CN1800453A - Mucilage glue fiber with antibiotic function and its production method - Google Patents
Mucilage glue fiber with antibiotic function and its production method Download PDFInfo
- Publication number
- CN1800453A CN1800453A CN 200610002004 CN200610002004A CN1800453A CN 1800453 A CN1800453 A CN 1800453A CN 200610002004 CN200610002004 CN 200610002004 CN 200610002004 A CN200610002004 A CN 200610002004A CN 1800453 A CN1800453 A CN 1800453A
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- viscose
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- bamboo vinegar
- grams per
- antibacterial functions
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- 239000000835 fiber Substances 0.000 title claims abstract description 29
- 238000004519 manufacturing process Methods 0.000 title claims description 13
- 230000003115 biocidal effect Effects 0.000 title abstract description 6
- 239000000853 adhesive Substances 0.000 title abstract 3
- 229920000715 Mucilage Polymers 0.000 title 1
- 239000003292 glue Substances 0.000 title 1
- 235000017166 Bambusa arundinacea Nutrition 0.000 claims abstract description 55
- 235000017491 Bambusa tulda Nutrition 0.000 claims abstract description 55
- 241001330002 Bambuseae Species 0.000 claims abstract description 55
- 235000015334 Phyllostachys viridis Nutrition 0.000 claims abstract description 55
- 239000011425 bamboo Substances 0.000 claims abstract description 55
- 239000000052 vinegar Substances 0.000 claims abstract description 53
- 235000021419 vinegar Nutrition 0.000 claims abstract description 53
- 238000009987 spinning Methods 0.000 claims description 53
- 229920000297 Rayon Polymers 0.000 claims description 45
- 230000000844 anti-bacterial effect Effects 0.000 claims description 27
- 239000007788 liquid Substances 0.000 claims description 25
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 22
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 12
- 238000001914 filtration Methods 0.000 claims description 10
- 239000002964 rayon Substances 0.000 claims description 8
- 239000002253 acid Substances 0.000 claims description 7
- 239000000470 constituent Substances 0.000 claims description 7
- 238000003756 stirring Methods 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 238000006477 desulfuration reaction Methods 0.000 claims description 6
- 230000023556 desulfurization Effects 0.000 claims description 6
- 238000004090 dissolution Methods 0.000 claims description 6
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 6
- 235000011152 sodium sulphate Nutrition 0.000 claims description 6
- 238000007711 solidification Methods 0.000 claims description 6
- 230000008023 solidification Effects 0.000 claims description 6
- 238000005406 washing Methods 0.000 claims description 6
- NWONKYPBYAMBJT-UHFFFAOYSA-L zinc sulfate Chemical compound [Zn+2].[O-]S([O-])(=O)=O NWONKYPBYAMBJT-UHFFFAOYSA-L 0.000 claims description 6
- 229960001763 zinc sulfate Drugs 0.000 claims description 6
- 229910000368 zinc sulfate Inorganic materials 0.000 claims description 6
- 240000007594 Oryza sativa Species 0.000 claims description 2
- 235000007164 Oryza sativa Nutrition 0.000 claims description 2
- 238000012805 post-processing Methods 0.000 claims description 2
- 235000009566 rice Nutrition 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 10
- 239000002994 raw material Substances 0.000 abstract description 7
- 230000001070 adhesive effect Effects 0.000 abstract 2
- 239000000243 solution Substances 0.000 description 42
- 230000008569 process Effects 0.000 description 9
- 230000001580 bacterial effect Effects 0.000 description 8
- 238000011282 treatment Methods 0.000 description 6
- 229920003043 Cellulose fiber Polymers 0.000 description 5
- 239000003513 alkali Substances 0.000 description 5
- 229920002678 cellulose Polymers 0.000 description 5
- 239000001913 cellulose Substances 0.000 description 5
- 238000010790 dilution Methods 0.000 description 5
- 239000012895 dilution Substances 0.000 description 5
- 238000007598 dipping method Methods 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 239000000463 material Substances 0.000 description 5
- 238000012856 packing Methods 0.000 description 5
- 238000010298 pulverizing process Methods 0.000 description 5
