CN115212823A - Emulsion production line - Google Patents
Emulsion production line Download PDFInfo
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- CN115212823A CN115212823A CN202210842471.1A CN202210842471A CN115212823A CN 115212823 A CN115212823 A CN 115212823A CN 202210842471 A CN202210842471 A CN 202210842471A CN 115212823 A CN115212823 A CN 115212823A
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- phase inversion
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/004—Multifunctional apparatus for automatic manufacturing of various chemical products
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
- B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
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Abstract
The invention provides an emulsion production line, which comprises a reactor, a concentration tank, a phase inversion/modification tank and a packaging tank, wherein the reactor is respectively connected with the concentration tank and the phase inversion/modification tank; reacting the raw materials in a reactor to obtain a material, passing the material through a concentration tank and a phase inversion/modification tank respectively, and feeding the material concentrated in the concentration tank into the phase inversion/modification tank for phase inversion/modification to obtain emulsion A; inputting the emulsion A into a packaging can, and inputting into the packaging can after transferring into a concentration can and concentrating again to obtain emulsion B. According to the invention, the front section and the rear section of the two reaction processes of the emulsion A and the emulsion B are shared, and the different ends are inserted and switched by using the three-way valve, so that the production line can simultaneously meet the production requirements of different products, the time for manual line changing is saved, the efficiency is improved, and the equipment cost is saved.
Description
Technical Field
The invention relates to the technical field of production lines, in particular to an emulsion production line.
Background
In chemical production, emulsions such as facial mask emulsions need to be further concentrated or modified based on the original emulsions according to production requirements, so that conventional emulsions, concentrated emulsions or modified emulsions are obtained. However, because the production characteristics of the conventional emulsion, the concentrated emulsion or the modified emulsion are different, the used processes are different, and different lines are required to be used for production in the production process (for example, a device and a method for producing the emulsion in CN202080010950.6, a reverse emulsion drag reducer production line in CN201621272620.1, and the like can only produce one product in one production line). The production lines need to be manually divided, the production progress is greatly reduced, and production line bodies need to be additionally prepared.
Disclosure of Invention
The invention aims to provide an emulsion production line to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
an emulsion production line comprises a reactor, a concentration tank, a phase inversion/modification tank and a packaging tank, wherein the reactor is respectively connected with the concentration tank and the phase inversion/modification tank;
reacting the raw materials in a reactor to obtain a material, respectively passing the material through a concentration tank and a phase inversion/modification tank, and feeding the material concentrated in the concentration tank into the phase inversion/modification tank for phase inversion/modification to obtain emulsion A;
inputting the emulsion A into a packaging can, and inputting into the packaging can after transferring into a concentration can and concentrating again to obtain emulsion B.
Preferably, the input of reactor is connected to the head tank, and the output is connected with the delivery pump, the defoaming jar is connected to the delivery pump, the defoaming jar passes through the three-way valve and is connected with looks/modified jar and concentrated jar respectively.
Preferably, concentrated jar is including concentrating jar I and concentrated jar II, concentrated jar I is connected with three-way valve and looks/modified jar respectively, the input port of double-tube passageway is connected to the jar of looks/modified, concentrated jar II and packing jar are connected respectively to the delivery outlet of double-tube passageway.
Preferably, the packing jar includes packing jar I and packing jar II, packing jar I is connected with one of them delivery outlet of double-barrelled passageway, packing jar II is connected with concentrated jar II.
Preferably, the packaging tank I is connected with one output port of the double-tube type channel through the homogenizer I, the packaging tank II is connected with the concentration tank II through the homogenizer II, and a check valve is arranged between the concentration tank II and the output port of the double-tube type channel.
Preferably, the gas filling structure comprises an inert gas tank and a gas filling pump, one end of the gas filling pump is connected with the inert gas tank, and the other end of the gas filling pump is connected with the concentration tank and the phase inversion/modification tank.
Preferably, still include the gas removal structure, the gas removal structure includes the seal box, installs preceding stage filter, preceding stage absorption pump, back level filter and back level absorption pump in this seal box, preceding stage filter is close to the air inlet department of seal box, back level absorption pump is close to the air outlet department of seal box, preceding stage absorption pump and back level absorption pump are located the both sides of back level filter respectively, the air inlet and the packing jar of seal box are connected, the air outlet and the inert gas jar of seal box are connected.
