CN1671774A - 在粉末涂料组合物中制备和使用新型复合颗粒的多种方法 - Google Patents
在粉末涂料组合物中制备和使用新型复合颗粒的多种方法 Download PDFInfo
- Publication number
- CN1671774A CN1671774A CNA038179628A CN03817962A CN1671774A CN 1671774 A CN1671774 A CN 1671774A CN A038179628 A CNA038179628 A CN A038179628A CN 03817962 A CN03817962 A CN 03817962A CN 1671774 A CN1671774 A CN 1671774A
- Authority
- CN
- China
- Prior art keywords
- particle
- mixture
- powder
- composition
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000843 powder Substances 0.000 title claims abstract description 180
- 238000000034 method Methods 0.000 title claims abstract description 141
- 239000011246 composite particle Substances 0.000 title claims abstract description 50
- 239000008199 coating composition Substances 0.000 title abstract description 5
- 230000008569 process Effects 0.000 title description 48
- 239000002245 particle Substances 0.000 claims abstract description 308
- 238000010438 heat treatment Methods 0.000 claims abstract description 56
- 239000000203 mixture Substances 0.000 claims description 237
- 238000000576 coating method Methods 0.000 claims description 90
- 239000011248 coating agent Substances 0.000 claims description 86
- 239000000463 material Substances 0.000 claims description 86
- 230000000694 effects Effects 0.000 claims description 71
- 229920005989 resin Polymers 0.000 claims description 60
- 239000011347 resin Substances 0.000 claims description 60
- 238000002156 mixing Methods 0.000 claims description 46
- 239000003973 paint Substances 0.000 claims description 46
- 238000005243 fluidization Methods 0.000 claims description 28
- 239000011159 matrix material Substances 0.000 claims description 20
- 230000009477 glass transition Effects 0.000 claims description 7
- 239000000758 substrate Substances 0.000 claims description 7
- 239000013078 crystal Substances 0.000 claims description 3
- 239000011238 particulate composite Substances 0.000 claims 1
- 239000002131 composite material Substances 0.000 abstract description 8
- 239000004615 ingredient Substances 0.000 abstract description 6
- 238000013459 approach Methods 0.000 abstract description 4
- 239000003814 drug Substances 0.000 abstract description 2
- 235000013305 food Nutrition 0.000 abstract description 2
- 239000002537 cosmetic Substances 0.000 abstract 1
- 229940079593 drug Drugs 0.000 abstract 1
- 239000000523 sample Substances 0.000 description 83
- 238000002360 preparation method Methods 0.000 description 49
- 239000000126 substance Substances 0.000 description 46
- 230000004927 fusion Effects 0.000 description 39
- 239000003795 chemical substances by application Substances 0.000 description 34
- 238000012545 processing Methods 0.000 description 29
- 239000010419 fine particle Substances 0.000 description 27
- 230000009471 action Effects 0.000 description 25
- 238000009826 distribution Methods 0.000 description 25
- 238000005516 engineering process Methods 0.000 description 23
- 238000001723 curing Methods 0.000 description 21
- 238000005275 alloying Methods 0.000 description 19
- 238000012360 testing method Methods 0.000 description 18
- 238000000227 grinding Methods 0.000 description 17
- 239000002994 raw material Substances 0.000 description 16
- 239000007789 gas Substances 0.000 description 15
- 239000008187 granular material Substances 0.000 description 15
- 230000008901 benefit Effects 0.000 description 14
- 239000002178 crystalline material Substances 0.000 description 13
- 239000000654 additive Substances 0.000 description 12
- 238000007600 charging Methods 0.000 description 12
- 238000003860 storage Methods 0.000 description 12
- 239000012159 carrier gas Substances 0.000 description 11
- 230000008859 change Effects 0.000 description 11
- 238000002425 crystallisation Methods 0.000 description 11
- 230000008025 crystallization Effects 0.000 description 11
- 238000002474 experimental method Methods 0.000 description 11
- 238000007906 compression Methods 0.000 description 10
- 230000006835 compression Effects 0.000 description 10
- 238000009792 diffusion process Methods 0.000 description 10
- 230000003068 static effect Effects 0.000 description 10
- 230000007704 transition Effects 0.000 description 10
- 230000000996 additive effect Effects 0.000 description 9
- 238000001125 extrusion Methods 0.000 description 9
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 8
- 229920006038 crystalline resin Polymers 0.000 description 8
- 239000000835 fiber Substances 0.000 description 8
- 230000006870 function Effects 0.000 description 8
- -1 glued board Substances 0.000 description 8
- 239000003112 inhibitor Substances 0.000 description 8
- 238000002844 melting Methods 0.000 description 8
- 230000008018 melting Effects 0.000 description 8
- 230000003647 oxidation Effects 0.000 description 8
- 238000007254 oxidation reaction Methods 0.000 description 8
- 239000000049 pigment Substances 0.000 description 8
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 7
- 230000008014 freezing Effects 0.000 description 7
- 238000007710 freezing Methods 0.000 description 7