- 238000012216 screening Methods 0.000 description 5
- 229920000742 Cotton Polymers 0.000 description 4
- 239000013068 control sample Substances 0.000 description 4
- 238000013461 design Methods 0.000 description 4
- 239000012153 distilled water Substances 0.000 description 4
- 238000003359 percent control normalization Methods 0.000 description 4
- 230000001954 sterilising effect Effects 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- FERIUCNNQQJTOY-UHFFFAOYSA-N Butyric acid Chemical compound CCCC(O)=O FERIUCNNQQJTOY-UHFFFAOYSA-N 0.000 description 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 description 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-N dimethylselenoniopropionate Natural products CCC(O)=O XBDQKXXYIPTUBI-UHFFFAOYSA-N 0.000 description 2
- QWVGKYWNOKOFNN-UHFFFAOYSA-N o-cresol Chemical compound CC1=CC=CC=C1O QWVGKYWNOKOFNN-UHFFFAOYSA-N 0.000 description 2
- 150000002989 phenols Chemical class 0.000 description 2
- JEFSTMHERNSDBC-UHFFFAOYSA-N 1,2-dimethylcyclohexa-2,4-dien-1-ol Chemical compound CC1=CC=CCC1(C)O JEFSTMHERNSDBC-UHFFFAOYSA-N 0.000 description 1
- 235000001674 Agaricus brunnescens Nutrition 0.000 description 1
- 239000005711 Benzoic acid Substances 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 208000002474 Tinea Diseases 0.000 description 1
- 241000893966 Trichophyton verrucosum Species 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 150000001335 aliphatic alkanes Chemical class 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- 230000000845 anti-microbial effect Effects 0.000 description 1
- 235000010233 benzoic acid Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 150000007524 organic acids Chemical group 0.000 description 1
- 230000003449 preventive effect Effects 0.000 description 1
- 235000019260 propionic acid Nutrition 0.000 description 1
- 238000000197 pyrolysis Methods 0.000 description 1
- IUVKMZGDUIUOCP-BTNSXGMBSA-N quinbolone Chemical compound O([C@H]1CC[C@H]2[C@H]3[C@@H]([C@]4(C=CC(=O)C=C4CC3)C)CC[C@@]21C)C1=CCCC1 IUVKMZGDUIUOCP-BTNSXGMBSA-N 0.000 description 1
- 238000010008 shearing Methods 0.000 description 1
- 208000017520 skin disease Diseases 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Landscapes
- Artificial Filaments (AREA)
Abstract
The invention discloses an adhesive fiber with antibiotic ability and relative producing method, with the density of 5-20.5% and the bamboo vinegar solution in 0.1-5% weight of adhesive fiber. The invention uses natural bamboo vinegar solution as antibiotic raw material with innocuous and better antibiotic ability.
Description
One, technical field
The present invention relates to a kind of viscose and production method thereof, more particularly relate to a kind of viscose with antibacterial functions and production method thereof of adding Bamboo vinegar solution with antibacterial functions.
Two, background technology
Bamboo vinegar solution is the product liquid that the bamboo wood pyrolysis obtains, and it is the quite complicated liquid mixture of a kind of constituent, and its main component is water, secondly is organic acid, comprises tens kinds of acid such as acetic acid, propionic acid, butyric acid and benzoic acid; Also have phenols, phenol, 2-methylphenol and 2, more than 20 kind of phenols such as 6-xylenol in addition; More than 30 kind of aldehydes, several alcohols and ketone also contain multiple alkane, alkene in addition, also contain a spot of tar.Bamboo vinegar solution has antibacterial and bactericidal action, multiple mushroom is had restrain and preventive and therapeutic effect, is commonly used to treat the ringworm of the foot and various skin disease in the medical treatment at present.
Up to now, do not see that Bamboo vinegar solution is used for the bibliographical information of viscose as additive.
Three, summary of the invention
Viscose with antibacterial functions of the present invention, to contain concentration be 5-20.5% (volume), account for the Bamboo vinegar solution of viscose gross weight 0.1-5%; Be preferably the Bamboo vinegar solution that to contain concentration be 10-20 (volume) %, account for viscose gross weight 0.2-3%; The Bamboo vinegar solution that is that to contain concentration be 14-17 (volume) %, accounts for viscose gross weight 0.5-2% that can select.
