CN1308378C - 基本上无定形的非氯化聚合物隔离膜 - Google Patents
基本上无定形的非氯化聚合物隔离膜 Download PDFInfo
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- CN1308378C CN1308378C CNB008098247A CN00809824A CN1308378C CN 1308378 C CN1308378 C CN 1308378C CN B008098247 A CNB008098247 A CN B008098247A CN 00809824 A CN00809824 A CN 00809824A CN 1308378 C CN1308378 C CN 1308378C
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Abstract
Description
3-甲基吲哚的突破时间(小时)2 | DEDS突破时间(分钟)2 | |||||||||||||||||
膜 | 2 | 4 | 10 | 20 | 40 | 80 | 150 | 200 | 300 | 8 | 20 | 50 | 100 | 150 | 300 | 500 | 1000 | 1200 |
SAN | Y | Y | Y | Y | Y | Y | Y | Y | N | Y | Y | Y | Y | N | N | N | N | N |
SAN-ESI | Y | Y | Y | Y | Y | Y | Y | N | N | Y | Y | Y | Y | N | N | N | N | N |
ABS | Y | Y | Y | Y | Y | Y | N | N | N | Y | Y | Y | Y | Y | N | N | N | N |
PMMA | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | N | N | N | N | N | N |
PMMA-IM′ | Y | Y | Y | Y | Y | Y | Y | N | N | Y | Y | Y | N | N | N | N | N | N |
PC | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y |
PC-IM′ | Y | Y | Y | Y | Y | Y | Y | Y | N | Y | Y | Y | Y | Y | Y | Y | N | N |
PC-ABS | Y | Y | Y | Y | Y | Y | Y | N | N | Y | Y | Y | Y | Y | Y | Y | Y | N |
PET-G | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | N | N | N |
PET-G/SB | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | N | N | N | N | N |
PET-G/SBS | Y | Y | Y | Y | Y | Y | Y | N | N | Y | Y | Y | N | N | N | N | N | N |
GPPS/SB | Y | Y | N | N | N | N | N | N | N | Y | Y | N | N | N | N | N | N | N |
GPPS/ESI | Y | Y | Y | Y | Y | Y | Y | Y | N | Y | Y | Y | Y | Y | N | N | N | N |
GPPS/SIS | Y | N | N | N | N | N | N | N | N | Y | N | N | N | N | N | N | N | N |
APE-1/PET-G(50/50%) | Y | Y | Y | Y | Y | Y | N | N | N | Y | Y | Y | Y | Y | N | N | N | N |
3-甲基吲哚的突破时间(小时)2 | H2S突破时间(秒)2 | ||||||||||||||
2 | 4 | 10 | 20 | 80 | 150 | 200 | 300 | 40 | 100 | 150 | 200 | 250 | 400 | >600 | |
SAN | Y | Y | Y | Y | Y | Y | Y | N | Y | Y | Y | N | N | N | N |
ABS | Y | Y | Y | Y | Y | N | N | N | Y | N | N | N | N | N | N |
PMMA | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | N | N |
PC | Y | Y | Y | Y | Y | Y | Y | Y | Y | N | N | N | N | N | N |
PC-IM′ | Y | Y | Y | Y | Y | Y | Y | N | Y | N | N | N | N | N | N |
PET-G | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | N |
APE-1/PET-G(50/50%) | Y | Y | Y | Y | Y | N | N | N | Y | Y | Y | Y | Y | Y | Y |
DEDS突破时间(分钟)2 | H2S突破时间(秒)2 | |||||||||||||||
8 | 20 | 50 | 100 | 150 | 300 | 500 | 1000 | 1200 | 40 | 100 | 150 | 200 | 250 | 400 | >600 | |
SAN | Y | Y | Y | Y | N | N | N | N | N | Y | Y | Y | N | N | N | N |
ABS | Y | Y | Y | Y | N | N | N | N | N | Y | N | N | N | N | N | N |
PMMA | Y | Y | Y | N | N | N | N | N | N | Y | Y | Y | Y | Y | N | N |
PC | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | N | N | N | N | N | N |
PC-IM′ | Y | Y | Y | Y | Y | Y | Y | N | N | Y | N | N | N | N | N | N |
PET-G | Y | Y | Y | Y | Y | Y | N | N | N | Y | Y | Y | Y | Y | Y | N |
APE-1/PET-G(50/50%) | Y | Y | Y | Y | Y | N | N | N | N | Y | Y | Y | Y | Y | Y | Y |
3-甲基吲哚突破时间(小时)2 | DEDS突破时间(分钟)2 | H2S突破时间(秒)2 | |||||||||||||||||||||||
2 | 4 | 10 | 20 | 40 | 80 | 150 | 200 | 300 | 8 | 20 | 50 | 10 | 150 | 300 | 500 | 1000 | 1200 | 40 | 100 | 150 | 200 | 250 | 400 | >600 | |
SAN | Y | Y | Y | Y | Y | Y | Y | Y | N | Y | Y | Y | Y | N | N | N | N | N | Y | Y | Y | N | N | N | N |