- 238000007499 fusion processing Methods 0.000 description 7
- 239000007787 solid Substances 0.000 description 7
- 239000004593 Epoxy Substances 0.000 description 6
- 239000003054 catalyst Substances 0.000 description 6
- 238000001816 cooling Methods 0.000 description 6
- 238000013461 design Methods 0.000 description 6
- 238000009472 formulation Methods 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 239000000155 melt Substances 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- 239000011812 mixed powder Substances 0.000 description 6
- 239000002904 solvent Substances 0.000 description 6
- 230000000007 visual effect Effects 0.000 description 6
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 5
- 238000004220 aggregation Methods 0.000 description 5
- 230000002776 aggregation Effects 0.000 description 5
- 150000001875 compounds Chemical group 0.000 description 5
- 238000007796 conventional method Methods 0.000 description 5
- 238000001035 drying Methods 0.000 description 5
- 239000012530 fluid Substances 0.000 description 5
- 238000012856 packing Methods 0.000 description 5
- 230000009467 reduction Effects 0.000 description 5
- 238000011160 research Methods 0.000 description 5
- 238000005507 spraying Methods 0.000 description 5
- OUPZKGBUJRBPGC-UHFFFAOYSA-N 1,3,5-tris(oxiran-2-ylmethyl)-1,3,5-triazinane-2,4,6-trione Chemical compound O=C1N(CC2OC2)C(=O)N(CC2OC2)C(=O)N1CC1CO1 OUPZKGBUJRBPGC-UHFFFAOYSA-N 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 230000003197 catalytic effect Effects 0.000 description 4
- 239000000945 filler Substances 0.000 description 4
- 239000003999 initiator Substances 0.000 description 4
- 238000013035 low temperature curing Methods 0.000 description 4
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 4
- 229920000728 polyester Polymers 0.000 description 4
- 229920000570 polyether Polymers 0.000 description 4
- 230000005855 radiation Effects 0.000 description 4
- 241000894007 species Species 0.000 description 4
- 229920001187 thermosetting polymer Polymers 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 229920013685 Estron Polymers 0.000 description 3
- DNXHEGUUPJUMQT-CBZIJGRNSA-N Estrone Chemical compound OC1=CC=C2[C@H]3CC[C@](C)(C(CC4)=O)[C@@H]4[C@@H]3CCC2=C1 DNXHEGUUPJUMQT-CBZIJGRNSA-N 0.000 description 3
- 239000004721 Polyphenylene oxide Substances 0.000 description 3
- 229910052782 aluminium Inorganic materials 0.000 description 3
- 238000004458 analytical method Methods 0.000 description 3
- 239000003153 chemical reaction reagent Substances 0.000 description 3
- 230000001427 coherent effect Effects 0.000 description 3
- 239000003086 colorant Substances 0.000 description 3
- 229960003399 estrone Drugs 0.000 description 3
- 230000002349 favourable effect Effects 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 230000006872 improvement Effects 0.000 description 3
- 239000012528 membrane Substances 0.000 description 3
- 239000012768 molten material Substances 0.000 description 3
- 239000000123 paper Substances 0.000 description 3
- 238000011056 performance test Methods 0.000 description 3
- 230000000704 physical effect Effects 0.000 description 3
- 238000010944 pre-mature reactiony Methods 0.000 description 3
- 238000010298 pulverizing process Methods 0.000 description 3
- 238000012216 screening Methods 0.000 description 3
- 230000035945 sensitivity Effects 0.000 description 3
- 239000007921 spray Substances 0.000 description 3
- 238000007669 thermal treatment Methods 0.000 description 3
- 239000004408 titanium dioxide Substances 0.000 description 3
- GJKGAPPUXSSCFI-UHFFFAOYSA-N 2-Hydroxy-4'-(2-hydroxyethoxy)-2-methylpropiophenone Chemical compound CC(C)(O)C(=O)C1=CC=C(OCCO)C=C1 GJKGAPPUXSSCFI-UHFFFAOYSA-N 0.000 description 2
- AIBRSVLEQRWAEG-UHFFFAOYSA-N 3,9-bis(2,4-ditert-butylphenoxy)-2,4,8,10-tetraoxa-3,9-diphosphaspiro[5.5]undecane Chemical compound CC(C)(C)C1=CC(C(C)(C)C)=CC=C1OP1OCC2(COP(OC=3C(=CC(=CC=3)C(C)(C)C)C(C)(C)C)OC2)CO1 AIBRSVLEQRWAEG-UHFFFAOYSA-N 0.000 description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 2
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 description 2
- 240000007651 Rubus glaucus Species 0.000 description 2
- 235000011034 Rubus glaucus Nutrition 0.000 description 2
- 235000009122 Rubus idaeus Nutrition 0.000 description 2
- 208000034189 Sclerosis Diseases 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 2
- 239000004902 Softening Agent Substances 0.000 description 2
- BGYHLZZASRKEJE-UHFFFAOYSA-N [3-[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxy]-2,2-bis[3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoyloxymethyl]propyl] 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CC(C)(C)C1=C(O)C(C(C)(C)C)=CC(CCC(=O)OCC(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)(COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)COC(=O)CCC=2C=C(C(O)=C(C=2)C(C)(C)C)C(C)(C)C)=C1 BGYHLZZASRKEJE-UHFFFAOYSA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000004411 aluminium Substances 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 2
