CN201410306Y - Quartz sub-boiling distiller - Google Patents
Quartz sub-boiling distiller Download PDFInfo
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- CN201410306Y CN201410306Y CN2009201318637U CN200920131863U CN201410306Y CN 201410306 Y CN201410306 Y CN 201410306Y CN 2009201318637 U CN2009201318637 U CN 2009201318637U CN 200920131863 U CN200920131863 U CN 200920131863U CN 201410306 Y CN201410306 Y CN 201410306Y
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Abstract
The utility model discloses a quartz sub-boiling distiller for preparing high-purity liquid. The quartz sub-boiling distiller comprises a plurality of groups of distilling tubes which are connected inturn, wherein each group of distilling tubes are provided with sealed outer shells, the distilling tubes are connected through quartz tubes, and the high-purity liquid flows among a plurality of groups of distilling tubes through the quartz tubes. Thereby the utility model provides a quartz sub-boiling distiller for realizing preparing high-purity liquid with few impurities.
Description
Technical field
The utility model belongs to the irradiation technique field, relates in particular to a kind of quartzy sub-boiling distillation device.
Background technology
Industrial distilled water normally extracts by distiller.General quartz still is carried the globule secretly because of the boiling distillation in the gas, gas-liquid separation is incomplete, causes water quality not high.Full glass distiller is more because of the contained pollution of glass itself, and water quality is poorer.Ion exchange water is brought organic interference into because of the dissolving of organic substance again.
And quartzy sub-boiling distillation device had both been avoided the pollution of glass impurities, was lower than boiling point because of liquidus temperature again.Reason is not seethed with excitement and carry the globule secretly in steam.Both gas-liquid separation was complete.Therefore water quality is high, analyzes heavy metal free through the nonflame atomic absorption method and detects.Quartzy sub-boiling distillation is to utilize heat radiation principle, keeps liquidus temperature to be lower than the boiling temperature evaporative condenser and to produce high purity water and high purity reagent.Quartzy sub-boiling distillation device is a totally-enclosed quartz glass instrument of producing high purity reagent and high purity water, and it has unique advantage.Its advanced technology, novel structure is attractive in appearance, easy for installation, simple to operate, the maintenance convenient.
Have at present quartzy Asia to boil on the domestic market and twoly steam the pure water distillers, but one steams and two be to connect with flexible rubber hose between steaming, cause the pure water quality not high enough.Especially can not satisfy the client that specific (special) requirements is arranged.
In summary, there is shortcoming in quartzy sub-boiling distillation device in the prior art, has inconvenience and defective on reality is used, so be necessary to be improved.
The utility model content
At above-mentioned defective, the purpose of this utility model is to provide a kind of quartzy sub-boiling distillation device, to realize producing the less high-purity liquid of impurity.
To achieve these goals, the utility model provides a kind of quartzy sub-boiling distillation device, be used to produce high-purity liquid, described quartzy sub-boiling distillation machine comprises the many groups distillation cascade that is linked in sequence, every group of distillation cascade has the sealing shell body, connect by quartz ampoule between the described distillation cascade, described high-purity liquid flows between described many group distillation cascades by described quartz ampoule.
According to described quartzy sub-boiling distillation device, the group number of described distillation cascade is three groups.
According to described quartzy sub-boiling distillation device, be provided with the heating electric furnace heating wire in the sealing shell body of described every group of distillation cascade.
According to described quartzy sub-boiling distillation device, be provided with condenser pipe in the sealing shell body of described every group of distillation cascade.
According to described quartzy sub-boiling distillation device, the sealing shell body of last group distillation cascade of described quartzy sub-boiling distillation device is provided with high-purity liquid liquid outlet; And described high-purity liquid liquid outlet correspondence is provided with the high-purity liquid header.
According to described quartzy sub-boiling distillation device, described condenser pipe bottom is provided with an opening, the corresponding quartz ampoule that leads to next distillation cascade of described opening, the high-purity liquid liquid outlet that is provided with on the sealing shell body of last group distillation cascade of the corresponding described quartzy sub-boiling distillation device of perhaps described opening.
According to described quartzy sub-boiling distillation device, described quartz ampoule junction is provided with sand-ground opening.
According to described quartzy sub-boiling distillation device, the sealing shell body surface of described every group of distillation cascade is provided with filling opening.
