CN114712279A - Deoiling shampoo - Google Patents
Deoiling shampoo Download PDFInfo
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- CN114712279A CN114712279A CN202210347598.6A CN202210347598A CN114712279A CN 114712279 A CN114712279 A CN 114712279A CN 202210347598 A CN202210347598 A CN 202210347598A CN 114712279 A CN114712279 A CN 114712279A
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- shampoo
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- 239000002453 shampoo Substances 0.000 title claims abstract description 54
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 65
- 240000001548 Camellia japonica Species 0.000 claims abstract description 50
- 241000196324 Embryophyta Species 0.000 claims abstract description 43
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 36
- 241000199919 Phaeophyceae Species 0.000 claims abstract description 28
- POJWUDADGALRAB-UHFFFAOYSA-N allantoin Chemical compound NC(=O)NC1NC(=O)NC1=O POJWUDADGALRAB-UHFFFAOYSA-N 0.000 claims abstract description 24
- 235000018597 common camellia Nutrition 0.000 claims abstract description 22
- 229940057950 sodium laureth sulfate Drugs 0.000 claims abstract description 21
- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 claims abstract description 21
- IXOCGRPBILEGOX-UHFFFAOYSA-N 3-[3-(dodecanoylamino)propyl-dimethylazaniumyl]-2-hydroxypropane-1-sulfonate Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC(O)CS([O-])(=O)=O IXOCGRPBILEGOX-UHFFFAOYSA-N 0.000 claims abstract description 19
- POJWUDADGALRAB-PVQJCKRUSA-N Allantoin Natural products NC(=O)N[C@@H]1NC(=O)NC1=O POJWUDADGALRAB-PVQJCKRUSA-N 0.000 claims abstract description 12
- 229960000458 allantoin Drugs 0.000 claims abstract description 12
- 229940045944 sodium lauroyl glutamate Drugs 0.000 claims abstract description 12
- IWIUXJGIDSGWDN-UQKRIMTDSA-M sodium;(2s)-2-(dodecanoylamino)pentanedioate;hydron Chemical compound [Na+].CCCCCCCCCCCC(=O)N[C@H](C([O-])=O)CCC(O)=O IWIUXJGIDSGWDN-UQKRIMTDSA-M 0.000 claims abstract description 12
- CFXSFDXXYYHZFU-UHFFFAOYSA-N 2-hydroxybenzoic acid;2-(trimethylazaniumyl)acetate Chemical compound C[N+](C)(C)CC(O)=O.OC(=O)C1=CC=CC=C1[O-] CFXSFDXXYYHZFU-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229940041488 betaine salicylate Drugs 0.000 claims abstract description 11
- 229940043264 dodecyl sulfate Drugs 0.000 claims abstract description 11
- 239000003755 preservative agent Substances 0.000 claims abstract description 11
- 230000002335 preservative effect Effects 0.000 claims abstract description 11
- 230000001139 anti-pruritic effect Effects 0.000 claims abstract description 10
- 239000003908 antipruritic agent Substances 0.000 claims abstract description 10
- 239000000049 pigment Substances 0.000 claims abstract description 10
- 238000002360 preparation method Methods 0.000 claims abstract description 9
- 239000007788 liquid Substances 0.000 claims description 50
- 239000002994 raw material Substances 0.000 claims description 45
- TXFPEBPIARQUIG-UHFFFAOYSA-N 4'-hydroxyacetophenone Chemical compound CC(=O)C1=CC=C(O)C=C1 TXFPEBPIARQUIG-UHFFFAOYSA-N 0.000 claims description 40
- 230000001804 emulsifying effect Effects 0.000 claims description 33
- 239000000843 powder Substances 0.000 claims description 30
- 235000006467 Camellia japonica Nutrition 0.000 claims description 28
- 241000831729 Phyllacantha Species 0.000 claims description 28
- 241000037740 Coptis chinensis Species 0.000 claims description 26
- 241001288870 Angelica polymorpha Species 0.000 claims description 25
- 238000013329 compounding Methods 0.000 claims description 24
- 239000000203 mixture Substances 0.000 claims description 24
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 20
- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 claims description 20
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims description 20
- 229960005323 phenoxyethanol Drugs 0.000 claims description 20
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 15
- 238000003756 stirring Methods 0.000 claims description 15
- 241000125175 Angelica Species 0.000 claims description 14