ABS | Y | Y | Y | Y | Y | Y | N | N | N | Y | Y | Y | Y | Y | N | N | N | N | Y | N | N | N | N | N | N |
PMMA | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | N | N | N | N | N | N | Y | Y | Y | Y | Y | N | N |
PC | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | N | N | N | N | N | N |
PC-1M′ | Y | Y | Y | Y | Y | Y | Y | Y | N | Y | Y | Y | Y | Y | Y | Y | N | N | Y | N | N | N | N | N | N |
PET-G | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | Y | N | N | N | Y | Y | Y | Y | Y | Y | N |
APE-1/PET-G(50/50%) | Y | Y | Y | Y | Y | Y | N | N | N | Y | Y | Y | Y | Y | N | N | N | N | Y | Y | Y | Y | Y | Y | Y |
树脂名称 | 类型 | 供应商 | 密度 | 熔体指数(g/10min) | 其它 |
AFFINITY*PL 1880 | INSITE*technology | 陶氏化学公司 | 0.902 | 1.01 | 低结晶乙烯和α烯烃均相共聚物 |
polymer(ITP-1) | |||||
AFFINITY*KC 8852 | INSITE*technologypolymer(ITP-2) | 陶氏化学公司 | 0.875 | 3.01 | 低结晶乙烯和α烯烃均相共聚物 |
AFFINITY*EG 8100 | INSITE*technologypolymer(ITP-3) | 陶氏化学公司 | 0.870 | 1.01 | 低结晶乙烯和α烯烃均相共聚物 |
ATTANE*4201 | ULDPE-1 | 陶氏化学公司 | 0.912 | 1.01 | 乙烯和辛烯共聚物 |
ATTANE*4202 | ULDPE-2 | 陶氏化学公司 | 0.913 | 3.21 | 乙烯和辛烯共聚物 |
ATTANE*4203 | ULDPE-3 | 陶氏化学公司 | 0.905 | 0.81 | 乙烯和辛烯共聚物 |
AFFINITY*PF 1140 | ITP-4 | 陶氏化学公司 | 0.896 | 1.61 | 低结晶乙烯和α烯烃均相共聚物 |
CN 4420 | 润滑和防粘连橡胶(ADD-1) | Southwest-Chemical | - | - | EVA载体中4%漂儿菜基酰胺+4%硬脂酸酰胺+20%硅石 |
REXFLEX_FPOWL101 | 聚丙烯均聚物(PP) | Huntsman | 0.88 | 148 | 低结晶和低模量PP(熔融热~25J/g) |
REFLEX_FPOWL201 | 聚丙烯共聚物(PCP-1) | Huntsman | 0.88 | 2.88 | 低结晶和低模量PP(熔融热~20J/g) |
REXFLEX_FPOWL210 | 聚丙烯共聚物(PCP-2) | Huntsman | 0.88 | 68 | 低结晶和低模量PP(熔融热~20J/g) |
REXFLEX_FPO | 聚丙烯共聚物(PCP-3) | Huntsman | 0.88 | 198 | 低结晶和低模量PP(熔融热~20J/g |
VISTAFLEXTM 671N | 非交联聚丙烯/乙烯-丙烯-二烯单体 | AdvancedElastomerSystems | 0.91 | - | - |
(PP-EPDM) | |||||
GRIVORYTM G21 | 无定形共聚酰胺(共聚PA-1) | EMSChemieAG. | 1.18 | - | Tg=125℃ |
GRILONTMF34 | 聚酰胺6(PA6) | EMSChemieAG. | 1.14 | - | |
EVAL EPE105 | 乙烯乙烯醇(EVOH) | Kuraray | 1.19 | 5.51 | 44mol%乙烯 |
GRILONTMBM FE4581 | 共聚酰胺(共聚PA-2) | EMSChemieA.G | 1.20 | - | Tg=96℃ |
GRILONTMCR9 | 聚酰胺6-12(PA6-12) | EMSChemieA.G | 1.10 | - | 熔点200℃ |
STYRON*637 | GPPS-1 | 陶氏化学公司 | 1.05 | 2.52 | |
STYRON*686 | GPPS-2 | 陶氏化学公司 | 1.05 | 2.52 | |
STYRON*665 | GPPS-3 | 陶氏化学公司 | 1.05 | 1.52 | |
STYRON*5192 | 高抗冲击聚苯乙烯(HIPS-1) | 陶氏化学公司 | 1.05 | 4.52 | 8.5%橡胶 |
STYRON*492U | HIPS-2 | 陶氏化学公司 | 1.05 | 3.02 | 7.2%橡胶 |
PET | 双轴拉伸聚对苯二甲酸丁二酯膜,热级B(130℃),中等光雾值H(PET) | MICEL,France | - | - | 12微米厚单层膜 |
B-100 | 无定形热塑性共聚酯树脂(APE-1) | MitsuiChemicalsEuropeGmbH | 1.35 | Tg 62℃ | |
EASTARTM6763 | PET-G | EastmanChemical | 1.27 | 特性粘度 | 1,4-苯二羧酸二甲酯聚合物和1,4-环 |
粘度0.75 | 酯聚合物和1,4-环己烷二甲醇和1,2-乙二醇的无定形聚酯 | ||||
FINACLEARTM 520 | SBS嵌段共聚物(SBS) | Fina | 1.01 | 7.52 | 70wt%苯乙烯 |
V920 | PMMA | Atohaas | 1.18 | 83 | |
HFI-7 | 抗冲击改性的聚甲基丙烯酸甲酯(PMMA-IM) | Atohaas | 1.17 | 113 | |
CALIBRE*0201-20 | PC-1 | 陶氏化学公司 | - | 204 | |
CALIBRE*200 | PC-2 | 陶氏化学公司 | - | 204 | |
CALIBRE*201-22 | PC-3 | 陶氏化学公司 | - | 224 | |
CALIBRE*IM401.11 | 抗冲击改性聚碳酸酯(PC-IM-1) | 陶氏化学公司 | - | 114 | |
PULSE*830 | PC-ABS三元共聚物合金 | 陶氏化学公司 | - | 2.53 | |
K-RESINKR01 | SB | PhilippsPetroleumChemicals | 1.01 | 8.02 | |
INDEX*DS201.00 | ESI | 陶氏化学公司 | - | 1.01 | 69wt%苯乙烯 |
TYRIL*790 | SAN-1 | 陶氏化学公司 | - | 9.03 | 29wt%丙烯腈 |
TYRIL*100 | SAN-2 | 陶氏化学公司 | - | 8.03 | 25%丙烯腈 |
MAGNUM*340 | ABS | 陶氏化学公司 | - | 2.83 | 25%丙烯腈,12%橡胶 |
ELVAX_3165 | EVA共聚物(EVA-1) | DuPont | 0.94 | 0.7 | 18wt%V.A. |
ELVAX_3174 | EVA共聚物(EVA-2) | DuPont | 0.94 | 81 | 18wt%V.A |
ELVAX_3190 | EVA共聚物(EVA-3) | Dupont | 0.94 | 21 | 25wt%V.A |
