CN116332621A - Wine storage device capable of promoting wine aging and preparation method thereof - Google Patents
Wine storage device capable of promoting wine aging and preparation method thereof Download PDFInfo
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- CN116332621A CN116332621A CN202310070592.3A CN202310070592A CN116332621A CN 116332621 A CN116332621 A CN 116332621A CN 202310070592 A CN202310070592 A CN 202310070592A CN 116332621 A CN116332621 A CN 116332621A
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Classifications
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- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/13—Compounding ingredients
- C04B33/131—Inorganic additives
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/52—Multiple coating or impregnating multiple coating or impregnating with the same composition or with compositions only differing in the concentration of the constituents, is classified as single coating or impregnation
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/89—Coating or impregnation for obtaining at least two superposed coatings having different compositions
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- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/327—Iron group oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3272—Iron oxides or oxide forming salts thereof, e.g. hematite, magnetite
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6562—Heating rate
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
- C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
- C04B2235/6565—Cooling rate
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/70—Aspects relating to sintered or melt-casted ceramic products
- C04B2235/96—Properties of ceramic products, e.g. mechanical properties such as strength, toughness, wear resistance
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
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- Manufacturing & Machinery (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
A wine storage device capable of promoting wine aging and a preparation method thereof are provided, wherein the blank material consists of clay, limonite-containing hydrorock, germanium mineral powder, attapulgite and tourmaline; the wine storage device capable of promoting wine aging can promote wine aging and optimize wine quality, and the result shows that when the wine is placed in the wine storage device for about 20 minutes, the wine becomes soft and the fragrance is multiplied, and the principle is that part of ethanol in the wine is rapidly converted into ester substances such as ethyl caproate, ethyl lactate and the like which increase the fragrance of wine under the action of various metal particles in the wine storage device. The wine storage device capable of promoting wine aging adopts the blank material which contains various microelements and mineral matters required by human body, and in the contact with wine, the microelements are separated and dissolved into the wine to become nutrient substances required by the body of drinkers, such as microelements of calcium, iron, germanium, strontium, silicon, molybdenum and the like, so that the white wine without microelements is converted into various microelements which are rich in the human body.
Description
Technical Field
The invention relates to the technical field of wine reservoirs and inorganic materials, in particular to a wine reservoir capable of promoting wine aging and a preparation method thereof.
Background
The wine storage can be made of various materials, such as glass containers, crystal bottles, simulated crystal bottles, ceramic bottles, stainless steel products or natural materials such as cucurbits, but has single performance, and only the wine containing equipment has no influence on the quality of the wine. In addition, some imitation crystal bottles or crystal bottles contain lead, so that lead pollution can be generated after long-term storage of wine, and the health of people is affected.
The newly brewed white spirit, ethanol and water are in a separation state, the ethanol has strong sensory stimulation to the oral cavity of a drinker, and has heavy spicy taste and poor mouthfeel, so that the white spirit needs to be aged after being brewed, and the ageing treatment can improve the softness of the alcoholic beverage and improve the mouthfeel; in addition, when the prior wine beverage is stored, the component of the wine is not improved greatly, the wine can only play a role of a container, the component and substance conversion of the wine is not greatly assisted, and the quality of the wine can not be improved.
Disclosure of Invention
In order to solve the problems, the invention aims to provide a wine storage device capable of promoting wine aging and a preparation method thereof.
The invention aims to achieve the aim, and the aim is achieved by the following technical scheme:
the wine storage device capable of promoting wine aging comprises the following raw materials in parts by weight: 95-105 parts of clay, 45-55 parts of limonite-containing water rock, 8-12 parts of germanium mineral powder, 8-12 parts of attapulgite and 25-35 parts of tourmaline.
Preferably, the weight ratio of limonite in the limonite-containing water rock is 15-25%.
Preferably, the germanium content in the germanium ore powder is 5-10%.
The invention also comprises a preparation method of the wine storage device capable of promoting wine aging, comprising the following steps:
(1) roasting 95-105 parts of clay, 45-55 parts of limonite-containing water rock, 8-12 parts of germanium mineral powder and 25-35 parts of tourmaline at 800-1100 ℃ for 30-45 minutes, then adding water into the clay, washing 3-4 times, filtering, sieving the clay by a 1200-mesh sieve, adding 8-12 parts of attapulgite into the clay, and uniformly mixing to obtain slurry;
(2) placing the slurry obtained in the step (1) in a gypsum mold, continuously shaking the mold to uniformly distribute slurry in the mold, adsorbing the moisture of the slurry by the gypsum mold, and taking down the mold when the moisture of the slurry reaches 15-25%, so as to obtain a wet blank;
(3) airing the wet blank at 40-45 ℃ until the moisture reaches 5-7%, putting the wet blank into a kiln for roasting, heating the wet blank to 1250-1300 ℃ for roasting for 24-48 hours, and cooling the wet blank to 25-35 ℃ to obtain a semi-finished wine storage device;
(4) the semi-finished wine storage Shi Na glaze and the outer glaze are put into a kiln and baked for 8 to 16 hours at 800 to 850 ℃ to obtain the wine storage capable of promoting the aging of wine; wherein the inner glaze is environment-friendly glaze, and the outer glaze is colored glaze.
The inner glaze adopts the conventional inner glaze material (silicon oxide, aluminum oxide, potassium oxide, sodium oxide, calcium oxide, magnesium oxide, ferric oxide or titanium oxide) as a main body, and limonite-containing hydrorock and tourmaline are added in the technology; the inner glaze material comprises the following components in parts by weight: 66-75 parts of conventional inner glaze material, 15-35 parts of limonite-containing hydrorock and 10-40 parts of tourmaline.