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 239000003899 bactericide agent Substances 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 2
- 239000011093 chipboard Substances 0.000 description 2
- 229920006026 co-polymeric resin Polymers 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 239000013068 control sample Substances 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- TVIDDXQYHWJXFK-UHFFFAOYSA-N dodecanedioic acid Chemical compound OC(=O)CCCCCCCCCCC(O)=O TVIDDXQYHWJXFK-UHFFFAOYSA-N 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 229910021485 fumed silica Inorganic materials 0.000 description 2
- ANSXAPJVJOKRDJ-UHFFFAOYSA-N furo[3,4-f][2]benzofuran-1,3,5,7-tetrone Chemical compound C1=C2C(=O)OC(=O)C2=CC2=C1C(=O)OC2=O ANSXAPJVJOKRDJ-UHFFFAOYSA-N 0.000 description 2
- 238000009998 heat setting Methods 0.000 description 2
- 230000003116 impacting effect Effects 0.000 description 2
- 230000001771 impaired effect Effects 0.000 description 2
- 239000010954 inorganic particle Substances 0.000 description 2
- 238000012423 maintenance Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000320 mechanical mixture Substances 0.000 description 2
- 239000007769 metal material Substances 0.000 description 2
- 239000003607 modifier Substances 0.000 description 2
- 229940031815 mycocide Drugs 0.000 description 2
- 229910052757 nitrogen Inorganic materials 0.000 description 2
- BKIMMITUMNQMOS-UHFFFAOYSA-N nonane Chemical compound CCCCCCCCC BKIMMITUMNQMOS-UHFFFAOYSA-N 0.000 description 2
- 239000004482 other powder Substances 0.000 description 2
- 239000013618 particulate matter Substances 0.000 description 2
- 230000002085 persistent effect Effects 0.000 description 2
- WLJVNTCWHIRURA-UHFFFAOYSA-N pimelic acid Chemical compound OC(=O)CCCCCC(O)=O WLJVNTCWHIRURA-UHFFFAOYSA-N 0.000 description 2
- 239000004033 plastic Substances 0.000 description 2
- 229920003023 plastic Polymers 0.000 description 2
- 238000004321 preservation Methods 0.000 description 2
- 230000009257 reactivity Effects 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 239000012925 reference material Substances 0.000 description 2
- 239000013074 reference sample Substances 0.000 description 2
- 230000008929 regeneration Effects 0.000 description 2
- 238000011069 regeneration method Methods 0.000 description 2
- 238000012827 research and development Methods 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 description 2
- 238000010008 shearing Methods 0.000 description 2
- 239000011343 solid material Substances 0.000 description 2
- 238000007711 solidification Methods 0.000 description 2
- 230000008023 solidification Effects 0.000 description 2
- 238000003786 synthesis reaction Methods 0.000 description 2
- 239000012745 toughening agent Substances 0.000 description 2
- 238000012546 transfer Methods 0.000 description 2
- 239000004034 viscosity adjusting agent Substances 0.000 description 2
- DSSYKIVIOFKYAU-XCBNKYQSSA-N (R)-camphor Chemical compound C1C[C@@]2(C)C(=O)C[C@@H]1C2(C)C DSSYKIVIOFKYAU-XCBNKYQSSA-N 0.000 description 1
- MNAHQWDCXOHBHK-UHFFFAOYSA-N 1-phenylpropane-1,1-diol Chemical compound CCC(O)(O)C1=CC=CC=C1 MNAHQWDCXOHBHK-UHFFFAOYSA-N 0.000 description 1
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- ZSSVCEUEVMALRD-UHFFFAOYSA-N 2-[4,6-bis(2,4-dimethylphenyl)-1,3,5-triazin-2-yl]-5-(octyloxy)phenol Chemical compound OC1=CC(OCCCCCCCC)=CC=C1C1=NC(C=2C(=CC(C)=CC=2)C)=NC(C=2C(=CC(C)=CC=2)C)=N1 ZSSVCEUEVMALRD-UHFFFAOYSA-N 0.000 description 1
- SWZOQAGVRGQLDV-UHFFFAOYSA-N 4-[2-(4-hydroxy-2,2,6,6-tetramethylpiperidin-1-yl)ethoxy]-4-oxobutanoic acid Chemical compound CC1(C)CC(O)CC(C)(C)N1CCOC(=O)CCC(O)=O SWZOQAGVRGQLDV-UHFFFAOYSA-N 0.000 description 1
- VQVIHDPBMFABCQ-UHFFFAOYSA-N 5-(1,3-dioxo-2-benzofuran-5-carbonyl)-2-benzofuran-1,3-dione Chemical compound C1=C2C(=O)OC(=O)C2=CC(C(C=2C=C3C(=O)OC(=O)C3=CC=2)=O)=C1 VQVIHDPBMFABCQ-UHFFFAOYSA-N 0.000 description 1
- 229920000178 Acrylic resin Polymers 0.000 description 1
- 239000004925 Acrylic resin Substances 0.000 description 1
- 238000012935 Averaging Methods 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- 241000723346 Cinnamomum camphora Species 0.000 description 1
- 206010010774 Constipation Diseases 0.000 description 1
- MQJKPEGWNLWLTK-UHFFFAOYSA-N Dapsone Chemical compound C1=CC(N)=CC=C1S(=O)(=O)C1=CC=C(N)C=C1 MQJKPEGWNLWLTK-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- JIGUQPWFLRLWPJ-UHFFFAOYSA-N Ethyl acrylate Chemical compound CCOC(=O)C=C JIGUQPWFLRLWPJ-UHFFFAOYSA-N 0.000 description 1
- OWYWGLHRNBIFJP-UHFFFAOYSA-N Ipazine Chemical compound CCN(CC)C1=NC(Cl)=NC(NC(C)C)=N1 OWYWGLHRNBIFJP-UHFFFAOYSA-N 0.000 description 1
- 229920005692 JONCRYL® Polymers 0.000 description 1
- 235000019738 Limestone Nutrition 0.000 description 1
- 240000007930 Oxalis acetosella Species 0.000 description 1
- 235000008098 Oxalis acetosella Nutrition 0.000 description 1
- 244000203593 Piper nigrum Species 0.000 description 1
