CN1502634A - 氟化聚合物的制备 - Google Patents
氟化聚合物的制备 Download PDFInfo
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- CN1502634A CN1502634A CNA2003101198990A CN200310119899A CN1502634A CN 1502634 A CN1502634 A CN 1502634A CN A2003101198990 A CNA2003101198990 A CN A2003101198990A CN 200310119899 A CN200310119899 A CN 200310119899A CN 1502634 A CN1502634 A CN 1502634A
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- gram
- monomer
- fluorinated
- methyl
- water
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
- Polymerisation Methods In General (AREA)
Abstract
Description
实施例 | 烃表面活性剂 | %重量 | ZonylFSN%重量 | CD%重量 | 湿凝胶(克) |
1 | Rhodapex CO-436 | 1 | 1 | 0.5 | 11 |
2 | Rhodapex CO-436 | 1 | 1 | 1 | 6 |
3 | Rhodapex CO-436 | 1 | 1 | 1 | 20 |
4 | Rhodapex CO-436 | 1 | 0.5 | 1 | 10 |
5 | SLS | 0.42 | 0.5 | 1 | 12 |
6 | Rhodapex CO-436 | 1 | 0 | 1 | 26 |
C-1 | SLS | 0.42 | 0.5 | 0 | 490 |
C-2 | Rhodapex CO-436 | 1 | 1 | 0 | 360 |
C-3 | Rhodapex CO-436 | 1 | 1 | 0 | 250 |
C-4 | Rhodapex CO-436 | 1 | 5 | 0 | 11 |
实施例号 | 单体组合物BA 2- MMA Sty Zonyl Zonyl MAAEHA A TM TM | Rhodapex 氟化 CDCO-436 表面活性剂%重量 类型 %重量 %重量 | 湿凝胶,克 |
7 | 0 28 0 41 30 0 1 | 1.5 Zonyl FSN 1.5 1 | 1.7 |
8 | 0 28 0 41 30 0 1 | 1.4 Zonyl FSN 0.6 1 | 2.5 |
9 | 0 28 0 41 30 0 1 | 1.4 Zonyl FSA 0.6 1 | 1.5 |
9A | 0 28 0 41 30 0 1 | 1.5 无 0 1 | 45 |
10 | 15 0 0 34 50 0 1 | 1 Zonyl FSN 1 1 | 20 |
11 | 15 0 34 0 50 0 1 | 1 Zonyl FSN 1 1 | 0.1 |
12 | 15 0 34 0 0 50 1 | 1 Zonyl FSN 1 1 | 0.1 |
13 | 9 0 0 20 70 0 1 | 0.6 Zonyl FSN 1.4 1 | 0.1 |
14 | 0 0 0 0 99 0 1 | 0 Zonyl FSN 1 1 | 0.6 |
试样 喷涂试验评价值 |
实施例4 90商业粘合剂 0 |
试样 | 16-1 | 16-2 | 16-3 | 16-4 | 16-5 | 16-6 | 未处理对比试样 | 16-C |
全氟烷基磺酸铵(1%),克 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | - | |
硅氧烷消泡剂 | 2滴 | 2滴 | 2滴 | 2滴 | 2滴 | 2滴 | - | |
二甘醇乙基醚,克 | 1.5 | 1.1 | 1.5 | 1.1 | 1.5 | 1.1 | - | |
增塑剂,克 | 0 | 0.2 | 0 | 0.2 | 0 | 0.2 | - | |
磷酸三丁氧基乙酯,克 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | 0.3 | - | |
氟聚合物(20%) | 13 | 13 | 11 | 11 | 12 | 12 | 无 | B-66 |
实施例号 | ||||||||
总重量,克 | 20 | 20 | 20 | 20 | 20 | 20 | - | |
膜数据: | ||||||||
水透过,小时 | >2 | 0.5 | >2 | >2 | >2 | 0.5 | 0 | <2 |
水珠 | 10 | 10 | 10 | 10 | 10 | 10 | 无 | 1 |
水标记 | 无 | 无 | 无 | 无 | 无 | 无 | 有 | 有 |
光泽: | 高 | 高 | 高 | 高 | 高 | 高 | 很低 | 很低 |
Claims (2)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US2556897A | 1997-07-11 | 1997-07-11 | |
US025568 | 1997-07-11 |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB981159354A Division CN1144822C (zh) | 1997-07-11 | 1998-07-10 | 制备氟化乳液聚合物的方法 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN1502634A true CN1502634A (zh) | 2004-06-09 |
Family
ID=34271713
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNA2003101198990A Pending CN1502634A (zh) | 1997-07-11 | 1998-07-10 | 氟化聚合物的制备 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN1502634A (zh) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101341179B (zh) * | 2005-12-23 | 2012-06-27 | 3M创新有限公司 | 含氟聚合物分散体及其制备方法 |
-
1998
- 1998-07-10 CN CNA2003101198990A patent/CN1502634A/zh active Pending
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101341179B (zh) * | 2005-12-23 | 2012-06-27 | 3M创新有限公司 | 含氟聚合物分散体及其制备方法 |
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