ESCORENETM 740.16 | EVA共聚物(EVA-4) | EXXON | - | 5.51 | 24.5%wt%V.A |
BYNELE_21 E533 | MAH-g-EVA共聚物(MAH-a-EVA-1) | DuPont | - | 7.71 | 粘合剂树脂 |
BYNELE_3860 | MAH-g-EVA-2 | DuPont | - | 5.71 | 粘合剂树脂 |
VECTOR_4411 | SIS-1 | Dexco | 402 | 44%苯乙烯 | |
VECTOR_4211 | SIS-2 | Dexco | 132 | 30%苯乙烯 | |
LOTRYLTM24 MA 005 | EMA | Atochem | - | 0.51 | 24wt%M.A. |
OREVACTM 18613 | MAH-g-EMA | Atochem | 3.51 | 28%马来酸酐 | |
LOTADERTM GMAAX 8900 | 乙烯-丙烯酸甲酯-甲基丙烯酸甘油酯(EMAGMA) | Atochem | 61 | ||
LDPE 320 | LDPE-1 | 陶氏化学公司 | 0.924 | 1.751 | |
LDPE 501 | LDPE-2 | 陶氏化学公司 | 0.922 | 1.91 | |
SARAN469 | PVDC | 陶氏化学公司 | - | - | 80/20wt%VDC/氯乙烯共聚物 |
ADMERTMNF 530 | MAH-g-PE | Mitsui &Co | - | 4.0 | 粘合剂树脂 |
KRATONTM FG1901X | 60%氯化聚乙烯(36wt%氯,2%剩余结晶度)和40%EVA(15wt% | - | - | - | - |
醋酸乙烯酯,熔融指数2.5@190/2.16)的混合物 | |||||
EVA | EVA | - | - | 0.5-5.0 | 15-25wt%醋酸乙烯酯 |
HDPE | 所有类型HDPE膜级 | - | 0.955-0.965 | 0.2-8.01 | |
EEA | 乙烯-丙烯酸乙酯 | - | - | 0.5-51 | 15-25wt%丙烯酸乙酯 |
EMA | 乙烯丙烯酸甲酯 | - | - | 0.5-5.0 | 15to 25wt%丙烯酸甲酯 |
XU73109.01 | PC-4 | 陶氏化学公司 | - | 12.55 | - |
XU73114.03 | PC-IM-2 | 陶氏化学公司 | - | 8.54 | - |
LDPE | 所有类型LDPE膜级 | - | 0.917-0.925 | 0.5-8.01 | - |
EAA | 乙烯-丙烯酸共聚物 | 陶氏化学公司 | - | 1.0-15.0 | 5to 10wt%丙烯酸 |
CN 706 | 润滑添加剂浓缩物(ADD-2) | SouthwestChemical | - | - | EVA树脂中10%的硬脂酰胺 |
100371 | 防粘连浓缩物(ADD-3) | Ampacet | - | - | 聚烯烃中20%硅石 |
100501 | 润滑防粘连浓缩物(ADD-4) | Ampacet | - | - | 聚烯烃中15%硅石+5%漂儿菜基酰胺 |
实施例或对比例 | 膜描述 | 隔离层 | 隔离层厚度(μm) | 总膜厚度(μm) | 氧气透过性(cm3/m2-天-atm) | 3-甲基吲哚B.T.(小时) |
A | LDPE/EVA/PVDC/EVA/LDPE | PVDC | 5.51 | 70 | 13 | 7 |
B | LDPE/EVA/PVDC/EVA/LDPE | PVDC | 10.12 | 75 | 4.5 | 24 |
C | CPE/EVA/PVDC/EVA | PVDC | 9.13 | 100 | 6 | 65 |
D | CPE/EVA/PVDC/EVA | PVDC | 10 | 70 | 7.5 | 50 |
E | EVA/MAH-g-EVA-2/共聚PA-1/MAH-g-EVA-2/EVA | 无定形共聚PA | 6.24 | 70 | 42 | 20 |
F | EVA/MAH-g-EVA-2/共聚PA-1/MAH-g-EVA-2/EVA | 无定形共聚PA | 10.25 | 70 | 30 | >50 |
G | EVA/MAH-g-PE/EVOH/MAH-g-PE/EVA | EVOH | 7 | 60 | 14 | 1/4.56 |
H | LDPE/5μm粘合剂/PA6 | PA6 | 18 | 70 | 41 | <2 |
I | 50μmLDPE/10μm粘合剂/PA6-12 | PA6-12 | 25 | 85 | 76 | <2 |
J | LDPE-1/MAHg-EVA-2/共聚PA-24581/MAH-g-EVA-2/LDPE-1 | 共聚PA | 5.2 | 93 | 6.9 | 3 |
1 | LDPE-10/EVA/50∶50GPPS-1和HIPS-1/EVA/LDPE-1 | 50/50的PPS和HIPS的混合物 | 10 | 100 | 1625 | 85 |
2 | LDPE/MAH-g-EVA-2/SAN-2/MAH-g-EVA-2/LDPE | SAN | 35 | 85 | 1360 | 200 |
3 | LDPE/MAH-g-EVA-2/PMMA/MAH-g-EVA-2/LDPE | PMMA | 35 | 85 | 138 | 390 |
4 | 50∶50GPPS-2和HIPS-27 | 50/50的GPPS/HIPS的混合物 | 19 | 19 | >2000 | >1490 |
K | 涂覆有10μm阳离子环氧清漆8的LDPE | 阳离子环氧树脂 | 10 | 100 | 44 | 1 |
L | EAA表层和4.5μm聚羟基氨基醚树脂的共挤出膜 | 聚羟基氨基醚 | 4.5 | 24 | 72 | <1 |
M | HDPE(臭味浸透速率为5的基准膜) | - | 15 | >2000 | <0.3 | |
5 | PETG9 | PET-G | 18 | 18 | 390 | >388 |
6 | LDPE/EVA/ABS/EVA/LDPE | ABS | 6 | 75 | 2260 | ~85 |
7 | LDPE/EVA/75∶25PET-G和SBS/EVA/LDPE10 | 75∶25PET-G和SBS的混合物 | 7.311 | 80 | 712 | 160 |
8 | LDPE501/MAH-g-EVA-2/V920/MAH-g-EVA-2/LDPE | PMMA | 5 | 75 | 665 | >175 |
9 | LDPE-2/MAH-g-EVA-2/PMMA-IM/MAH-g-EVA-2/LDPE-2 | 抗冲击改性的PMMA | 10 | 75 | 607 | 175 |
10 | LDPE-2/EEA/PC/EEA/LDPE-212 | PC | 9.014 | 75 | 1740 | >147 |
11 | LDPE-2/MAH-g-EVA-2/PC-IM-2/MAH-gEVA-2/LDPE-215 | 抗冲击改性PC | 5.716 | 75 | 2375 | -270 |
12 | LDPE-2/EEA/PC-ABS/EEA/LDPE-2 | PC/ABS合金 | 3.0 | 75 | 4390 | 185 |
13 | LDPE-2/EVA/70∶30PET-G和SB/EVA/LDPE-2 | 70∶30的PET-G和SB混合物 | 10 | 75 | 962 | >147 |
N | PET17 | PET | 13 | 13 | 141 | 175 |
14 | LDPE-2/EVA/70∶30GPPS-3和SB/EVA/LDPE-2 | 70∶30的GPPS和SB混合物 | 10 | 75 | 3865 | 4 |
15 | LDPE-2/EMA/PC-1/MEA/LDPE-218 | PC | 7.4 | 75 | 1995 | ~315 |