The inner glaze material can be placed on the inner wall of a ceramic wine storage device or a stainless steel wine storage device, and can play a role in promoting white spirit aging.
The external glaze material adopted by the invention can be added with a certain amount of raw materials (the raw materials comprise, by weight, 95-105 parts of clay, 45-55 parts of limonite-containing hydrorock, 8-12 parts of germanium mineral powder, 8-12 parts of attapulgite and 25-35 parts of tourmaline) in the conventional external glaze component, so that the external glaze material can play a role in promoting ageing for white wine permeation and also play a role in preventing wine leakage of a bottle body; the material can be mixed with conventional ceramic outer glaze, and is coated on the outer surface of a ceramic wine container and is fired frequently, but the outer glaze material does not act on a metal wine container (stainless steel, aluminum and other wine containers). The outer glaze is of various types, taking cobalt-containing sapphire blue outer glaze as an example, and adding 5-15% of the component material; the addition amount is too small, is easy to dilute by the conventional components, cannot play a corresponding role, and the addition amount is too much, so that the appearance of the sapphire blue is influenced.
Preferably, the temperature raising process in step (8) is as follows:
preheating: starting from room temperature in the kiln, and uniformly raising the temperature to 400-450 ℃ within 5 hours;
constant-speed heating stage: the temperature is increased from 400 to 450 ℃ to 1250 to 1300 ℃ at a constant speed, and the temperature increasing rate is 15 to 20 ℃/min.
Preferably, the cooling process in step (8) is as follows:
naturally cooling to 1000 ℃ at 1250-1300 ℃, opening the kiln door, rapidly cooling to 300-250 ℃, closing the kiln door, and naturally cooling to 25-35 ℃.
Compared with the prior art, the invention has the following advantages:
the wine storage device capable of promoting wine aging can promote wine aging, optimize wine quality, and the result shows that when the wine is placed in the wine storage device for about 20 minutes, the wine becomes soft and the fragrance is multiplied, and the principle is that part of ethanol in the wine is rapidly converted into ester substances such as ethyl caproate, ethyl lactate and the like which increase the fragrance of wine under the action of various metal particles in the wine storage device;
the wine storage device capable of promoting wine aging can rapidly improve the taste of the freshly brewed white wine, the combination of the wine is stable after the freshly brewed white wine is placed in the wine storage device for 20 minutes, wine molecules are large, water molecules are small, and the water molecules surround the wine molecules, so that although the alcohol component is not changed, the alcohol cannot directly stimulate the sense in the oral cavity of a person, so that the drinker has soft feeling, reduced pungency and strong palatability; on the other hand, the newly brewed white spirit contains trace impurities such as methanol and formaldehyde, which can affect health and even have serious consequences, and the newly brewed white spirit can adsorb or degrade the impurities such as methanol and acetaldehyde after being placed in a wine storage device, and tests show that after 24 hours of filling the newly brewed white spirit, the methanol content can be reduced by more than 50%, the fusel oil can be reduced by more than 65%, and the alcohol content is unchanged. As the aging process is shortened, the funds turnover of the production enterprises is fast, the storage period is shortened, and the income of the enterprises is increased.
The wine container capable of promoting wine aging provided by the invention adopts the blank material which contains various microelements and mineral matters required by human body, and in the contact with wine, the microelements are separated and dissolved into the wine material to become nutrient substances required by the body of a drinker, such as microelements of calcium, iron, germanium, strontium, silicon, molybdenum and the like, so that the white wine without microelements is converted into various microelements required by the human body, cancer is prevented, positive effects are played for the drinker, and meanwhile, the aging process of the white wine is accelerated and the quality of the wine is optimized due to the action of the microelements.
The wine storage device capable of promoting wine aging can be large or small, can be manufactured into small wine bottles with different capacities, is convenient to carry and sell, can be manufactured into a tank or a jar, and is beneficial to ripening wine bodies; or making into tablet or ball, and placing in large storage tank to promote ripening of wine body for a long time, which can reach several tons to tens tons at a time or more.
Detailed Description
The invention aims to provide a wine storage device capable of promoting wine aging and a preparation method thereof, and the wine storage device is realized by the following technical scheme:
the wine storage device capable of promoting wine aging comprises the following raw materials in parts by weight: 95-105 parts of clay, 45-55 parts of limonite-containing water rock, 8-12 parts of germanium mineral powder, 8-12 parts of attapulgite and 25-35 parts of tourmaline.
Preferably, the weight ratio of limonite in the limonite-containing water rock is 15-25%.
Preferably, the germanium content in the germanium ore powder is 5-10%.
The invention also discloses a preparation method of the wine storage device capable of promoting wine aging, which comprises the following steps:
(1) roasting 95-105 parts of clay, 45-55 parts of limonite-containing water rock, 8-12 parts of germanium mineral powder and 25-35 parts of tourmaline at 800-1100 ℃ for 30-45 minutes to convert calcium bicarbonate in the material into calcium oxide, then adding water into the calcium oxide, washing the calcium oxide for 3-4 times to convert the calcium oxide into calcium hydroxide, filtering the calcium hydroxide, passing through a 1200-mesh sieve, preventing calcium components in larger particles from entering the next process, adding 8-12 parts of attapulgite into the calcium carbonate, and uniformly mixing to obtain slurry;
(2) placing the slurry obtained in the step (1) in a gypsum mold, continuously shaking the mold to uniformly distribute slurry in the mold, adsorbing the moisture of the slurry by the gypsum mold, and taking down the mold when the moisture of the slurry reaches 15-25%, so as to obtain a wet blank;
(3) airing the wet blank at 40-45 ℃ until the moisture reaches 5-7%, putting the wet blank into a kiln for roasting, heating the wet blank to 1250-1300 ℃ for roasting for 24-48 hours, and cooling the wet blank to 25-35 ℃ to obtain a semi-finished wine storage device; the temperature of the air drying cannot be too high, otherwise, the wet blank is easy to crack;
(4) the semi-finished wine storage Shi Na glaze and the outer glaze are put into a kiln and baked for 8 to 16 hours at 800 to 850 ℃ to obtain the wine storage capable of promoting the aging of wine; wherein the inner glaze is environment-friendly glaze, and the outer glaze is colored glaze.