- 235000001287 Guettarda speciosa Nutrition 0.000 claims description 14
- 235000005979 Citrus limon Nutrition 0.000 claims description 12
- 244000131522 Citrus pyriformis Species 0.000 claims description 12
- 238000004945 emulsification Methods 0.000 claims description 11
- 241001135871 Gentiana scabra Species 0.000 claims description 10
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 10
- 241001343339 Swertia bimaculata Species 0.000 claims description 10
- 238000000605 extraction Methods 0.000 claims description 9
- 239000000463 material Substances 0.000 claims description 9
- 230000001105 regulatory effect Effects 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 241000597000 Freesia Species 0.000 claims description 6
- 241000501743 Gentiana macrophylla Species 0.000 claims description 6
- 230000002421 anti-septic effect Effects 0.000 claims description 6
- 239000006185 dispersion Substances 0.000 claims description 6
- 229940100555 2-methyl-4-isothiazolin-3-one Drugs 0.000 claims description 5
- CYDQOEWLBCCFJZ-UHFFFAOYSA-N 4-(4-fluorophenyl)oxane-4-carboxylic acid Chemical compound C=1C=C(F)C=CC=1C1(C(=O)O)CCOCC1 CYDQOEWLBCCFJZ-UHFFFAOYSA-N 0.000 claims description 5
- LVDKZNITIUWNER-UHFFFAOYSA-N Bronopol Chemical compound OCC(Br)(CO)[N+]([O-])=O LVDKZNITIUWNER-UHFFFAOYSA-N 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 238000010438 heat treatment Methods 0.000 claims description 5
- BEGLCMHJXHIJLR-UHFFFAOYSA-N methylisothiazolinone Chemical compound CN1SC=CC1=O BEGLCMHJXHIJLR-UHFFFAOYSA-N 0.000 claims description 5
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 5
- 235000010234 sodium benzoate Nutrition 0.000 claims description 5
- 239000004299 sodium benzoate Substances 0.000 claims description 5
- 239000011780 sodium chloride Substances 0.000 claims description 5
- 229940046000 sodium isostearoyl lactylate Drugs 0.000 claims description 5
- 239000001540 sodium lactate Substances 0.000 claims description 5
- 229940005581 sodium lactate Drugs 0.000 claims description 5
- 235000011088 sodium lactate Nutrition 0.000 claims description 5
- FOSNFLMXYRQNAF-UHFFFAOYSA-M sodium;2-[2-(16-methylheptadecanoyloxy)propanoyloxy]propanoate Chemical compound [Na+].CC(C)CCCCCCCCCCCCCCC(=O)OC(C)C(=O)OC(C)C([O-])=O FOSNFLMXYRQNAF-UHFFFAOYSA-M 0.000 claims description 5
- 238000004140 cleaning Methods 0.000 claims description 4
- PYIXHKGTJKCVBJ-UHFFFAOYSA-N Astraciceran Natural products C1OC2=CC(O)=CC=C2CC1C1=CC(OCO2)=C2C=C1OC PYIXHKGTJKCVBJ-UHFFFAOYSA-N 0.000 claims description 3
- NDVRQFZUJRMKKP-UHFFFAOYSA-N Betavulgarin Natural products O=C1C=2C(OC)=C3OCOC3=CC=2OC=C1C1=CC=CC=C1O NDVRQFZUJRMKKP-UHFFFAOYSA-N 0.000 claims description 3
- IHPVFYLOGNNZLA-UHFFFAOYSA-N Phytoalexin Natural products COC1=CC=CC=C1C1OC(C=C2C(OCO2)=C2OC)=C2C(=O)C1 IHPVFYLOGNNZLA-UHFFFAOYSA-N 0.000 claims description 3
- 238000001816 cooling Methods 0.000 claims description 3
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- 239000000280 phytoalexin Substances 0.000 claims description 3
- 150000001857 phytoalexin derivatives Chemical class 0.000 claims description 3
- 238000005070 sampling Methods 0.000 claims description 3
- 238000007789 sealing Methods 0.000 claims description 3
- 238000007873 sieving Methods 0.000 claims description 3
- 238000001291 vacuum drying Methods 0.000 claims description 3
- 238000005238 degreasing Methods 0.000 claims 8
- YGSDEFSMJLZEOE-UHFFFAOYSA-N salicylic acid Chemical compound OC(=O)C1=CC=CC=C1O YGSDEFSMJLZEOE-UHFFFAOYSA-N 0.000 claims 2
- JZKFHQMONDVVNF-UHFFFAOYSA-N dodecyl sulfate;tris(2-hydroxyethyl)azanium Chemical compound OCCN(CCO)CCO.CCCCCCCCCCCCOS(O)(=O)=O JZKFHQMONDVVNF-UHFFFAOYSA-N 0.000 claims 1
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 claims 1
- 229960004889 salicylic acid Drugs 0.000 claims 1
- 239000000686 essence Substances 0.000 abstract description 12
- 235000002991 Coptis groenlandica Nutrition 0.000 abstract description 9
- 230000000694 effects Effects 0.000 abstract description 8
- 206010039792 Seborrhoea Diseases 0.000 abstract description 4
