CN1699163A - 用硫酸钠法生产白炭黑和亚硫酸钠的工艺 - Google Patents
用硫酸钠法生产白炭黑和亚硫酸钠的工艺 Download PDFInfo
- Publication number
- CN1699163A CN1699163A CNA2005102003147A CN200510200314A CN1699163A CN 1699163 A CN1699163 A CN 1699163A CN A2005102003147 A CNA2005102003147 A CN A2005102003147A CN 200510200314 A CN200510200314 A CN 200510200314A CN 1699163 A CN1699163 A CN 1699163A
- Authority
- CN
- China
- Prior art keywords
- sodium
- carbon black
- white carbon
- sodium sulfate
- sodium sulfite
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 title claims abstract description 38
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 title claims abstract description 29
- 238000000034 method Methods 0.000 title claims abstract description 20
- 235000010265 sodium sulphite Nutrition 0.000 title claims abstract description 19
- 239000006229 carbon black Substances 0.000 title claims abstract description 18
- 229910052938 sodium sulfate Inorganic materials 0.000 title claims abstract description 14
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 title claims abstract description 13
- 235000011152 sodium sulphate Nutrition 0.000 title claims abstract description 13
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 claims abstract description 14
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims abstract description 12
- 239000004115 Sodium Silicate Substances 0.000 claims abstract description 11
- 238000006243 chemical reaction Methods 0.000 claims abstract description 11
- 229910052911 sodium silicate Inorganic materials 0.000 claims abstract description 11
- 238000001914 filtration Methods 0.000 claims abstract description 10
- 238000001035 drying Methods 0.000 claims abstract description 7
- 239000007787 solid Substances 0.000 claims abstract description 6
- 239000000706 filtrate Substances 0.000 claims abstract description 5
- 239000006004 Quartz sand Substances 0.000 claims abstract description 4
- 239000000126 substance Substances 0.000 claims abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 238000004321 preservation Methods 0.000 claims description 3
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 238000004090 dissolution Methods 0.000 claims description 2
- 229940044609 sulfur dioxide Drugs 0.000 claims 2
- 235000010269 sulphur dioxide Nutrition 0.000 claims 2
- 239000007788 liquid Substances 0.000 abstract description 3
- 238000002156 mixing Methods 0.000 abstract description 3
- 239000003610 charcoal Substances 0.000 abstract 1
- 238000009991 scouring Methods 0.000 abstract 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000007832 Na2SO4 Substances 0.000 description 1
- 229910052681 coesite Inorganic materials 0.000 description 1
- 229910052906 cristobalite Inorganic materials 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 239000000123 paper Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 235000019353 potassium silicate Nutrition 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000010791 quenching Methods 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 235000017550 sodium carbonate Nutrition 0.000 description 1
- 229910000029 sodium carbonate Inorganic materials 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
- 229910052682 stishovite Inorganic materials 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- 229910052905 tridymite Inorganic materials 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000012463 white pigment Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
- C01B33/187—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates
- C01B33/193—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof by acidic treatment of silicates of aqueous solutions of silicates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/113—Silicon oxides; Hydrates thereof
- C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
- C01B33/18—Preparation of finely divided silica neither in sol nor in gel form; After-treatment thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B33/00—Silicon; Compounds thereof
- C01B33/20—Silicates