16 | LDPE-2/EVA/85∶15PET-G和SB/EVA/LDPE-219 | 85∶15的PET-G和SB的混合物 | 4.520 | 75 | 1070 | >147 |
对比例/实施例编号 | 膜结构 | 隔离层 | 隔离层厚度(μm) | DEDS的B.T.(分钟) | DEDS相对浸透速率(相对单位) |
A | LDPE/EVA/PVDC/EVA/LDPE | PVDC | 5.51 | 71 | 450 |
B | LDPE/EVA/PVDC/EVA/LDPE | PVDC | 10.12 | 136 | 200 |
C | CPE/EVA/PVDC/EVA | PVDC | 9.13 | 139 | >350 |
0 | LDPE/EVA/PVDC/EVA/LDPE | PVDC | 4.8 | 47 | 500 |
E | EVA/MAH-g-EVA-2/GRIVORY-G21/MAH-g-EVA-2/EVA | 无定形共聚PA | 6.24 | 226 | 120 |
F | EVA/MAH-g-EVA-2/共聚PA-1/MAH-g-EVA-2/EVA | 无定形共聚PA | 10.25 | 190 | 250 |
M | LDPE | 基准样品(速率为5) | 25 | 5 | 6000000 |
17 | LDPE-I/EVA/70∶30的GPPS-1和ESI的混合物/EVA/LDPE-1 | 70∶30的GPPS和ESI的混合物 | 4.6 | 129 | 1000 |
18 | LDPE-I/EVA/70∶30的GPPS-3和ESI的混合物/EVA/LDPE-1 | 70∶30的GPPS和ESI的混合物 | 8.4 | 193 | >600 |
P | LDPE-2/EVA/70∶30的GPPS-3和SIS-1的混合物 | 70∶30的GPPS和SIS-1的混合 | 5.6 | 8 | >4500 |
/EVA/LDPE-2 | 物 | ||||
19 | LDPE-2/EVA/70∶30的GPPS-3和SB的混合物/EVA/LDPE-2 | 70∶30的GPPS和SB的混合物 | 12.2 | 30 | 1400 |
20 | LDPE-2/EVA/70∶30的SAN-1和ESI的混合物/EVA/LDPE-2 | 70∶30的SAN和ESI的混合物 | 8.1 | 116 | ~350 |
21 | LDPE-2/MAH-g-EVA-2/SAN-2/MAH-g-EVA-2/LDPE-26 | SAN | 10.27 | 142 | 700 |
22 | LDPE-2/MAH-g-EVA-2/SAN-2/MAH-g-EVA-2/LDPE-2 | SAN | 11.2 | 125 | 450 |
23 | LDPE-2/MAH-g-EVA-2/PMMA/MAH-g-EVA-2/LDPE8 | PMMA | 11.4 | 82 | 350 |
24 | LDPE-2/MAH-g-EVA-2/PMMA-IM/MAH-g-EVA-2/LDPE-2 | PMMA-IM | 8.9 | 77 | 500 |
25 | LDPE-1/EVA/ABS/EVA/LDPE-1 | ABS | 7.1 | 112 | 500 |
26 | LDPE-1/EVA/ABS/EVA/LDPE-1 | ABS | 16.5 | 169 | 450 |
27 | LDPE-2/MAH-g-EVA-2/PET-G/MAH-g-EVA-2/LDPE-2 | PET-G | 8.1 | 166 | 65 |
28 | LDPE-2/MAH-g-EVA-2/PET-G/MAH-g-EVA-2/LDPE-2 | PET-G | 10.4 | 187 | 80 |
29 | LDPE/EVA/75∶ | 75∶25的 | 7.310 | 70 | 250 |
25的PET-G和SBS的混合物/EVA/LDPE9 | PET-G和SBS的混合物 | ||||
30 | LDPE-2/EVA/85∶15的PET-G和SB的混合物/EVA/LDPE-211 | 85∶15的PET-G和SB的混合物 | 4.512 | 92 | 85 |
31 | LDPE-2/EVA/85∶15的PET-G和SB的混合物/EVA/LDPE-2 | 85∶15的PET-G和SB的混合物 | 9.4 | 119 | - |
32 | LDPE-2/EVA/70∶30的PET-G和SB的混合物/EVA/LDPE-2 | 70∶30的PET-G和SB的混合物 | 8.1 | 115 | >90 |
33 | LDPE-2/EEA/PC-4/EEA/LDPE-2 | PC | 4.8 | 800 | >45 |
34 | LDPE-2/EMA/PC-1/EMA/LDPE-2 | PC | 5.8 | 1105 | >18 |
35 | LDPE-2/EMA/PC-1/EMA/LDPE-213 | PC | 7.4 | 1315 | - |
36 | LDPE-2/EEA/PC/EEA/LDPE-214 | PC15 | 9.016 | >1440 | - |
37 | LDPE-2/MAH-g-EVA-1/PC-IM-1/MAH-g-EVA-1/LDPE-2 | 抗冲击改性PC | 4.6 | 615 | >400 |
38 | LDPE-2/EEA/PC-IM-2/EEA/LDPE-2 | 抗冲击改性PC | 7.9 | 916 | >55 |
39 | LDPE-2/MAH-g-EVA-2/PC-IM-2/MAH-g-EVA-2/LDPE-217 | 抗冲击改性PC | 5.7187 | 455 | 150 |
40 | LDPE-2/EEA/PC-ABS/EEA/LDPE-2 | PC-ABS合金 | 15 | 1180 | >30 |
41 | LDPE-2/MAH-g-EVA-2/PET-G/MAH-g-EVA-2/LDPE-2 | PET-G | 9.2 | 188 | 72 |
42 | LDPE-2/MAH-g-EVA-2/PET-G/MAH-g-EVA-2/LDPE-2 | PET-G | 5.2 | 273 | 40 |
43 | LDPE-2/MAH-g-EVA-2/PET-G/MAH-g-EVA-2/LDPE-2 | PET-G | 7.4 | 312 | 33 |
对比例/实施例编号 | 膜结构 | 隔离层 | 隔离层厚(μm) | H2S的B.T.(秒) | H2S浸透速率(cm3/天-m2) |
C | CPE/EVA/PVDC/EVA | PVDC | 9.1 | 450 | 3.55 |
44 | LDPE-2/MAH-g-EVA-2/PC/MAH-g-EVA-2/LDPE-2 | PC | 6.0 | 68 | 192 |
45 | LDPE-2/MAH-g-EVA-2/PET-G/MAH-g-EVA-2/LDPE-2 | PET-G | 8.0 | 263 | 24.3 |
41 | LDPE-2/MAH-g-EVA-2/PT-G2/MAH-g-EVA-2/LDPE-2 | PET-G | 9.2 | 155 | 34.0 |
46 | LDPE-2/MAH-g-EVA-2/PC-IM-23/MAH-g-EVA-2/LDPE-2 | 抗冲击改性的PC | 6.0 | 65 | 168 |
47 | LDPE-2/MAH-g-EVA-2/PC-IM-1/MAH-g-EVA-2/LDPE-2 | 抗冲击改性的PC | 4.6 | 73 | 162 |
48 | LDPE-2/MAH-g-EVA-2/ABS/MAH-g-EVA-2/LDPE-2 | ABS | 6.0 | 65 | 116 |
49 | LDPE-1/EVA/HIPS-1/EVA/LDPE-1 | HIPS | 10 | 53 | 162 |
21 | LDPE-2/MAH-g-EVA-2/SAN-2/MAH-g-EVA-2/LDPE-2 | SAN | 10.2 | 195 | 70 |