- 235000015097 nutrients Nutrition 0.000 abstract description 3
- 238000005202 decontamination Methods 0.000 abstract description 2
- 230000003588 decontaminative effect Effects 0.000 abstract description 2
- 230000003648 hair appearance Effects 0.000 abstract description 2
- 239000013589 supplement Substances 0.000 abstract description 2
- 244000247747 Coptis groenlandica Species 0.000 abstract 1
- 239000001180 angelica archangelica l. root extract Substances 0.000 abstract 1
- 230000003700 hair damage Effects 0.000 abstract 1
- 241000382455 Angelica sinensis Species 0.000 description 8
- 241000218202 Coptis Species 0.000 description 8
- CEZCCHQBSQPRMU-UHFFFAOYSA-L chembl174821 Chemical compound [Na+].[Na+].COC1=CC(S([O-])(=O)=O)=C(C)C=C1N=NC1=C(O)C=CC2=CC(S([O-])(=O)=O)=CC=C12 CEZCCHQBSQPRMU-UHFFFAOYSA-L 0.000 description 4
- 230000009286 beneficial effect Effects 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000003205 fragrance Substances 0.000 description 2
- 239000011148 porous material Substances 0.000 description 2
- 230000002633 protecting effect Effects 0.000 description 2
- 210000004761 scalp Anatomy 0.000 description 2
- 229940095673 shampoo product Drugs 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 240000002262 Litsea cubeba Species 0.000 description 1
- 235000012854 Litsea cubeba Nutrition 0.000 description 1
- 239000004721 Polyphenylene oxide Substances 0.000 description 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 238000007605 air drying Methods 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 229920000570 polyether Polymers 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 238000005728 strengthening Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/008—Preparations for oily hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/02—Preparations for cleaning the hair
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Biotechnology (AREA)
- Engineering & Computer Science (AREA)
- Botany (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a deoiling shampoo, which comprises the components of water, sodium laureth sulfate, citric acid, cocamide MEA, allantoin, polyquaternium-10, betaine salicylate, sodium lauroyl glutamate, cocamide DEA, lauryl sulfate TEA salt, cocamidopropyl hydroxysultaine, TRH-80, polyquaternium-6, a preservative, plant antipruritic, essence, angelica root extract, brown algae extract, camellia leaf extract, coptis extract and pigment. The shampoo disclosed by the invention is simple in preparation process, mild and free of hair damage, has excellent oil removal and decontamination functions, has a certain nourishing and repairing effect on hair, can supplement nutrient balance water and oil required by hair, and is especially suitable for people with oily hair quality.
Description
Technical Field
The invention belongs to the technical field of daily washing and chemical products, and particularly relates to a deoiling shampoo.
Background
The shampoo is also called shampoo, shampoo and the like, and has various kinds on the market, and the respective efficacies are also different, and the quality difference is larger.
At present, the development trend of shampoo products is diversified, and people select the shampoos with different efficacies according to the problems of the people. Although the existing shampoos can play a basic decontamination function, a plurality of chemical components are added into the components, for example, the addition of various essences has poor oil removal effect on people with oily hair, thereby influencing the using effect of the shampoos.
Disclosure of Invention
The invention mainly solves the technical problem of providing the deoiling shampoo, the preparation process of the shampoo is simple, the prepared shampoo is mild and does not damage hair, the shampoo has excellent deoiling and decontaminating functions, simultaneously has certain nourishing and repairing functions on the hair, replenishes nutrient balance water and oil required by the hair, and is particularly suitable for people with oily hair.
