CN201737724U - Circulating treatment device for carbonized tower boiled liquid - Google Patents

Circulating treatment device for carbonized tower boiled liquid Download PDF

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Publication number
CN201737724U
CN201737724U CN2010202616354U CN201020261635U CN201737724U CN 201737724 U CN201737724 U CN 201737724U CN 2010202616354 U CN2010202616354 U CN 2010202616354U CN 201020261635 U CN201020261635 U CN 201020261635U CN 201737724 U CN201737724 U CN 201737724U
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CN
China
Prior art keywords
tower
liquid
ammonia
distillation tower
carbonized
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN2010202616354U
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Chinese (zh)
Inventor
黄伟
孙兆飞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shanxi Yangmei Fengxi Fertilizer Industry (Group) Co Ltd
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Shanxi Yangmei Fengxi Fertilizer Industry (Group) Co Ltd
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Publication date
Application filed by Shanxi Yangmei Fengxi Fertilizer Industry (Group) Co Ltd filed Critical Shanxi Yangmei Fengxi Fertilizer Industry (Group) Co Ltd
Priority to CN2010202616354U priority Critical patent/CN201737724U/en
Application granted granted Critical
Publication of CN201737724U publication Critical patent/CN201737724U/en
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Abstract

The utility model belongs to the field of soda ash production and discloses a circulating treatment device for carbonized tower boiled liquid, which solves the problems of high cost and the loss of sodium bicarbonate during the treatment of conventional carbonized tower boiled liquid. The circulating treatment device for carbonized boiled liquid comprises an accident barrel, a waste liquid tank, a heat exchanger, a distillation tower, a condenser, an absorber, an ammonia mother liquid barrel and a pump, wherein the accident barrel, the waste liquid tank and the inlet of a cooling liquid tube of the heat exchanger are connected in sequence through a pipeline, the outlet of the cooling liquid tube of the heat exchanger is connected with a feed opening at the top of the distillation tower though the pipeline, an exhaust opening at the top of the distillation tower is connected with the condenser, the absorber and the ammonia mother liquid barrel in sequence through the pipeline, the ammonia mother liquid barrel is connected with the pump and the absorber to form circulation, and a discharge port at the bottom of the distillation tower is connected with the inlet of a heating liquid tube of the heat exchanger. The utility model can greatly save steam and water for tower boiling, the ammonia in the carbonized tower boiled liquid can be recycled through ammonia steaming, and ammonia nitrogen in the tower boiled liquid after ammonia steaming through the distillation tower can reach emission standards.

Description

Tower liquid cyclic processing device is boiled in carbonization
Technical field
The utility model belongs to the soda ash production field, relates to a kind of carbonization and boils tower liquid cyclic processing device.
Background technology
In the soda ash production process, carbonating tower is behind for some time system alkali, and the sodium bicarbonate that adheres on tower wall, cap, the cooling tube scabs influences ordinary production, therefore must boil tower and clean.Carbonating tower boils and has dissolved the sodium bicarbonate crystallization in the tower liquid after boiling the tower cleaning.It is a more unmanageable ring in the soda ash production process that tower liquid is boiled in carbonization always, and for a long time, producer all takes the directly measure of discharging mostly, has caused environmental pollution.At present indivedual producers reduce ammonia nitrogen by joining a water, carry out sewage disposal again, do making that the sewage disposal expense is higher like this, have caused the loss of sodium bicarbonate simultaneously.
Summary of the invention
The present invention boils the problem that tower liquid expense height and sodium bicarbonate when handling run off in order to solve existing carbonization, and provides a kind of carbonization to boil tower liquid cyclic processing device.
The utility model is achieved through the following technical solutions:
Tower liquid cyclic processing device is boiled in a kind of carbonization, comprise accident bucket, waste liquid tank, interchanger, distillation tower, condenser, resorber, ammonia mother vat, pump, wherein accident bucket, waste liquid tank, be connected successively by pipeline with the cooling liquid tube import of interchanger, the cooling liquid tube outlet of interchanger is connected by the opening for feed of pipeline with the distillation tower top, the distillation tower top vent is connected with condenser, resorber, ammonia mother vat successively by pipeline, the ammonia mother vat connects and composes circulation by pump and resorber, and the discharge port of distillation tower bottom is connected with the import of interchanger hydrothermal solution pipe.In use, the accident bucket is connected with the carbonating tower bottom, the outlet of interchanger hydrothermal solution pipe is connected with carbonating tower its top feed mouth, that comes out from carbonating tower bottom boils tower liquid, pass through accident bucket, waste liquid tank, interchanger successively by pipeline, enter the distillation tower distillation, in distillation tower, be expelled to interchanger from the distillation tower bottom after the ammonia still process, squeeze into carbonating tower by pump after the heat exchange, the gas that steams in the distillation tower behind condenser condenses water vapour, enters resorber earlier, mix with the mother liquor of sending here from the ammonia mother vat, absorb ammonia.Like this circulation treatment reaches the purpose of environmental protection.
The utility model compared with prior art has the following advantages:
(1) the light liquid distillation soft water temperature height of arranging by the condenser heat exchange, can significantly be saved steam.
(2) the used water of tower is boiled in saving.
(3) the ammoniacal liquor titre of boiling tower liquid in the distillation tower is about 30tt, by the recyclable ammonia that boils in the tower liquid of ammonia still process.
(4) but after distillation tower ammonia still process, boil the ammonia nitrogen qualified discharge of tower liquid.
(5) soft water is little to the corrosion of equipment, prolongs service life of equipment.
Description of drawings
Fig. 1 boils tower liquid cyclic processing device structural representation for the utility model carbonization
Among the figure: 1-accident bucket, 2-waste liquid tank, 3-interchanger, 4-distillation tower, 5-condenser, 6-resorber, 7-ammonia mother vat bucket, 8-pump.
Embodiment
Below in conjunction with accompanying drawing the utility model is further specified.
As shown in Figure 1, tower liquid cyclic processing device is boiled in a kind of carbonization, comprise accident bucket 1, waste liquid tank 2, interchanger 3, distillation tower 4, condenser 5, resorber 6, ammonia mother vat 7, pump 8, wherein the accident bucket 1, waste liquid tank 2, be connected successively by pipeline with the cooling liquid tube import of interchanger 3, the cooling liquid tube outlet of interchanger 3 is connected by the opening for feed of pipeline with distillation tower 4 tops, distillation tower 4 top vent by pipeline successively with condenser 5, resorber 6, ammonia mother vat 7 connects, ammonia mother vat 7 connects and composes circulation by pump 8 and resorber 6, and the discharge port of distillation tower 4 bottoms is connected with interchanger 3 hydrothermal solution pipe imports.