23 | LDPE-2/MAH-g-EVA-2/PMMA/MAH-g-EVA-2/LDPE-2 | PMMA | 11.4 | 275 | 8.2 |
N | PET | PET | 13 | 185 | 10.9 |
柔性树脂 | PET-G树脂中柔性树脂的% | 氧气透过性(10μm树脂的cm3/m2-天-atm) | 1%模量(MPa)(MD和TD的平均值) |
SIS-2 | 0 | 698 | 1682 |
SIS-2 | 8 | 896 | 1442 |
SIS-2 | 16 | 1229 | 1316 |
MAH-g-EMA | 0 | 698 | 1682 |
MAH-g-EMA | 8 | 989 | 1328 |
MAH-g-EMA | 16 | 1115 | 1061 |
EMAGMA | 0 | 698 | 1682 |
EMAGMA | 8 | 900 | 1411 |
EMAGMA | 16 | 1162 | 1092 |
MAH-g-SEBS | 0 | 698 | 1682 |
MAH-g-SEBS | 8 | 1040 | 1405 |
MAH-g-SEBS | 16 | 970 | 1390 |
实施例编号 | 23℃下氧气透过性(cm3/m2-天-atm) | DEDS的B.T.(分钟) | DEDS的相对透过速率(cm3/天-m2) |
27 | 467 | 166 | 65 |
32 | 675 | 115 | >90 |
对比例 | 表层A | 连接层B | 芯层C | 芯层厚度μm | 总厚度μm | 膜类型 |
Q | LDPE-2 | - | - | -- | 75 | 单层 |
R | LDPE-2 | MAH-g-EVA-2 | PET-G | 7.5 | 78 | 5层 |
S | LDPE-2 | MAH-g-EVA-2 | ABS | 7.5 | 78 | 5层 |
T | LDPE-2 | MAH-g-EVA-2 | 共聚PA-1 | 61 | 76 | 5层 |
U | LDPE-2 | EMA | PC-3 | 8 | 95 | 5层 |
V | EVA-4 | - | - | - | 72 | 单层 |
W | EVA-4 | MAH-g-EVA-2 | PET-G | 6.5 | 90 | 5层 |
树脂 | G′(10E-5N/cm2) |
LDPE-2 | 1.57E+09 |
EVA-4 | 1.20E+08 |
PET-G | 7.3E+09 |
ABS | 1.03E+10 |
共聚PA-1 | 1.08E+10 |
PC-3 | 8.64E+09 |
对比例 | 63Hz | 125Hz | 250Hz | 500Hz | 1kHz | 2kHz | 4kHz | 8kHz | 16kHz |
Q | 36.2 | 46.2 | 58.5 | 60.8 | 62.5 | 65.1 | 68.4 | 61.9 | 48.9 |
R | 49.3 | 54.4 | 66.6 | 77.3 | 76.1 | 78.1 | 75.7 | 71.0 | 65.4 |
S | 47.7 | 54.5 | 65.6 | 72.3 | 75.2 | 78.6 | 76.6 | 71.5 | 63.3 |
T | 45.2 | 54.1 | 65.0 | 70.9 | 72.1 | 77.4 | 75.1 | 71.8 | 64.2 |
U | 50.9 | 58.0 | 69.6 | 73.8 | 75.6 | 77.3 | 75.3 | 71.4 | 63.6 |
V | 37.6 | 38.1 | 41.6 | 44.3 | 43.0 | 47.0 | 42.8 | 35.5 | 25.7 |
W | 38.8 | 50.3 | 57.5 | 62.9 | 69.2 | 74.1 | 73 | 68.2 | 54.6 |
对比例和实施例编号 | 表层A | 连接层B | 隔离层C | 总厚度μm | 隔离层厚度μm |
X | LDPE-2/ADD-1(96/4%) | MAH-g-EVA-2 | PET-G | 75 | 5.0 |
Y | ITP-4/ADD-1(96/4%) | MAH-g-EVA-2 | PET-G | 72 | 6.0 |
Z | EMA/ADD-1(96/4%) | MAH-g-EVA-2 | PET-G | 75 | 6.3 |
AA | EMA/ITP-4/ADD- | MAH-g-EVA-2 | PET-G | 75 | 5.0 |
4(48/48/4%) | _3860 | ||||
50 | PP/ADD-1(96/4%) | MAH-g-EVA-2 | PET-G | 70 | 8.3 |
51 | PP/ITP-4/ADD-1(48/48/4%) | MAH-g-EVA-2 | PET-G | 78 | 6.9 |
对比例和实施例编号 | 63Hz | 125Hz | 250Hz | 500Hz | 1kHz | 2kHz | 4kHz | 8kHz | 16kHz |
X | 36.8 | 48.3 | 63.7 | 72.9 | 71 | 77.7 | 75.5 | 69.7 | 59.8 |
Y | 38.5 | 48.4 | 56 | 59.6 | 62.4 | 72 | 74 | 67.6 | 57.9 |
Z | 37.3 | 43.9 | 52.2 | 57 | 58.2 | 65.3 | 69.9 | 63.2 | 50.2 |
AA | 37.9 | 45.5 | 54.8 | 60.5 | 60.6 | 69.8 | 75 | 67.2 | 49.2 |
50 | 38.1 | 42.6 | 51.3 | 56 | 57.4 | 65.4 | 67 | 56.6 | 40.7 |
51 | 38.5 | 45.6 | 54.6 | 57.5 | 60.9 | 66.6 | 68 | 61.1 | 39.3 |
对比例/实施例编号 | 表层A | 连接层B | 隔离层C | 总厚度μm | 隔离层厚度μm |
AB | EVA-1/EVA-2/ADD-1(72%/24%/4%) | MAH-g-EVA-2 | PET-G | 80 | 5.0 |
AC | EVA-1/EVA-2/ADD-1(72%/24%/4%) | MAH-g-EVA-2 | PET-G | 95 | 4.8 |
52 | PCP-2/ADD-1(92%/8%) | MAH-g-EVA-2 | PET-G | 79 | 9.4 |
53 | PCP-2/ADD-1(92%/8%) | MAH-g-EVA-2 | PET-G | 90 | 10.0 |
对比例/实施例编号 | 63Hz | 125Hz | 250Hz | 500Hz | 1kHz | 2kHz | 4kHz | 8kHz | 16kHz |
AB | 37.2 | 46 | 53.3 | 58.9 | 61.7 | 70.6 | 73.5 | 64 | 55.1 |
AC | 37.5 | 48.8 | 59.7 | 63.6 | 65.1 | 74.2 | 75.6 | 69.1 | 58.1 |
52 | 37.6 | 41.1 | 49.7 | 55.6 | 58.6 | 67.6 | 66.9 | 56.6 | 37.2 |
53 | 37.9 | 44.5 | 53.8 | 57.1 | 60.1 | 66 | 64.9 | 55.1 | 31 |
对比例/实施例编号 | 表层A | 连接层B | 隔离层C | 总厚度μm | 隔离层厚度μm |
X | LDPE-2 | MAH-g-EVA-2 | PET-G | 75 | 5.0 |
AD | PP-EPDM/ADD-1(98/2%) | MAH-g-EVA-2 | PET-G | 75 | 6.0 |
54 | PP/PP-EPDM/ADD-1(72/24/4%) | MAH-g-EVA-2 | PET-G | 80 | 7.5 |
