CN1306926C - Bathing liquid composition and its preparing method - Google Patents

Bathing liquid composition and its preparing method Download PDF

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Publication number
CN1306926C
CN1306926C CNB2005100336352A CN200510033635A CN1306926C CN 1306926 C CN1306926 C CN 1306926C CN B2005100336352 A CNB2005100336352 A CN B2005100336352A CN 200510033635 A CN200510033635 A CN 200510033635A CN 1306926 C CN1306926 C CN 1306926C
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liquid composition
bath foam
gross weight
content
extract
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CN1682690A (en
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黄恒燊
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Abstract

The present invention relates to a bathing liquid composition and a preparation method thereof. The bathing liquid contains chitosan. The bathing liquid composition of the present invention has the advantages of few manufacturing devices and simple technology. A prepared product has the advantages of mild property and abundant foam. After the present invention is used, the skin is clean and does not feel dry or unsmooth. The present invention has the functions of sterilization, itching relieving, inflammation relieving and anaphylaxis resistance. Long term use of the present invention has the effects of promoting metabolism and enhancing the vitality of a body.

Description

Bathing liquid composition and preparation method thereof
Technical field
The present invention relates to a kind of bathing liquid composition and preparation method thereof.
Background technology
Along with the raising of people's living standard, to improved also corresponding of quality of cosmetics especially bath foam with effect.The alkalescence of existing soap base type bath foam product is strong, bathes the back skin ph value and raises, and produces and tightens sense, causes easily that skin is dry and astringent, coarse, pruritus etc.Development trend along with naturalization of cosmetics, nutrient laden and curative effectization, with the animals and plants extract and the natural nutriment that have no side effect, have curative effect and Nutrition is functional component, with the bath foam of soap base and other surfactant compounds, more and more be subjected to the favor of consumer.
Adding in the market the plant extraction liquid that added in the shower product of plant extract be the higher mixture of impurity content, therefore, at these is in the bath foam of primary raw material with the plant extract, the addition of plant extract must account for very at high proportion, just can manifest effect, and the nutrition of these bath foam and curative effect effect are not remarkable yet.So the cost height, effect is low.
Chinese patent publication number CN1524515A discloses a kind of natural bath foam of plant essence that extracts the flavonoid material that contains from the rutaceae leaf, and this bath foam has effects such as sterilization, antipruritic, antiinflammatory, antiallergic.But prepare this bath foam complex process, and be added with antiseptic, be not easy to promote.
Summary of the invention
For the bathing liquid composition that overcomes prior art can not solve that poor efficiency is expensive, manufacturing process is complicated, add problem such as antiseptic and a kind of bathing liquid composition and preparation method thereof is provided.
For solving the problems of the technologies described above, technical scheme of the present invention is, comprises that content is that the carboxymethyl chitosan of bath foam gross weight 0.5~10%, extract Oleum Hippophae and the content of desert plant Fructus Hippophae that content is bath foam gross weight 5~20% are the Aloe extract of bath foam gross weight 5~25%.
Described Aloe extract is at least a to be concentrated Folium Aloe juice or Aloe gel concentrated juice.
Described bathing liquid composition also contains the penetration enhancer laurocapram, and its content is 0.1~1.0% of bath foam gross weight.
The surfactant of described bathing liquid composition selects for use in soap base, dodecyl sodium sulfate, fatty alcohol-ether sodium sulfate and the polyoxyethylenated alcohol sodium sulfate one or more for the first type surface activating agent; With in coconut monoethanolamide, cocoanut oil diethan olamide and the cocamidopropyl betaine one or more is auxilliary surfactant.
Described bathing liquid composition is pearling agent with the polyethylene glycol stearate diester, and the PH regulator is a citric acid.