The inner glaze is made of environment-friendly materials which are white, lead-free and other harmful components, is diluted as much as possible, and mainly fills the leakage-proof holes of the bottle wall fully and covers the bottle wall as much as possible; the external glaze can be a bright-colored glaze.
The wine storage device capable of promoting wine aging can be prepared into a bottle, a jar or a pot with the thickness of 0.5-1 cm according to the requirement, or pressed and roasted into a sheet-like object, or made into various shapes such as a ball shape, a triangle shape and the like, and can be placed into the existing wine storage device to play a role in promoting wine aging.
The wine storage device capable of promoting wine aging has the advantages that the cover is tightly matched with the wine storage device main body, so that air leakage, water and alcohol escape are avoided; the material of the cover is the same as that of the wine container.
Preferably, the temperature raising process in step (8) is as follows:
preheating: starting from room temperature in the kiln, and uniformly raising the temperature to 400-450 ℃ within 5 hours;
constant-speed heating stage: the temperature is increased from 400 to 450 ℃ to 1250 to 1300 ℃ at a constant speed, and the temperature increasing rate is 15 to 20 ℃/min.
Preferably, the cooling process in step (8) is as follows: naturally cooling to 1000 ℃ at 1250-1300 ℃, opening the kiln door, rapidly cooling to 300-250 ℃, closing the kiln door, and naturally cooling to 25-35 ℃.
The raw materials adopted by the wine storage device comprise silicon dioxide, aluminum oxide, titanium dioxide, calcium oxide, magnesium oxide, phosphorus trioxide, manganese oxide, potassium oxide, sodium oxide and various metal oxides, and the clay can be mixed with ceramic materials and baked into a wine container by a ceramic process.
The plasticity of clay is the basis of ceramic blank clay forming, and in the technology, the clay contains 40-70 percent of the proportion, and other materials can be organically combined together only when the clay is used as the basis. The clay contains alumina and silica, is white and fireproof, has clay particles smaller than 2 mu m, has strong cohesiveness, and contains quartz, feldspar, mica, sulfate, sulfide, carbonate and other impurities. The clay has suspension property and stability of grouting slurry and glaze, is in the form of finely dispersed particles, and is stable in combination with the clay, so that the formulation dosage is easy to master. The clay particles are small, the specific surface area is large, and the particles are negatively charged, so that the clay particles have strong physical adsorptivity and surface chemistry and have the capability of exchanging with other cations.
The limonite-containing water rock contains 2Fe 2 O 3 ·3H 2 O is an independent mineral product. X-ray diffraction shows that the goethite is a aphanitic goethite, is mixed with hematite, quartz, clay and the like, contains adsorbed water and capillary water, has variable components and is basically FeO (OH) xH 2 O contains various mineral elements and trace elements, and the components of the limonite are slightly different due to different production places, and the limonite is mixed with other components which are washed and silted by water under the action of water, so that water rock is formed under the action of gravity of the water. Although this type of waterstone contains the inner glaze and outer glaze components (mainly aluminum, calcium, etc.) for making ceramics, limonite alone is not useful as a ceramic material (no formability, heavy metals, etc.).
When the wine is stored in a glass bottle, a conventional ceramic bottle, stainless steel or a glass wine storage device, the iron element in the wine body is not increased, and by adopting the wine storage device capable of promoting the aging of the wine, the iron element in the wine bottle can be separated out, and the wine body can be accelerated to age, so that the effect of supplementing iron to the human body is achieved.
The total amount of iron in human body is 4-5 g, most of iron is obtained from diet, the iron exists in the form of hemoglobin about 72%, myoglobin about 3%, other compounds about 0.2%, and iron is reserved in the body with a large proportion, and the iron is sourced from food, so that the iron can be separated out by the wine storage device capable of promoting the aging of wine. Iron is the main component of many enzymes such as superoxide and immune system compounds, is an activator of antioxidant enzymes, and iron deficiency can reduce immunity and anti-infection capability, iron deficiency anemia is one of four recognized nutritional deficiency diseases of world health organization, iron deficiency can cause damage and behavior change of mental activities and intelligence development, and serious capability can be damaged and other various diseases.
Research shows that thrombus is more easily caused by the too low content of blood, and the improvement of the iron content level in the blood is of great significance for preventing the thrombus. Iron has an anti-fatigue effect even in women with normal hemoglobin, and after iron supplementation in the diet, their physical performance, mood and concentration are improved. When the wine storage device of the invention is drunk in proper quantity to ripening white wine, the effect of iron supplement can be achieved.