- 239000004642 Polyimide Substances 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- 229920002396 Polyurea Polymers 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 238000005411 Van der Waals force Methods 0.000 description 1
- CVPZXHCZKMFVOZ-UHFFFAOYSA-N [4-(benzoyloxymethyl)cyclohexyl]methyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC(CC1)CCC1COC(=O)C1=CC=CC=C1 CVPZXHCZKMFVOZ-UHFFFAOYSA-N 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000004931 aggregating effect Effects 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 150000008064 anhydrides Chemical class 0.000 description 1
- 229910052786 argon Inorganic materials 0.000 description 1
- HBPTUDIZKSGJNN-UHFFFAOYSA-N benzoic acid;cyclohexane;methanol Chemical compound OC.OC.C1CCCCC1.OC(=O)C1=CC=CC=C1.OC(=O)C1=CC=CC=C1 HBPTUDIZKSGJNN-UHFFFAOYSA-N 0.000 description 1
- FLPKSBDJMLUTEX-UHFFFAOYSA-N bis(1,2,2,6,6-pentamethylpiperidin-4-yl) 2-butyl-2-[(3,5-ditert-butyl-4-hydroxyphenyl)methyl]propanedioate Chemical compound C1C(C)(C)N(C)C(C)(C)CC1OC(=O)C(C(=O)OC1CC(C)(C)N(C)C(C)(C)C1)(CCCC)CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 FLPKSBDJMLUTEX-UHFFFAOYSA-N 0.000 description 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical compound O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 description 1
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 description 1
- 229960000846 camphor Drugs 0.000 description 1
- 229930008380 camphor Natural products 0.000 description 1
- 235000011089 carbon dioxide Nutrition 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000004581 coalescence Methods 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 239000004567 concrete Substances 0.000 description 1
- 229920001577 copolymer Polymers 0.000 description 1
- 238000012937 correction Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000012217 deletion Methods 0.000 description 1
- 230000037430 deletion Effects 0.000 description 1
- 238000001514 detection method Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000018109 developmental process Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000001938 differential scanning calorimetry curve Methods 0.000 description 1
- 238000002050 diffraction method Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000007590 electrostatic spraying Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 239000007888 film coating Substances 0.000 description 1
- 238000009501 film coating Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229920002313 fluoropolymer Polymers 0.000 description 1
- 239000012634 fragment Substances 0.000 description 1
- 230000008570 general process Effects 0.000 description 1
- VOZRXNHHFUQHIL-UHFFFAOYSA-N glycidyl methacrylate Chemical compound CC(=C)C(=O)OCC1CO1 VOZRXNHHFUQHIL-UHFFFAOYSA-N 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 238000010237 hybrid technique Methods 0.000 description 1
- 238000007373 indentation Methods 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000012784 inorganic fiber Substances 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- WTFXARWRTYJXII-UHFFFAOYSA-N iron(2+);iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[O-2].[Fe+2].[Fe+3].[Fe+3] WTFXARWRTYJXII-UHFFFAOYSA-N 0.000 description 1
- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Natural products OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 description 1
- 238000002372 labelling Methods 0.000 description 1
- 238000002356 laser light scattering Methods 0.000 description 1
- 230000002045 lasting effect Effects 0.000 description 1
- 239000006028 limestone Substances 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000010445 mica Substances 0.000 description 1
- 229910052618 mica group Inorganic materials 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- OKRNLSUTBJUVKA-UHFFFAOYSA-N n,n,n',n'-Tetrakis(2-hydroxyethyl)adipamide Chemical compound OCCN(CCO)C(=O)CCCCC(=O)N(CCO)CCO OKRNLSUTBJUVKA-UHFFFAOYSA-N 0.000 description 1
- 239000011824 nuclear material Substances 0.000 description 1
- SSDSCDGVMJFTEQ-UHFFFAOYSA-N octadecyl 3-(3,5-ditert-butyl-4-hydroxyphenyl)propanoate Chemical compound CCCCCCCCCCCCCCCCCCOC(=O)CCC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 SSDSCDGVMJFTEQ-UHFFFAOYSA-N 0.000 description 1
- 238000011017 operating method Methods 0.000 description 1
- 239000011368 organic material Substances 0.000 description 1
- 230000001151 other effect Effects 0.000 description 1
- 150000002924 oxiranes Chemical class 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 238000007415 particle size distribution analysis Methods 0.000 description 1
- 239000011236 particulate material Substances 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 229940059574 pentaerithrityl Drugs 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- PNJWIWWMYCMZRO-UHFFFAOYSA-N pent‐4‐en‐2‐one Natural products CC(=O)CC=C PNJWIWWMYCMZRO-UHFFFAOYSA-N 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 229920002492 poly(sulfone) Polymers 0.000 description 1
- 229920001721 polyimide Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 229920001296 polysiloxane Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 238000009700 powder processing Methods 0.000 description 1