Compared with the prior art, the invention has the beneficial effects that:
the invention provides a degassing structure which can adsorb and remove harmful components in gas, particularly harmful gas such as VOC gas, in a packaging tank, and then convey inert gas doped in a pipeline and emulsion into an inert gas tank for recycling. The air-entrapping structure is arranged to ensure the quality of emulsion production and synthesis.
According to the invention, the front section and the rear section of the two reaction processes of the emulsion A and the emulsion B are shared, and the differential end is inserted and switched by using the three-way valve, so that the production line can simultaneously meet the production of different products, the time for manually changing the line is saved, the efficiency is improved, and the equipment cost is saved.
Drawings
FIG. 1 is a schematic view of the structure of the present invention;
FIG. 2 is a schematic view of the degassing structure of the present invention.
In the figure: the device comprises a reactor 1, a delivery pump 2, a defoaming tank 3, a three-way valve 4, a phase inversion/modification tank 5, a concentration tank I6, a double-tube channel 7, a one-way valve 8, a concentration tank II 9, a homogenizer I10, a homogenizer II 11, an inert gas tank 12, a degassing structure 13, a packaging tank I14, a packaging tank II 15, a sealing box 16, a pre-stage filter 17, a pre-stage absorption pump 18, a post-stage filter 19, an air feeding pump 20 and a post-stage absorption pump 21.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be obtained by a person skilled in the art without making any creative effort based on the embodiments in the present invention, belong to the protection scope of the present invention.
Referring to fig. 1 to 2, the present invention provides a technical solution:
the emulsion production line of the invention is a multifunctional emulsion production line of various products which can be simultaneously suitable for the production process of a plurality of products of conventional emulsion, concentrated or modified emulsion. Including reactor 1, concentrated jar, looks/modified jar 5 and packing jar, the input of reactor 1 is connected to the head tank, and the output is connected with delivery pump 2, defoaming jar 3 is connected to delivery pump 2, defoaming jar 3 is connected with looks/modified jar 5 and concentrated jar respectively through three-way valve 4 and is connected. Concentrated jar is including concentrated jar I6 and concentrated jar II 9, concentrated jar I6 is connected with three-way valve 4 and looks/modified jar 5 respectively, the input port of two tubular passageway 7 is connected to looks/modified jar 5, concentrated jar II 9 and packing jar are connected respectively to the delivery outlet of two tubular passageway 7. The packaging can comprises a packaging can I14 and a packaging can II 15, wherein the packaging can I14 is connected with one of the output ports of the double-tube type channel 7, and the packaging can II 15 is connected with a concentration can II 9. The packaging can I14 is connected with one of the output ports of the double-tube type channel 7 through the homogenizer I10, the packaging can II 15 is connected with the concentration can II 9 through the homogenizer II 11, and the one-way valve 8 is arranged between the concentration can II 9 and the output port of the double-tube type channel 7.
The device also comprises a gas filling structure, wherein the gas filling structure comprises an inert gas tank 12 and a gas filling pump 20, one end of the gas filling pump 20 is connected with the inert gas tank 12, and the other end of the gas filling pump 20 is connected with a concentration tank and a phase inversion/modification tank 5. Still include the degasification structure 13, the degasification structure 13 includes the seal box 16, installs preceding stage filter 17, preceding stage absorption pump 18, back level filter 19 and back level absorption pump 21 in this seal box 16, preceding stage filter 17 is close to the air inlet department of seal box 16, back level absorption pump 21 is close to the air outlet department of seal box 16, preceding stage absorption pump 18 and back level absorption pump 21 are located the both sides of back level filter 19 respectively, the air inlet and the packing jar of seal box 16 are connected, the air outlet and the inert gas jar 12 of seal box 16 are connected.
The raw materials are reacted in a reactor 1 to obtain materials, the materials respectively pass through a concentration tank and a phase inversion/modification tank 5, the materials concentrated in the concentration tank are sent into the phase inversion/modification tank 5 for phase inversion/modification, and emulsion A is obtained; inputting the emulsion A into a packaging can, and inputting into the packaging can after transferring into a concentration can and concentrating again to obtain emulsion B.
Specifically, the raw materials of the raw material tank are conveyed into the reactor 1 through a pipeline to react to obtain a middle material of the emulsion, then the middle material is concentrated by the concentration tank I6 and is converted into common (conventional) emulsion, namely emulsion A, by the phase inversion/modification tank 5, and then the common (conventional) emulsion is further conveyed to the packaging tank I14, and the emulsion in the packaging tank I14 is filled and packaged to obtain the independently packaged/filled emulsion A. And the emulsion A after passing through the phase inversion/modification tank 5 is sent to a concentration tank II 9 again for concentration to obtain concentrated/modified emulsion, namely emulsion B, and then is further sent to a packaging tank II 15, and the emulsion in the packaging tank II 15 is filled and packaged to obtain independently packaged/filled emulsion B.