In order to solve the technical problems, the invention adopts a technical scheme that:
a deoiling shampoo is prepared from water, sodium laureth sulfate, citric acid, cocamide MEA, allantoin, polyquaternium-10, betaine salicylate, sodium lauroyl glutamate, cocamide DEA, lauryl sulfate TEA salt, cocamidopropyl hydroxysultaine, TRH-80, polyquaternium-6, antiseptic, plant antipruritic essence, radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, brown algae (PHYLLACANTHA FIBROSA) extract, folium Camelliae Japonicae (Camellia JAPONICA) extract, Coptidis rhizoma (Coptis CHINENSIS) extract and pigment by mixing, heating, emulsifying, and homogenizing.
Further, the deoiling shampoo comprises the following components in percentage by weight: 54-69% of water, 14-18% of sodium laureth sulfate, 0.03-0.06% of citric acid, 1.5-2.5% of cocamide MEA, 0.1-0.3% of allantoin, 0.2-0.3% of polyquaternium-10, 0.3-0.35% of betaine salicylate, 6-6.5% of sodium lauroyl glutamate, 1.5-2.5% of cocamide DEA, 3-5% of lauryl sulfate TEA salt, 1-3% of cocamidopropyl hydroxysultaine, 1-3% of TRH-80, 0.4-1.4% of polyquaternium-6, 0.1-0.3% of preservative, 0.3-0.7% of phytoanthelmicin, 0.1-1% of essence, 0.1-0.3% of Angelica SINENSIS (GEANLIENSINSIS) root extract, 0.1-0.3% of PHA (PO PHYLLACANTHA FIBROSA) extract, 0.1-0.3% of Camellia JAPONICA (CAJACA) leaf extract, 0.1-0.3% of Coptidis rhizoma (Coptis CHINENSIS) extract and 0.1-0.2% of pigment.
Further, the sodium laureth sulfate is prepared by compounding 30% of water and 70% of sodium laureth sulfate in percentage by weight;
the cocamidopropyl hydroxysultaine is prepared by compounding 29.5% of cocamidopropyl hydroxysultaine, 4.5% of sodium chloride, 0.5% of sodium benzoate and 65.5% of water in percentage by weight.
Further, the TRH-80 components are, by weight, 70% water, 20% oleamidopropyl PG-dimethylammonium chloride, 8.5% sodium lactate and 1.5% sodium isostearoyl lactylate.
The preservative comprises 94% of water, 2.5% of methylisothiazolinone and 3.5% of 2-bromo-2-nitropropane-1, 3-diol in percentage by weight.
Further, the plant antipruritic comprises, by weight, 0.135% of Gentiana MACROPHYLLA (Gentiana MACROPHYLLA) extract, 0.75% of SWERTIA BIMACULATA (SWERTIA BIMACULATA) extract, 0.135% of Gentiana SCABRA (Gentiana SCABRA) extract, 59.98% of water and 39% of propylene glycol.
Further, the ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract is specifically composed of 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract in percentage by weight;
the brown algae (PHYLLACANTHA FIBROSA) extract is specifically composed of 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of brown algae (PHYLLACANTHA FIBROSA) extract in percentage by weight;
the CAMELLIA (CAMELLIA JAPONICA) leaf extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of CAMELLIA (CAMELLIA JAPONICA) leaf extract in percentage by weight;
the COPTIS CHINENSIS (coptidis CHINENSIS) extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of COPTIS CHINENSIS (coptidis CHINENSIS) extract in percentage by weight.
Further, the essence is freesia; the pigments are lemon yellow CI19140 and red 40CI 16035.