- 230000002028 premature Effects 0.000 description 1
- 230000000750 progressive effect Effects 0.000 description 1
- 239000001327 prunus amygdalus amara l. extract Substances 0.000 description 1
- 238000011158 quantitative evaluation Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- 230000011218 segmentation Effects 0.000 description 1
- 238000005204 segregation Methods 0.000 description 1
- 238000001338 self-assembly Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000007619 statistical method Methods 0.000 description 1
- SYDJVRWZOWPNNO-UHFFFAOYSA-N sucrose-benzoate Natural products OCC1OC(OC2(COC(=O)c3ccccc3)OC(CO)C(O)C2O)C(O)C(O)C1O SYDJVRWZOWPNNO-UHFFFAOYSA-N 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 239000008399 tap water Substances 0.000 description 1
- 235000020679 tap water Nutrition 0.000 description 1
- 230000002277 temperature effect Effects 0.000 description 1
- BFKJFAAPBSQJPD-UHFFFAOYSA-N tetrafluoroethene Chemical group FC(F)=C(F)F BFKJFAAPBSQJPD-UHFFFAOYSA-N 0.000 description 1
- 229920001169 thermoplastic Polymers 0.000 description 1
- 239000004416 thermosoftening plastic Substances 0.000 description 1
- WCLDITPGPXSPGV-UHFFFAOYSA-N tricamba Chemical compound COC1=C(Cl)C=C(Cl)C(Cl)=C1C(O)=O WCLDITPGPXSPGV-UHFFFAOYSA-N 0.000 description 1
- 229920006337 unsaturated polyester resin Polymers 0.000 description 1
- 238000012800 visualization Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
- 239000010456 wollastonite Substances 0.000 description 1
- 229910052882 wollastonite Inorganic materials 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/03—Powdery paints
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B9/00—Making granules
- B29B9/12—Making granules characterised by structure or composition
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B9/00—Making granules
- B29B9/16—Auxiliary treatment of granules
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J3/00—Processes of treating or compounding macromolecular substances
- C08J3/20—Compounding polymers with additives, e.g. colouring
- C08J3/203—Solid polymers with solid and/or liquid additives
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B9/00—Making granules
- B29B9/12—Making granules characterised by structure or composition
- B29B2009/125—Micropellets, microgranules, microparticles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B9/00—Making granules
- B29B9/16—Auxiliary treatment of granules
- B29B2009/163—Coating, i.e. applying a layer of liquid or solid material on the granule
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B9/00—Making granules
- B29B9/16—Auxiliary treatment of granules
- B29B2009/166—Deforming granules to give a special form, e.g. spheroidizing, rounding
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Paints Or Removers (AREA)
Abstract
Description
样品ID | 7634-19A(℃) | 6401-61E(℃) | 7480-22A(℃) |
0次通过 | 54.8 | 46.6 | 45.7 |
1次通过 | 53.5 | 45.8 | 46.2 |
2次通过 | 54.9 | 46.9 | 46.7 |
3次通过 | 54.7 | 47.4 | 未测定 |
粒度分布(按体积) | 平均粒度(按数量) | ||||
通过次数 | d10 | d50 | d90 | 平均 | |
0 | 9.5μm | 30.0μm | 56.2μm | 32.2μm | 0.11μm |
1 | 15.7μm | 34.1μm | 56.1μm | 35.1μm | 8.41μm |
原料 | 基础树脂配方(wt.%) | 基础树脂配方(wt.%) | 对照样品 |
7634-15B | 7634-15E | 7634-15J | |
Uracross P3125(UCB的不饱和聚酯树脂) | 61.03 | 58.45 | 52.25 |
Uracross P3307(UCB的结晶性聚醚树脂) | 0.00 | 4.23 | 11.11 |
Irgacure 819(Ciba-Geigy的光引发剂) | 0.74 | 0.70 | 0.65 |
Irgacure 2959(Ciba-Geigy的光引发剂) | 0.37 | 0.35 | 0.33 |
Resiflow P-67(聚结剂) | 1.10 | 1.06 | 0.98 |
Nyad 325硅灰石(填料) | 18.38 | 17.61 | 16.34 |
Tiona RCL-2二氧化钛(颜料) | 18.38 | 17.61 | 16.34 |
样品ID | 7634-15B | 7634-15E | ||||
研磨尺寸 | 研磨尺寸 | |||||
细小 | 中等 | 粗糙 | 细小 | 中等 | 粗糙 | |
d10(μm) | 9.75 | 12.37 | 13.16 | 10.30 | 12.77 | 14.30 |
D50(μm) | 25.04 | 33.20 | 43.85 | 26.35 | 36.38 | 46.93 |
D90(μm) | 67.97 | 75.14 | 117.64 | 74.79 | 88.48 | 121.17 |
7634-15B/12.5phr Uracross3307 | 60°光泽 |
通过0次 | 66.9±2.8 |
通过1次 | 73.1±0.3 |
通过2次 | 70.5±1.0 |
B | Tg(℃) |
通过0次 | 41.9 |
通过1次 | 39.7 |
通过3次 | 36.8 |
通过5次 | 35.2 |
原料 | 重量份 |
EPO-THOTO KD-6812(GCA Chemical Corp.的双酚A环氧化合物) | 44.78 |
GMA-301(Estron Chemical的甲基丙烯酸缩水甘油酯功能性丙烯酸聚合物) | 27.79 |
Resiflow P67(Estron Chemical的聚结剂) | 1.09 |
Uraflow B(GAC Chemical Corp.的熔体流动改进剂) | 0.36 |
Dyhard PI(Degussa Corp.的胺催化剂) | 1.45 |
Ultranox 626(Ashland Chemical Co.的抗氧剂) | 1.45 |
Cyasorb UV-1164(Cytec Industries Inc.的UV稳定剂) | 0.73 |
Kronos 2310(Kronos Titan GMBH &Co.的二氧化钛) | 21.77 |
Black Iron Oxide BK-4799(颜料) | 0.07 |
Honey Yellow #29(颜料) | 0.29 |
Kroma Red Iron Oxide RO-3097(颜料) | 0.02 |
样品ID | 60°光泽度 |
对比(挤出的-参考) | 44.4±1.1 |
6-0(V混合-混合) | 50.9±1.2 |
6-1(通过急速熔合1次) | 47.0±1.1 |
6-2(通过急速熔合2次) | 45.5±2.3 |
15-0(V混合-混合) | 36.3±1.2 |
15-1(通过急速熔合1次) | 36.6±0.7 |
15-2(通过急速熔合2次) | 36.8±3.5 |
样品ID | %压缩率 |
对比(挤出的-参考) | 31.3 |
6-0(V混合-混合) | 44.8 |
6-1(通过急速熔合1次) | 31.9 |
6-2(通过急速熔合2次) | 26.1 |
15-0(V混合-混合) | 37.8 |
15-1(通过急速熔合1次) | 27.7 |
15-2(通过急速熔合2次) | 21.7 |
原料 | 重量份 |
Crylcoat 490(UCB Chemicals Corp.的羧酸官能化聚酯) | 67.51 |
Araldite PT-810(Ciba Geigy Corp.的异氰脲酸三缩水甘油酯树脂) | 7.50 |