According to described quartzy sub-boiling distillation device, the sealing shell body inside of described every group of distillation cascade is provided with gap.
According to described quartzy sub-boiling distillation device, second group of distillation cascade bottom of described quartzy sub-boiling distillation device is provided with the first water water inlet; The 3rd group of distillation cascade bottom of described quartzy sub-boiling distillation device is provided with the redistilled water water inlet.
The utility model adopts quartz ampoule by many groups of connecting pipes of steaming between the distillation cascade with quartzy sub-boiling distillation device, hidden danger decontaminates, the contained impurity of the high-purity liquid that quartzy sub-boiling distillation device is extracted is less, provides quality higher high-purity liquid to the user.In addition, the distillation cascade of the quartzy sub-boiling distillation device that the utility model provides is three groups, has realized three distillation purposes to liquid, has simplified distillation sequence.Further, on every group of distillation cascade, also add artificial filler, the convenient requirement of client that needs with special water distillation.
Description of drawings
Fig. 1 is the structural representation of the quartzy sub-boiling distillation device that provides of the utility model.
The specific embodiment
In order to make the purpose of this utility model, technical scheme and advantage clearer,, the utility model is further elaborated below in conjunction with drawings and Examples.Should be appreciated that specific embodiment described herein only in order to explanation the utility model, and be not used in qualification the utility model.
Basic thought of the present utility model is: connect by quartz ampoule between many groups distillation cascade of quartzy sub-boiling distillation device, owing to adopt quartz ampoule to connect many group distillation cascades, the contained impurity of the high-purity liquid that extracts is less, improves the quality high-purity liquid higher to the user.
As shown in Figure 1, a kind of quartzy sub-boiling distillation device 1 is provided in the utility model, be used to produce high-purity liquid, quartzy sub-boiling distillation device 1 comprises the many groups distillation cascade that is linked in sequence, every group of distillation cascade has sealing shell body 12, connect by quartz ampoule 13 between the distillation cascade, high-purity liquid flows between many group distillation cascades by quartz ampoule 13.
Quartzy Asia of the prior art two pure water distillers that steam that boil, it two is to connect with flexible rubber hose between steaming, and easily pollutes pure water, cause the pure water quality not high enough, so that water quality does not reach the special industry that water quality is had high requirement.The total interface of the quartzy sub-boiling distillation device 1 that the utility model provides is quartzy interface, and the overall process of distillating liquid is totally-enclosed quartz glass instrument, has avoided all pollutions that may exist, therefore the based on very high purity of the liquid of producing.
As shown in Figure 1, in an embodiment of the present utility model, the group number of distillation cascade is three groups.Comprise 11, the second groups of distillation cascades 21 of first group of distillation cascade and the 3rd group of distillation cascade 31.These three groups of distillation cascades from top to bottom connect successively.Second group of distillation cascade 21 bottom of quartzy sub-boiling distillation device 1 are provided with first water water inlet 24; The 3rd group of distillation cascade 31 bottoms of quartzy sub-boiling distillation device 1 are provided with redistilled water water inlet 25.With water is example, and the distilled water that first group of distillation cascade 11 distills out enters into second group of distillation cascade 21 by first water water inlet 24; And the distilled water that second group of distillation cascade 21 distills out enters into the 3rd group of distillation cascade 31 by redistilled water water inlet 25.Therefore, quartzy sub-boiling distillation device that the utility model provides 1 is complete quartzy closed distillation, not ingress of air and other materials in the transmittance process of one, two, three distilled water.
In the sealing shell body 12 of every group of distillation cascade, be provided with heating electric furnace heating wire 22, and condenser pipe 14.Heat by ccontaining liquid in 22 pairs of every group of distillation cascades of heating electric furnace heating wire, make its vaporization.Heater strip is enclosed in the housing, receives water ingress of air not again, and whole purification process is not subjected to environmental pollution.Carry out condensation by the steam after 14 pairs of vaporizations of condenser pipe then.Be provided with a water inlet in condenser pipe 14 bottoms, the corresponding quartz ampoule 13 that leads to next distiller of this water inlet.By this water inlet, condensed liquid is transported to quartz ampoule 13, be sent in next distiller by quartz ampoule 13 condensed liquid.In purification process,,, can produce aseptic no hot ultra-pure water generally greater than 200 degrees centigrade because of condensation space temperature height.Be provided with sand-ground opening 16 in quartz ampoule 13 junctions.And condenser pipe 14 two ends can be connected to tap water interface by sebific duct, with condensed fluid steam.