Because the concentration tank I6 is arranged for concentration in advance, the concentration of the emulsion A obtained after the phase inversion/modification tank 5 is slightly higher than that of the emulsion A obtained after the emulsion A directly passes through the phase inversion/modification tank 5 without passing through the concentration tank I6, but is lower than that of the concentrated emulsion B, so that not only the emulsion B can be obtained after the emulsion A passes through the concentration tank II 9 again, but also the time for obtaining the emulsion B is shortened, and the emulsion A can be ensured to meet the requirements of use or later processing.
According to the invention, the front section and the rear section of the two reaction processes of the emulsion A and the emulsion B are shared, and the differential end is inserted and switched by using the three-way valve 4, so that the production line can simultaneously meet the production of different products, the time for manually changing the line is saved, the efficiency is improved, and the equipment cost is saved.
According to the invention, the material obtained after the reaction in the reactor 1 is fed into the defoaming tank 3 for defoaming, so that generated bubbles are completely removed before the material enters the phase inversion/modification tank 5 and the concentration tank I, and the synthesis quality is not influenced. And emulsion A output into the packaging can I14 through the double-pipe type channel 7 and emulsion B entering into the packaging can II 15 from the concentration can II 9 are homogenized and stabilized in homogenizers, namely a homogenizer I10 and a homogenizer II 11, and finally, online packaging/filling is carried out through the packaging can.
According to the invention, a gas filling structure is arranged, the gas filling structure comprises an inert gas tank 12, and inert gases such as nitrogen and carbon dioxide are filled in the inert gas tank 12 through a gas filling pump 20 to protect the gas, preferably nitrogen, in the phase inversion/modification tank 5, the concentration tank I6 and the concentration tank II 9, so as to ensure the quality of emulsion production and synthesis.
The invention is provided with a degassing structure 13, which can lead the gas in the packaging tank, especially the harmful gas such as VOC gas, to enter the sealed box 16 from the gas inlet by the action of a front-stage absorption pump 18, firstly pass through a front-stage filter 17 for primary absorption and filtration, then pass through a rear-stage filter 19 for secondary absorption and filtration under the action of a rear-stage absorption pump 21, absorb and remove the harmful components in the gas, and then convey the inert gas mixed in the pipeline and the emulsion into the inert gas tank 12 for the recycling use through the gas outlet with the sealed box 16.
In the present invention, the pre-filter 17 and the post-filter 19 are filter membrane filters, and the pre-absorption pump 18 and the post-absorption pump 21 are centrifugal absorption pumps. The sealed box 16 is used as an adsorption tower, and the spaces in the sealed box 16, such as between the pre-filter 17 and the sealed box 16, between the pre-filter 17 and the post-filter 19, are filled with an adsorbent, which is one or a combination of more of activated carbon, macroporous resin and zeolite. When the emulsion to be treated is sent into a packaging tank, the residual micro VOC in the emulsion can be effectively removed under the action of the adsorbent. Of course, the degassing structure 13 may also be a stripper or a mixture of both.
In the invention, a control system is adopted to carry out logic control on electric elements such as the delivery pump 2, the electromagnetic three-way valve 4, the pre-stage absorption pump, the gas filling pump 20, the post-stage absorption pump 21 and the like, and the control system can be a PLC control system or a DCS control system and the like.
The invention, the remaining parts not described, are the same as, or known or realizable by the prior art and will not be described in detail here.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. The emulsion production line is characterized by comprising a reactor (1), a concentration tank, a phase inversion/modification tank (5) and a packaging tank, wherein the reactor (1) is respectively connected with the concentration tank and the phase inversion/modification tank (5), and the phase inversion/modification tank (5) is connected with the packaging tank;
reacting the raw materials in a reactor (1) to obtain materials, passing the materials through a concentration tank and a phase inversion/modification tank (5), respectively, and feeding the materials concentrated in the concentration tank into the phase inversion/modification tank (5) for phase inversion/modification to obtain emulsion A;
inputting the emulsion A into a packaging can, and inputting into the packaging can after transferring into a concentration can and concentrating again to obtain emulsion B.