A-C 540 Pellets(Allied Signal Corp.的乙烯和丙烯酸单体的共聚物树脂) | 0.98 |
Resiflow P67(Estron Chemical的聚结剂) | 1.13 |
Powdertex 61(Shamrock Technologies Inc.的聚四氟乙烯和滑石的混合物) | 0.19 |
Tiona RCL-2(Millennium Inorganic Chemicals的二氧化钛) | 22.50 |
峰值放热温度(℃) | |||
通过急速熔合步骤的次数 | A1(每百份树脂2份催化剂) | A2(每百份树脂3份催化剂) | A1(每百份树脂4份催化剂) |
0次 | 159.4 | 150.4 | 148.4 |
2次 | 160.7 | 158.1 | 153.7 |
玻璃化转变温度(℃) | |||
0次 | 51.6 | 53.3 | 52.4 |
2次 | 52.2 | 53.8 | 52.7 |
峰值放热温度(℃) | |||
通过次数 | (700°F) | (800°F) | (900°F) |
0次 | 159.1 | 160.4 | 159.7 |
2次 | 159.4 | 164.4 | 166.7 |
玻璃化转变温度(℃) | |||
0次 | 51.6 | 51.3 | 51.8 |
2次 | 52.3 | 49.9 | 52.5 |
原料 | 重量份 |
Crylcoat 440(UCB Chemicals Corp.的羧酸官能聚酯) | 92.17 |
Araldite PT-810(Ciba-Geigy Corp.的异氰脲酸三缩水甘油酯树脂) | 5.11 |
Modaflow 2000(Solutia的丙烯酸乙酯和丙烯酸2-乙基己酯单体的共聚物树脂) | 1.46 |
Uraflow B(GAC Chemical Corp.的熔体流动改性剂) | 0.34 |
Accelerator DT 3162-2(Vantico Inc.的固化催化剂) | 0.24 |
Ultranox 626(Ashland Chemical Co.的抗氧剂) | 0.19 |
Irganox 1010(Ciba-Geigy的抗氧剂) | 0.49 |
原料 | 每100份主颗粒物料的添加量 |
PCF 200AG(Toyal的铝片) | 4.39 |
PCR-214F(Eckart America的铝片) | 3.08 |
样品ID | 涂覆电压(KV) | 平均膜厚度(mils) | 视觉外观 |
干混 | 30 | 1.1 | 干燥喷涂 |
通过1次 | 30 | 1.5 | 干燥喷涂 |
干混 | 40 | 0.9 | 轻微的干燥喷涂,掩饰效果差 |
通过1次 | 40 | 3.3 | 比对照物厚,掩饰效果好 |
干混 | 60 | 1.9 | 掩饰效果差 |
通过1次 | 60 | 3.8 | 比对照物厚,掩饰效果好 |
干混 | 80 | 1.5 | 掩饰效果差 |
通过1次 | 80 | 4.0 | 比对照物厚,掩饰效果好 |
Claims (15)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US10/206,482 | 2002-07-26 | ||
US10/206,482 US7105201B2 (en) | 2002-07-26 | 2002-07-26 | Versatile processes for preparing and using novel composite particles in powder coating compositions |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1671774A true CN1671774A (zh) | 2005-09-21 |
CN100509925C CN100509925C (zh) | 2009-07-08 |
Family
ID=30770298
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB038179628A Expired - Fee Related CN100509925C (zh) | 2002-07-26 | 2003-07-24 | 在粉末涂料组合物中制备和使用新型复合颗粒的多种方法 |
Country Status (7)
Country | Link |
---|---|
US (2) | US7105201B2 (zh) |
EP (2) | EP2267063B8 (zh) |
CN (1) | CN100509925C (zh) |
AU (1) | AU2003256734A1 (zh) |
CA (1) | CA2489543A1 (zh) |
MX (1) | MXPA05000869A (zh) |
WO (1) | WO2004011531A1 (zh) |
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101454074B (zh) * | 2006-03-29 | 2011-11-16 | 比克化学股份有限公司 | 由粉末团聚体制造纳米粒,特别是纳米粒复合材料 |
CN108473809A (zh) * | 2016-01-04 | 2018-08-31 | 旭硝子株式会社 | 粉体涂料、粉体涂料的制造方法、及涂装物品 |
CN109046079A (zh) * | 2018-10-09 | 2018-12-21 | 廊坊艾格玛新立材料科技有限公司 | 一种新型的粉末涂料邦定设备及其邦定工艺 |
CN114667327A (zh) * | 2019-11-14 | 2022-06-24 | Swimc有限公司 | 金属封装粉末涂料组合物、涂覆的金属基材和方法 |
CN116234880A (zh) * | 2020-09-24 | 2023-06-06 | Ppg工业俄亥俄公司 | 效应颜料的声学粘结 |
Families Citing this family (27)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US7105201B2 (en) * | 2002-07-26 | 2006-09-12 | H.B. Fuller Licensing & Financing, Inc. | Versatile processes for preparing and using novel composite particles in powder coating compositions |
DE10306887A1 (de) * | 2003-02-18 | 2004-08-26 | Daimlerchrysler Ag | Verfahren zur Beschichtung von Partikeln für generative rapid prototyping Prozesse |
DE10319507A1 (de) * | 2003-04-30 | 2004-11-25 | Sto Ag | Verfahren zur Herstellung eines Reaktionsharzgemisches |
EP1477534A3 (en) * | 2003-05-16 | 2005-01-19 | Rohm And Haas Company | Multiple-part fast cure powder coatings |
US7867555B2 (en) | 2004-02-13 | 2011-01-11 | Valspar Sourcing Inc. | Dispersion-coated powder coloring system |
US20060084707A1 (en) * | 2004-10-15 | 2006-04-20 | Aspen Aerogels, Inc. | Methods for manufacture of aerogels |
US7468401B2 (en) * | 2005-02-18 | 2008-12-23 | Ppg Industries Ohio, Inc. | Bonding of powder coating compositions |
US20060274990A1 (en) * | 2005-06-06 | 2006-12-07 | Gergely John S | Glass microspheres having optimized resonant light scattering properties |
GB0514698D0 (en) * | 2005-07-18 | 2005-08-24 | Danisco | Process |
WO2007050417A2 (en) | 2005-10-21 | 2007-05-03 | Valspar Sourcing, Inc. | Novel powder coloring system |
US20090098396A1 (en) * | 2007-10-10 | 2009-04-16 | Ppg Industries Ohio, Inc. | Powder coating compositions, methods for their preparation and related coated substrates |
US20090252988A1 (en) * | 2008-04-04 | 2009-10-08 | Honeywell International Inc. | Coated components for use in high temperature environments and methods of forming a coating on the component |
ES2332079B1 (es) | 2008-07-22 | 2010-10-27 | Consejo Superior De Investigaciones Cientificas (Csic) | Procedimiento para la dispersion de nanoparticulas en seco y la obtencion de estructuras jerarquicas y recubrimientos. |
CN101914266B (zh) * | 2010-07-30 | 2012-03-07 | 温州市龙电绝缘材料有限公司 | 一种用于电机集电环的绝缘材料 |
DE102013009148B4 (de) * | 2013-05-31 | 2016-02-11 | Fl Services Gmbh | Mischung zur Herstellung einer Schicht in einem Schichtaufbau, Verfahren zum Herstellen eines Schichtaufbaus, Schichtaufbau und Verwendung des Schichtaufbaus |
GB201316450D0 (en) * | 2013-08-26 | 2013-10-30 | Tate & Lyle Ingredients | Method of preparing edible composition |
US9718997B2 (en) | 2013-11-13 | 2017-08-01 | R.R. Donnelley & Sons Company | Battery |