The copper element in the material adopted by the technology is up to 27 mug/g. Copper has very practical medical application, and medical inventor uses trace elements copper and iron as break-through, so as to successfully prepare anticancer drug "Keai 7851". Copper is about 100-150 mg in human body, the normal value of serum copper is 100 mug/dl-120 mug/dl, and is the second essential trace element in human body, copper is the activator of various enzymes, such as oxygen free radical scavenger-superoxide dismutase (SOD-Cu), tyrosinase, monoamine oxidase, superoxide, hemocopper blue protein and the like, which form melanin, copper activates the formation of hemoglobin, and promotes the absorption and utilization of iron. In the transport of electrons, elastin synthesis, connective tissue metabolism, purine metabolism, phospholipid and nerve tissue formation, have a significant impact on the development and function of the viscera of the blood, central nervous and immune system, hair, skin, skeletal tissue, brain, liver, heart, etc. According to the recommendation of the world health organization, adults should take 2-3 mg of white spirit every day, and the product has the advantage of promoting the ripeness of the white spirit and being suitable for drinking (50 ml is the standard), thereby being beneficial to the overall health of human bodies.
The storage amount of zinc in limonite adopted in the technology is 10.0 mug/g, zinc is one of microelements with more human body requirement, is a composition component of more than 200 zinc-containing enzymes, such as DNA polymerase, alcohol dehydrogenase, glutamate dehydrogenase and the like, and zinc is also an activator of the enzymes. Zinc lipoproteins which are mainly composed of zinc play an important role in nucleic acid metabolism and protein synthesis. Zinc is a judging material for normal or death of main cells and has the capacity of reviving aged thymus cells.
Zinc can promote growth and development of human body, maintain normal appetite of human body, enhance immunity of human body, promote wound healing, influence normal metabolism and vision of vitamin A, and maintain male sexual function and spermatogenic capacity. Mineral elements and trace elements of the ripening white spirit of the product are all extremely increased compared with those of the conventional white spirit. For example, cobalt (Co), manganese (Mn), molybdenum (Mo), vanadium (V), tin (Sn), iodine (I), fluorine (F), chromium (Cr), nickel (Ni) and the like are all important elements for maintaining human health and play an important role in the aging process of white spirit.
Attapulgite is an aqueous magnesium aluminosilicate of the formula (Mg 5 (H 2 O) 4 [Si 4 O 10 ] 2 (OH) 2 ) Is a kind of water-containing magnesia-alumina salt clay sand with a stinky chain layer structure. The attapulgite is widely distributed, can be found in the world, but has small ore deposit ratio with industrial significance, mainly has high reserve of 5 hundred million tons which can be used only in Xuyi province in China, and lays a foundation for project implementation. The attapulgite contains Na + 、Ca 2+ 、Fe 3+ 、Al 3+ The crystal is needle-shaped, fibrous or fiber-gathered, has unique dispersibility, good colloid properties such as high temperature resistance, salt and alkali resistance and the like, adsorption decoloration capability and certain plasticity cohesiveness. In the technology, attapulgite is used as a binder, more importantly, the attapulgite is uniformly distributed in an appliance in the manufacturing process of wine tools, and when the wine tools are sintered, after crystal water and gas in the attapulgite escape, uniform micro-pores are formed, and the micro-pores are favorable for gas permeation and accelerating oxidation of wine bodies and have good effect of promoting aging of the wine.
The surface area of the attapulgite reaches 9.6-36m 2 And/g, good colloid valence and swelling capacity. The attapulgite clay does not contain harmful components to human bodies, can be even used as food additive components, has no pollution to chemical constitution, can inhibit microorganism growth, absorbs toxic volatile components, is environment-friendly, and is heavy metals and carcinogensExhibit extraordinary characteristics.
In the process, the germanium ore powder accounts for 3 percent. The green tyre is heated to 1300 deg.C during the production process, and germanium reacts with oxygen to produce germanium oxide (GeO) 2 ) The germanium component is exposed, showing its nature. Germanium contains five nuclides, and the germanium mineral powder also contains calcium, iron, copper and other components, which are all materials for promoting the aging of wine. After germanium in the wine bottle is separated out and enters the wine body, the wine has positive effects on human body:
the germanium element can remove various fats in the human body so as not to induce various diseases, such as hyperlipidemia, hypertension and the like; germanium is stored in the human body, and can provide sufficient oxygen to keep the human body sufficiently active; preventing anemia, germanium element and iron element, and has effects of correcting anemia and recovering hematopoiesis for preventing and treating iron deficiency anemia, thalassemia or anemia caused by excessive blood cell loss; germanium has targeted attack effect on cancer cells, so that the cancer cells lose protein absorption and die due to lack of nutrition, thereby playing a role in preventing and treating cancers.
Tourmaline is also called tourmaline, and is a general term of tourmaline family, and is a silicate mineral with a ring structure of elements such as aluminum, iron, magnesium, lithium and the like, which are characterized by boron. The tourmaline contains multiple elements, and has unique properties such as piezoelectricity, heat release electricity, conductivity, far infrared radiation property, negative ion release and the like.
The electric effect, ion adsorptivity and the like of tourmaline can be enhanced along with the reduction of the diameter of powder and the increase of the specific surface, and the tourmaline has a series of excellent surface and interface properties, and the larger the specific surface area of the powder is, the higher the specific surface energy is, and the tourmaline is thinned to 1200-4000 meshes and then is mixed with other materials when the tourmaline is applied.
As the tourmaline has permanent and spontaneous electrodes, the generated electrostatic field has adsorption effect on heavy metal ions such as lead ions, zinc ions, cadmium ions and impurities in water, and the white wine is a mixture of water and ethanol, the tourmaline has adsorption and purification effects on the impurities and heavy metals in the wine, and the edible safety of the product and the comprehensive quality of the wine are improved.