Another kind of technical scheme of the present invention is: a kind of bathing liquid composition, it contains the first type surface activating agent, auxilliary surfactant, pearling agent, chitosan, Oleum Hippophae, Fructus Hippophae extract and penetration enhancer, the preparation method of this bathing liquid composition may further comprise the steps: in proportion the first type surface activating agent is added in the deionized water in mixing kettle, be stirred and heated to 75~80 ℃, dissolving fully, add auxilliary surfactant and pearling agent again, constant temperature stirring and emulsifying 40~90 minutes, stop heating after the emulsifying fully, continue to stir and be cooled to 40~70 ℃, add chitosan, Fructus Hippophae extract and penetration enhancer, reuse NaCl and citric acid are regulated viscosity and pH value, sampling and testing after stirring requires pH value 6.5~7.5, and viscosity is 6000~8000mPas, continue to stir and add essence when being cooled to 30~60 ℃, stir, deposit appearance stablity after, sampling detects can use or pack after qualified.
Described chitosan is a carboxymethyl chitosan, and its content is 0.5~10% of bath foam gross weight, and the content of Fructus Hippophae extract is 5~20% of bath foam gross weight.
The invention has the beneficial effects as follows: contain chitosan in the bath foam of the present invention, it has moisture absorbability and moisture retentivity, low price, have outstanding water solublity, stability, the water-retaining property of preserving moisture, film property, conditioning, gelling, emulsibility, thickening property, emollient, hair strengthening and antibiotic property, nontoxic, have no side effect, biodegradable, it is ideal water-soluble high-molecular compound in the cosmetics, chitosan can be used as antiseptic, and the bath foam that has therefore added carboxymethyl chitosan does not need to add other chemical preservatives.
Also containing Oleum Hippophae in the bath foam of the present invention, is the complex of multivitamin and bioactive substance.It can nourishes rough skin, enhances metabolism, and antiallergic, bactericidal antiphlogistic promote epithelial tissue regeneration, and skin is had repair, can keep the sour environment of skin, have stronger permeability, and is safe in utilization, have no side effect.
Also contain Aloe in the bath foam of the present invention, its have well preserve moisture, go speckle, whiten, anti-inflammatory analgetic, effect such as sun-proof.
In addition, contain laurocapram in the bathing liquid composition of the present invention, be a kind of new and effective safe osmotic absorption promoter, has good lubricity, can promote that nutritional labeling is permeated in the activity of hydrophilic and lipophilic medicament goods or the cosmetics in skin, the result of use of remarkable medicament curative effect enhancement and cosmetics, therefore can reduce the consumption of principal agent, reduced production cost, and laurocapram has no side effect, the skin residual quantity is low, and nutritional labeling was prolonged in the time of staying of human body skin, reaches preserving moisture of high-efficient and lasting, nourishes rough skin, antiallergic, bactericidal antiphlogistic and anti-ultraviolet effect.
It is few that bathing liquid composition of the present invention is made equipment needed thereby, and technology is simple.Obtained properties of product gentleness, foam is abundant, and is salubrious with back skin, and no sensation of dryness, and have sterilization, antipruritic, antiinflammatory anti-allergic effects, life-time service have and enhance metabolism the effect of enhancing physical vigor.
The specific embodiment
Bath foam of the present invention contains kinds of surface activating agent, suds booster, viscosifier, PH regulator, essence, deionized water, biological elite.Wherein, biological elite comprises the chitosan that is made by marine organisms, extract Oleum Hippophae and the Aloe extract of desert plant Fructus Hippophae.
The chitosan that described marine organisms make is a carboxymethyl chitosan, and its content is 0.5~10% of bath foam gross weight.
Fructus Hippophae extract is an Oleum Hippophae, and its content is 5~20% of bath foam gross weight.
Aloe extract is at least a to be concentrated Folium Aloe juice or Aloe gel concentrated juice, and its content is 5~25% of bath foam gross weight.
This bath foam also contains a kind of efficient penetration enhancer---laurocapram, and its content is 0.1~1.0% of bath foam gross weight.
Carboxymethyl chitosan is by the product after the chitosan carboxy methylation, is a kind of water soluble polymer, have the moisture absorbability and moisture retentivity similar to hyaluronic acid, but low price is a lot.Carboxymethyl chitosan has outstanding water solublity, stability, the water-retaining property of preserving moisture, film property, conditioning, gelling, emulsibility, thickening property, emollient, hair strengthening and antibiotic property, nontoxic, have no side effect, biodegradable, it is ideal water-soluble high-molecular compound in the cosmetics, chitosan can be used as antiseptic, and the bath foam that has therefore added carboxymethyl chitosan does not need to add other chemical preservatives.