EP3197942A4 (en) * | 2014-09-22 | 2018-03-28 | Valspar Sourcing, Inc. | Microwave bonding for coating compositions |
GB2536302B (en) * | 2015-02-25 | 2017-04-12 | Tate & Lyle Ingredients Americas Llc | Free-flowing edible composition |
PL3293232T3 (pl) | 2016-09-08 | 2021-01-25 | Igp Pulvertechnik Ag | Farba proszkowa i sposób wytwarzania farby proszkowej |
NL2019197B1 (en) * | 2017-07-07 | 2019-01-16 | Stahl Int B V | Powder coating method and coated article |
CA3072305A1 (en) * | 2017-09-12 | 2019-03-21 | Dressler Group GmbH & Co. KG | Method and device for thermal rounding or spheronization of pulverulent plastic particles |
CN107459926B (zh) * | 2017-09-20 | 2019-11-15 | 江南载福粉末涂料(张家港)有限公司 | 一种汽车排气管和消音器粉末涂料及其制备方法 |
WO2020118231A1 (en) * | 2018-12-06 | 2020-06-11 | Jabil Inc. | Apparatus, system and method of forming polymer microspheres for use in additive manufacturing |
WO2020132221A1 (en) * | 2018-12-19 | 2020-06-25 | Pison Stream Solutions Inc. | Pro gel cap style multifunctional composition |
EP3898854B1 (en) * | 2018-12-21 | 2024-04-10 | Eastman Kodak Company | Low specular reflectance surface and coating composition |
JP7186197B2 (ja) * | 2020-07-03 | 2022-12-08 | 日本ペイント・オートモーティブコーティングス株式会社 | 塗料組成物および塗料組成物の製造方法 |
Family Cites Families (33)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2976574A (en) | 1956-07-31 | 1961-03-28 | Union Carbide Corp | Chemical process and product |
US3263980A (en) | 1963-02-19 | 1966-08-02 | Wedco | Apparatus for treating thermoplastic material to improve flowability thereof |
US3548782A (en) | 1967-11-30 | 1970-12-22 | Hanningsen Foods Inc | Means for forming a continuous coating on particles |
US3632369A (en) * | 1969-12-11 | 1972-01-04 | Coaden Oil & Chemical Co | Polymer pigmentation |
GB1434085A (en) * | 1972-08-28 | 1976-04-28 | Cosden Technology | Pigmentation of polymer powders |
US4154871A (en) | 1975-09-12 | 1979-05-15 | Minnesota Mining And Manufacturing Company | Electrostatic coating method utilizing mixture of rough and spheroidized resin particles |
US4163031A (en) | 1977-10-25 | 1979-07-31 | Celanese Corporation | Powder composition and method of preparation |
US4243794A (en) | 1978-10-10 | 1981-01-06 | Minnesota Mining And Manufacturing Company | Mixture of rough and spheroidized resin particles |
US4720397A (en) * | 1985-12-12 | 1988-01-19 | General Technology Applications, Inc. | Rapid dissolving polymer compositions and uses therefor |
DE3546113A1 (de) * | 1985-12-24 | 1987-06-25 | Santrade Ltd | Verbundpulverteilchen, verbundkoerper und verfahren zu deren herstellung |
JPH07122035B2 (ja) | 1986-06-12 | 1995-12-25 | 日本ペイント株式会社 | 粉体塗料 |
US4788080A (en) * | 1987-04-27 | 1988-11-29 | Canadian Patents And Development Limited | Process and apparatus for coating particles with fine powder |
US5006368A (en) * | 1988-10-19 | 1991-04-09 | The Dow Chemical Company | Plastic particle coated with processing aid and method of coating |
US5470893A (en) | 1990-06-01 | 1995-11-28 | Courtaulds Coatings (Holdings) Limited | Powder coating compositions |
US5856378A (en) | 1988-12-02 | 1999-01-05 | Courtaulds Coatings (Holdings) Limited | Powder coating compositions |
GB9012315D0 (en) | 1990-06-01 | 1990-07-18 | Courtaulds Coatings Holdings | Powder coating compositions |
GB8828225D0 (en) | 1988-12-02 | 1989-01-05 | Int Paint Plc | Coating compositions |
JPH02155932A (ja) | 1988-12-07 | 1990-06-15 | Nippon Paint Co Ltd | 複合化粒子ならびにその製法 |
JPH0796660B2 (ja) | 1989-03-23 | 1995-10-18 | 日本ペイント株式会社 | 粉体塗料 |
JPH05345316A (ja) * | 1990-07-31 | 1993-12-27 | Shell Oil Co | 熱可塑性ポリマー中への添加剤配合方法 |
US5300539A (en) * | 1992-12-28 | 1994-04-05 | Shell Oil Company | Post-polymerization additive incorporation process |
US5585426A (en) | 1994-10-05 | 1996-12-17 | Nexus Corporation | Process for imparting an electrostatic charge to powders to render them useful for coating application |
US5684066A (en) | 1995-12-04 | 1997-11-04 | H.B. Fuller Licensing & Financing, Inc. | Protective coatings having enhanced properties |
AU4239997A (en) | 1996-08-30 | 1998-03-19 | Thomas F. Bernecki | Polymer coating by means of hot gases |
US5919530A (en) * | 1997-06-30 | 1999-07-06 | Basf Corporation | Process for producing customized thermoplastic resins |
US5962082A (en) | 1997-08-19 | 1999-10-05 | Aveka, Inc. | Process for applying liquid coatings to solid particulate substrates |
GB9814534D0 (en) * | 1998-07-03 | 1998-09-02 | Courtaulds Coatings Holdings | Powder coating compositions |
GB9905522D0 (en) * | 1999-03-10 | 1999-05-05 | Int Coatings Ltd | Powder coating compositions |
US6197369B1 (en) * | 1999-09-30 | 2001-03-06 | New Jersey Institute Of Technology | Method of particle coating |
GB0011284D0 (en) | 2000-05-11 | 2000-06-28 | Univ Belfast | Coating process |
US6224798B1 (en) * | 2000-07-31 | 2001-05-01 | Delphi Technologies, Inc. | Method for fabricating powdered metal cores |
DE10162348A1 (de) * | 2001-12-18 | 2003-07-10 | Basf Ag | Verfahren zur Aufbringung von Funktionsmaterialien auf thermoplastisches Polyurethan |