Tourmaline is a functional mineral with boron as a characteristic, and when the temperature of the tourmaline is 900 ℃, boron ions, fluorine ions and hydroxyl ions in the molecular structure of the tourmaline volatilize, and the temperature of the tourmaline and other materials made into a glaze material can keep the characteristics of the tourmaline (namely, the low-temperature glazing is 700-900 ℃).
The ceramic wine bottle is prepared by firing at high temperature, has high physical and chemical stability, oxidation resistance, corrosion resistance and long-term storage, and the ceramic has weak permeability and gas permeability, thereby being beneficial to aging of white spirit.
The raw materials adopted by the technology, namely clay, attapulgite, tourmaline powder (ore powder), germanite powder and hydrated rock powder, all contain CaHCO with certain components 3 。CaHCO 3 Can be decomposed into CaO in the sintering process of bottle blanks, and Ca (OH) can be generated when the wall of the bottle body contacts with wine 2 (i.e., slaked lime) can cause holes in the bottle that can make the bottle super-aerated and leak wine, thus the following treatments are needed before making the preform:
(1) High temperature: heating the above materials to 800 deg.C for 1-2 hr, caHCO 3 The decomposition temperature is 700 ℃, and CaHO in the material is obtained at 800 DEG C 3 The decomposition is more thorough.
(2) Immersing the above pyrolysis-decomposed material in water, caHCO 3 Decomposing the generated CaO and water to generate Ca (OH) 2 Is easy to be flushed out by water flow, and most CaHCO is removed in a water flushing mode 3 。
(3) The attapulgite and germanium ore powder which are decomposed at high temperature and washed by water are made into water rock containing brown iron component, and tourmaline powder is further refined by a colloid mill to make the residual CaHCO 3 (also includes Ca (OH) 2 With CO in air 2 Regenerated CaHCO 3 ) Refining to near nanometer level by colloid mill. And (3) preparing bottle blanks from the materials which are passed through a colloid mill according to the components. Due to CaHCO 3 The above treatment has little, if any, residual in the material, and the particle size has become very small by colloid milling, and Ca (OH) is formed with wine at a high Wen Shifen Jie Cheng CaO 2 The particle size is also small (nano-scale or near nano-scale) and is breathable without leaking wine.
After the treatment, the small aperture generated on the bottle body is beneficial to air penetration, so that the wine is oxidized more rapidly, and the aging of the wine is accelerated.
The invention is further described below in connection with specific embodiments.
Example 1
A wine storage device capable of promoting wine aging, wherein the blank consists of the following raw materials: 95kg of clay, 45kg of limonite-containing hydrorock, 8kg of germanium mineral powder, 8kg of attapulgite and 25kg of tourmaline.
Example 2
A wine storage device capable of promoting wine aging, wherein the blank consists of the following raw materials: 105kg of clay, 55kg of limonite-containing hydrorock, 12kg of germanium mineral powder, 12kg of attapulgite and 35kg of tourmaline;
the weight ratio of limonite in the limonite-containing water rock is 22%;
the germanium content in the germanium mineral powder is 8%.
Example 3
A wine storage device capable of promoting wine aging, wherein the blank consists of the following raw materials: 98kg of clay, 48kg of limonite-containing hydrorock, 9kg of germanium mineral powder, 9kg of attapulgite and 28kg of tourmaline;
the weight ratio of limonite in the limonite-containing water rock is 15%;
the germanium content in the germanium mineral powder is 5%.
Example 4
A wine storage device capable of promoting wine aging, wherein the blank consists of the following raw materials: 100kg of clay, 50kg of limonite-containing hydrorock, 9kg of germanium mineral powder, 10kg of attapulgite and 28kg of tourmaline;
the weight ratio of limonite in the limonite-containing water rock is 25%;
the germanium content in the germanium mineral powder is 10%.
Example 5
A wine storage device capable of promoting wine aging, wherein the blank consists of the following raw materials: 102kg of clay, 52kg of limonite-containing hydrorock, 10kg of germanium mineral powder, 11kg of attapulgite and 30kg of tourmaline;
the weight ratio of limonite in the limonite-containing water rock is 20%;
the germanium content in the germanium mineral powder is 9%.
Example 6
The method for manufacturing a wine container for promoting aging of wine according to example 1, comprising the steps of:
(1) roasting 95kg of clay, 45kg of limonite-containing water rock, 8kg of germanium mineral powder and 25kg of tourmaline at 800 ℃ for 30 minutes, then adding water into the mixture, washing the mixture for 3 times, filtering the mixture, passing through a 1200-mesh sieve, adding 8kg of attapulgite into the mixture, and uniformly mixing the mixture to obtain slurry;
(2) placing the slurry obtained in the step (1) in a gypsum mold, continuously shaking the mold to uniformly distribute slurry in the mold, adsorbing the moisture of the slurry by the gypsum mold, and taking down the mold when the moisture of the slurry reaches 15%, so as to obtain a wet blank;
(3) airing the wet blank at 40 ℃ until the moisture reaches 5%, putting the wet blank into a kiln for roasting, heating the wet blank to 1250 ℃ for roasting for 24 hours, and cooling the wet blank to 25 ℃ to obtain a semi-finished wine storage device;
(4) the semi-finished wine storage Shi Na glaze and the outer glaze are put into a kiln and baked for 8 hours at 800 ℃ to obtain the wine storage capable of promoting the aging of wine; wherein the inner glaze is environment-friendly glaze, and the outer glaze is colored glaze;
wherein the composition of the inner glaze is as follows: 2kg of silicon oxide, 2kg of aluminum oxide, 2.6kg of potassium oxide, 1.5kg of limonite-containing hydrorock and 1kg of tourmaline;
the composition of the outer glaze is 2kg of cobalt-containing sapphire outer glaze and 0.1kg of wine storage material capable of promoting wine aging in example 1.
