CN1154466C - Composition of hair cosmetics - Google Patents

Composition of hair cosmetics Download PDF

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Publication number
CN1154466C
CN1154466C CNB991270762A CN99127076A CN1154466C CN 1154466 C CN1154466 C CN 1154466C CN B991270762 A CNB991270762 A CN B991270762A CN 99127076 A CN99127076 A CN 99127076A CN 1154466 C CN1154466 C CN 1154466C
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Prior art keywords
hair
composition
hair cosmetics
expression
acid
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Expired - Fee Related
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CNB991270762A
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Chinese (zh)
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CN1258494A (en
Inventor
��߾û�
田边久辉
长瀬忍
四分一敬
新井贤二
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Kao Corp
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Kao Corp
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/41—Amines
    • A61K8/416—Quaternary ammonium compounds
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/362—Polycarboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/36—Carboxylic acids; Salts or anhydrides thereof
    • A61K8/368—Carboxylic acids; Salts or anhydrides thereof with carboxyl groups directly bound to carbon atoms of aromatic rings
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
    • A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q5/00—Preparations for care of the hair
    • A61Q5/12—Preparations containing hair conditioners

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Emergency Medicine (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

This invention relates to a hair cosmetic composition, which comprises (A) glycine or alanine, (B) an alpha -hydroxy acid, beta -hydroxy acid, 1,2-dicarboxylic acid, 1,3-dicarboxylic acid or aromatic carboxylic acid, and (C) a cationic surfactant. The hair cosmetic composition is excellent in the effect of improving optical or mechanical properties of hair.

