CN201101905Y - Continuous evaporation crystallizer - Google Patents
Continuous evaporation crystallizer Download PDFInfo
- Publication number
- CN201101905Y CN201101905Y CNU2007201779066U CN200720177906U CN201101905Y CN 201101905 Y CN201101905 Y CN 201101905Y CN U2007201779066 U CNU2007201779066 U CN U2007201779066U CN 200720177906 U CN200720177906 U CN 200720177906U CN 201101905 Y CN201101905 Y CN 201101905Y
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- China
- Prior art keywords
- crystal
- discharge nozzle
- floater
- pipeline
- chamber
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- Expired - Fee Related
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a continuous evaporated crystallizer, which comprises a vapour liquid separator. A suspension chamber is formed at the lower part of the vapour liquid separator, the lower part of the suspension chamber is connected with a crystal store tank, the inner part of which is connected with a crystal discharge nozzle, a discharge pump is arranged on the crystal discharge nozzle which is connected to the bottom of the crystal store tank through a circulation tube, and a circulation tube valve, a discharge valve, and a discharge hole are arranged on the circulation tube, a block mass discharge hole is arranged at the bottom of the crystal store tank, the top part of an evaporator cell is connected with the vapour liquid separator through a pipeline, the bottom of the evaporator cell is connected with the suspension chamber through the pipeline, a forced circulation pump is arranged on the pipeline connected with the evaporator cell and the suspension chamber, a solid liquid separation chamber is arranged in the suspension chamber, and division boards are arranged at the two sides of the solid liquid separation chamber.
Description
Technical field
The utility model relates to the solution-treated equipment technical field, a kind of specifically high-efficiency and continuous crystallizing evaporator.
Background technology
Evaporimeter is to be widely used in fields such as food processing, concentration of juices, beverage production, Dairy Production, chemical industry, pharmaceutical industry, wastewater treatment, environment-friendly engineering.Concentration generates crystalline solid thereby wherein most of inorganic salts, organic salt product all need to reach capacity.Ordinary mould is divided into top vapor-liquid separation chamber, is the crystal basin below, after equipment operation a period of time, after reaching capacity the concentration crystallization, material reaches a constant volume, open the discharging pump discharging again, close discharging pump after the crystalline solid emptying again, thus discharging continuously.After discharging pump was closed, macrocrystalline cognition entered the pipeline that joins with discharging pump, and can't in time discharge this moment, thus cause the obstruction of discharge nozzle sometimes, and remove very trouble, and can make and produce delay, can't reach continuous operation.
Summary of the invention
The purpose of this utility model can satisfy continuous feed, discharge for providing a kind of, and crystalline solid is separated out a mouthful not susceptible to plugging continuous evaporative crystallization device.
The technical scheme that realizes the foregoing invention purpose is as follows:
The continuous evaporative crystallization device, comprise vapour liquid separator, floater is formed at the vapour liquid separator bottom, the floater bottom is connected with the crystal basin, the crystal basin is internally connected with the crystal discharge nozzle, and crystal discharge nozzle lower end is provided with discharging pump, and the crystal discharge nozzle is connected to the crystal tank bottom by circulation pipe, circulation pipe is provided with circulation pipe valve, discharging valve and discharging opening, and the crystal tank bottom is provided with agglomerate thing discharging opening.The vaporization chamber top is connected with vapour liquid separator by the vapour liquid-phase tube, the vaporization chamber bottom is connected with floater by pipeline, the pipeline that connects vaporization chamber and floater is provided with forced circulation pump, to improve heat transfer coefficient, be provided with the Separation of Solid and Liquid chamber in the floater, both sides, described Separation of Solid and Liquid chamber are provided with division board.Suspension enters after the vaporization chamber heating continuously, after vapour liquid separator separates, solution concentration is improved reach supersaturation formation crystalline solid, because the proportion of crystalline solid is greater than liquid (suspension), so the crystal rapid subsidence is to advancing the crystal basin, liquid (suspension) floats over above the crystal all the time, enter the crystal discharge nozzle, through discharging pump discharging then, can enter the circulation of crystal basin once more through circulation pipe, the circulation mouth of pipe circulates into to living the discharging mouth of pipe, in case the phenomenon that the discharging opening upper end is blocked by crystal occurs, causing can't continuous operation.
The utility model can satisfy continuous feed, the requirement of continuous pulp discharge (crystalline solid solution).Adopt forced circulation to form best cooperating between vaporization chamber and the crystallizer.Its inside is provided with Separation of Solid and Liquid chamber and division board, make crystal and clear liquid obtain effectively, separate fast, with the crystalline solid of growing up in the solution for continuous of satiety, effectively the avoid evaporating formation of chamber tubulation inner surface fouling (dirt) has improved the heat transfer coefficient of vaporization chamber greatly.Inner surface treatment.No dead angle, easily the crystalline solid liquation goes out, and to separate out that mouth is not subjected to stop up be most critical to crystalline solid when continuous or discontinuous operation.Which is provided with manhole, window, lamp hole, thermometer, vacuum meter, fluid level control device etc.
It is (anti-blocking that floater is provided with the Separation of Solid and Liquid chamber, antiscale) and the both sides division board, the liquid (suspension) that Figure 11 does not form crystal in this circulation through forced circulation pump once more through vaporization chamber circulation heating (see for details in the accompanying drawing floater to the arrow flow process of vaporization chamber), crystalline solid passes through the crystal discharge nozzle to discharging pump, enter circulation pipe again, arrive the crystal basin by circulation pipe then.Crystal discharge nozzle import department is provided with baffle plate (seeing Fig. 2 for details), thereby the effect of baffle plate is in order to prevent that discharging pump from shutting down back macrocrystalline thing and directly entering the crystal discharge nozzle and can't discharge and cause that crystalline solid stops up.The utility model also can be realized the multiple-effect evaporation crystallization
Macrocrystalline body in the crystal basin can be discharged from agglomerate thing discharging opening.