Oleum Hippophae is the complex of multivitamin and bioactive substance.Its energy nourishes rough skin enhances metabolism, and antiallergic, bactericidal antiphlogistic promote epithelial tissue regeneration, and skin is had repair, can keep the sour environment of skin, have stronger permeability, become one of beauty and skin care product preferred raw materials in recent years.Cosmetic mede from sand bramble is safe in utilization, have no side effect, and favored by common people.
Preserve moisture, go speckle because of Aloe has well, whiten, anti-inflammatory analgetic, effect such as sun-proof, and its distinctive safety makes it obtain to use widely at cosmetic field.The Aloe cosmetics are directly to use Aloe extract to carry out processing and fabricating, contain abundant active aloe composition in the Aloe original juice, the state that has kept to maximum its pure natural, product can embody ideally that Aloe contains to skin high-quality preserve moisture, antiinflammatory, moisten, the result of anti-ultraviolet.With emulsifying and the non-emulsive cosmetics that Aloe is made, have the very wicked external world and rheological property, can reflect the distinguished quality of Aloe cosmetics truly.
Laurocapram is called for short azone, chemistry 1-positive dodecyl aza cyclohepta ketone by name-2-ketone, be a kind of new and effective safe osmotic absorption promoter, effect obviously is better than penetration enhancer dimethyl sulfoxide (DMSO), dimethyl formamide (DMF) and the dimethyl acetylamide (DMAc) used always.Laurocapram is the colorless and odorless transparency liquid, water insoluble, form emulsion with water, be soluble in various organic solvents, have very wicked lubricity, can promote that nutritional labeling is permeated in the activity of hydrophilic and lipophilic medicament goods or the cosmetics in skin, the remarkable result of use of medicament curative effect enhancement and cosmetics, so can reduce the consumption of principal agent, reduced production cost, and laurocapram has no side effect, and the skin residual quantity is low.The present invention is exactly the short osmotic absorption effect that utilizes laurocapram, allow human epidermal absorb nutritional labeling in Oleum Hippophae and the Aloe extract fast, nutritional labeling was prolonged in time of staying of human body skin, reach the preserving moisture of high-efficient and lasting, nourishes rough skin, antiallergic, bactericidal antiphlogistic and anti-ultraviolet effect.
Aspect surfactant, selecting soap base, dodecyl sodium sulfate, fatty alcohol-ether sodium sulfate and polyoxyethylenated alcohol sodium sulfate for use is the first type surface activating agent, and its weight percentage can be 10~30%; With coconut monoethanolamide, cocoanut oil diethan olamide and cocamidopropyl betaine is auxilliary surfactant, play foam enhancing, surely steep and tackify, and just said suds booster and viscosifier, its weight percentage can be 5~15%.With the polyethylene glycol stearate diester is pearling agent, gives product with pearl effect.The PH regulator is a citric acid.
The production procedure of the bath foam of a kind of matters of containing biological activities of the present invention is as follows:
In mixing kettle, in proportion the first type surface activating agent is added in the deionized water, be stirred and heated to 75~80 ℃, dissolving fully, add auxilliary surfactant and pearling agent again, constant temperature stirring and emulsifying 40~90 minutes, stop heating after the emulsifying fully, continue stirring and be cooled to 60 ℃, add carboxymethyl chitosan, Oleum Hippophae, Fructus Hippophae extract and efficient penetration enhancer, reuse NaCl and citric acid are regulated viscosity and pH value, sampling and testing after stirring requires pH value 6.5~7.5, and viscosity is 6000~8000mPas, continue to stir and add essence when being cooled to 40 ℃, stir, deposit appearance stablity after, sampling detects can use or pack after qualified.It is few that product of the present invention is made equipment needed thereby, and technology is simple.
Provide three example products with three prescriptions (by weight percentage) below
Composition Prescription 1 Prescription 2 Prescription 3
CMC Seabuckthorn Oil concentrated Folium Aloe juice aloe gel soap base dodecyl sodium sulfate fatty alcohol-ether sodium sulfate sodium sulfate of polyethenoxy ether of fatty alcohol coconut monoethanolamide coconut acid diethanolamide cocamidopropyl betaine polyethylene glycol stearate diester citric acid azone NaCl spices deionized water 1.0 15 5.0 10 4.0 8.0 6.0 2.0 3.0 1.5 4.5 2.0 0.3 0.2 1.0 0.4 36.1 3.0 5.0 10 8.0 4.0 10 5.0 3.0 2.0 2.0 5.0 2.0 0.5 0.5 1.5 0.5 3 8 5.0 10 12 10 4.0 6.0 6.0 2.0 2.0 1.5 6.5 2.0 0.4 0.2 0.5 0.4 31.5
To fill a prescription by preceding method and 1~3 to make bath foam.Obtained properties of product gentleness, foam is abundant, and is salubrious with back skin, and no sensation of dryness, and have sterilization, antipruritic, antiinflammatory anti-allergic effects, life-time service have and enhance metabolism the effect of enhancing physical vigor.

