CN115340796A - 一种转锈固锈防水涂料及其制备方法 - Google Patents
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Abstract
本发明公开了一种转锈固锈防水涂料，其特征在于，包括如下质量份数的组分：纯丙乳液70‑80份，焦性没食子酸2‑10份，铵盐分散剂0.1‑0.3份，成膜助剂4.2‑4.8份，纳米氧化锌0.1‑0.3份，亚硝酸钠0.3‑0.6份，基材润湿剂0.1‑0.3份，磷酸0.1‑1份，消泡剂0.1‑0.3份，杀菌防腐剂0.1‑0.3份，锂基膨润土0.1‑0.3份，憎水剂0.5‑1份，去离子水9.4‑11份。本发明还提供了一种转锈固锈防水涂料的制备方法。本发明的涂料具有良好的转锈固锈防水性能。
Description
技术领域
本发明涉及一种转锈固锈防水涂料及其制备方法，属于涂料技术领域。
背景技术
目前对于生铁锈的基材通常采用打磨和涂刷防锈底漆的方法来处理，也有涂刷转锈剂或固锈剂的。打磨再刷防锈底漆工序繁杂，成本高。涂刷普通转锈剂转锈效果可以，但没有加固的作用，耐水也差，转锈好仍需要打磨下。刷固锈剂仅仅是把铁锈密封在里面，时间长了还是会慢慢返锈。
针对上述工序繁杂，转锈效果差等缺点，本发明通过纯丙树脂，焦性没食子酸和磷酸，复配各种助剂，有效解决了转锈差，抗冲击差，附着力差，耐水差等问题。
发明内容
为解决上述问题，本发明提供一种转锈固锈防水涂料，其组成包括如下质量份的组分：纯丙乳液70-80份，焦性没食子酸2-10份，铵盐分散剂0.1-0.3 份，成膜助剂4.2-4.8份，纳米氧化锌0.1-0.3份，亚硝酸钠0.3-0.6份，基材润湿剂0.1-0.3份，磷酸0.1-1份，消泡剂0.1-0.3份，杀菌防腐剂0.1-0.3份，锂基膨润土0.1-0.3份，憎水剂0.5-1份，去离子水9.4-11份。
优选地，所述成膜助剂包括醇酯十二；所述润湿剂包括磺化琥珀酸二辛酯钠盐类；所述消泡剂包括矿物油类；所述杀菌防腐剂包括卡松类；所述憎水剂包括有机硅类。
本发明还提供一种转锈固锈防水涂料的制备方法，其具体步骤包括：
步骤1，添加纯丙乳液，开启高速分散机；
步骤2，添加成膜助剂和消泡剂，进行分散；
步骤3，添加去离子水和杀菌防腐剂，继续分散；
步骤4，添加焦性没食子酸，继续分散；
步骤5，添加铵盐分散剂和纳米氧化锌，继续分散；
步骤6，添加基材润湿剂和亚硝酸钠，继续分散；
步骤7，添加锂基膨润土，继续分散；
步骤8，添加磷酸，继续分散；
步骤9，添加憎水剂，继续分散，制得所述转锈固锈防水涂料。
优选地，所述步骤1-9中，高速分散机的转速为400-600r/min。
优选地，所述步骤1-9中，每一步的分散时间为2-30min。
在所述组分中，各组分的主要作用为：
纯丙乳液：可提高耐候性，成膜后具有加固基材作用，还有透气不透水功能；焦性没食子酸：把铁锈转化成稳定的螯合物；铵盐分散剂：分散，提高耐水性；成膜助剂：促进本发明产品成膜；纳米氧化锌：提高与基材的附着力，同时也有抗菌作用；亚硝酸钠：起到阻锈的作用；基材润湿剂：降低表面张力，对光泽度有一定帮助；磷酸：腐蚀铁锈，同时调整本产品PH，酸性环境更加稳定；消泡剂：消除气泡，增加光泽度；杀菌防腐剂：杀菌，有利于储存稳定；锂基膨润土：提高悬浮性，抗沉淀，改善施工；憎水剂：提高耐水性。
与现有技术相比，首先本发明配方里引用纯丙乳液，极大提高耐候性和耐水性，其次本配方引入焦性没食子酸和磷酸的组合，转锈能力比没食子酸和单宁酸效果都要好；再次，本发明选用了纳米氧化锌和亚硝酸钠，前者可以促进乳液交联增强对基材的附着力，增加干燥时间，后者可以抗闪锈，可促进乳液交联，这样就做到了转锈固锈效果好，优异耐水性等优点的转锈固锈防水涂料。
具体实施方式
结合下面实施例对本发明进行进一步的阐述，但本发明的保护范围并不限于此。
实施例1
一种转锈固锈防水涂料，其组成包括如下质量份数的组分：纯丙乳液72份，焦性没食子酸9份，铵盐分散剂0.3份，成膜助剂4.2份，纳米氧化锌0.2份，亚硝酸钠0.5份，基材润湿剂0.2份，磷酸1份，消泡剂0.1份，杀菌防腐剂0.3 份，锂基膨润土0.3份，憎水剂1份，去离子水10.9份。
本发明还提供一种转锈固锈防水涂料的制备方法，其具体步骤包括：
步骤1，添加纯丙乳液，开启高速分散机，转速400-600r/min；
步骤2，添加成膜助剂和消泡剂，分散15min；
步骤3，添加去离子水和杀菌防腐剂，其中卡松类杀菌防腐剂与水1:1稀释后缓慢添加，继续分散5min；
步骤4，添加焦性没食子酸，分散10min；
步骤5，添加铵盐分散剂和纳米氧化锌，缓慢滴加，分散20min；
步骤6，添加基材润湿剂和亚硝酸钠，分散10min；