Preferably, sealing shell body 12 surfaces of every group of distillation cascade are provided with filling opening 17.Can debug by this filling opening 17 and to add water to satisfy the particular client needs.Make the client of the artificial interpolation water that needs adding reagent realize its demands by this filling opening 17.
In addition, sealing shell body 12 inside of every group of distillation cascade are provided with gap 18.Overflow pipe is downwards with outside the water delivery line.When the liquid level in every group of distillation cascade surpass set up standard after, the liquid that has more will overflow outside the distillation cascade by gap 18, prevent to enter in the next stage rectifying tube without the water of distillation, to guarantee the normal use of quartzy sub-boiling distillation device 1.
The sealing shell body 12 of last group distillation cascade of quartzy sub-boiling distillation device 1 is provided with high-purity liquid liquid outlet 19, and high-purity liquid liquid outlet 19 correspondences are provided with high-purity liquid header 20.Referring to Fig. 1, the liquid outlet 19 that is provided with in shell 12 bottoms of the 3rd group of distillation cascade 31 flows out by liquid outlet 19 through the high-purity liquid that repeatedly distills, and is collected in the liquid header 20.Therefore, the high-purity liquid liquid outlet that is provided with on the sealing shell body 12 of last group distillation cascade of the corresponding quartzy sub-boiling distillation device 1 of opening of condenser pipe 14 bottoms setting.In addition, also be provided with piston 23 every group of distillation cascade sealing shell body 12 bottoms.The effect of piston 23 makes things convenient for the discharging of cleaning fluid when being the scavenge pipe body.
The quartzy sub-boiling distillation device 1 that the utility model provides can not only be produced high purity water. and can also be as the purification of liquid reagent.As prepare superfine pure hydrochloric acid, sulfuric acid, nitric acid, perchloric acid, ammoniacal liquor etc.The manufacturing and the use of present quartzy sub-boiling distillation device 1 belong to special trade, the dosimeter of its use must use the water that adds reagent to carry out the high purity water preparation of three distillations according to the standard code of preparation, and can not contact with any material beyond the quartz to guarantee water quality in the distillation overall process.Distillation equipment of the prior art can not satisfy above-mentioned needs.And quartzy sub-boiling distillation device 1 can be realized above-mentioned requirements, and the distilled water that quartzy sub-boiling distillation device 1 is per hour produced in experiment is 1000mL.
In sum, the utility model is by adopting quartz ampoule with the connecting pipe between many groups distillation cascade of quartzy sub-boiling distillation device, the hidden danger that decontaminates, the contained impurity of the high-purity liquid that quartzy sub-boiling distillation device is extracted is less, improves the quality high-purity liquid higher to the user.In addition, the distillation cascade of the quartzy sub-boiling distillation device that the utility model provides is three groups, has realized three distillation purposes to liquid, has simplified distillation sequence.Further, on every group of distiller, also add artificial filler, the convenient requirement of client that needs with special water distillation.
Certainly; the utility model also can have other various embodiments; under the situation that does not deviate from the utility model spirit and essence thereof; those of ordinary skill in the art work as can make various corresponding changes and distortion according to the utility model, but these corresponding changes and distortion all should belong to the protection domain of the appended claim of the utility model.
Claims (10)
1, a kind of quartzy sub-boiling distillation device, be used to produce high-purity liquid, described quartzy sub-boiling distillation device comprises the many groups distillation cascade that is linked in sequence, every group of distillation cascade has the sealing shell body, it is characterized in that, connect by quartz ampoule between the described distillation cascade, described high-purity liquid flows between described many group distillation cascades by described quartz ampoule.
2, according to right 1 described quartzy sub-boiling distillation device, it is characterized in that the group number of described distillation cascade is three groups.
3, according to right 1 described quartzy sub-boiling distillation device, it is characterized in that, be provided with the heating electric furnace heating wire in the sealing shell body of described every group of distillation cascade.
4, according to right 2 described quartzy sub-boiling distillation devices, it is characterized in that, be provided with condenser pipe in the sealing shell body of described every group of distillation cascade.