Example 7
The method for producing a wine container for promoting aging of wine according to example 2, comprising the steps of:
(1) roasting 105kg of clay, 55kg of limonite-containing water rock, 12kg of germanium mineral powder and 35kg of tourmaline at 900 ℃ for 45 minutes, then adding water into the mixture, washing the mixture for 4 times, filtering the mixture, passing through a 1200-mesh sieve, adding 12kg of attapulgite into the mixture, and uniformly mixing the mixture to obtain slurry;
(2) placing the slurry obtained in the step (1) in a gypsum mold, continuously shaking the mold to uniformly distribute slurry in the mold, adsorbing the moisture of the slurry by the gypsum mold, and taking down the mold when the moisture of the slurry reaches 25%, so as to obtain a wet blank;
(3) airing the wet blank at 45 ℃ until the moisture reaches 7%, putting the wet blank into a kiln for roasting, heating the wet blank to 1300 ℃ for roasting for 48 hours, and cooling the wet blank to 35 ℃ to obtain a semi-finished wine storage device;
(4) the semi-finished wine storage Shi Na glaze and the outer glaze are then put into a kiln and baked for 16 hours at 850 ℃ to obtain the wine storage capable of promoting the aging of wine; wherein the inner glaze is environment-friendly glaze, and the outer glaze is colored glaze; wherein the composition of the inner glaze is as follows: 2.5kg of sodium oxide, 2.5kg of calcium oxide, 2.5kg of magnesium oxide, 3.5kg of limonite-containing hydrated rock and 4kg of tourmaline;
the composition of the outer glaze is 2kg of cobalt-containing sapphire outer glaze and 0.3kg of wine storage material capable of promoting wine aging in example 2.
Example 8
The method for producing a wine container for promoting aging of wine according to example 3, comprising the steps of:
(1) roasting 98kg of clay, 48kg of limonite-containing water rock, 9kg of germanium mineral powder and 28kg of tourmaline at 1000 ℃ for 40 minutes, then adding water into the mixture, washing the mixture for 3 times, filtering the mixture, passing through a 1200-mesh sieve, adding 9kg of attapulgite into the mixture, and uniformly mixing the mixture to obtain slurry;
(2) placing the slurry obtained in the step (1) in a gypsum mold, continuously shaking the mold to uniformly distribute slurry in the mold, adsorbing the moisture of the slurry by the gypsum mold, and taking down the mold when the moisture of the slurry reaches 15%, so as to obtain a wet blank;
(3) airing the wet blank at 42 ℃ until the moisture reaches 5.5%, putting the wet blank into a kiln for roasting, and starting from room temperature in the kiln, and uniformly heating to 400 ℃ within 5 hours; heating to 1280 ℃ at a constant speed of 15 ℃/min, roasting for 30 hours, naturally cooling to 1000 ℃, opening a kiln door, quickly cooling to 300 ℃, closing the kiln door, and naturally cooling to 28 ℃ to obtain a semi-finished wine storage device;
(4) the semi-finished wine storage Shi Na glaze and the outer glaze are put into a kiln and baked for 10 hours at 820 ℃ to obtain the wine storage capable of promoting the aging of wine; wherein the inner glaze is environment-friendly glaze, and the outer glaze is colored glaze; wherein the composition of the inner glaze is as follows: magnesium oxide, ferric oxide, titanium oxide 7kg, limonite-containing hydrorock 2kg, tourmaline 2kg;
the composition of the outer glaze is 2kg of cobalt-containing sapphire outer glaze and 0.2kg of wine storage material capable of promoting wine aging in example 3.
Example 9
The method for producing a wine container for promoting aging of wine according to example 4, comprising the steps of:
(1) roasting 100kg of clay, 50kg of limonite-containing water rock, 9kg of germanium mineral powder and 28kg of tourmaline at 950 ℃ for 42 minutes, then adding water into the clay, washing for 4 times, filtering, passing through a 1200-mesh sieve, adding 10kg of attapulgite into the clay, and uniformly mixing to obtain slurry;
(2) placing the slurry obtained in the step (1) in a gypsum mold, continuously shaking the mold to uniformly distribute slurry in the mold, adsorbing the moisture of the slurry by the gypsum mold, and taking down the mold when the moisture of the slurry reaches 25%, so as to obtain a wet blank;
(3) airing the wet blank at 42 ℃ until the moisture reaches 6.5%, putting the wet blank into a kiln for roasting, and starting from room temperature in the kiln, and uniformly heating to 450 ℃ within 5 hours; heating to 1270 ℃ at a constant speed of 20 ℃/min, roasting for 36 hours, naturally cooling to 1000 ℃ at 1300 ℃, opening a kiln door, quickly cooling to 250 ℃, closing the kiln door, and naturally cooling to 32 ℃ to obtain a semi-finished wine storage device;
(4) the semi-finished wine storage Shi Na glaze and the outer glaze are put into a kiln and baked for 12 hours at 820 ℃ to obtain the wine storage capable of promoting the aging of wine; wherein the inner glaze is environment-friendly glaze, and the outer glaze is colored glaze;
wherein the inner glaze comprises 2kg of silicon oxide, 2kg of magnesium oxide, 3kg of titanium oxide, 3kg of limonite-containing hydrated rock and 2.5kg of tourmaline;
the composition of the outer glaze is 2kg of cobalt-containing sapphire outer glaze and 0.25kg of wine storage material capable of promoting ageing of wine in example 4.