- C01B33/32—Alkali metal silicates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01D—COMPOUNDS OF ALKALI METALS, i.e. LITHIUM, SODIUM, POTASSIUM, RUBIDIUM, CAESIUM, OR FRANCIUM
- C01D5/00—Sulfates or sulfites of sodium, potassium or alkali metals in general
- C01D5/14—Preparation of sulfites
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Silicon Compounds (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Battery Electrode And Active Subsutance (AREA)
Abstract
Description
Claims (2)
Priority Applications (10)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US11/916,863 US20080202387A1 (en) | 2005-06-08 | 2005-06-06 | Process For Producing Silica and Sodium Sulfite With Sodium Sulfate |
CNB2005102003147A CN100345754C (zh) | 2005-06-08 | 2005-06-08 | 用硫酸钠法生产白炭黑和亚硫酸钠的工艺 |
KR1020077028661A KR20080016835A (ko) | 2005-06-08 | 2006-06-06 | 황산 나트륨을 사용한 실리카 및 아황산 나트륨의 제조방법 |
CNA2006800191430A CN101184693A (zh) | 2005-06-08 | 2006-06-06 | 一种用硫酸钠法生产轻质二氧化硅和亚硫酸钠的工艺 |
RU2007148703/15A RU2007148703A (ru) | 2005-06-08 | 2006-06-06 | Способ получения двуокиси кремния и сульфита натрия с использованием сульфата натрия |
PCT/CN2006/001226 WO2006131064A1 (en) | 2005-06-08 | 2006-06-06 | A process for producing silica and sodium sulfite with sodium sulfate |
BRPI0612021-0A BRPI0612021B1 (pt) | 2005-06-08 | 2006-06-06 | Process for the production of sodium soil and sulfite with sodium sulfate |
EP06742112A EP1888460A1 (en) | 2005-06-08 | 2006-06-06 | A process for producing silica and sodium sulfite with sodium sulfate |
JP2008515031A JP2008542185A (ja) | 2005-06-08 | 2006-06-06 | 硫酸ナトリウムを用いてシリカと亜硫酸ナトリウムとを製造する方法 |
IL186751A IL186751A0 (en) | 2005-06-08 | 2007-10-18 | A process for producing silica and sodium sulfite with sodium sulfate |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2005102003147A CN100345754C (zh) | 2005-06-08 | 2005-06-08 | 用硫酸钠法生产白炭黑和亚硫酸钠的工艺 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1699163A true CN1699163A (zh) | 2005-11-23 |
CN100345754C CN100345754C (zh) | 2007-10-31 |
Family
ID=35475448
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB2005102003147A Active CN100345754C (zh) | 2005-06-08 | 2005-06-08 | 用硫酸钠法生产白炭黑和亚硫酸钠的工艺 |
CNA2006800191430A Pending CN101184693A (zh) | 2005-06-08 | 2006-06-06 | 一种用硫酸钠法生产轻质二氧化硅和亚硫酸钠的工艺 |
Family Applications After (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNA2006800191430A Pending CN101184693A (zh) | 2005-06-08 | 2006-06-06 | 一种用硫酸钠法生产轻质二氧化硅和亚硫酸钠的工艺 |
Country Status (9)
Country | Link |
---|---|
US (1) | US20080202387A1 (zh) |
EP (1) | EP1888460A1 (zh) |
JP (1) | JP2008542185A (zh) |
KR (1) | KR20080016835A (zh) |
CN (2) | CN100345754C (zh) |
BR (1) | BRPI0612021B1 (zh) |
IL (1) | IL186751A0 (zh) |
RU (1) | RU2007148703A (zh) |
WO (1) | WO2006131064A1 (zh) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101774591A (zh) * | 2010-02-26 | 2010-07-14 | 无锡恒诚硅业有限公司 | 一种白色微珠状高强度白炭黑的生产工艺 |
CN102083752A (zh) * | 2008-07-04 | 2011-06-01 | 罗地亚管理公司 | 由焦亚硫酸钠或亚硫酸钠制备沉淀二氧化硅的方法 |
CN104724712A (zh) * | 2015-03-12 | 2015-06-24 | 确成硅化学股份有限公司 | 利用硫酸生产尾气制备白炭黑的方法 |
CN108043198A (zh) * | 2017-12-06 | 2018-05-18 | 安徽凤阳赛吉元无机材料有限公司 | 一种利用水玻璃水淬水制备脱硫液的方法 |
CN114436271A (zh) * | 2021-12-29 | 2022-05-06 | 四川马边龙泰磷电有限责任公司 | 一种利用硫循环的白炭黑生产工艺 |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1331744C (zh) * | 2005-06-08 | 2007-08-15 | 德固赛嘉联白炭黑(南平)有限公司 | 一种用硫酸钠法生产白炭黑和亚硫酸钠的工艺 |
CN100545085C (zh) * | 2005-06-10 | 2009-09-30 | 德固赛嘉联白炭黑(南平)有限公司 | 硫酸钠法生产白炭黑、亚硫酸钠和亚硫酸氢钠的工艺 |
KR101064246B1 (ko) * | 2009-08-06 | 2011-09-14 | 오준석 | 수맥파 차단용 페인트 |
CN103482809A (zh) * | 2013-08-26 | 2014-01-01 | 厦门世达膜科技有限公司 | 一种白炭黑生产废水零排放工艺 |
CN111153412A (zh) * | 2020-01-15 | 2020-05-15 | 河南省睿博环境工程技术有限公司 | 一种基于滤洗液与硫酸钠循环利用的白炭黑生产流程 |
CN111620348B (zh) * | 2020-06-22 | 2022-11-22 | 安徽龙泉硅材料有限公司 | 一种纳米二氧化硅用硅酸钠的制备方法 |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3241990A (en) * | 1965-03-10 | 1966-03-22 | Harrison John Gordon | Alkali metal silicate compositions and process of manufacture |
CN1037110C (zh) * | 1993-06-18 | 1998-01-21 | 鞍山钢铁学院 | 一种生产白炭黑的方法 |
CN1039219C (zh) * | 1993-12-21 | 1998-07-22 | 冯中一 | 一种雾化法生产水合硅酸的方法 |
US6395247B1 (en) * | 1997-12-12 | 2002-05-28 | Degussa Ag | Precipitated silica |