55 | PCP-3/ADD-1(98/2%) | MAH-g-EVA-2 | PET-G | 85 | 6.0 |
56 | PCP-3/ADD-1(98/2%) | MAH-g-EVA-2 | PET-G | 79 | 9.4 |
57 | PP/PCP-1/ADD-1(72/24/4%) | MAH-g-EVA-2 | PET-G | 77 | 10 |
58 | PP/PCP-2/ADD-1(72/24/4%) | EMA | PET-G | 74 | 8.5 |
59 | PCP-1/ITP-4/ADD-1(46/46/8%) | EVA-3 | PET-G | 76 | 9.2 |
对比例/实施例编号 | 63Hz | 125Hz | 250Hz | 500Hz | 1kHz | 2kHz | 4kHz | 8kHz | 16kHz |
X | 36.8 | 48.3 | 63.7 | 72.9 | 71 | 77.7 | 75.5 | 69.7 | 59.8 |
AD | 43.7 | 50.7 | 55.9 | 57.9 | 57.8 | 64.7 | 66.7 | 64.1 | 52 |
54 | 36.9 | 43.5 | 52.4 | 55.3 | 59.2 | 66.9 | 65.3 | 58.3 | 38.8 |
55 | 37.2 | 43.8 | 49.2 | 52.2 | 53.9 | 61.2 | 60.9 | 48.6 | 28.4 |
56 | 36.3 | 43.6 | 51.2 | 55.7 | 57.9 | 67.2 | 66.9 | 57.1 | 41.6 |
57 | 37.9 | 46 | 55.7 | 59.6 | 61 | 63.8 | 64.3 | 54 | 37.7 |
58 | 38 | 41.5 | 53.2 | 59.4 | 60.6 | 67 | 68.7 | 58.5 | 49.6 |
59 | 36.4 | 46.4 | 54.1 | 57.3 | 58.8 | 65 | 65.8 | 62.4 | 49.3 |
对比例/实施例编号 | 表层A | 连接层B | 隔离层C | 总厚度μm | 隔离层厚度μm |
AE | LDPE-2 | MAH-g-EVA-2 | 共聚PA-1 | 86 | 9.6(**) |
AF | EVA-1/ADD-1(95%/5%) | MAH-g-EVA-2 | 共聚PA-1 | 75 | 10.0 |
60 | PCP-2/ITP-4/ADD-1(46%/46%/8%) | MAH-g-EVA-2 | 共聚PA-1 | 75 | 7.5 |
61 | PCP-2/ITP-4/ADD-1(46%/46%/8%) | MAH-g-EVA-2 | 共聚PA-1 | 75 | 9.0 |
对比例/实施例编号 | 63Hz | 125Hz | 250Hz | 500Hz | 1kHz | 2kHz | 4kHz | 8kHz | 16kHz |
AE | 51.8 | 56.3 | 66.4 | 76.5 | 77.3 | 78.6 | 75.4 | 72.6 | 66.2 |
AF | 42.5 | 54.1 | 66.7 | 70.7 | 74.6 | 76.6 | 76.7 | 75.2 | 65.8 |
60 | 36.0 | 39.5 | 50.5 | 52.7 | 55.8 | 64.4 | 61.8 | 56.1 | 42.3 |
61 | 38.9 | 44.6 | 58.0 | 60.0 | 63.7 | 73.3 | 70.6 | 68.3 | 54.9 |
最大TanΔ | 选择温度下的TanΔ值 | 选择温度下的储能模量G′(10E-5N/cm2) | ||||||||||||||
树脂 | ℃ | 值 | -20℃ | -10℃ | 0℃ | 10℃ | 20℃ | 30℃ | 40℃ | -20℃ | -10℃ | 0℃ | 10℃ | 20℃ | 30℃ | 40℃ |
PP | 2.2 | 0.46 | 0.03 | 0.068 | 0.43 | 0.313 | 0.16 | 0.125 | 0.13 | 1.10E+10 | 1.01E+10 | 4.20E+09 | 8.18E+08 | 4.70E+08 | 3.60E+08 | 2.40E+08 |
PCP-1 | 1.6 | 0.41 | 0.028 | 0.074 | 0.395 | 0.291 | 0.167 | 0.12 | 0.115 | 1.12E+10 | 9.91E+90 | 3.24E+09 | 8.91E+08 | 5.34E+08 | 3.97E+08 | 2.97E+08 |
PCP-2 | 1.5 | 0.59 | 0.033 | 0.099 | 0.575 | 0.366 | 0.186 | 0.134 | 0.137 | 1.05E+10 | 8.94E+09 | 1.89E+09 | 4.01E+08 | 2.41E+08 | 1.74E+08 | 1.27E+08 |
PCP-3 | 0.2 | 0.64 | 0.037 | 0.14 | 0.644 | 0.349 | 0.178 | 0.135 | 0.137 | 1.08E+10 | 8.50E+09 | 1.41E+09 | 3.27E+08 | 2.05E+08 | 1.58E+08 | 1.23E+08 |
EVA-4 | -19 | 0.28 | 0.27 | 0.249 | 0.21 | 0.154 | 0.08 | 0.053 | 0.06 | 1.20E+09 | 4.82E+08 | 2.50E+08 | 1.56E+08 | 1.20E+08 | 9.25E+07 | 5.70E+07 |
ITP-4 | -15-01 | 0.19 | 0.19 | 0.19 | 0.19 | 0.168 | 0.12 | 0.072 | 0.05 | 1.45E+9 | 8.87E+8 | 5.71E+08 | 3.99E+08 | 2.92E+08 | 2.33E+08 | 1.72E+08 |
LDPE-2 | 63 | 0.23 | 0.08 | 0.092 | 0.01 | 0.11 | 0.13 | 0.14 | 0.17 | 4.68E+09 | 3.53E+09 | 2.70E+09 | 2.10E+09 | 1.57E+09 | 1.18E+09 | 8.11E+08 |
EMA | -21.6 | 0.317 | 0.312 | 0.24 | 0.189 | 0.123 | 0.066 | 0.049 | 0.053 | 8.60E+08 | 3.66E+08 | 2.17E+08 | 1.40E+08 | 1.08E+08 | 9.00E+07 | 6.45E+07 |
PP-EPDM | -21 | 0.305 | 0.3 | 0.218 | 0.165 | 0.122 | 0.077 | 0.066 | 0.078 | 2.91E+08 | 1.32E+08 | 8.22E+07 | 5.38E+07 | 4.11E+07 | 3.46E+07 | 2.55E+07 |
EVA-1 | -151 | 0.20 | 0.197 | 0.20 | 0.192 | 0.188 | 0.158 | 0.10 | 0.06 | 1.98E+09 | 1.90E+09 | 5.80E+08 | 3.57E+08 | 2.47E+08 | 1.85E+08 | 1.50E+08 |
EVA-2 | -18.5 | 0.23 | 0.23 | 0.217 | 0.21 | 0.189 | 0.125 | 0.071 | 0.06 | 1.70E+09 | 8.18E+08 | 4.54E+08 | 2.81E+08 | 1.97E+08 | 1.47E+08 | 9.68E+07 |
实施例编号 | 表层A | 连接层B | 隔离层C | 总厚度μm | 隔离层厚度μm | 膜/膜的密封强度(N/25mm) | 膜/LDPE的密封强度(N/25mm) |