The preparation method of the deoiling shampoo comprises the following steps:
s1, heating an emulsification pot filled with pure water with corresponding weight percentage to 80-90 ℃, adding sodium laureth sulfate with corresponding weight percentage into the emulsification pot, homogenizing and stirring at a rotating speed of 400r/min, and fully dissolving to obtain a first mixture;
s2, sequentially adding citric acid, cocamide MEA and allantoin in corresponding weight percentages into the first mixture obtained in the step S1, and homogenizing and stirring for 3-8min to obtain a second mixture;
s3, slowly adding polyquaternium-10 into cold pure water according to the formula amount, uniformly mixing to obtain polyquaternium-10 dispersion liquid, adding the polyquaternium-10 dispersion liquid into the second mixture obtained in the step S2, continuously and uniformly stirring for 3-8min in an emulsifying pot, fully mixing, keeping the temperature at 80-85 ℃ for 5-15min, and cooling to 40-60 ℃ to obtain a third mixture;
s4, adding betaine salicylate and sodium lauroyl glutamate with corresponding weight percentage into the emulsifying pot filled with the third mixture in the step S3, and homogenizing and stirring for 3-8min to obtain a fourth mixture;
s5, adding cocamide DEA, lauryl sulfate TEA salt, cocamidopropyl hydroxysulfobetaine, TRH-80, polyquaternium-6, antiseptic, phytoalexin, essence, radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, brown algae (PHYLLACANTHA FIBROSA) extract, herba Camelliae Japonicae (Camellia JAPONICA) leaf extract, rhizoma Coptidis (Coptis CHINENSIS) extract, lemon yellow CI19140 and red 40CI 5 in sequence with corresponding weight percentage to the fourth mixture obtained in step S4, homogenizing and stirring for 5-15min, sampling and inspecting to obtain deoiling shampoo.
Further, the ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract, brown algae (PHYLLACANTHA FIBROSA) extract, CAMELLIA (CAMELLIA JAPONICA) leaf extract and COPTIS (coptidis CHINENSIS) extract are prepared based on the following extraction process steps, and specifically comprise:
s1, removing impurities in the plant raw materials, cleaning the plant raw materials with water, and then placing the plant raw materials in an air-blast drying oven at 50-55 ℃ for drying treatment to obtain the purified plant raw materials;
s2, placing the plant raw material cleaned in the step S1 into a flash extractor at room temperature, and extracting the plant raw material according to the proportion of 1: adding 80-100% ethanol water solution into 10-30 of the material-liquid ratio, extracting the cleaned plant raw material by using a flash extractor under the conditions of 200-230V voltage and 7500-10000r/min rotating speed for 50-100s, sieving the prepared extracting solution by using a 50-60 mesh sieve, and collecting to obtain the filtered plant raw material extracting solution;
s3, placing the plant material extracting solution obtained in the step S2 in a rotary evaporator for vacuum concentration, and then transferring the plant material extracting solution into a vacuum drying oven to be dried at 40-50 ℃ to obtain the plant material extract.
Further, in the above process of preparing the deoiling shampoo, the cover of the emulsifying pot is provided with an independent feeding device:
the feeding device comprises a feeding cylinder, a liquid feeding pipeline and a powder feeding pipeline;
a cylinder cover is arranged above the feeding cylinder, and an annular sealing ring is arranged on the inner side of the cylinder cover, so that the feeding cylinder is in a sealed environment after the cylinder cover is arranged on the feeding cylinder cover;
a rotary table is fixedly connected below the feeding cylinder, and the feeding cylinder is connected with the liquid feeding pipeline and the powder feeding pipeline through the rotary table; one or more small holes are formed in the rotary table, and the diameter of each small hole is the same as that of the liquid feeding pipeline or the powder feeding pipeline; the feed cylinder is selected to be communicated with the liquid feed pipeline or the powder feed pipeline through the rotation of the turntable, and liquid or powder raw materials are conveyed;
the rotation of the rotary disc is controlled by a PLC control system of the emulsifying pot;
the liquid feeding pipeline penetrates through the pot cover and extends into the emulsifying pot;
the liquid feeding pipeline positioned outside the pot cover is provided with a pressure regulating valve, the pressure regulating valve is connected with a booster pump through a pipeline, and the liquid feeding pipeline realizes the rapid conveying of liquid raw materials in the pipeline by virtue of the pressurization of the booster pump;
the tail end of a liquid feeding pipe which is positioned at the inner side of the pot cover and extends into the emulsifying pot is provided with a hollow cone nozzle which is used for generating raw material liquid drops with uniform size and falling into mixed liquid in the emulsifying pot so as to increase the contact area of each liquid raw material and accelerate emulsification;
the powder feeding pipeline penetrates through the pot cover and extends into the emulsifying pot;
and an air exhaust regulating valve is arranged on the powder feeding pipeline outside the pot cover and is connected with the micro vacuum pump through a pipeline, and air flow in the pipeline is formed in the powder feeding pipeline by means of air pressure difference, so that the powder raw materials are driven to move, and the purpose of conveying the powder raw materials is achieved.