Production method with viscose of antibacterial functions of the present invention, comprise filtration, yellow, spinning and post-processing step, wherein earlier raw liquid of bamboo vinegar is filtered (secondary or three times), filter out suspended matter wherein, being diluted with water to needs concentration again, then with pH value adjusted value 3.0-6.0, color is faint yellow, temperature is a normal temperature, and good seal, prevent the volatilization and foreign material fall into.
Cellulose pulp through common process such as blank, screening, preliminary treatment, dipping, pulverizing, experienced and yellows after, when the yellow of alkali cellulose fiber, by adding dilution heat of sulfuric acid, the pH value of spinning solution is adjusted between the 7.5-9.5 dissolution phase adding Bamboo vinegar solution when yellow finishes.After Bamboo vinegar solution added, through 1-2 hour stirring, making viscosity was 20-45 second, and the first fibre is 9.0-9.5%, and ripe degree is a 5-13 milliliter bamboo vinegar liquid rayon spinning stoste.
In the production method of the viscose with antibacterial functions of the present invention, after the viscose spinning solution of bamboo vinegar liquid filtered through three times, on short silk spinning machine, carry out spinning, spinning head 1.5-3.0D, aperture ratio＞3, spinning pressure 15-30kPa, spinning speed 35-50 rice/minute, spinning humidity is 60-70%, and temperature is 20-25 ℃.The solidification liquid constituent is: sulfuric acid 90-110 grams per liter, sodium sulphate 310-330 grams per liter, zinc sulfate 10-15 grams per liter, acid bath drop＜4 grams per liters, temperature 30-45 ℃.After fibre bundle solidified, through three washings, wash temperature was 60-70 ℃, and desulfurization temperature is 70-80 ℃, and concentration is the 3.5-4.5 grams per liter, and then through oiling, oil bath concentration is the 2.5-3.5 grams per liter, and after oiling, classification and packing are sheared in oven dry.
In the present invention owing to adopt natural Bamboo vinegar solution as antibiotic raw material, so product is nontoxic, harmless to human body, has fabulous anti-microbial property.
Further, the viscose the key technical indexes with antibacterial functions of the present invention can be or greater than:
Line density (dtex) 1.67-3.33
Do fracture strength cN/dtex 1.95 elongation at breaks (%) 17.4
Ultimate strength CV (%) 6.63 elongation at break CV (%) 6.9
Wet breaking strength cN/dtex 1.98 ultimate strength CV (%) 2.62
Antibiotic index＞95% regain (%) 13
PH value 6-7
Four, the specific embodiment
Describe the present invention in detail below in conjunction with specific embodiment; described embodiment is in order better to explain the present invention; rather than to the restriction of claim protection domain of the present invention, all belong to the scope that the present invention asks for protection based on the modification and the change of basic thought of the present invention.
In the present invention, if not refer in particular to, all parts, amount are the unit of weight based on gross weight, and all raw materials all can be buied from market.
Embodiment 1:
1.5D, 38 centimetres of antibacterial viscose fibers, raw material: former Bamboo vinegar solution (concentration 21 (volume) %), former cotton pulp.It is 1.5% that the design Bamboo vinegar solution accounts for fiber weight percentage.
At first Bamboo vinegar solution is carried out twice filtration, the filtering suspended material, and Bamboo vinegar solution concentration is modulated to 12.5% with distilled water, pH value is adjusted to about 4.
Cellulose pulp process: behind the common process such as blank, screening, preliminary treatment, dipping, pulverizing, experienced and yellow, when the yellow of alkali cellulose fiber, by adding dilution heat of sulfuric acid, spinning solution PH is transferred to about 8, in the course of dissolution when yellow finishes, the Bamboo vinegar solution modulating liquid of getting ready is added, stirring through 1 hour, making viscosity is 35 ± 1, and the first fibre is 9.4 ± 0.1%, and ripe degree is the rayon spinning stoste of 9 ± 1 milliliters bamboo vinegar liquid.
Through after the above-mentioned technology, after the rayon spinning stoste of bamboo vinegar liquid filtered through three times, on short silk spinning machine, carry out spinning, its solidification liquid constituent is: sulfuric acid 95 ± 2 grams per liters, sodium sulphate 325 ± 2 grams per liters, zinc sulfate 11 ± 1 grams per liters, acid bath drop＜4 grams per liters, 35 ± 1 ℃ of temperature.Spinning head 1.5D, the aperture ratio is 4.5, spinning pressure 21 ± 0.5kPa, 40 meters/minute of spinning speeds.