Claims (7)

1, a kind of Mu Yu Ye Group compound, it comprises that content is that the carboxymethyl chitosan of bath foam gross weight 0.5~10%, extract Oleum Hippophae and the content of desert plant Fructus Hippophae that content is bath foam gross weight 5~20% are the Aloe extract of bath foam gross weight 5~25%.
2, Mu Yu Ye Group compound as claimed in claim 1 is characterized in that: described Aloe extract is at least a to be concentrated Folium Aloe juice or Aloe gel concentrated juice.
3, Mu Yu Ye Group compound as claimed in claim 1, it is characterized in that: described bathing liquid composition also contains the penetration enhancer laurocapram, and its content is 0.1~1.0% of bath foam gross weight.
4, Mu Yu Ye Group compound as claimed in claim 1 is characterized in that: the surfactant of described bathing liquid composition with one or more the mixture in soap base, dodecyl sodium sulfate, fatty alcohol-ether sodium sulfate and the polyoxyethylenated alcohol sodium sulfate as the first type surface activating agent; With one or more the mixture in coconut monoethanolamide, cocoanut oil diethan olamide and the cocamidopropyl betaine as auxilliary surfactant.
5, Mu Yu Ye Group compound as claimed in claim 1, it is characterized in that: described bathing liquid composition is pearling agent with the polyethylene glycol stearate diester, the pH regulator agent is a citric acid.
6, a kind of Mu Yu Ye Group compound, it contains the first type surface activating agent, auxilliary surfactant, pearling agent, chitosan, Oleum Hippophae, Fructus Hippophae extract and penetration enhancer, the preparation method of this bathing liquid composition may further comprise the steps: in proportion the first type surface activating agent is added in the deionized water in mixing kettle, be stirred and heated to 75~80 ℃, dissolving fully, add auxilliary surfactant and pearling agent again, constant temperature stirring and emulsifying 40~90 minutes, stop heating after the emulsifying fully, continue to stir and be cooled to 40~70 ℃, add chitosan, Fructus Hippophae extract and penetration enhancer, reuse NaCl and citric acid are regulated viscosity and pH value, sampling and testing after stirring requires pH value 6.5~7.5, and viscosity is 6000~8000mPas, continue to stir and add essence when being cooled to 30~60 ℃, stir, deposit appearance stablity after, sampling detects can use or pack after qualified.
7, the preparation method of bathing liquid composition as claimed in claim 6 is characterized in that: described chitosan is a carboxymethyl chitosan, and its content is 0.5~10% of bath foam gross weight, and the content of Fructus Hippophae extract is 5~20% of bath foam gross weight.
CNB2005100336352A 2005-03-11 2005-03-11 Bathing liquid composition and its preparing method Expired - Fee Related CN1306926C (en)