According to right 4 described quartzy sub-boiling distillation devices, it is characterized in that 5, the sealing shell body of last group distiller of described quartzy sub-boiling distillation device is provided with high-purity liquid liquid outlet; And described high-purity liquid liquid outlet correspondence is provided with the high-purity liquid header.
6, according to right 5 described quartzy sub-boiling distillation devices, it is characterized in that, described condenser pipe bottom is provided with an opening, the corresponding quartz ampoule that leads to next distillation cascade of described opening, the high-purity liquid liquid outlet that is provided with on the sealing shell body of last group distillation cascade of the corresponding described quartzy sub-boiling distillation device of perhaps described opening.
7, according to right 6 described quartzy sub-boiling distillation devices, it is characterized in that described quartz ampoule junction is provided with sand-ground opening.
8, according to right 1 described quartzy sub-boiling distillation device, it is characterized in that the sealing shell body surface of described every group of distillation cascade is provided with filling opening.
9, according to right 1 described quartzy sub-boiling distillation device, it is characterized in that the sealing shell body inside of described every group of distillation cascade is provided with gap.
According to right 2 described quartzy sub-boiling distillation devices, it is characterized in that 10, second group of distiller bottom of described quartzy sub-boiling distillation device is provided with the first water water inlet; The 3rd group of distillation cascade bottom of described quartzy sub-boiling distillation device is provided with the redistilled water water inlet.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009201318637U CN201410306Y (en) | 2009-05-15 | 2009-05-15 | Quartz sub-boiling distiller |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2009201318637U CN201410306Y (en) | 2009-05-15 | 2009-05-15 | Quartz sub-boiling distiller |
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| CN201410306Y true CN201410306Y (en) | 2010-02-24 |
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| CN2009201318637U Expired - Fee Related CN201410306Y (en) | 2009-05-15 | 2009-05-15 | Quartz sub-boiling distiller |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102976424A (en) * | 2012-12-24 | 2013-03-20 | 济南大学 | Installation method of automatic liquid feeding and second boiling high-purity water distiller |
| CN102992428A (en) * | 2012-12-24 | 2013-03-27 | 济南大学 | Preparation of high-purity water by use of quartz sub-boiling high-purity water distiller |
| CN103204558A (en) * | 2013-04-15 | 2013-07-17 | 济南大学 | Integrated multistage sub-boiling distiller |
| CN103214048A (en) * | 2013-04-22 | 2013-07-24 | 济南大学 | Multi-level combined type secondary distillation heat control ultrapure water continuous generator |
| CN107515148A (en) * | 2017-08-07 | 2017-12-26 | 袁洪林 | A kind of sub-boiling distillation device equipment |
-
2009
- 2009-05-15 CN CN2009201318637U patent/CN201410306Y/en not_active Expired - Fee Related
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102976424A (en) * | 2012-12-24 | 2013-03-20 | 济南大学 | Installation method of automatic liquid feeding and second boiling high-purity water distiller |
| CN102992428A (en) * | 2012-12-24 | 2013-03-27 | 济南大学 | Preparation of high-purity water by use of quartz sub-boiling high-purity water distiller |
| CN102992428B (en) * | 2012-12-24 | 2013-12-04 | 济南大学 | Preparation of high-purity water by use of quartz sub-boiling high-purity water distiller |
| CN103204558A (en) * | 2013-04-15 | 2013-07-17 | 济南大学 | Integrated multistage sub-boiling distiller |
| CN103214048A (en) * | 2013-04-22 | 2013-07-24 | 济南大学 | Multi-level combined type secondary distillation heat control ultrapure water continuous generator |
| CN103922432A (en) * | 2013-04-22 | 2014-07-16 | 济南大学 | Multistage combined heat control ultra-pure water continuous generator |
| CN103922432B (en) * | 2013-04-22 | 2015-07-22 | 济南大学 | Multistage combined heat control ultra-pure water continuous generator |
| CN107515148A (en) * | 2017-08-07 | 2017-12-26 | 袁洪林 | A kind of sub-boiling distillation device equipment |
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Legal Events
| Date | Code | Title | Description |
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| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20100224 Termination date: 20150515 |
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| EXPY | Termination of patent right or utility model |