CN115212823B - Emulsion production line - Google Patents
Emulsion production line Download PDFInfo
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- CN115212823B CN115212823B CN202210842471.1A CN202210842471A CN115212823B CN 115212823 B CN115212823 B CN 115212823B CN 202210842471 A CN202210842471 A CN 202210842471A CN 115212823 B CN115212823 B CN 115212823B
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- tank
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- modification
- phase inversion
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/004—Multifunctional apparatus for automatic manufacturing of various chemical products
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
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- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The invention provides an emulsion production line which comprises a reactor, a concentration tank, a phase inversion/modification tank and a packaging tank, wherein the reactor is respectively connected with the concentration tank and the phase inversion/modification tank, and the phase inversion/modification tank is connected with the packaging tank; the raw materials are reacted in a reactor to obtain materials, the materials respectively pass through a concentrating tank and a phase inversion/modification tank, and the materials concentrated in the concentrating tank are sent into the phase inversion/modification tank for phase inversion/modification to obtain emulsion A; and (3) inputting the emulsion A into a packaging tank, transferring the emulsion A into a concentrating tank, concentrating again, and inputting the emulsion A into the packaging tank to obtain emulsion B. According to the invention, the front section and the rear section of the two reaction processes of the emulsion A and the emulsion B are shared, and the differential ends are inserted and switched by the three-way valve, so that the production line can simultaneously meet the production of different products, the time of manually changing the line is saved, the efficiency is improved, and the equipment cost is saved.
Description
Technical Field
The invention relates to the technical field of production lines, in particular to an emulsion production line.
Background
In chemical production, the emulsion such as mask emulsion needs to be further concentrated or modified based on the original emulsion according to production requirements, so that conventional emulsion, concentrated emulsion or modified emulsion is obtained. However, because the production characteristics of the conventional emulsion, the concentrated emulsion or the modified emulsion are different, the process is different, and different line bodies are required to be used for production in the production process (such as a device and a method for producing the emulsion in CN202080010950.6, a production line of an inverse emulsion resistance-reducing agent in CN201621272620.1 and the like, and only one product can be produced in one production line). The production lines are manually divided, so that the production progress is greatly reduced, and the production line body is additionally prepared.
Disclosure of Invention
The present invention is directed to an emulsion production line, which solves the above-mentioned problems in the prior art.
In order to achieve the above purpose, the present invention provides the following technical solutions:
an emulsion production line comprises a reactor, a concentration tank, a phase inversion/modification tank and a packaging tank, wherein the reactor is respectively connected with the concentration tank and the phase inversion/modification tank, and the phase inversion/modification tank is connected with the packaging tank;
the raw materials are reacted in a reactor to obtain materials, the materials respectively pass through a concentrating tank and a phase inversion/modification tank, and the materials concentrated in the concentrating tank are sent into the phase inversion/modification tank for phase inversion/modification to obtain emulsion A;
and (3) inputting the emulsion A into a packaging tank, transferring the emulsion A into a concentrating tank, concentrating again, and inputting the emulsion A into the packaging tank to obtain emulsion B.
Preferably, the input of reactor is connected to the head tank, and the output is connected with the delivery pump, the delivery pump is connected to the defoaming jar, the defoaming jar is connected with phase inversion/modification jar and enrichment jar respectively through the three-way valve.
Preferably, the concentrating tank comprises a concentrating tank I and a concentrating tank II, wherein the concentrating tank I is respectively connected with the three-way valve and the phase inversion/modification tank, the phase inversion/modification tank is connected with an input port of the double-pipe channel, and an output port of the double-pipe channel is respectively connected with the concentrating tank II and the packaging tank.
Preferably, the packaging tank comprises a packaging tank I and a packaging tank II, wherein the packaging tank I is connected with one of the output ports of the double-pipe channel, and the packaging tank II is connected with the concentrating tank II.
Preferably, the packaging tank I is connected with one of the output ports of the double-pipe channel through the homogenizer I, the packaging tank II is connected with the concentrating tank II through the homogenizer II, and a one-way valve is arranged between the concentrating tank II and the output port of the double-pipe channel.
Preferably, the gas filling structure comprises an inert gas tank and a gas filling pump, one end of the gas filling pump is connected with the inert gas tank, and the other end of the gas filling pump is connected with the concentration tank and the phase inversion/modification tank.
Preferably, the device further comprises a degassing structure, the degassing structure comprises a sealing box, a front-stage filter, a front-stage absorption pump, a rear-stage filter and a rear-stage absorption pump are arranged in the sealing box, the front-stage filter is close to an air inlet of the sealing box, the rear-stage absorption pump is close to an air outlet of the sealing box, the front-stage absorption pump and the rear-stage absorption pump are respectively located at two sides of the rear-stage filter, the air inlet of the sealing box is connected with a packaging tank, and the air outlet of the sealing box is connected with an inert gas tank.
