CN1845945A - 可固化液态树脂组合物 - Google Patents
可固化液态树脂组合物 Download PDFInfo
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- CN1845945A CN1845945A CNA200480025646XA CN200480025646A CN1845945A CN 1845945 A CN1845945 A CN 1845945A CN A200480025646X A CNA200480025646X A CN A200480025646XA CN 200480025646 A CN200480025646 A CN 200480025646A CN 1845945 A CN1845945 A CN 1845945A
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- methyl
- resin composition
- curable liquid
- liquid resin
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- 239000007788 liquid Substances 0.000 title claims abstract description 76
- 239000000203 mixture Substances 0.000 title claims description 47
- QEVHRUUCFGRFIF-MDEJGZGSSA-N reserpine Chemical compound O([C@H]1[C@@H]([C@H]([C@H]2C[C@@H]3C4=C(C5=CC=C(OC)C=C5N4)CCN3C[C@H]2C1)C(=O)OC)OC)C(=O)C1=CC(OC)=C(OC)C(OC)=C1 QEVHRUUCFGRFIF-MDEJGZGSSA-N 0.000 title 1
- 239000011342 resin composition Substances 0.000 claims abstract description 63
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- 238000000576 coating method Methods 0.000 claims description 46
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- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 30
- 239000000835 fiber Substances 0.000 claims description 29
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- YOQPJXKVVLAWRU-UHFFFAOYSA-N ethyl carbamate;methyl prop-2-enoate Chemical compound CCOC(N)=O.COC(=O)C=C YOQPJXKVVLAWRU-UHFFFAOYSA-N 0.000 claims description 24
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- 125000002947 alkylene group Chemical group 0.000 description 10
- 238000000034 method Methods 0.000 description 10
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- 238000007151 ring opening polymerisation reaction Methods 0.000 description 7
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- MNAHQWDCXOHBHK-UHFFFAOYSA-N 1-phenylpropane-1,1-diol Chemical compound CCC(O)(O)C1=CC=CC=C1 MNAHQWDCXOHBHK-UHFFFAOYSA-N 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 6
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- PSGCQDPCAWOCSH-UHFFFAOYSA-N (4,7,7-trimethyl-3-bicyclo[2.2.1]heptanyl) prop-2-enoate Chemical compound C1CC2(C)C(OC(=O)C=C)CC1C2(C)C PSGCQDPCAWOCSH-UHFFFAOYSA-N 0.000 description 5
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- 206010065042 Immune reconstitution inflammatory syndrome Diseases 0.000 description 4
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- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 3
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- INQDDHNZXOAFFD-UHFFFAOYSA-N 2-[2-(2-prop-2-enoyloxyethoxy)ethoxy]ethyl prop-2-enoate Chemical compound C=CC(=O)OCCOCCOCCOC(=O)C=C INQDDHNZXOAFFD-UHFFFAOYSA-N 0.000 description 2
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- 229920003171 Poly (ethylene oxide) Polymers 0.000 description 2
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 2
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- CGRTZESQZZGAAU-UHFFFAOYSA-N [2-[3-[1-[3-(3-tert-butyl-4-hydroxy-5-methylphenyl)propanoyloxy]-2-methylpropan-2-yl]-2,4,8,10-tetraoxaspiro[5.5]undecan-9-yl]-2-methylpropyl] 3-(3-tert-butyl-4-hydroxy-5-methylphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C)=CC(CCC(=O)OCC(C)(C)C2OCC3(CO2)COC(OC3)C(C)(C)COC(=O)CCC=2C=C(C(O)=C(C)C=2)C(C)(C)C)=C1 CGRTZESQZZGAAU-UHFFFAOYSA-N 0.000 description 2