Example 10
The method for producing a wine container for promoting aging of wine according to example 5, comprising the steps of:
(1) 102kg of clay, 52kg of limonite-containing water rock, 10kg of germanium mineral powder and 30kg of tourmaline are roasted for 40 minutes at 1050 ℃, then water is added into the clay, the clay is washed for 3 times, filtered, and filtered through a 1200-mesh sieve, 11kg of attapulgite is added into the clay, and the clay slurry is obtained after uniform mixing;
(2) placing the slurry obtained in the step (1) in a gypsum mold, continuously shaking the mold to uniformly distribute slurry in the mold, adsorbing the moisture of the slurry by the gypsum mold, and taking down the mold when the moisture of the slurry reaches 15%, so as to obtain a wet blank;
(3) airing the wet blank at 44 ℃ until the moisture is 6%, putting the wet blank into a kiln for roasting, and starting from room temperature in the kiln, and uniformly heating to 420 ℃ within 5 hours; heating to 1280 ℃ at a constant speed of 18 ℃ per minute, roasting for 42 hours, naturally cooling to 1000 ℃ at 1260 ℃, opening a kiln door, quickly cooling to 280 ℃, closing the kiln door, and naturally cooling to 25 ℃ to obtain a semi-finished wine storage device;
(4) the semi-finished wine storage Shi Na glaze and the outer glaze are put into a kiln and baked for 12 hours at 820 ℃ to obtain the wine storage capable of promoting the aging of wine; wherein the inner glaze is environment-friendly glaze, and the outer glaze is colored glaze; wherein the inner glaze comprises 3.5kg of aluminum oxide, 3.5kg of magnesium oxide, 2.5kg of limonite-containing water rock and 2.5kg of tourmaline;
the composition of the outer glaze is 2kg of cobalt-containing sapphire outer glaze and 0.15kg of wine storage material capable of promoting wine aging in example 5.
The raw materials adopted by the invention contain various microelements and mineral elements required by human body, and after the raw materials are contacted with the wine, the elements are separated out and dissolved in the wine to become nutrient substances required by the body of a drinker, and taking microelements in limonite-containing waterstone as an example:
at normal temperature, 100g of limonite-containing waterstone was put into 1000ml of water, the trace element content was measured after 3 hours, the limonite-containing waterstone was prepared into a wine bottle according to the proportion in example 10, and distilled spirit with 52% ethanol content was put into 500ml (the capacity of the wine bottle was 515 ml), and the trace element content was measured after 24 hours, and the results are shown in table 1.
TABLE 1 microelement content table
Microelements | Limonite-containing water rock | Wine storage device capable of promoting ageing of wine |
Calcium | 1100mg | 135mg |
Iron (Fe) | 1600mg | 22mg |
Molybdenum (Mo) | 11.2mg | 1.8mg |
Strontium (strontium) | 22.3mg | 18mg |
Selenium (Se) | 41μg | 14μg |
Lithium ion battery | 160mg | 60mg |
Silicon (Si) | 200mg | 160mg |
Aluminum (Al) | 70mg | 40mg |
Magnesium (Mg) | 180mg | 140mg |
Sodium salt | 35mg | 20mg |
Potassium | 7.8mg | 2.2mg |
Zinc alloy | 75mg | 0.3mg |
Copper (Cu) | 4.5mg | 1.0mg |
Silver (Ag) | 0.1mg | 0.01mg |
Chromium (Cr) | 1.8mg | 0.4mg |
Mercury | 0 | 0 |
As can be seen from the results in Table 1, the components such as calcium, iron, molybdenum, magnesium, silicon and the like in the raw materials can be separated out into the wine body, thereby meeting the requirements of people on essential trace elements.
The white spirit is distilled out from the fermentation raw materials, only the impurities such as ethanol and fusel oil are contained, the nutrient components in the raw materials are not contained, and after the wine storage device is used, various microelements are separated out, so that the white spirit is rich in various microelements required by human bodies and plays a positive role for drinkers: germanium has anticancer effect, and germanium and iron are combined to form good blood replenishing preparation, and can promote multiple health functions of human body. Copper has close beneficial effects on human hematopoietic function; copper plays a critical role in the conversion of ferrous iron to ferric iron in the process of human iron participating in the formation of hemoglobin. If copper is deficient in human body, the oxidation activity of ceruloplasmin of blood plasma is reduced, so that the change of the value of iron is difficult, and anemia symptoms of human body are caused. The oxidation resistance of human body is related to copper in vivo, copper-containing proteins in vivo, such as metallothionein and copper-zinc superoxide dismutase, have strong oxidation resistance, can remove oxygen free radicals, and copper has positive effects in removing oxygen free radicals in human body and metabolic wastes, and has a certain relationship in avoiding tumor generation and slowing down atherosclerosis. The wine storage device (bottle) of the technology has the advantages that precipitated copper is proper, and the defect that too much copper element is generated and negative influence is generated on human body is avoided.
In order to detect the aging effect of the wine storage device capable of promoting the aging of the wine, the following experiment is carried out: the wine container (500 ml) obtained in example 5 of the present invention was filled with Maotai-flavor liquor produced in a certain winery in Guizhou, and aged at room temperature for 20 minutes, 40 minutes and 60 minutes, and physical and chemical properties thereof were measured, and the results are shown in Table 2.