DE19755287A1 (de) * | 1997-12-12 | 1999-07-08 | Degussa | Fällungskieselsäure |
JP3824047B2 (ja) * | 2000-02-04 | 2006-09-20 | 信越化学工業株式会社 | 非晶質酸化珪素粉末の製造方法 |
CN1301902C (zh) * | 2004-05-21 | 2007-02-28 | 云南化工实业股份有限公司 | 一种高纯二氧化硅的生产方法 |
CN1331744C (zh) * | 2005-06-08 | 2007-08-15 | 德固赛嘉联白炭黑(南平)有限公司 | 一种用硫酸钠法生产白炭黑和亚硫酸钠的工艺 |
CN100545085C (zh) * | 2005-06-10 | 2009-09-30 | 德固赛嘉联白炭黑(南平)有限公司 | 硫酸钠法生产白炭黑、亚硫酸钠和亚硫酸氢钠的工艺 |
-
2005
- 2005-06-06 US US11/916,863 patent/US20080202387A1/en not_active Abandoned
- 2005-06-08 CN CNB2005102003147A patent/CN100345754C/zh active Active
-
2006
- 2006-06-06 EP EP06742112A patent/EP1888460A1/en not_active Withdrawn
- 2006-06-06 JP JP2008515031A patent/JP2008542185A/ja active Pending
- 2006-06-06 BR BRPI0612021-0A patent/BRPI0612021B1/pt not_active IP Right Cessation
- 2006-06-06 KR KR1020077028661A patent/KR20080016835A/ko not_active Application Discontinuation
- 2006-06-06 CN CNA2006800191430A patent/CN101184693A/zh active Pending
- 2006-06-06 WO PCT/CN2006/001226 patent/WO2006131064A1/en active Application Filing
- 2006-06-06 RU RU2007148703/15A patent/RU2007148703A/ru not_active Application Discontinuation
-
2007
- 2007-10-18 IL IL186751A patent/IL186751A0/en unknown
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102083752A (zh) * | 2008-07-04 | 2011-06-01 | 罗地亚管理公司 | 由焦亚硫酸钠或亚硫酸钠制备沉淀二氧化硅的方法 |
CN102083752B (zh) * | 2008-07-04 | 2013-06-26 | 罗地亚管理公司 | 由焦亚硫酸钠或亚硫酸钠制备沉淀二氧化硅的方法 |
CN101774591A (zh) * | 2010-02-26 | 2010-07-14 | 无锡恒诚硅业有限公司 | 一种白色微珠状高强度白炭黑的生产工艺 |
CN101774591B (zh) * | 2010-02-26 | 2012-06-27 | 无锡恒诚硅业有限公司 | 一种白色微珠状高强度白炭黑的生产工艺 |
CN104724712A (zh) * | 2015-03-12 | 2015-06-24 | 确成硅化学股份有限公司 | 利用硫酸生产尾气制备白炭黑的方法 |
CN108043198A (zh) * | 2017-12-06 | 2018-05-18 | 安徽凤阳赛吉元无机材料有限公司 | 一种利用水玻璃水淬水制备脱硫液的方法 |
CN114436271A (zh) * | 2021-12-29 | 2022-05-06 | 四川马边龙泰磷电有限责任公司 | 一种利用硫循环的白炭黑生产工艺 |
Also Published As
Publication number | Publication date |
---|---|
RU2007148703A (ru) | 2009-07-20 |
KR20080016835A (ko) | 2008-02-22 |
CN100345754C (zh) | 2007-10-31 |
WO2006131064A1 (en) | 2006-12-14 |
JP2008542185A (ja) | 2008-11-27 |
BRPI0612021A2 (pt) | 2010-10-13 |
CN101184693A (zh) | 2008-05-21 |
US20080202387A1 (en) | 2008-08-28 |
IL186751A0 (en) | 2008-02-09 |
EP1888460A1 (en) | 2008-02-20 |
BRPI0612021B1 (pt) | 2017-10-31 |
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ASS | Succession or assignment of patent right |
Owner name: DEGUSSA WELLINK SILICA (NANPING) CO. Free format text: FORMER OWNER: LU YUANJIAN Effective date: 20060915 |
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C41 | Transfer of patent application or patent right or utility model | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20060915 Address after: 353000 Jia Lian building, 136 Xinjian Road, Fujian, Nanping, China Applicant after: DEGUSSA WELLINK SILICA (NANPING) CO.,LTD. Address before: 353000 Nanping city of Fujian province Nanping city Ziyun Street Yanping District progress road No. 18 Applicant before: Lu Yuanjian Effective date of registration: 20060915 Address after: 353000 Nanping city of Fujian province Nanping city Ziyun Street Yanping District progress road No. 18 Applicant after: Lu Yuanjian Address before: 353000, No. 143, Xinjian Road, Nanping, Fujian, Nanping Applicant before: Lu Yuanjian |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
CP01 | Change in the name or title of a patent holder | ||
CP01 | Change in the name or title of a patent holder |
Address after: 353000 Jia Lian building, 136 Xinjian Road, Fujian, Nanping Patentee after: Win jiaxen white carbon black (Nanping) Co.,Ltd. Address before: 353000 Jia Lian building, 136 Xinjian Road, Fujian, Nanping Patentee before: DEGUSSA WELLINK SILICA (NANPING) CO.,LTD. |
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TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20180613 Address after: 353000 Jia Lian building, 136 Xinjian Road, Fujian, Nanping Patentee after: Fujian Nanping Sanyuan Circulation Technology Co.,Ltd. Address before: 353000 Jia Lian building, 136 Xinjian Road, Fujian, Nanping Patentee before: Win jiaxen white carbon black (Nanping) Co.,Ltd. |