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- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 description 1
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Classifications
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/67—Unsaturated compounds having active hydrogen
- C08G18/671—Unsaturated compounds having only one group containing active hydrogen
- C08G18/672—Esters of acrylic or alkyl acrylic acid having only one group containing active hydrogen
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/104—Coating to obtain optical fibres
- C03C25/105—Organic claddings
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/104—Coating to obtain optical fibres
- C03C25/106—Single coatings
- C03C25/1061—Inorganic coatings
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C25/00—Surface treatment of fibres or filaments made from glass, minerals or slags
- C03C25/10—Coating
- C03C25/104—Coating to obtain optical fibres
- C03C25/1065—Multiple coatings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4854—Polyethers containing oxyalkylene groups having four carbon atoms in the alkylene group
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L33/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- C08L33/04—Homopolymers or copolymers of esters
- C08L33/06—Homopolymers or copolymers of esters of esters containing only carbon, hydrogen and oxygen, which oxygen atoms are present only as part of the carboxyl radical
- C08L33/10—Homopolymers or copolymers of methacrylic acid esters
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- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/14—Polyurethanes having carbon-to-carbon unsaturated bonds
- C09D175/16—Polyurethanes having carbon-to-carbon unsaturated bonds having terminal carbon-to-carbon unsaturated bonds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/02—Polymer mixtures characterised by other features containing two or more polymers of the same C08L -group
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2666/00—Composition of polymers characterized by a further compound in the blend, being organic macromolecular compounds, natural resins, waxes or and bituminous materials, non-macromolecular organic substances, inorganic substances or characterized by their function in the composition
- C08L2666/02—Organic macromolecular compounds, natural resins, waxes or and bituminous materials
- C08L2666/14—Macromolecular compounds according to C08L59/00 - C08L87/00; Derivatives thereof
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- C08L75/00—Compositions of polyureas or polyurethanes; Compositions of derivatives of such polymers
- C08L75/04—Polyurethanes
- C08L75/14—Polyurethanes having carbon-to-carbon unsaturated bonds
- C08L75/16—Polyurethanes having carbon-to-carbon unsaturated bonds having terminal carbon-to-carbon unsaturated bonds
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2913—Rod, strand, filament or fiber
- Y10T428/2933—Coated or with bond, impregnation or core