Description

Composition of hair cosmetics
The present invention relates to a kind of aspect optics that improves hair and engineering properties fabulous composition of hair cosmetics.
The various composition of hair cosmetics that contain cationic surfactant used a lot of years, and they are in order to the optics that improves hair and engineering properties for example gloss, flexibility, quality etc.The effect of these composition of hair cosmetics or temporary transient or not enough.
JP 10-236927A discloses a kind of hair-treatment composition that the associating lipid fatty acid (lipofatty) of hair is offered the hair vesicle, wherein added: the first fatty acid precursor that (i) is selected from leucine, isoleucine, methionine or valine, (ii) be selected from saccharide or single-, two-or the tricarboxylic second fatty acid precursor and (iii) a kind of anion, both sexes or cationic surfactant.Yet this invention gains enlightenment from said components (i) and this fact of lipid fatty acid precursor effect of (ii) being used from the associating of hair follicle, hair and forms.Therefore, can not predict, should add what component for optics or the engineering properties of improving hair from this invention.
Therefore, the purpose of this invention is to provide a kind of aspect optics that improves hair and engineering properties fabulous composition of hair cosmetics.
The inventor has been found that: glycine or alanine and a kind of specific acid compound and cationic surfactant are used in combination, can obtain aspect optics that improves hair and engineering properties for example at fabulous composition of hair cosmetics in aspect such as gloss, flexibility, quality.
Therefore, the invention provides a kind of composition of hair cosmetics, it contains: (A) glycine or alanine, (B) malic acid, succinic acid and maleic acid and (C) a kind of cationic surfactant.
The component (A) that is used for the present invention is glycine or alanine.In the middle of them, particularly preferably be glycine and α-Bing Ansuan.
As component (A), can use glycine and alanine in combination.Consider from giving hair dark colour angle, by composition total weight, can be preferably with 0.01-20%, more preferably 0.05-10%, most preferably the ratio of 0.1-5% adds component (A).
As component (B), can use one or more of above-mentioned acid.Consider from the angle of giving the hair transparency, by composition total weight, can be preferably with 0.01-5%, more preferably 0.05-3%, most preferably the ratio of 0.1-2% adds component (B).
As the cationic surfactant of component (C) can be in the present invention, for example, by the quaternary ammonium salt of facial (1) expression down:
Figure C9912707600041
R wherein 1, R 2, R 3And R 4At least one expression alkyl or alkenyl; it can randomly be replaced and have altogether 8-28 carbon atom by one or more alkoxyls, alkene oxygen base, alkanoylamino, enoyl-amino; remaining one or more benzyl, the alkyl with 1-5 carbon atom or hydroxy alkyl or total addition molal quantity represented independently of one another is not more than 10 polyoxyethylene groups, Z -Represent a halide ion or organic anion.
In such quaternary ammonium salt, preferably by those of formula (1) expression, R wherein 1, R 2, R 3And R 41 or 2 expressions have the straight or branched alkyl of 12-24 carbon atom, perhaps benzyl, remaining represents methyl, Z independently of one another -The expression halide ion; Especially preferably by those of formula (1) expression, R wherein 1, R 2, R 3And R 4An expression have the straight or branched alkyl of 12-22 carbon atom, remaining represents methyl, Z independently of one another -The expression halide ion.
These cationic surfactants can use alone or in combination.Consider from the angle of giving hair soft, by composition total weight, can be preferably with 0.1-20%, more preferably 0.2-10%, most preferably the ratio of 0.5-5% adds this cationic surfactant.
Can also in composition of hair cosmetics of the present invention, add (D) a kind of higher alcohol.This higher alcohol can further improve the sense of touch of hair.
The example of higher alcohol is those alcohol with 6-30 carbon atom, and those alcohol with 8-22 carbon atom are preferred.In addition, not to be higher than those alcohol of 55 ℃ be preferred to fusing point.
Such higher alcohol can use alone or in combination.The ratio that adds this higher alcohol be the cationic surfactant that adds as component (C) the 3-10 mole doubly, preferred 4-8 mole is doubly.
In composition of hair cosmetics of the present invention, can also add (E) a kind of siloxanes.This siloxanes can provide no greasy feeling to hair.
The preferred example of this siloxanes is the methyl polysiloxane by following formula (2) expression:
Figure C9912707600051
R wherein 5The expression methyl or phenyl, R 6Expression methyl or hydroxyl, m represents the number of 100-2000.
These siloxanes can use alone or in combination.By composition total weight, preferably with 0.01-10%, more preferably 0.05-10%, most preferably the ratio of 0.1-5% adds this siloxanes.
Except above-mentioned component, can also in compositions of the present invention, add the surfactant except above-mentioned surfactant as required, cationic polymer, cosmetics oil, dyestuff, Reducing agent, oxidant, metal-chelator, antioxidant, viscosity improver, antiseptic, animal-and plant extract, antiinflammatory, disinfectant, dandruff removing agent, oxidation retarder, pearling agent, UV absorbent, pH regulator agent, colorant, solvent, spice etc.
The pH of composition of hair cosmetics of the present invention can preferably not be higher than the pKa of used 'alpha '-hydroxy acids (B), and can be in the scope of 2-6, and pH2.5-3.5 is particularly preferred.
Composition of hair cosmetics of the present invention can prepare with usual way, and can be used as, for example, and hair irrigation, conditioner, inorganic agent, hair frost, hair cover agent (pack) or analog.
Embodiment 1
Respective components by mixing is shown in Table 1 prepares conditioner, and evaluates outward appearance, flexibility/quality, handlability and the sense of touch of hair when using shampoo.In every kind of evaluation, use infiltration (permed) and hair sample bleaching.The result also lists in table 1.
(assessment method)
Behind a few bundle hairs of commercially available shampoo (" Lavenus Cleansing Shampoo ", trade name, the product of Kao Corp.) washing (its every bundle 20cm is long and 10g is heavy), each conditioner with every part of 3g is applied to this bundle of hair respectively.This bundle of hair is through after 30 minutes, with 40 ℃ warm water washing.After drying, compare according to following evaluation criteria and untreated bundle of hair by panel of expert, evaluate these bundle of hair.
The outward appearance of＜hair 〉
Gloss and color are dark, high transparent and luminous+1 point
Can not agree or bad 0 point
Tarnish, color are not full, and be opaque ,-1 point
And it is dry and lax
According to always counting of all members of panel of expert, each sample obtains+4 or higher being rated as " A ", each sample obtains+3 to-3 be rated as " B ", each sample obtains or lower being rated as " C " at-4.
＜flexibility/quality 〉
Soft and have enough elastic+1 point
Silk quality sense of touch and good quality
Can not agree or bad 0 point
The difference quality and do not have silk quality sense of touch-1 point
According to always counting of all members of panel of expert, each sample obtains+4 or higher being rated as " A ", each sample obtains+3 to-3 be rated as " B ", each sample obtains or lower being rated as " C " at-4.
＜handlability 〉
Handle well, do not have hair to give a tongue-lashing and draw+1 point
Can not agree or bad 0 point
Can not handle, hair is given a tongue-lashing and is drawn-1 point
According to always counting of all members of panel of expert, each sample obtains+4 or higher being rated as " A ", each sample obtains+3 to-3 be rated as " B ", each sample obtains or lower being rated as " C " at-4.
＜sense of touch 〉
Silk quality sense of touch+1 point
Can not agree or bad 0 point
There is not silk quality sense of touch-1 point
According to always counting of all members of panel of expert, each sample obtains+4 or higher being rated as " A ", each sample obtains+3 to-3 be rated as " B ", each sample obtains or lower being rated as " C " at-4.
Table 1
Component (wt.%) Product of the present invention Comparative product
1 2 3 4 5 6 7 1 2 3
Stearyl trimethyl ammonium chloride two (hexadecane base) alkyl dimethyl ammonium chloride mountain base trimethyl ammonium chloride hexadecane alcohol glycine alanine benzene formic acid maleic acid butanedioic acid pH adjusting agent (HCl) spice water 1.0 3.0 1.0 0.5 0.5 surpluses 1.0 3.0 1.0 0.5 0.5 surpluses 1.0 3.0 1.0 0.5 0.5 surpluses 1.0 1.0 0.5 0.5 surpluses 0.5 0.5 3.0 1.0 0.5 0.5 surpluses 1.0 3.0 2.0 0.5 0.5 surpluses 1.0 3.0 1.0 0.5 0.5 surpluses 1.0 3.0 an amount of 0.5 surpluses 1.0 3.0 an amount of 0.5 surpluses 1.0 3.0 0.5 an amount of 0.5 surpluses
pH 3.3 3. 3.3 3.3 3.3 3.3 3.3 5.5 5.5 5.0
Hair outward appearance flexibility/quality hair handlability sense of touch A C A A A C A A A C A A A C A B A C A A A C A A A A A A C B C C C A C B B B B B
Embodiment 2
Prepare conditioner (product 8-14 of the present invention with the method that is similar to product 1-7 of the present invention among the embodiment 1; PH3.3), exception is that the ratio with 1% weight adds methyl polysiloxane (" KF96A 5000cs ", trade name in addition; Shin-Etsu Chemical Co., the product of Ltd.).
To the conditioner that obtains like this, evaluate the outward appearance of its hair, flexibility/quality, hair handlability and sense of touch.Product 8-14 of the present invention has all provided the result similar with embodiment 1.In addition, use the method similar,, also evaluated their no greasy according to following evaluation criteria with embodiment 1.
The no greasy of＜hair 〉
No greasy+1 point
Can not agree or bad 0 point
Greasy-1 point is arranged
According to always counting of all members of panel of expert, each sample obtains+4 or higher being rated as " A ", each sample obtains+3 to-3 be rated as " B ", each sample obtains or lower being rated as " C " at-4.
As a result, product 8-14 of the present invention is being rated as " A " aspect the no greasy of hair.
Embodiment 3
Inorganic agent (pH3.5) with surface compositions under the methods known in the art preparation:
(component) (% weight)
Mountain Yu base trimethyl ammonium chloride 2.0
Cetyl (cetaryl) alcohol 5.0
Glycine 1.0
Malic acid 0.5
Methyl p-Hydroxybenzoate (paraben) 0.1
Spice 0.5
Water surplus
Embodiment 4
Conditioning foam (pH3.5) with surface compositions under the methods known in the art preparation:
(component) (% weight)
Mountain Yu base trimethyl ammonium chloride 0.3
Cetyl (cetaryl) alcohol 1.0
Glycine 1.0
Malic acid 0.5
Methyl p-Hydroxybenzoate 0.1
Spice 0.5
LPG 10.0
Water surplus
Embodiment 5
Suppurative mastitis (pH3.0) with surface compositions under the methods known in the art preparation:
(component) (% weight)
Mountain Yu base trimethyl ammonium chloride 1.5
PEG-20 Arlacel-60 0.5
Cetyl (cetaryl) alcohol 3.0
Liquid paraffin 5.0
PEG-3 2-ethylhexoate 2.5
Glycine 1.0
Malic acid 0.5
Spice 0.5
Hydroxypropyl cellulose (1% solution, viscosity: 6Pas) 0.3
Water surplus
The composition of hair cosmetics that obtains in embodiment 3-5 is all given the good gloss of hair, flexibility and quality, and has improved the handlability of hair.
Composition of hair cosmetics of the present invention has fabulous cleansing power and can improve the optics and the engineering properties of hair significantly.They give hair dark colour, the transparency and luminous gloss.Transparently also give the quality that hair soft is become reconciled, cause the handlability of having improved hair.