50 | PCP-1/ADD-1/(96/4%) | MAH-g-EVA-2 | PET-G | 70 | 8.3 | 14.5 | 1.1 |
57 | PCP-1/PCP-2/ADD-1(72/24/4%) | MAH-g-EVA-2 | PET-G | 77 | 10 | 10.4 | 1.5 |
51 | PCP-1/ITP-4/ADD-1(48/48/4%) | MAH-g-EVA-2 | PET-G | 78 | 6.9 | 17.0 | 13.9 |
62 | PCP-1/ITP-4/ADD-1(46/46/8%) | EVA-3 | PET-G | 80 | 7.0 | 22.3 | 18.7 |
63 | PCP-2/ITP-4/ADD-1(69/23/8%) | EVA-3 | PET-G | 75 | 6.0 | 18.0 | 17.2 |
64 | PCP-2/ITP-4/ITP-1/ADD-1/ADD-4/ADD-3/ADD-2(46/21.3/21.2/6/3.5/2%) | EVA-3 | PET-G | 80 | 6.0 | 21.4 | 没测定 |
65 | PCP-2/ITP-4/ULDPE-3/ADD-1/ADD-4/ADD-3/ADD-2(46/21.3/21.2/6/3.5/2%) | EVA-3 | PET-G | 75 | 6.0 | 20.2 | 没测定 |
66 | PCP-2/ITP-3/ULDPE-3/ADD-1/ADD-4/ADD-3/ADD-2(46/10.6/31.9/6/3.5/2%) | EVA-3 | PET-G | 81 | 7.0 | 19.6 | 没测定 |
67 | PCP-2/ITP-2/ULDPE-1/ADD-1/ADD-4/ADD-3/ADD-24420(46/19.1/23.4/6/3.5/2%) | EVA-3 | PET-G | 75 | 7.0 | 21.1 | 没测定 |
68 | PCP-2/ITP-3/ULDPE-2/ADD-1/ADD-4/ADD-3/ADD-2(46/17/25.5/6/3.5/2%) | EVA-3 | PET-G | 74 | 8.0 | 20.4 | 没测定 |
实施例编号 | 表层A | 连接层B | 隔离层C | 总厚度μm | 隔离层厚度μm | 膜/膜的密封强度(N/25mm,MD) |
69 | PCP-2/ITP-4/ADD-1(46/46/8%) | EMA | PET-G | 75 | 7.5 | 23.7 |
实施例编号 | 表层A | 连接层B | 隔离层C |
70 | PCP-2/ITP-2/ULDPE-1/ADD-1(46/19.2/23.3/11.5%)41.3μm | EVA-3,7.5μm | PET-G,10.4μm |
71 | PCP-2/ITP-2/ULDPE-1/ADD-1(46/19.2/23.3/11.5%)39.6μm | EVA-3,7.5μm | PET-G/APE-1,(70/30)9.9μm |
72 | PCP-2/ITP-2/ULDPE-1/ADD-1(46/21.2/25.8/7%)38.9μm | MAH-g-EVA-2/ADD-1(98/2%),7.5μm | PET-G/APE-1,(50/50)4.5μm |
73 | PCP-2/ITP-2/ULDPE-1/ADD-1(46/21.2/25.8/7%)40.8μm | EVA-3,7.5μm | PET-G/APE-1,(50/50)6.7μm |
频率(Hz) | 与实施例对应的噪音(dBA) | ||||
70 | 71 | 72 | 73 | 74 | |
63 | 23.7 | 24.0 | 25.1 | 25.2 | 30.4 |
80 | 29.2 | 28.5 | 20.2 | 21.0 | 22.8 |
100 | 22.5 | 22.7 | 22.5 | 24.5 | 25.2 |
125 | 26.7 | 26.9 | 27.8 | 29.8 | 28.6 |
160 | 32.7 | 32.7 | 33.7 | 35.7 | 33.9 |
200 | 39.0 | 38.6 | 38.8 | 41.1 | 36.7 |
250 | 43.0 | 42.0 | 42.7 | 43.8 | 38.2 |
315 | 45.3 | 43.4 | 45.2 | 45.2 | 38.6 |
400 | 46.6 | 46.2 | 45.9 | 45.8 | 40.5 |
500 | 46.3 | 46.2 | 45.8 | 46.0 | 41.2 |
630 | 45.0 | 44.3 | 44.7 | 45.6 | 40.7 |
800 | 44.3 | 43.8 | 44.2 | 45.3 | 40.2 |
1000 | 44.7 | 43.7 | 44.2 | 44.9 | 39.2 |
1250 | 44.9 | 44.1 | 44.1 | 45.9 | 39.2 |
1600 | 45.9 | 44.9 | 45.6 | 47.7 | 40.7 |
2000 | 51.7 | 50.4 | 52.1 | 54.1 | 46.1 |
2500 | 50.0 | 50.1 | 50.3 | 52.4 | 47.1 |
3150 | 43.6 | 45.1 | 45.1 | 45.8 | 42.7 |
4000 | 40.2 | 42.1 | 43.0 | 42.7 | 39.9 |
5000 | 40.2 | 42.1 | 43.0 | 43.0 | 36.3 |
6300 | 38.3 | 39.5 | 39.8 | 39.2 | 31.7 |
8000 | 32.9 | 37.4 | 34.7 | 36.8 | 30.0 |
10000 | 27.6 | 32.2 | 27.9 | 26.8 | 26.0 |
12500 | 21.9 | 27.3 | 20.8 | 21.2 | 18.2 |
16000 | 16.1 | 21.3 | 8.9 | 13.5 | 7.6 |
化合物 | 测试* | 单位 | 实施例70 | 实施例71 | 实施例72 | 实施例73 |
H2S | 透过性 | Cm3/m2-天 | 23.6 | 8.8 | 5.9 | 4.9 |
H2S | B.T. | 秒 | 455 | 575 | 695 | 1010 |
DEDS | B.T. | 分钟 | 194 | 270 | 151 | 179 |
3-甲基吲哚 | B.T. | 小时 | 100 | 45 | 110 | 120 |
测试 | 实施例70 | 实施例71 | 实施例72 | 实施例73 | 对比例A | 对比例D |
断裂伸长MD(%) | 328 | 330 | 293 | 443 | 450 | 465 |
断裂伸长TD(%) | 350 | 369 | 449 | 485 | 483 | 533 |
断裂应力MD(MPa) | 19.5 | 19.6 | 18.8 | 21.7 | 25.1 | 18.0 |
断裂应力TD(MPa) | 16.2 | 17.3 | 15.4 | 17.5 | 17.2 | 14.3 |
1%割线模量TD(MPa) | 250 | 292 | 223 | 149 | 170 | 120 |
1%割线模量MD(MPa) | 210 | 285 | 218 | 148 | 160 | 120 |
膜/膜密封强度MD(N/25mm) | 没测定 | 没测定 | 22.3 | 没测定 | 27.7 | 21.3 |
Claims (10)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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US14174499P | 1999-06-30 | 1999-06-30 | |