US7105201B2 (en) * | 2002-07-26 | 2006-09-12 | H.B. Fuller Licensing & Financing, Inc. | Versatile processes for preparing and using novel composite particles in powder coating compositions |
-
2002
- 2002-07-26 US US10/206,482 patent/US7105201B2/en not_active Expired - Lifetime
-
2003
- 2003-07-24 CN CNB038179628A patent/CN100509925C/zh not_active Expired - Fee Related
- 2003-07-24 WO PCT/US2003/023123 patent/WO2004011531A1/en not_active Application Discontinuation
- 2003-07-24 MX MXPA05000869A patent/MXPA05000869A/es active IP Right Grant
- 2003-07-24 EP EP10180342.7A patent/EP2267063B8/en not_active Expired - Lifetime
- 2003-07-24 EP EP03771779.0A patent/EP1525251B1/en not_active Expired - Lifetime
- 2003-07-24 CA CA002489543A patent/CA2489543A1/en not_active Abandoned
- 2003-07-24 AU AU2003256734A patent/AU2003256734A1/en not_active Abandoned
-
2006
- 2006-01-12 US US11/331,247 patent/US7622072B2/en not_active Expired - Lifetime
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101454074B (zh) * | 2006-03-29 | 2011-11-16 | 比克化学股份有限公司 | 由粉末团聚体制造纳米粒,特别是纳米粒复合材料 |
CN108473809A (zh) * | 2016-01-04 | 2018-08-31 | 旭硝子株式会社 | 粉体涂料、粉体涂料的制造方法、及涂装物品 |
CN108473809B (zh) * | 2016-01-04 | 2020-06-23 | Agc株式会社 | 粉体涂料、粉体涂料的制造方法、及涂装物品 |
CN109046079A (zh) * | 2018-10-09 | 2018-12-21 | 廊坊艾格玛新立材料科技有限公司 | 一种新型的粉末涂料邦定设备及其邦定工艺 |
CN114667327A (zh) * | 2019-11-14 | 2022-06-24 | Swimc有限公司 | 金属封装粉末涂料组合物、涂覆的金属基材和方法 |
US11834585B2 (en) | 2019-11-14 | 2023-12-05 | Swimc Llc | Metal packaging powder coating compositions, coated metal substrates, and methods |
CN116234880A (zh) * | 2020-09-24 | 2023-06-06 | Ppg工业俄亥俄公司 | 效应颜料的声学粘结 |
Also Published As
Publication number | Publication date |
---|---|
MXPA05000869A (es) | 2005-07-29 |
EP2267063A1 (en) | 2010-12-29 |
EP1525251A1 (en) | 2005-04-27 |
CA2489543A1 (en) | 2004-02-05 |
US20040018109A1 (en) | 2004-01-29 |
US7105201B2 (en) | 2006-09-12 |
CN100509925C (zh) | 2009-07-08 |
EP2267063B1 (en) | 2018-09-05 |
US7622072B2 (en) | 2009-11-24 |
AU2003256734A1 (en) | 2004-02-16 |
US20060120912A1 (en) | 2006-06-08 |
EP2267063B8 (en) | 2018-12-26 |
WO2004011531A1 (en) | 2004-02-05 |
EP1525251B1 (en) | 2018-04-25 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN1671774A (zh) | 在粉末涂料组合物中制备和使用新型复合颗粒的多种方法 | |
JP4405938B2 (ja) | 原料ミックス粉末組成物およびその製造法 | |
CN101258185B (zh) | 粉末涂料 | |
CN1942533A (zh) | 新型粉末着色*** | |
EP0539385B1 (en) | Powder coating compositions | |
CN1222581C (zh) | 粉末涂料组合物 | |
CN101048463A (zh) | 基于热塑性聚合物的颗粒的制备方法和由此得到的粉末 | |
CN1733851A (zh) | 含水油漆组合物及其用途 | |
CN101065454A (zh) | 复合粉体涂料、其制造方法及粉体涂料的调色方法 | |
CN1203619A (zh) | 热固性粉末涂料组合物 | |
CN101291997B (zh) | 新型粉末着色体系 | |
CN1330693A (zh) | 粉末涂料组合物 | |
CN1198457A (zh) | 粉末涂料 | |
CN1751105A (zh) | 抗静电涂覆的模塑件及其生产方法 | |
CN1018459B (zh) | 制备有机调色剂粉料的方法 | |
CN1671771A (zh) | 包括酯酰胺缩合产物的粉末涂料消光剂 | |
CN1055936A (zh) | 可分散于水介质中的固体添加剂、其制法及将其涂布到聚合物颗粒上的方法 | |
CN1820057A (zh) | 固体颜料制剂及其在有机溶剂中的分散体,其制备和用途 | |
CN1189519A (zh) | 改良粉末涂料组合物带电能力的方法 | |
CN1436819A (zh) | 半导体密封材料用黑色复合颗粒和半导体密封材料 | |
JPS6359431B2 (zh) | ||
CN1262612C (zh) | 粉末涂料组合物 | |
CN115667421A (zh) | 粉末涂料组合物及经此粉末涂料组合物涂覆的基材 | |
JP2000281978A (ja) | 粉体塗料の調色方法 | |
JP2006016432A (ja) | 熱硬化型粉体塗料の調色方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
ASS | Succession or assignment of patent right |
Owner name: VALSPAR RESOURCES Free format text: FORMER OWNER: FULLER H. B. CO. Effective date: 20070427 |
|
C41 | Transfer of patent application or patent right or utility model | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20070427 Address after: American Minnesota Applicant after: VALSPAR SOURCING, Inc. Address before: American Minnesota Applicant before: H.B. FULLER CO. |
|
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C56 | Change in the name or address of the patentee |
Owner name: VALSPAR BUYING COMPANY Free format text: FORMER NAME: VALSPAR RESOURCES COMPANY |
|
CP01 | Change in the name or title of a patent holder |
Address after: American Minnesota Patentee after: VALSPAR SOURCING, Inc. Address before: American Minnesota Patentee before: Valspar Sourcing, Inc. |
|
TR01 | Transfer of patent right |
Effective date of registration: 20190202 Address after: Ohio, USA Patentee after: Industrial solution Co. Address before: American Minnesota Patentee before: VALSPAR SOURCING, Inc. Effective date of registration: 20190202 Address after: Ohio, USA Patentee after: Valspar Corp. Address before: Ohio, USA Patentee before: Industrial solution Co. Effective date of registration: 20190202 Address after: Ohio, USA Patentee after: Xuanwei Investment Management Co.,Ltd. Address before: Ohio, USA Patentee before: Xuanwei Headquarters Co. Effective date of registration: 20190202 Address after: Ohio, USA Patentee after: THE SHERWIN WILLIAMS Co. Address before: Ohio, USA Patentee before: Valspar Corp. Effective date of registration: 20190202 Address after: Ohio, USA Patentee after: Xuanwei Headquarters Co. Address before: Ohio, USA Patentee before: THE SHERWIN WILLIAMS Co. |
|
TR01 | Transfer of patent right | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20090708 |
|
CF01 | Termination of patent right due to non-payment of annual fee |