After fibre bundle solidified, through three washings, wash temperature was 65 ℃, and desulfurization temperature is 70 ℃, and concentration is 3.5 ± 0.1 grams per liters.And then through oiling, oil bath concentration is 2.7 ± 0.1 grams per liters, after oiling, and oven dry, shearing, classification and packing.
Testing result:
ASTM E 2149
| Specimen | ' 0 hour ' bacterial population | ' 24 hours ' bacterial population | Bacteriostasis rate | Sterilizing rate |
| Antibacterial viscose fiber | / | 1.4×10 3 | 100％ | 98.5％ |
| Control sample | 9.5×10 4 | 1.1×10 7 | / | / |
| N 3 | 114.3 |
Embodiment 2:
3D, random length antibacterial viscose fiber, raw material: former Bamboo vinegar solution (concentration 21 (volume) %), former cotton pulp.It is 0.7% that the design Bamboo vinegar solution accounts for fiber weight percentage.
At first Bamboo vinegar solution is carried out twice filtration, the filtering suspended material, and Bamboo vinegar solution concentration is modulated to 17% with distilled water, pH value is adjusted to about 3.5.
Cellulose pulp process: behind the common process such as blank, screening, preliminary treatment, dipping, pulverizing, experienced and yellow, when the yellow of alkali cellulose fiber, by adding dilution heat of sulfuric acid, spinning solution PH is transferred to about 8.5, in the course of dissolution when yellow finishes, the Bamboo vinegar solution modulating liquid of getting ready is added, stirring through 2 hours, making viscosity is 37 ± 1, and the first fibre is 9.2 ± 0.1%, and ripe degree is the rayon spinning stoste of 10 ± 1 milliliters of bamboo vinegar liquids
Through after the above-mentioned technology, after Bamboo vinegar solution viscose spinning solution filtered through three times, on short silk spinning machine, carry out spinning, its solidification liquid constituent is: sulfuric acid 100 ± 2 grams per liters, sodium sulphate are 320 ± 2 grams per liters, and zinc sulfate is 12 ± 1 grams per liters, acid bath drop＜4 grams per liters, 35 ± 1 ℃ of temperature.Spinning head 3D, the aperture ratio is 3.5, spinning pressure 20 ± 0.5kPa, 40 meters/minute of spinning speeds.
After fibre bundle solidified, through three washings, wash temperature was 65 ℃, and desulfurization temperature is 70 ℃, and concentration is 4 ± 0.1 grams per liters.And then through oiling, oil bath concentration is 3.2 ± 0.1 grams per liters, and after oiling, oven dry is sheared, classification, packing.
Testing result:
ASTME 2149
| Specimen | ' 0 hour ' bacterial population | ' 24 hours ' bacterial population | Bacteriostasis rate | Sterilizing rate |
| Antibacterial viscose fiber | / | 1.0×10 3 | 100％ | 99.8％ |
| Control sample | 5.9×10 4 | 6.0×10 7 | / | / |
| N 3 | 1017 |
Embodiment 3
2.5D, 36 centimetres of antibacterial viscose fibers, raw material: former Bamboo vinegar solution (concentration 20 (volume) %), bamboo fibre and former cotton pulp.It is 0.4% that the design Bamboo vinegar solution accounts for fiber weight percentage.
At first Bamboo vinegar solution is carried out twice filtration, the filtering suspended material, and Bamboo vinegar solution concentration is modulated to 10% with distilled water, pH value is adjusted to about 4.5.
Cellulose pulp process: behind the common process such as blank, screening, preliminary treatment, dipping, pulverizing, experienced and yellow, when the yellow of alkali cellulose fiber, by adding dilution heat of sulfuric acid, spinning solution PH is transferred to about 7.5, in the course of dissolution when yellow finishes, the Bamboo vinegar solution modulating liquid of getting ready is added, stirring through 1.5 hours, making viscosity is 22 ± 1, and the first fibre is 9.1 ± 0.1%, and ripe degree is the rayon spinning stoste of 7 ± 1 milliliters of bamboo vinegar liquids
Through after the above-mentioned technology, after Bamboo vinegar solution viscose spinning solution filtered through three times, on short silk spinning machine, carry out spinning, its solidification liquid constituent is: sulfuric acid 94 ± 2 grams per liters, sodium sulphate are 320 ± 2 grams per liters, and zinc sulfate is 11 ± 1 grams per liters, acid bath drop 2.5 grams per liters, 31 ± 1 ℃ of temperature.Spinning head 1.5D, the aperture ratio is 3.5, spinning pressure 16 ± 0.5kPa, 40 meters/minute of spinning speeds.