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Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102908283A (en) * 2012-11-20 2013-02-06 陈永娟 Seabuckthorn face cream
CN102908284A (en) * 2012-11-21 2013-02-06 安文娟 Composition for facial mask
CN103893027A (en) * 2012-12-25 2014-07-02 青岛海芬海洋生物科技有限公司 Shower gel containing marine biological ingredient and preparing method thereof
CN103720615B (en) * 2013-12-20 2015-11-25 韩后化妆品有限公司 A kind of betaplex gentle cleansing milk
CN104095768B (en) * 2014-07-16 2016-05-18 福建广和堂生物科技有限公司 A kind of faintly acid antibacterial bath liquor containing aurantiin and preparation method thereof
CN104188865A (en) * 2014-09-09 2014-12-10 青岛润鑫伟业科贸有限公司 Bath foam capable of preserving moisture and relieving itching
CN105748355A (en) * 2016-03-10 2016-07-13 蚌埠团结日用化学有限公司 Chinese herbal medicine shower gel and preparation method thereof
CN105796417A (en) * 2016-03-22 2016-07-27 广东嘉丹婷日用品有限公司 Chlorine-removing anti-allergic skin care composition
CN106176380A (en) * 2016-08-11 2016-12-07 王君 A kind of enzyme natural ecological bath lotion
CN110946809A (en) * 2018-09-26 2020-04-03 台山美环健芦荟制品有限公司 Non-irritant aloe bath lotion
CN110946806A (en) * 2018-09-26 2020-04-03 台山美环健芦荟制品有限公司 Non-irritant aloe bath foam

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JP2000169327A (en) * 1998-12-03 2000-06-20 Pias Arise Kk Low irritant preparation for external use for skin and bathing agent
WO2001047626A1 (en) * 1999-12-23 2001-07-05 Henkel Kommanditgesellschaft Auf Aktien Dyed chitosan capsules
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CN1513438A (en) * 2003-08-08 2004-07-21 新疆奥斯曼生物科技有限公司 Qiamuwuer shower cream, and its prepn. method
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Patent Citations (7)

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Publication number Priority date Publication date Assignee Title
JP2000169327A (en) * 1998-12-03 2000-06-20 Pias Arise Kk Low irritant preparation for external use for skin and bathing agent
CN1347302A (en) * 1999-03-12 2002-05-01 生物技术公司 Cosmetic preparations
WO2001047626A1 (en) * 1999-12-23 2001-07-05 Henkel Kommanditgesellschaft Auf Aktien Dyed chitosan capsules
CN1468297A (en) * 2000-10-06 2004-01-14 �׿��ر���˹��(Ӣ��)���޹�˾ Cleaning compositions containing chitosan
US20030091612A1 (en) * 2001-11-06 2003-05-15 Subramaniam Sabesan Antimicrobial polyolefin articles and methods for their preparation
CN1513438A (en) * 2003-08-08 2004-07-21 新疆奥斯曼生物科技有限公司 Qiamuwuer shower cream, and its prepn. method
CN1524515A (en) * 2003-09-17 2004-09-01 李慧娟 Natural plant distillate bath lotion

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甲壳素/壳聚糖及其衍生物的开发与应用进展 周友亚,河北师范大学学报(自然科学版),第2卷第26期 2002 *

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