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- Surface Treatment Of Glass Fibres Or Filaments (AREA)
Abstract
Description
实施例 | 对比例 | ||||||||
1 | 2 | 3 | 4 | 5 | 1 | 2 | 3 | ||
(A) | UA-1 | 52.37 | 52.37 | 52.37 | 52.37 | 52.37 | |||
UA-2 | 76.31 | 76.31 | 76.31 | ||||||
(B) | UB-1 | 2.00 | |||||||
UB-2 | 2.00 | 10 | 25 | ||||||
UB-3 | 0.50 | ||||||||
UB-4 | 1.00 | ||||||||
(C) | M113 | 12.89 | 12.89 | 12.89 | 12.89 | 12.89 | |||
N-乙烯基己内酰胺 | 4.93 | 4.93 | 9.65 | 9.65 | 4.93 | 4.93 | 9.65 | 4.93 | |
丙烯酸月桂酯 | 10.88 | 10.88 | 10.88 | ||||||
(C2) | Viscoat#700 | 26.65 | 26.65 | 26.65 | 26.65 | 26.65 | |||
(D) | Irgacure 184 | 1.97 | 1.97 | 1.97 | 1.97 | 1.97 | 1.97 | 1.97 | 1.97 |
TPO-X | 0.89 | 0.89 | 0.89 | 0.89 | 0.89 | 0.89 | 0.89 | 0.89 | |
其它 | Sumilizer GA-80 | 0.30 | 0.30 | 0.30 | 0.30 | 0.30 | 0.30 | 0.30 | 0.30 |
(B)/(A)+(B)(wt%) | 3.7 | 3.7 | 0.7 | 1.3 | 16.0 | 0 | 0 | 32.3 | |
评估 | |||||||||
液体树脂组合物的性质 | 透明 | 透明 | 透明 | 透明 | 透明 | 透明 | 透明 | 混浊 | |
杨氏模量(MPa) | 520 | 530 | 740 | 730 | 410 | 530 | 750 | 450 | |
粘性(N/m) | 3 | 3 | 4 | 3 | 2 | 15 | 6 | 2 |
实施例 | 对比例 | ||
组分 | 6 | 7 | 4 |
UA-3 | 40.09 | 38.86 | 40.91 |
BU-4 | 2 | 5 | |
CN 120Z(环氧丙烯酸酯) | 25.76 | 24.96 | 26.29 |
1,6-己二醇二丙烯酸酯(HDDA) | 8.01 | 7.77 | 8.18 |
丙烯酸异冰片酯(IBOA) | 10.16 | 9.85 | 10.37 |
丙烯酸2-苯氧基乙酯(PEA) | 9.99 | 9.86 | 10.2 |
二苯基(2,4,6-三甲基苯甲酰基)氧化膦 | 1.99 | 1.93 | 2.03 |
二(1,2,2,6,6-五甲基-4-哌啶基)癸二酸酯 | 0.49 | 0.47 | 0.5 |
亚乙基二(氧化亚乙基)二[3-(5-叔丁基-4-羟基邻甲苯基)丙酸酯] | 0.49 | 0.47 | 0.5 |
DC 190(硅氧烷表面活性剂) | 0.66 | 0.66 | 0.66 |
DC 57(硅氧烷表面活性剂) | 0.36 | 0.36 | 0.36 |
总量 | 100 | 100 | 100 |
(B)/(A)+(B)(wt%) | 4.75 | 11.40 | 0 |
杨氏模量(MPa) | 820 | 800 | 870 |
摩擦系数(单根缓冲纤维对带测试) | 0.67 | 0.67 | 0.90 |
稳态柔量(Je)(MPa-1) | 3.0 | 4.0 | 1.1 |
实施例 | 对比例 | |||
组分 | 8 | 9 | 10 | 4 |
UV-3 | 38.0 | 36.9 | 35.1 | 38.8 |
BU-5 | 2.0 | 4.8 | 9.5 | |
乙氧化(2EO/Ph)双酚A二丙烯酸酯(eBPADA) | 28.5 | 27.7 | 26.3 | 29.1 |
丙氧化新戊二醇二丙烯酸酯(pNPGDA) | 9.5 | 9.2 | 8.8 | 9.7 |
丙烯酸异冰片酯(IBOA) | 19.0 | 18.5 | 17.6 | 19.4 |
Lucerine TPO | 1.0 | 1.0 | 0.9 | 1.0 |
Irgacure 184 | 1.9 | 1.8 | 1.7 | 1.9 |
总量 | 100 | 100 | 100 | 100 |
(B)/(A)+(B)(wt%) | 5 | 11.5 | 21.3 | 0 |
杨氏模量(MPa) | 763 | 673 | 571 | 884 |
稳态柔量(Je)(MPa-1) | 2.4 | 3.6 | 6.6 | 1.4 |
Claims (16)
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JP2003323908A JP4143508B2 (ja) | 2003-09-17 | 2003-09-17 | 液状硬化性樹脂組成物 |
JP323908/2003 | 2003-09-17 |
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US (1) | US7906566B2 (zh) |
EP (1) | EP1664149A1 (zh) |
JP (1) | JP4143508B2 (zh) |
KR (1) | KR20060115353A (zh) |
CN (1) | CN100528923C (zh) |
WO (1) | WO2005026228A1 (zh) |
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-
2004
- 2004-09-17 EP EP20040774948 patent/EP1664149A1/en not_active Withdrawn
- 2004-09-17 US US10/571,758 patent/US7906566B2/en active Active
- 2004-09-17 WO PCT/NL2004/000644 patent/WO2005026228A1/en active Application Filing
- 2004-09-17 CN CNB200480025646XA patent/CN100528923C/zh active Active
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JP2005089586A (ja) | 2005-04-07 |
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US20070203258A1 (en) | 2007-08-30 |
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