Claims (1)

1. tower liquid cyclic processing device is boiled in a carbonization, it is characterized in that comprising accident bucket (1), waste liquid tank (2), interchanger (3), distillation tower (4), condenser (5), resorber (6), ammonia mother vat (7), pump (8), described accident bucket (1), waste liquid tank (2), be connected successively by pipeline with the cooling liquid tube import of interchanger (3), the cooling liquid tube outlet of interchanger (3) is connected by the opening for feed of pipeline with distillation tower (4) top, distillation tower (4) top vent by pipeline successively with condenser (5), resorber (6), ammonia mother vat (7) connects, ammonia mother vat (7) connects and composes circulation by pump (8) and resorber (6), and the discharge port of distillation tower (4) bottom is connected with the import of interchanger (3) hydrothermal solution pipe.
CN2010202616354U 2010-07-15 2010-07-15 Circulating treatment device for carbonized tower boiled liquid Expired - Fee Related CN201737724U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN2010202616354U CN201737724U (en) 2010-07-15 2010-07-15 Circulating treatment device for carbonized tower boiled liquid

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN2010202616354U CN201737724U (en) 2010-07-15 2010-07-15 Circulating treatment device for carbonized tower boiled liquid

Publications (1)

Publication Number Publication Date
CN201737724U true CN201737724U (en) 2011-02-09

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Application Number Title Priority Date Filing Date
CN2010202616354U Expired - Fee Related CN201737724U (en) 2010-07-15 2010-07-15 Circulating treatment device for carbonized tower boiled liquid

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CN (1) CN201737724U (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102935438A (en) * 2012-10-16 2013-02-20 河南骏化发展股份有限公司 Cleaning system and method for alkali-associated carbonation tower
CN103936091A (en) * 2013-12-26 2014-07-23 重庆宜化化工有限公司 Weak liquid distillation method
CN104016541A (en) * 2014-05-09 2014-09-03 唐金荣 Method for treating wastewater generated in carbonization of bamboo
CN114147016A (en) * 2021-12-09 2022-03-08 广东南方碱业股份有限公司 Cleaning system for carbonization tower

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102935438A (en) * 2012-10-16 2013-02-20 河南骏化发展股份有限公司 Cleaning system and method for alkali-associated carbonation tower
CN102935438B (en) * 2012-10-16 2015-09-16 河南骏化发展股份有限公司 Connection alkali carbonators purging system and cleaning method
CN103936091A (en) * 2013-12-26 2014-07-23 重庆宜化化工有限公司 Weak liquid distillation method
CN103936091B (en) * 2013-12-26 2015-09-02 重庆宜化化工有限公司 A kind of light liquid distil process method
CN104016541A (en) * 2014-05-09 2014-09-03 唐金荣 Method for treating wastewater generated in carbonization of bamboo
CN104016541B (en) * 2014-05-09 2016-04-06 唐金荣 A kind ofly carbonize the method for wastewater treatment that produces in bamboo wood process
CN114147016A (en) * 2021-12-09 2022-03-08 广东南方碱业股份有限公司 Cleaning system for carbonization tower

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20110209

Termination date: 20150715

EXPY Termination of patent right or utility model