步骤7，添加锂基膨润土，分散10min；
步骤8，添加磷酸，继续分散5min；
步骤9，添加憎水剂，分散20min，制得所述转锈固锈防水涂料。
实施例2
一种转锈固锈防水涂料，其组成包括如下质量份数的组分：纯丙乳液75份，焦性没食子酸8份，铵盐分散剂0.3份，成膜助剂4.4份，纳米氧化锌0.1份，亚硝酸钠0.3份，基材润湿剂0.2份，磷酸0.8份，消泡剂0.1份，杀菌防腐剂 0.3份，锂基膨润土0.2份，憎水剂0.8份，去离子水9.5份。
转锈固锈防水涂料的制备方法同实施例1。
实施例3
一种转锈固锈防水涂料，其组成包括如下质量份数的组分：纯丙乳液78份，焦性没食子酸5份，铵盐分散剂0.3份，成膜助剂4.5份，纳米氧化锌0.1份，亚硝酸钠0.3份，基材润湿剂0.1份，磷酸1份，消泡剂0.1份，杀菌防腐剂0.3 份，锂基膨润土0.2份，憎水剂0.5份，去离子水9.6份。
转锈固锈防水涂料的制备方法同实施例1。
实施例4
一种转锈固锈防水涂料，其组成包括如下质量份数的组分：纯丙乳液80份，焦性没食子酸3份，铵盐分散剂0.3份，成膜助剂4.5份，纳米氧化锌0.1份，亚硝酸钠0.5份，基材润湿剂0.1份，磷酸0.5份，消泡剂0.1份，杀菌防腐剂 0.3份，锂基膨润土0.2份，憎水剂0.5份，去离子水9.9份。
转锈固锈防水涂料的制备方法同实施例1。
实施效果
表1为依据GB/T 9286-1998、GB/T 1732-1993、GB/T 9274-1988对上述实施例1-4所得的转锈固锈防水涂料性能分析检测结果。
表1转锈固锈防水涂料性能分析检测结果
由表1可以看出，根据上述实施例制备的转锈固锈防水涂料的转锈效果良好，其他各种性能指标都达到技术指标要求。
Claims (5)
1.一种转锈固锈防水涂料，其特征在于，包括如下质量份数的组分：纯丙乳液70-80份，焦性没食子酸2-10份，铵盐分散剂0.1-0.3份，成膜助剂4.2-4.8份，纳米氧化锌0.1-0.3份，亚硝酸钠0.3-0.6份，基材润湿剂0.1-0.3份，磷酸0.1-1份，消泡剂0.1-0.3份，杀菌防腐剂0.1-0.3份，锂基膨润土0.1-0.3份，憎水剂0.5-1份，去离子水9.4-11份。
2.如权利要求1所述的一种转锈固锈防水涂料，其特征在于，所述成膜助剂包括醇酯十二；
和/或，所述润湿剂包括磺化琥珀酸二辛酯钠盐类；
和/或，所述消泡剂包括矿物油类；
和/或，所述杀菌防腐剂包括卡松类；
和/或，所述憎水剂包括有机硅类。
3.如权利要求1-2任一项所述的一种转锈固锈防水涂料的制备方法，其特征在于，具体步骤包括：
步骤1，添加纯丙乳液，开启高速分散机；
步骤2，添加成膜助剂和消泡剂，进行分散；
步骤3，添加去离子水和杀菌防腐剂，继续分散；
步骤4，添加焦性没食子酸，继续分散；
步骤5，添加铵盐分散剂和纳米氧化锌，继续分散；
步骤6，添加基材润湿剂和亚硝酸钠，继续分散；
步骤7，添加锂基膨润土，继续分散；
步骤8，添加磷酸，继续分散；
步骤9，添加憎水剂，继续分散，制得所述转锈固锈防水涂料。
4.如权利要求3所述的一种转锈固锈防水涂料的制备方法，其特征在于，所述步骤1-9中，高速分散机的转速为400-600r/min。
5.如权利要求3所述的一种转锈固锈防水涂料的制备方法，其特征在于，所述步骤1-9中，每一步的分散时间为2-30min。
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| CN105255281A (zh) * | 2015-10-08 | 2016-01-20 | 怡成屏障（张家港）科技有限公司 | 一种环保低碳自转锈涂料及其制备方法 |
| CN114540805A (zh) * | 2022-01-21 | 2022-05-27 | 山东鑫泰水处理技术股份有限公司 | 一种钢铁化锈、防锈、发黑一步处理方法 |
| CN114656848A (zh) * | 2022-03-11 | 2022-06-24 | 上海保立佳新材料有限公司 | 一种抗开裂耐老化防水装饰一体化涂料及其制备方法 |
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| CN114540805A (zh) * | 2022-01-21 | 2022-05-27 | 山东鑫泰水处理技术股份有限公司 | 一种钢铁化锈、防锈、发黑一步处理方法 |
| CN114656848A (zh) * | 2022-03-11 | 2022-06-24 | 上海保立佳新材料有限公司 | 一种抗开裂耐老化防水装饰一体化涂料及其制备方法 |
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