Description of drawings
Fig. 1 is the utility model structural representation
Fig. 2 is the enlarged drawing of crystal discharge nozzle in the utility model
Arrow is represented the flow direction of feed liquid and material in the course of work among the figure
The specific embodiment
The utility model is described in further detail below in conjunction with the drawings and specific embodiments.
As shown in Figure 1, the continuous evaporative crystallization device comprises vapour liquid separator 9 and vaporization chamber 3, floater 11 is formed at vapour liquid separator 9 bottoms, floater 11 bottoms are connected with crystal basin 13, and crystal basin 13 is internally connected with crystal discharge nozzle 15, crystal discharge nozzle 15; Be connected to discharging pump 18, be connected to crystal basin 13 bottoms by discharging pump by circulation pipe 16 again, circulation pipe 16 is provided with discharging opening 17, circulation pipe valve 19 and discharging opening valve 20, crystal basin 13 bottoms are provided with agglomerate thing discharging opening 14, vaporization chamber 3 tops are connected with vapour liquid separator by pipeline, vaporization chamber 3 bottoms are connected with floater 11 by pipeline, the pipeline that connects vaporization chamber 3 and floater 11 is provided with forced circulation pump 21, be provided with Separation of Solid and Liquid chamber 10 in the floater 11, feed liquid enters Separation of Solid and Liquid chamber 10 along feed liquid flow trace 4,10 both sides, described Separation of Solid and Liquid chamber are provided with division board 12, vapour liquid separator 9 tops are provided with indirect steam outlet 8, indirect steam 5 is discharged by indirect steam outlet 8, and vaporization chamber 3 upper side are provided with steam inlet 2, and lower side is provided with condensation-water drain 1.
As shown in Figure 2, crystal discharge nozzle import department is provided with baffle plate.Prevent that effectively thereby discharging pump from shutting down back macrocrystalline thing and directly entering the crystal discharge nozzle and can't discharge and cause that crystalline solid stops up.
Discharging flow process: when material enters discharging pump 18 by crystal discharge nozzle 15 after the crystallization in the crystal basin, receive circulation pipe 16 by discharging pump 18 again, enter crystal basin 13, form a circulation process.Wherein circulation pipe 16 is provided with circulation pipe valve 19 and discharging valve 20, when solution does not arrive the operation of discharging concentration in the equipment, open circulation pipe valve 19, close discharging valve 20, when material reaches capacity concentration (when material becomes the mass crystallization body), close circulation pipe valve 19, open discharging valve 20, at this moment material will be discharged from discharging opening 17.
Claims (2)
1. continuous evaporative crystallization device, it is characterized by: comprise vaporization chamber and vapour liquid separator, floater is formed at described vapour liquid separator bottom, the floater bottom is connected with the crystal basin, the crystal basin is internally connected with the crystal discharge nozzle, the crystal discharge nozzle is provided with discharging pump, the crystal discharge nozzle is connected to the crystal tank bottom by circulation pipe, circulation pipe is provided with the circulation pipe valve, discharging valve and discharging opening, the crystal tank bottom is provided with agglomerate thing discharging opening, the vaporization chamber top is connected with vapour liquid separator by pipeline, the vaporization chamber bottom is connected with floater by pipeline, the pipeline that connects vaporization chamber and floater is provided with forced circulation pump, is provided with the Separation of Solid and Liquid chamber in the floater, and both sides, described Separation of Solid and Liquid chamber are provided with division board.
2. continuous evaporative crystallization device according to claim 1 is characterized by: described crystal discharge nozzle import department is provided with baffle plate.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNU2007201779066U CN201101905Y (en) | 2007-09-28 | 2007-09-28 | Continuous evaporation crystallizer |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNU2007201779066U CN201101905Y (en) | 2007-09-28 | 2007-09-28 | Continuous evaporation crystallizer |
Publications (1)
Publication Number | Publication Date |
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CN201101905Y true CN201101905Y (en) | 2008-08-20 |
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CNU2007201779066U Expired - Fee Related CN201101905Y (en) | 2007-09-28 | 2007-09-28 | Continuous evaporation crystallizer |
Country Status (1)
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CN (1) | CN201101905Y (en) |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103432756A (en) * | 2013-08-16 | 2013-12-11 | 江苏嘉泰蒸发结晶设备有限公司 | All-in-one evaporation and crystallization device |
CN105129890A (en) * | 2015-10-07 | 2015-12-09 | 中国轻工业长沙工程有限公司 | Evaporating crystallizer |
CN105561624A (en) * | 2016-01-29 | 2016-05-11 | 太仓市微贯机电有限公司 | Reactor equipment for spherical crystals |
CN105688439A (en) * | 2014-11-23 | 2016-06-22 | 天津市泰河金岸科技有限公司 | Evaporative crystallizer |
-
2007
- 2007-09-28 CN CNU2007201779066U patent/CN201101905Y/en not_active Expired - Fee Related
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103432756A (en) * | 2013-08-16 | 2013-12-11 | 江苏嘉泰蒸发结晶设备有限公司 | All-in-one evaporation and crystallization device |
CN105688439A (en) * | 2014-11-23 | 2016-06-22 | 天津市泰河金岸科技有限公司 | Evaporative crystallizer |
CN105129890A (en) * | 2015-10-07 | 2015-12-09 | 中国轻工业长沙工程有限公司 | Evaporating crystallizer |
CN105561624A (en) * | 2016-01-29 | 2016-05-11 | 太仓市微贯机电有限公司 | Reactor equipment for spherical crystals |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C17 | Cessation of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20080820 Termination date: 20130928 |