The invention has the following beneficial effects:
(1) the deoiling shampoo disclosed by the invention is simple in preparation process, can deeply clean greasy dirt, and also has a certain nourishing and repairing effect on hair and even scalp to tighten pores;
(2) the deoiling shampoo is mild and does not damage hair, can supplement nutrients required by hair, balance grease secretion, dredge pores, strengthen hair roots and is suitable for people with oily hair quality;
(3) the deoiling shampoo disclosed by the invention is prepared by extracting effective components in ANGELICA (ANGELICA POLYMORPHA SINENSIS) root, brown algae (PHYLLACANTHA FIBROSA), CAMELLIA (CAMELLIA JAPONICA) leaf and COPTIS (coptidis CHINENSIS) to the maximum extent through a flash extraction technology, has the advantages of high extraction efficiency, short extraction time and the like, and effectively enhances the effects of applying the ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract, the brown algae (PHYLLACANTHA FIBROSA) extract, the CAMELLIA (CAMELLIA JAPONICA) leaf extract and the COPTIS (coptidis CHINENSIS) extract to the deoiling shampoo, and has the nourishing and protecting effects on hair;
(4) in the process of preparing the deoiling shampoo, the independent feeding device is arranged on the pot cover of the emulsifying pot, the operation is simple and easy, the cost is low, the complex operation that the pot cover needs to be opened repeatedly in the process of emulsifying the homogenized deoiling shampoo raw material in the emulsifying pot is reduced, the working efficiency of the equipment is improved, and the emulsification effect of the deoiling shampoo mixed raw material is enhanced in an auxiliary manner; also ensures the stability of the environment in the emulsifying pot in the preparation process and avoids the condition that the quality of the deoiling shampoo product is not stable due to the preparation environment.
Detailed Description
The following detailed description of the preferred embodiments of the present invention is provided to enable those skilled in the art to more readily understand the advantages and features of the present invention, and to clearly and unequivocally define the scope of the present invention.
Example 1
Deoiling shampoo
The deoiling shampoo comprises water, sodium laureth sulfate, citric acid, cocamide MEA, allantoin, polyquaternium-10, betaine salicylate, sodium lauroyl glutamate, cocamide DEA, lauryl sulfate TEA salt, cocamidopropyl hydroxysultaine, TRH-80, polyquaternium-6, antiseptic, plant antipruritic, essence, radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, brown algae (PHYLLACANTHA FIBROSA) extract, folium Camelliae Japonicae (Camellia JAPONICA) extract, Coptidis rhizoma (Coptis CHINENSIS) extract, lemon yellow CI19140 and Red 40CI 16035.
The contents of the components are respectively as follows according to the weight percentage: 61.7175% water, 16% sodium laureth sulfate, 0.05% citric acid, 2% cocamide MEA, 0.2% allantoin, 0.25% polyquaternium-10, 0.32% betaine salicylate, 6.3% sodium lauroyl glutamate, 2% cocamide DEA, 4% lauryl sulfate TEA salt, 2% cocamidopropyl hydroxysultaine, 2% TRH-80, 1% polyquaternium-6, 0.2% preservative, 0.5% phytoncide, 0.3% freesia, 0.25% Angelica SINENSIS (ANGELICA POLYMORPA SINENSIS) root extract, 0.25% brown algae (PHYLLACANTHA FIBROSA) extract, 0.25% CAMELLIA (CAMELLIA JANICA) leaf extract, 0.25% COPTIS (COPTIS) extract, 0.154% lemon yellow 19140, and 0.0085% red 40/red 40 (16035);
the sodium laureth sulfate is prepared by compounding 30% of water and 70% of sodium laureth sulfate in percentage by weight;
according to the weight percentage, the cocamidopropyl hydroxysultaine is specifically prepared by compounding 29.5 percent of cocamidopropyl hydroxysultaine, 4.5 percent of sodium chloride, 0.5 percent of sodium benzoate and 65.5 percent of water;
the TRH-80 comprises the components of 70 percent of water, 20 percent of oleamidopropyl PG-dimethyl ammonium chloride, 8.5 percent of sodium lactate and 1.5 percent of sodium isostearoyl lactylate in percentage by weight;