2. An emulsion production line according to claim 1, characterized in that the input end of the reactor (1) is connected to a raw material tank, the output end is connected to a transfer pump (2), the transfer pump (2) is connected to a defoaming tank (3), and the defoaming tank (3) is connected to a phase inversion/modification tank (5) and a concentration tank respectively through a three-way valve (4).
3. An emulsion production line according to claim 2, characterized in that the concentration tank comprises a concentration tank I (6) and a concentration tank II (9), the concentration tank I (6) is respectively connected with the three-way valve (4) and the phase inversion/modification tank (5), the phase inversion/modification tank (5) is connected with the input port of the double-pipe passage (7), and the output port of the double-pipe passage (7) is respectively connected with the concentration tank II (9) and the packaging tank.
4. The emulsion production line of claim 3, wherein the packaging can comprises a packaging can I (14) and a packaging can II (15), the packaging can I (14) is connected with one of the output ports of the double-tube channel (7), and the packaging can II (15) is connected with the concentration can II (9).
5. An emulsion production line according to claim 4, characterized in that the packaging can I (14) is connected with one of the outlets of the double-tube channel (7) through a homogenizer I (10), the packaging can II (15) is connected with the concentration can II (9) through a homogenizer II (11), and a one-way valve (8) is arranged between the concentration can II (9) and the outlet of the double-tube channel (7).
6. An emulsion production line according to claim 1, further comprising an air-entrapping structure, wherein the air-entrapping structure comprises an inert gas tank (12) and an air-entrapping pump (20), one end of the air-entrapping pump (20) is connected with the inert gas tank (12), and the other end of the air-entrapping pump (20) is connected with the concentration tank and the phase inversion/modification tank (5).
7. The emulsion production line of claim 6, further comprising a degassing structure (13), wherein the degassing structure (13) comprises a sealed box (16), a pre-filter (17), a pre-absorption pump (18), a post-filter (19) and a post-absorption pump (21) are installed in the sealed box (16), the pre-filter (17) is close to an air inlet of the sealed box (16), the post-absorption pump (21) is close to an air outlet of the sealed box (16), the pre-absorption pump (18) and the post-absorption pump (21) are respectively located on two sides of the post-filter (19), the air inlet of the sealed box (16) is connected with the packaging can, and the air outlet of the sealed box (16) is connected with the inert gas can (12).
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CN202210842471.1A CN115212823B (en) | 2022-07-18 | 2022-07-18 | Emulsion production line |
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CN202210842471.1A CN115212823B (en) | 2022-07-18 | 2022-07-18 | Emulsion production line |
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CN115212823B CN115212823B (en) | 2023-07-28 |
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Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006297360A (en) * | 2005-04-20 | 2006-11-02 | Toyo Kasei Kogyo Co Ltd | High speed decompressing/concentrating device |
CN101143927A (en) * | 2007-04-30 | 2008-03-19 | 慈溪市洁达纳米复合材料有限公司 | Copolymerization modified PA612 and preparation method thereof |
CN206731027U (en) * | 2017-05-15 | 2017-12-12 | 广州市美夫兰化妆品有限公司 | A kind of facial mask emulsion synthesizes filling production lines |
CN209393122U (en) * | 2018-03-26 | 2019-09-17 | 抚顺新跃化学制品有限公司 | It is a kind of for making the environment-friendly type production equipment of dish washing liquid |
CN112999703A (en) * | 2021-01-28 | 2021-06-22 | 江西三越新材料有限公司 | Production method of special defoaming agent for water-based concentrated pigment color paste |
-
2022
- 2022-07-18 CN CN202210842471.1A patent/CN115212823B/en active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2006297360A (en) * | 2005-04-20 | 2006-11-02 | Toyo Kasei Kogyo Co Ltd | High speed decompressing/concentrating device |
CN101143927A (en) * | 2007-04-30 | 2008-03-19 | 慈溪市洁达纳米复合材料有限公司 | Copolymerization modified PA612 and preparation method thereof |
CN206731027U (en) * | 2017-05-15 | 2017-12-12 | 广州市美夫兰化妆品有限公司 | A kind of facial mask emulsion synthesizes filling production lines |
CN209393122U (en) * | 2018-03-26 | 2019-09-17 | 抚顺新跃化学制品有限公司 | It is a kind of for making the environment-friendly type production equipment of dish washing liquid |
CN112999703A (en) * | 2021-01-28 | 2021-06-22 | 江西三越新材料有限公司 | Production method of special defoaming agent for water-based concentrated pigment color paste |
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