipe 13 is around inner barrel 1 shape setting in the shape of a spiral; Water flowing steam in the coil pipe 13, coil pipe 13 high-order tops are provided with steam-out (SO) inlet 14, and coil pipe 13 lowest orders are provided with condensed water discharge outlet 15.Inner barrel 1 bottom of tank body be provided with resin isolation screen cloth 3, resin isolation screen cloth 3 is a double-decker, comprises silk screen and orifice plate, silk screen is fixed on the orifice plate end face, resin isolation screen cloth 3 is obliquely installed, an end and discharge opening 5 that it is lower are in sustained height.The top of inner barrel 1 is provided with the motor 9 that is connected with inner barrel 1; Motor 9 outputs are connected with decelerator 10; Decelerator 10 outputs are connected with agitator axostylus axostyle 11, and agitator axostylus axostyle 11 is along the axis setting of inner barrel 1, and the middle part of agitator axostylus axostyle 11 and bottom are respectively equipped with stirring vane 12.Inlet opening 6, liquid outlet 7, heat-conductive water filler 16, heat-conductive water change on the port of the mouth of a river 17 and condensed water discharge outlet 15 and are equipped with mozzle.
When using this resin elution jar to carry out the wash-out operation, with adding from charging hole 4 in the resin that is adsorbed with heparin, from the salt solution of inlet opening 6 adding high salinity, the stirring vane 12 that starter motor 9 drives on the agitator axostylus axostyles 11 rotates, and stirs salt solution and carries out wash-out.Last heparin is dissolved in the salt solution, and resin is a solid particle, is insoluble to salt solution.Eluent behind the wash-out is that soup promptly is that to carry out next procedure needed, opens liquid outlet 7, and emptying is also collected soup.Eluted resins is then stopped by resin isolation screen cloth 3, stops to be deposited on the resin isolation screen cloth 3.Open discharge opening 5, resin just rolls to the lowland from high along the resin isolation screen cloth that tilts 3, discharges this resin elution jar and is collected confession and utilizes.

Claims (7)

1. a resin elution jar comprises closed tubular tank body, and said tank body is provided with charging hole (4), discharge opening (5), inlet opening (6), liquid outlet (7) and temp probe (8); It is characterized in that said tank body is a double-jacket formula structure; Comprise inner barrel (1) and heat exchange outer sleeve body (2), heat exchange outer sleeve body (2) is a hollow structure, in be provided with and lead warm medium; Heat exchange outer sleeve body (2) is fitted and is surrounded on the lateral surface of inner barrel (1); Be provided with resin isolation screen cloth (3) in the said tank body, resin isolation screen cloth (3) is obliquely installed, and end that it is lower and discharge opening (5) are in sustained height.
2. resin elution jar according to claim 1 is characterized in that the inwall of inner barrel (1) is provided with the Teflon sheath.
3. resin elution jar according to claim 1 is characterized in that being provided with in the heat exchange outer sleeve body (2) coil pipe (13), and coil pipe (13) is around inner barrel (1) shape setting in the shape of a spiral.
4. resin elution jar according to claim 1, the material that it is characterized in that said tank body is a stainless steel.
5. resin elution jar according to claim 1 is characterized in that resin isolation screen cloth (3) is a double-decker, comprises silk screen and orifice plate, and silk screen is fixed on the orifice plate end face.
6. according to claim 1 or 2 or 3 or 4 or 5 described resin elution jars; The top that it is characterized in that inner barrel (1) is provided with the motor (9) that is connected with inner barrel (1); Motor (9) output is connected with decelerator (10); Decelerator (10) output is connected with agitator axostylus axostyle (11), and agitator axostylus axostyle (11) is along the axis setting of inner barrel (1), and the middle part of agitator axostylus axostyle (11) and bottom are respectively equipped with stirring vane (12).
7. according to claim 1 or 2 or 3 or 4 or 5 described resin elution jars, it is characterized in that being equipped with mozzle on the port of inlet opening (6) and liquid outlet (7).
CN2012201128884U 2012-03-22 2012-03-22 Resin elution tank Expired - Fee Related CN202526939U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2012201128884U CN202526939U (en) 2012-03-22 2012-03-22 Resin elution tank

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2012201128884U CN202526939U (en) 2012-03-22 2012-03-22 Resin elution tank

Publications (1)

Publication Number Publication Date
CN202526939U true CN202526939U (en) 2012-11-14

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN2012201128884U Expired - Fee Related CN202526939U (en) 2012-03-22 2012-03-22 Resin elution tank

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103570847A (en) * 2013-11-15 2014-02-12 重庆三腾食品有限公司 Heparin sodium processing method
CN103585786A (en) * 2013-11-15 2014-02-19 重庆三腾食品有限公司 Resin eluting method and corresponding heparin sodium processing method
CN108996745A (en) * 2018-07-30 2018-12-14 东吴环保科技(珠海)有限公司 A kind of broken cyanide formula gold recovery method

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103570847A (en) * 2013-11-15 2014-02-12 重庆三腾食品有限公司 Heparin sodium processing method
CN103585786A (en) * 2013-11-15 2014-02-19 重庆三腾食品有限公司 Resin eluting method and corresponding heparin sodium processing method
CN103585786B (en) * 2013-11-15 2015-09-02 重庆三腾食品有限公司 A kind of resin elution method and corresponding liquaemin processing method
CN103570847B (en) * 2013-11-15 2015-11-18 重庆三腾食品有限公司 A kind of heparin sodium working method
CN108996745A (en) * 2018-07-30 2018-12-14 东吴环保科技(珠海)有限公司 A kind of broken cyanide formula gold recovery method

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20121114

Termination date: 20150322

EXPY Termination of patent right or utility model