US60/141,744 | 1999-06-30 |
Publications (2)
Publication Number | Publication Date |
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CN1365373A CN1365373A (zh) | 2002-08-21 |
CN1308378C true CN1308378C (zh) | 2007-04-04 |
Family
ID=22497033
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CNB008098247A Expired - Fee Related CN1308378C (zh) | 1999-06-30 | 2000-06-29 | 基本上无定形的非氯化聚合物隔离膜 |
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US (2) | US6455161B1 (zh) |
EP (1) | EP1196482B1 (zh) |
JP (2) | JP2003503572A (zh) |
KR (1) | KR100720845B1 (zh) |
CN (1) | CN1308378C (zh) |
AT (1) | ATE384093T1 (zh) |
AU (1) | AU774358B2 (zh) |
BR (1) | BR0012459B1 (zh) |
CA (1) | CA2377235A1 (zh) |
CZ (1) | CZ20014670A3 (zh) |
DE (1) | DE60037812T2 (zh) |
DK (1) | DK1196482T3 (zh) |
MX (1) | MXPA01013389A (zh) |
PL (1) | PL352904A1 (zh) |
TW (1) | TW553982B (zh) |
WO (1) | WO2001000716A2 (zh) |
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- 2000-06-28 US US09/605,496 patent/US6455161B1/en not_active Expired - Lifetime
- 2000-06-29 JP JP2001506723A patent/JP2003503572A/ja not_active Withdrawn
- 2000-06-29 CN CNB008098247A patent/CN1308378C/zh not_active Expired - Fee Related
- 2000-06-29 AU AU57793/00A patent/AU774358B2/en not_active Ceased
- 2000-06-29 MX MXPA01013389A patent/MXPA01013389A/es active IP Right Grant
- 2000-06-29 CA CA002377235A patent/CA2377235A1/en not_active Abandoned
- 2000-06-29 DE DE60037812T patent/DE60037812T2/de not_active Expired - Lifetime
- 2000-06-29 BR BRPI0012459-1A patent/BR0012459B1/pt not_active IP Right Cessation
- 2000-06-29 WO PCT/US2000/017945 patent/WO2001000716A2/en active IP Right Grant
- 2000-06-29 DK DK00943303T patent/DK1196482T3/da active
- 2000-06-29 EP EP00943303A patent/EP1196482B1/en not_active Expired - Lifetime
- 2000-06-29 KR KR1020017016886A patent/KR100720845B1/ko not_active IP Right Cessation
- 2000-06-29 AT AT00943303T patent/ATE384093T1/de not_active IP Right Cessation
- 2000-06-29 CZ CZ20014670A patent/CZ20014670A3/cs unknown
- 2000-06-29 PL PL00352904A patent/PL352904A1/xx unknown
- 2000-07-12 TW TW089112869A patent/TW553982B/zh not_active IP Right Cessation
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2002
- 2002-09-20 US US10/251,356 patent/US6620474B1/en not_active Expired - Lifetime
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2011
- 2011-03-16 JP JP2011058223A patent/JP5385327B2/ja not_active Expired - Fee Related
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Also Published As
Publication number | Publication date |
---|---|
JP2003503572A (ja) | 2003-01-28 |
KR20020022735A (ko) | 2002-03-27 |
BR0012459A (pt) | 2002-03-26 |
EP1196482A2 (en) | 2002-04-17 |
BR0012459B1 (pt) | 2010-11-03 |
CN1365373A (zh) | 2002-08-21 |
WO2001000716A2 (en) | 2001-01-04 |
AU5779300A (en) | 2001-01-31 |
MXPA01013389A (es) | 2002-07-02 |
WO2001000716A3 (en) | 2001-05-31 |
CZ20014670A3 (cs) | 2002-07-17 |
DE60037812D1 (de) | 2008-03-06 |
ATE384093T1 (de) | 2008-02-15 |
JP5385327B2 (ja) | 2014-01-08 |
CA2377235A1 (en) | 2001-01-04 |
PL352904A1 (en) | 2003-09-22 |
JP2011174072A (ja) | 2011-09-08 |
DE60037812T2 (de) | 2009-01-02 |
US6455161B1 (en) | 2002-09-24 |
US6620474B1 (en) | 2003-09-16 |
DK1196482T3 (da) | 2008-07-07 |
AU774358B2 (en) | 2004-06-24 |
TW553982B (en) | 2003-09-21 |
KR100720845B1 (ko) | 2007-05-25 |
EP1196482B1 (en) | 2008-01-16 |
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