Compared with the prior art, the invention has the beneficial effects that:
according to the invention, the degassing structure is arranged, so that the harmful components in the gas existing in the packaging tank, especially the harmful gas such as VOC gas, can be adsorbed and removed, and then the inert gas doped in the pipeline and the emulsion is conveyed into the inert gas tank again for recycling. An air-entrapping structure is arranged to ensure the quality of emulsion production synthesis.
According to the invention, the front section and the rear section of the two reaction processes of the emulsion A and the emulsion B are shared, and the differential ends are inserted and switched by the three-way valve, so that the production line can simultaneously meet the production of different products, the time of manually changing the line is saved, the efficiency is improved, and the equipment cost is saved.
Drawings
FIG. 1 is a schematic diagram of the structure of the present invention;
FIG. 2 is a schematic view of the degassing structure of the present invention.
In the figure: 1 reactor, 2 transfer pump, 3 defoaming jar, 4 three-way valve, 5 change phase/modification jar, 6 concentrate jar I, 7 double tube passageway, 8 check valve, 9 concentrate jar II, 10 homogenizer I, 11 homogenizer II, 12 inert gas jar, 13 degassing structure, 14 packaging jar I, 15 packaging jar II, 16 seal box, 17 preceding stage filter, 18 preceding stage absorption pump, 19 later stage filter, 20 gas pump, 21 later stage absorption pump.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Referring to fig. 1 to 2, the present invention provides a technical solution:
the emulsion production line is a multifunctional emulsion production line which can be simultaneously applicable to a plurality of products of the conventional emulsion, concentrated or modified emulsion production processes. The device comprises a reactor 1, a concentration tank, a phase inversion/modification tank 5 and a packaging tank, wherein the input end of the reactor 1 is connected to a raw material tank, the output end of the reactor is connected with a delivery pump 2, the delivery pump 2 is connected with a defoaming tank 3, and the defoaming tank 3 is respectively connected with the phase inversion/modification tank 5 and the concentration tank through a three-way valve 4. The concentrating tank comprises a concentrating tank I6 and a concentrating tank II 9, wherein the concentrating tank I6 is respectively connected with the three-way valve 4 and the phase inversion/modification tank 5, the phase inversion/modification tank 5 is connected with an input port of the double-pipe type channel 7, and an output port of the double-pipe type channel 7 is respectively connected with the concentrating tank II 9 and the packaging tank. The packaging tank comprises a packaging tank I14 and a packaging tank II 15, wherein the packaging tank I14 is connected with one of the output ports of the double-pipe type channel 7, and the packaging tank II 15 is connected with a concentrating tank II 9. The packaging tank I14 is connected with one of the output ports of the double-pipe channel 7 through the homogenizer I10, the packaging tank II 15 is connected with the concentrating tank II 9 through the homogenizer II 11, and a one-way valve 8 is arranged between the concentrating tank II 9 and the output port of the double-pipe channel 7.
The invention further comprises an air-filling structure, wherein the air-filling structure comprises an inert gas tank 12 and an air-filling pump 20, one end of the air-filling pump 20 is connected with the inert gas tank 12, and the other end of the air-filling pump 20 is connected with the concentration tank and the phase inversion/modification tank 5. The air removal device further comprises an air removal structure 13, the air removal structure 13 comprises a sealing box 16, a front-stage filter 17, a front-stage absorption pump 18, a rear-stage filter 19 and a rear-stage absorption pump 21 are arranged in the sealing box 16, the front-stage filter 17 is close to an air inlet of the sealing box 16, the rear-stage absorption pump 21 is close to an air outlet of the sealing box 16, the front-stage absorption pump 18 and the rear-stage absorption pump 21 are respectively positioned on two sides of the rear-stage filter 19, the air inlet of the sealing box 16 is connected with a packaging tank, and the air outlet of the sealing box 16 is connected with the inert gas tank 12.
The raw materials are reacted in a reactor 1 to obtain materials, the materials respectively pass through a concentrating tank and a phase inversion/modification tank 5, and the materials concentrated in the concentrating tank are sent into the phase inversion/modification tank 5 for phase inversion/modification to obtain emulsion A; and (3) inputting the emulsion A into a packaging tank, transferring the emulsion A into a concentrating tank, concentrating again, and inputting the emulsion A into the packaging tank to obtain emulsion B.