TABLE 2 physicochemical detection results of aged white spirit
As can be seen from the results of Table 2, the wine container for promoting aging of wine of the present invention has a large change in 20 minutes after the wine sample is placed therein, little increase in beneficial components occurs after 60 minutes, and the decrease in harmful components (acetaldehyde, acetal, isopropyl alcohol, etc.) is remarkable. Heavy metals (arsenic, lead, mercury, cadmium, etc.) were detected to be zero after the present container was aged for one hour. The wine storage device capable of promoting wine aging has positive effects on promoting wine aging, obviously adsorbs harmful components in wine bodies, improves the safety standard of wine eating, increases the flavor of wine, and improves the flavor of wine.
And carrying out sensory evaluation on the white spirit, wherein sensory evaluation staff are professional testers with abundant experience, and a blind evaluation mode is adopted. The result shows that the white spirit which is not subjected to ageing has a relatively sharp smell, is not obvious in gas color, is hot in mouth feel and is poor in taste; after aging for 20 minutes, the wine has soft smell, fresh and cool gas color, reduced pungent taste in mouth and strong palatability.
Claims (6)
1. A wine storage device capable of promoting wine aging, which is characterized in that: the blank consists of the following raw materials in parts by weight: 95-105 parts of clay, 45-55 parts of limonite-containing water rock, 8-12 parts of germanium mineral powder, 8-12 parts of attapulgite and 25-35 parts of tourmaline.
2. The wine container for promoting aging of wine according to claim 1, wherein: the weight ratio of limonite in the limonite-containing water rock is 15-25%.
3. The wine container for promoting aging of wine according to claim 1, wherein: the germanium content in the germanium mineral powder is 5-10%.
4. The method for preparing a wine container for promoting aging of wine according to claim 1, wherein: the method comprises the following steps:
(1) roasting 95-105 parts of clay, 45-55 parts of limonite-containing water rock, 8-12 parts of germanium mineral powder and 25-35 parts of tourmaline at 800-1100 ℃ for 30-45 minutes, then adding water into the clay, washing 3-4 times, filtering, sieving the clay by a 1200-mesh sieve, adding 8-12 parts of attapulgite into the clay, and uniformly mixing to obtain slurry;
(2) placing the slurry obtained in the step (1) in a gypsum mold, continuously shaking the mold to uniformly distribute slurry in the mold, adsorbing the moisture of the slurry by the gypsum mold, and taking down the mold when the moisture of the slurry reaches 15-25%, so as to obtain a wet blank;
(3) airing the wet blank at 40-45 ℃ until the moisture reaches 5-7%, putting the wet blank into a kiln for roasting, heating the wet blank to 1250-1300 ℃ for roasting for 24-48 hours, and cooling the wet blank to 25-35 ℃ to obtain a semi-finished wine storage device;
(4) the semi-finished wine storage Shi Na glaze and the outer glaze are put into a kiln and baked for 8 to 16 hours at 800 to 850 ℃ to obtain the wine storage capable of promoting the aging of wine; wherein the inner glaze is environment-friendly glaze, and the outer glaze is colored glaze.
5. The method for producing a wine container for promoting aging of wine according to claim 4, wherein: the temperature rising process in the step (8) is as follows:
preheating: starting from room temperature in the kiln, and uniformly raising the temperature to 400-450 ℃ within 5 hours;
constant-speed heating stage: the temperature is increased from 400 to 450 ℃ to 1250 to 1300 ℃ at a constant speed, and the temperature increasing rate is 15 to 20 ℃/min.
6. The method for producing a wine container for promoting aging of wine according to claim 4, wherein: the cooling process in step (8) is as follows:
naturally cooling to 1000 ℃ at 1250-1300 ℃, opening the kiln door, rapidly cooling to 300-250 ℃, closing the kiln door, and naturally cooling to 25-35 ℃.
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CN104556978A (en) * | 2014-12-24 | 2015-04-29 | 唐山立雄峰汇材料科技有限公司 | Functional ceramic wine set |
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CN105110778A (en) * | 2015-07-22 | 2015-12-02 | 唐山立雄峰汇材料科技有限公司 | Beer mate ceramic ball |
CN105777063A (en) * | 2016-01-13 | 2016-07-20 | 唐山立雄峰汇材料科技有限公司 | Natural energy Baijiu cup |
CN106430972A (en) * | 2016-09-30 | 2017-02-22 | 董爱凤 | Ceramic glaze for ceramic vessel |
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KR20050036061A (en) * | 2003-10-15 | 2005-04-20 | 김규종 | Liquor enclosed with material to activate water and its aging method |
CN104556978A (en) * | 2014-12-24 | 2015-04-29 | 唐山立雄峰汇材料科技有限公司 | Functional ceramic wine set |
CN104496419A (en) * | 2015-01-13 | 2015-04-08 | 唐山立雄峰汇材料科技有限公司 | Ceramic white spirit bottle for accelerating aging |
CN105036719A (en) * | 2015-07-22 | 2015-11-11 | 唐山立雄峰汇材料科技有限公司 | Accompanying ceramic ball for Baijiu |
CN105110778A (en) * | 2015-07-22 | 2015-12-02 | 唐山立雄峰汇材料科技有限公司 | Beer mate ceramic ball |
CN105084863A (en) * | 2015-08-02 | 2015-11-25 | 唐山立雄峰汇材料科技有限公司 | Ceramic liquor activation and distribution device |
CN105777063A (en) * | 2016-01-13 | 2016-07-20 | 唐山立雄峰汇材料科技有限公司 | Natural energy Baijiu cup |
CN106430972A (en) * | 2016-09-30 | 2017-02-22 | 董爱凤 | Ceramic glaze for ceramic vessel |
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