After fibre bundle solidified, through three washings, wash temperature was 75 ℃, and desulfurization temperature is 70 ℃, and concentration is 4 ± 0.1 grams per liters.And then through oiling, oil bath concentration is 4.2 ± 0.1 grams per liters, and after oiling, oven dry is sheared, classification, packing.
Testing result:
ASTME 2149
| Specimen | ' 0 hour ' bacterial population | ' 24 hours ' bacterial population | Bacteriostasis rate | Sterilizing rate |
| Antibacterial viscose fiber | / | 0.9×10 3 | 100％ | 99.8％ |
| Control sample | 6.3×10 4 | 6.3×10 7 | / | / |
| N 3 | 1017 |
Embodiment 4
2.5D, 42 centimetres of antibacterial viscose fibers, raw material: former Bamboo vinegar solution (concentration 25 (volume) %), former cotton pulp.It is 4.7% that the design Bamboo vinegar solution accounts for fiber weight percentage.
At first Bamboo vinegar solution is carried out twice filtration, the filtering suspended material, and Bamboo vinegar solution concentration is modulated to 6% with distilled water, pH value is adjusted to about 5.5.
Cellulose pulp process: behind the common process such as blank, screening, preliminary treatment, dipping, pulverizing, experienced and yellow, when the yellow of alkali cellulose fiber, by adding dilution heat of sulfuric acid, spinning solution PH is transferred to about 9.0, in the course of dissolution when yellow finishes, the Bamboo vinegar solution modulating liquid of getting ready is added, stirring through 2 hours, making viscosity is 40 ± 1, and the first fibre is 9.4 ± 0.1%, and ripe degree is the rayon spinning stoste of 12 ± 1 milliliters of bamboo vinegar liquids
Through after the above-mentioned technology, after Bamboo vinegar solution viscose spinning solution filtered through three times, on short silk spinning machine, carry out spinning, its solidification liquid constituent is: sulfuric acid 92 ± 2 grams per liters, sodium sulphate are 310 ± 2 grams per liters, and zinc sulfate is 13 ± 1 grams per liters, acid bath drop 3 grams per liters, 40 ± 1 ℃ of temperature.Spinning head 2.0D, the aperture ratio is 4.5, spinning pressure 25 ± 0.5kPa, 50 meters/minute of spinning speeds.
After fibre bundle solidified, through three washings, wash temperature was 75 ℃, and desulfurization temperature is 70 ℃, and concentration is 4 ± 0.1 grams per liters.And then through oiling, oil bath concentration is 4.2 ± 0.1 grams per liters, and after oiling, oven dry is sheared, classification, packing.
Testing result:
ASTME 2149
| Specimen | ' 0 hour ' bacterial population | ' 24 hours ' bacterial population | Bacteriostasis rate | Sterilizing rate |
| Antibacterial viscose fiber | / | 1.1×10 3 | 100％ | 99.8％ |
| Control sample | 6.3×10 4 | 6.5×10 7 | / | / |
| N 3 | 1017 |
Claims (9)
1, a kind of viscose with antibacterial functions is characterized in that containing concentration the Bamboo vinegar solution that is 5-20.5%, accounts for viscose gross weight 0.1-5%.
2, the viscose with antibacterial functions according to claim 1 is characterized in that containing concentration the Bamboo vinegar solution that is 10-20%, accounts for viscose gross weight 0.2-3%.
3, the viscose with antibacterial functions according to claim 1 and 2 is characterized in that containing concentration the Bamboo vinegar solution that is 14-17%, accounts for viscose gross weight 0.5-2%.
4, according to the described production method of one of claim 1-3 with viscose of antibacterial functions, it is characterized in that comprising filtration, yellow, spinning and post-processing step, wherein elder generation is adjusted to the pH value of spinning solution between the 7.5-9.5, and the dissolution phase when yellow finishes adds Bamboo vinegar solution.