Specifically, the raw materials of the raw material tank are conveyed into a reactor 1 through a pipeline to react to obtain intermediate materials of emulsion, then the intermediate materials are concentrated and phase-inverted/modified in a concentration tank I6 to form common (conventional) emulsion, namely emulsion A, and then the common (conventional) emulsion A is further conveyed into a packaging tank I14, and the emulsion in the packaging tank I14 is filled and packaged to obtain the independently packaged/filled emulsion A. And the emulsion A after phase inversion/modification tank 5 is sent to a concentration tank II 9 again for concentration, so that concentrated/modified emulsion, namely emulsion B, can be obtained, and then the concentrated/modified emulsion is further sent to a packaging tank II 15, and the emulsion in the packaging tank II 15 is filled and packaged, so that independent packaged/filled emulsion B can be obtained.
Because the concentration tank I6 is arranged for concentration in advance, the concentration of the emulsion A obtained after the phase inversion/modification tank 5 is slightly higher than that of the emulsion A obtained after the phase inversion/modification tank 5 is directly carried out without the concentration tank I6, but is lower than that of the concentrated emulsion B, so that the emulsion B can be obtained after the emulsion A passes through the concentration tank II 9 again, the time for obtaining the emulsion B is shortened, and meanwhile, the emulsion A can meet the requirements of use or post-processing.
According to the invention, the front section and the rear section of the two reaction processes of the emulsion A and the emulsion B are shared, and the three-way valve 4 is utilized to insert and switch the difference ends, so that the production line can simultaneously meet the production of different products, the time of manually changing the line is saved, the efficiency is improved, and the equipment cost is saved.
According to the invention, the materials obtained after the reaction in the reactor 1 are sent into the defoaming tank 3 for defoaming, so that generated bubbles are ensured to be removed completely before entering the phase inversion/modification tank 5 and the concentration tank I, and the synthesis quality is not influenced. And emulsion A in the packing jar I14 is exported through double tube passageway 7 and emulsion B in the packing jar II 15 is gone into to by concentrate jar II 9 is through setting up and go on the homogeneity stability in the homogenizer, i.e. homogenizer I10 and homogenizer II 11, finally carries out online package/filling through the packing jar.
According to the invention, an air-entrapping structure is provided, which comprises an inert gas tank 12, wherein inert gas such as nitrogen and carbon dioxide is provided in the inert gas tank 12, and protective gas, preferably nitrogen, is introduced into the phase inversion/modification tank 5, the concentration tank I6 and the concentration tank II 9 through an air-entrapping pump 20 so as to ensure the quality of emulsion production synthesis.
According to the invention, the degassing structure 13 is arranged, so that gas existing in the packaging tank, especially harmful gas such as VOC gas, can enter the sealing box 16 from the gas inlet under the action of the pre-stage absorption pump 18, is firstly subjected to primary absorption and filtration through the pre-stage filter 17, is then subjected to secondary absorption and filtration through the post-stage filter 19 under the action of the post-stage absorption pump 21, and is subjected to secondary absorption and removal of harmful components, and then the inert gas doped in the pipeline and emulsion is conveyed into the inert gas tank 12 again through the gas outlet of the sealing box 16 for recycling.
In the present invention, the front filter 17 and the rear filter 19 are based on filter membrane filters, and the front absorption pump 18 and the rear absorption pump 21 are based on centrifugal absorption pumps. The sealed box 16 is used as an adsorption tower, and spaces such as between the front-stage filter 17 and the sealed box 16, between the front-stage filter 17 and the rear-stage filter 19 and the like in the sealed box 16 are filled with an adsorbent, and the adsorbent is one or a combination of a plurality of active carbon, macroporous resin and zeolite. When the emulsion to be treated is sent into a packaging tank, trace VOC remained in the emulsion can be effectively removed under the action of the adsorbent. Of course the degassing structure 13 may also be a stripper, or a mixture of both.
The invention adopts a control system to carry out logic control on electric elements such as the delivery pump 2, the electromagnetic three-way valve 4, the front-stage absorption pump, the air-entrapping pump 20, the rear-stage absorption pump 21 and the like, and the control system can be a PLC control system or a DCS control system and the like.
The remaining non-described portions of the present invention may be the same as, or known in the art or may be implemented using, the prior art, and are not described in detail herein.
Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (2)
1. The emulsion production line is characterized by comprising a reactor (1), a concentration tank, a phase inversion/modification tank (5) and a packaging tank, wherein the reactor (1) is respectively connected with the concentration tank and the phase inversion/modification tank (5), and the phase inversion/modification tank (5) is connected with the packaging tank;
the raw materials are reacted in a reactor (1) to obtain materials, the materials respectively pass through a concentrating tank and a phase inversion/modification tank (5), and the materials concentrated in the concentrating tank are sent into the phase inversion/modification tank (5) for phase inversion/modification to obtain emulsion A;
inputting the emulsion A into a packaging tank, transferring into a concentrating tank, concentrating again, and inputting into the packaging tank to obtain emulsion B;
the input end of the reactor (1) is connected to a raw material tank, the output end of the reactor is connected with a delivery pump (2), the delivery pump (2) is connected with a defoaming tank (3), and the defoaming tank (3) is respectively connected with a phase inversion/modification tank (5) and a concentration tank through a three-way valve (4);
the concentrating tank comprises a concentrating tank I (6) and a concentrating tank II (9), wherein the concentrating tank I (6) is respectively connected with a three-way valve (4) and a phase inversion/modification tank (5), the phase inversion/modification tank (5) is connected with an input port of a double-pipe type channel (7), and an output port of the double-pipe type channel (7) is respectively connected with the concentrating tank II (9) and a packaging tank;
the packaging tank comprises a packaging tank I (14) and a packaging tank II (15), wherein the packaging tank I (14) is connected with one of the output ports of the double-pipe channel (7), and the packaging tank II (15) is connected with the concentrating tank II (9);
the packaging tank I (14) is connected with one of the output ports of the double-pipe channel (7) through the homogenizer I (10), the packaging tank II (15) is connected with the concentrating tank II (9) through the homogenizer II (11), and a one-way valve (8) is arranged between the concentrating tank II (9) and the output port of the double-pipe channel (7);
the gas filling device is characterized by further comprising a gas filling structure, wherein the gas filling structure comprises an inert gas tank (12) and a gas filling pump (20), one end of the gas filling pump (20) is connected with the inert gas tank (12), and the other end of the gas filling pump (20) is connected with a concentration tank and a phase inversion/modification tank (5).
2. An emulsion production line as claimed in claim 1, characterized in that the emulsion production line further comprises a degassing structure (13), the degassing structure (13) comprises a sealing box (16), a front-stage filter (17), a front-stage absorption pump (18), a rear-stage filter (19) and a rear-stage absorption pump (21) are arranged in the sealing box (16), the front-stage filter (17) is close to an air inlet of the sealing box (16), the rear-stage absorption pump (21) is close to an air outlet of the sealing box (16), the front-stage absorption pump (18) and the rear-stage absorption pump (21) are respectively arranged on two sides of the rear-stage filter (19), the air inlet of the sealing box (16) is connected with a packaging tank, and the air outlet of the sealing box (16) is connected with an inert gas tank (12).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210842471.1A CN115212823B (en) | 2022-07-18 | 2022-07-18 | Emulsion production line |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210842471.1A CN115212823B (en) | 2022-07-18 | 2022-07-18 | Emulsion production line |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115212823A CN115212823A (en) | 2022-10-21 |
| CN115212823B true CN115212823B (en) | 2023-07-28 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202210842471.1A Active CN115212823B (en) | 2022-07-18 | 2022-07-18 | Emulsion production line |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006297360A (en) * | 2005-04-20 | 2006-11-02 | Toyo Kasei Kogyo Co Ltd | High speed decompressing/concentrating device |
| CN101143927A (en) * | 2007-04-30 | 2008-03-19 | 慈溪市洁达纳米复合材料有限公司 | Copolymerization modified PA612 and preparation method thereof |
| CN206731027U (en) * | 2017-05-15 | 2017-12-12 | 广州市美夫兰化妆品有限公司 | A kind of facial mask emulsion synthesizes filling production lines |
| CN209393122U (en) * | 2018-03-26 | 2019-09-17 | 抚顺新跃化学制品有限公司 | It is a kind of for making the environment-friendly type production equipment of dish washing liquid |
| CN112999703A (en) * | 2021-01-28 | 2021-06-22 | 江西三越新材料有限公司 | Production method of special defoaming agent for water-based concentrated pigment color paste |
-
2022
- 2022-07-18 CN CN202210842471.1A patent/CN115212823B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2006297360A (en) * | 2005-04-20 | 2006-11-02 | Toyo Kasei Kogyo Co Ltd | High speed decompressing/concentrating device |
| CN101143927A (en) * | 2007-04-30 | 2008-03-19 | 慈溪市洁达纳米复合材料有限公司 | Copolymerization modified PA612 and preparation method thereof |
| CN206731027U (en) * | 2017-05-15 | 2017-12-12 | 广州市美夫兰化妆品有限公司 | A kind of facial mask emulsion synthesizes filling production lines |
| CN209393122U (en) * | 2018-03-26 | 2019-09-17 | 抚顺新跃化学制品有限公司 | It is a kind of for making the environment-friendly type production equipment of dish washing liquid |
| CN112999703A (en) * | 2021-01-28 | 2021-06-22 | 江西三越新材料有限公司 | Production method of special defoaming agent for water-based concentrated pigment color paste |
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| CN115212823A (en) | 2022-10-21 |
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