Claims (4)

1, a kind of composition of hair cosmetics, it contains: (A) 0.01-20 weight % glycine or alanine, (B) 0.01-5 weight % malic acid, succinic acid or maleic acid and (C) 0.1-20 weight % cationic surfactant.
2, according to the composition of hair cosmetics of claim 1, wherein said cationic surfactant (C) is the quaternary ammonium salt of following formula (1) expression:
Wherein
R 1, R 2, R 3And R 4An expression have the straight or branched alkyl of 12-22 carbon atom, remaining represents methyl, Z independently of one another -The expression halide ion.
3, according to the composition of hair cosmetics of claim 1 or 2, it also contains the alcohol of (D) a kind of 6-30 carbon atom, its ratio be described component (C) the 3-10 mole doubly.
4, according to the composition of hair cosmetics of claim 1 or 2, it also contains (E) a kind of siloxanes.
CNB991270762A 1998-12-28 1999-12-28 Composition of hair cosmetics Expired - Fee Related CN1154466C (en)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP374708/1998 1998-12-28
JP37470898 1998-12-28
JP01749299A JP3208381B2 (en) 1998-12-28 1999-01-26 Hair cosmetics
JP017492/1999 1999-01-26

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CN1258494A CN1258494A (en) 2000-07-05
CN1154466C true CN1154466C (en) 2004-06-23

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US (1) US6358502B1 (en)
EP (1) EP1016402B1 (en)
JP (1) JP3208381B2 (en)
CN (1) CN1154466C (en)
DE (1) DE69933191T2 (en)
TW (1) TW585781B (en)

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EP1016402B1 (en) 2006-09-13
CN1258494A (en) 2000-07-05
EP1016402A3 (en) 2003-09-17
JP2000247841A (en) 2000-09-12
US6358502B1 (en) 2002-03-19
EP1016402A2 (en) 2000-07-05
DE69933191T2 (en) 2007-08-23
TW585781B (en) 2004-05-01
DE69933191D1 (en) 2006-10-26

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