5, according to the described production method with viscose of antibacterial functions of one of claim 1-3, it is characterized in that raw liquid of bamboo vinegar is filtered, filter out suspended matter wherein, being diluted with water to needs concentration again, then with pH value adjusted value 3.0-6.0.
6, according to the described production method of one of claim 1-3 with viscose of antibacterial functions, it is characterized in that through 1-2 hour stirring, making viscosity was 20-45 second with after the Bamboo vinegar solution adding, the first fibre is 9.0-9.5%, and ripe degree is a 5-13 milliliter bamboo vinegar liquid rayon spinning stoste.
7, the production method with viscose of antibacterial functions according to claim 6, it is characterized in that through 1-2 hour stirring, making viscosity was 30-38 second with after the Bamboo vinegar solution adding, the first fibre is 9.1-9.5%, and ripe degree is the rayon spinning liquid of 7-11 milliliter bamboo vinegar liquid.8, according to the described production method of one of claim 1-3 with viscose of antibacterial functions, after it is characterized in that the viscose spinning solution of bamboo vinegar liquid filtered through three times, on short silk spinning machine, carry out spinning, spinning head 1.5-3.0D, aperture ratio＞3, spinning pressure 15-30kPa, spinning speed 35-50 rice/minute, spinning humidity is 60-70%, and temperature is 20-25 ℃.
9, the production method with viscose of antibacterial functions according to claim 8, it is characterized in that the solidification liquid constituent is: sulfuric acid 90-110 grams per liter, sodium sulphate 310-330 grams per liter, zinc sulfate 10-15 grams per liter, acid bath drop＜4 grams per liters, temperature 30-45 ℃.
10, according to the described production method of one of claim 1-3 with viscose of antibacterial functions, it is characterized in that fibre bundle solidifies after, through three times the washing, wash temperature is 60-70 ℃, desulfurization temperature is 70-80 ℃, and concentration is the 3.5-4.5 grams per liter, and oil bath concentration is the 2.5-3.5 grams per liter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100020049A CN100398706C (en) | 2006-01-20 | 2006-01-20 | Mucilage glue fiber with antibiotic function and its production method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2006100020049A CN100398706C (en) | 2006-01-20 | 2006-01-20 | Mucilage glue fiber with antibiotic function and its production method |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1800453A true CN1800453A (en) | 2006-07-12 |
| CN100398706C CN100398706C (en) | 2008-07-02 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2006100020049A Expired - Fee Related CN100398706C (en) | 2006-01-20 | 2006-01-20 | Mucilage glue fiber with antibiotic function and its production method |
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| Country | Link |
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| CN (1) | CN100398706C (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101928998A (en) * | 2010-03-19 | 2010-12-29 | 安吉谈竹庄竹纤维有限公司 | Bamboo viscose fiber and preparation method thereof |
| CN102995141A (en) * | 2012-10-25 | 2013-03-27 | 郭荣才 | Bamboo fiber |
| CN105506822A (en) * | 2015-12-21 | 2016-04-20 | 山东如意科技集团有限公司 | Fabric with antibacterial effect and dyeing and finishing method of fabric |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1293180C (en) * | 2003-07-14 | 2007-01-03 | 陈双贵 | Bamboo vinegar production processes and apparatus |
| JP2005179245A (en) * | 2003-12-18 | 2005-07-07 | Yamanashi Yagen Kk | Antiallergic composition containing wood vinegar/bamboo vinegar distillate |
-
2006
- 2006-01-20 CN CNB2006100020049A patent/CN100398706C/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101928998A (en) * | 2010-03-19 | 2010-12-29 | 安吉谈竹庄竹纤维有限公司 | Bamboo viscose fiber and preparation method thereof |
| CN102995141A (en) * | 2012-10-25 | 2013-03-27 | 郭荣才 | Bamboo fiber |
| CN102995141B (en) * | 2012-10-25 | 2014-06-18 | 郭荣才 | Bamboo fiber |
| CN105506822A (en) * | 2015-12-21 | 2016-04-20 | 山东如意科技集团有限公司 | Fabric with antibacterial effect and dyeing and finishing method of fabric |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100398706C (en) | 2008-07-02 |
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