the preservative comprises the components of 94% of water, 2.5% of methylisothiazolinone and 3.5% of 2-bromo-2-nitropropane-1, 3-diol in percentage by weight;
the plant antipruritic comprises (by weight percentage) radix Gentianae Macrophyllae (GENTIANA MACROPHYLLA) extract 0.135%, SWERTIA BIMACULATA (SWERTIA BIMACULATA) extract 0.75%, GENTIANA SCABRA (GENTIANA SCABRA) extract 0.135%, 59.98% water and 39% propylene glycol;
the ANGELICA SINENSIS (ANGELICA POLYMORPHA SINENSIS) root extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of ANGELICA SINENSIS (ANGELICA POLYMORPHA SINENSIS) root extract according to weight percentage;
the brown algae (PHYLLACANTHA FIBROSA) extract is specifically composed of 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of brown algae (PHYLLACANTHA FIBROSA) extract in percentage by weight;
the CAMELLIA (CAMELLIA JAPONICA) leaf extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of CAMELLIA (CAMELLIA JAPONICA) leaf extract in percentage by weight;
the COPTIS CHINENSIS (Coptis CHINENSIS) extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of COPTIS CHINENSIS (Coptis CHINENSIS) extract according to weight percentage;
the essence is freesia; the pigments are lemon yellow CI19140 and red 40CI 16035.
Example 2
Deoiling shampoo
The difference from the embodiment 1 is that the contents of the components are respectively as follows according to the weight percentage: 62.6245% water, 15% sodium laureth sulfate, 0.06% citric acid, 2% cocamide MEA, 0.25% allantoin, 0.27% polyquaternium-10, 0.33% betaine salicylate, 6.1% sodium lauroyl glutamate, 2% cocamide DEA, 3.8% lauryl sulfate TEA salt, 2% cocamidopropyl hydroxysultaine, 2% TRH-80, 1.3% polyquaternium-6, 0.2% preservative, 0.6% phytoanthelmicin, 0.3% litsea cubeba, 0.2% Angelica SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, 0.3% brown algae (PHYLLACANTHA FIBROSA) extract, 0.25% CAMELLIA (Camellia JAPONICA) leaf extract, 0.25% COPTIS CHINENSIS (Coptis CHINENSIS NSIS) extract, 0.157% lemon yellow extract, 0.19140% and 0.0085% red 40 CI;
the sodium laureth sulfate is prepared by compounding 30% of water and 70% of sodium laureth sulfate in percentage by weight;
according to the weight percentage, the cocamidopropyl hydroxysultaine is specifically prepared by compounding 29.5 percent of cocamidopropyl hydroxysultaine, 4.5 percent of sodium chloride, 0.5 percent of sodium benzoate and 65.5 percent of water;
the TRH-80 comprises the components of 70 percent of water, 20 percent of oleamidopropyl PG-dimethyl ammonium chloride, 8.5 percent of sodium lactate and 1.5 percent of sodium isostearoyl lactylate in percentage by weight;
the preservative comprises the components of 94% of water, 2.5% of methylisothiazolinone and 3.5% of 2-bromo-2-nitropropane-1, 3-diol in percentage by weight;
the plant antipruritic comprises (by weight percentage) radix Gentianae Macrophyllae (GENTIANA MACROPHYLLA) extract 0.135%, SWERTIA BIMACULATA (SWERTIA BIMACULATA) extract 0.75%, GENTIANA SCABRA (GENTIANA SCABRA) extract 0.135%, 59.98% water and 39% propylene glycol;
the ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract in percentage by weight;
the brown algae (PHYLLACANTHA FIBROSA) extract is specifically composed of 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of brown algae (PHYLLACANTHA FIBROSA) extract in percentage by weight;
the CAMELLIA (CAMELLIA JAPONICA) leaf extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of CAMELLIA (CAMELLIA JAPONICA) leaf extract in percentage by weight;
the COPTIS CHINENSIS (coptidis CHINENSIS) extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of COPTIS CHINENSIS (coptidis CHINENSIS) extract in percentage by weight;
the essence is freesia; the pigments are lemon yellow CI19140 and red 40CI 16035.
Example 3
Deoiling shampoo
The difference from the embodiment 1 is that the contents of the components are respectively as follows according to the weight percentage: 60.5565% water, 16% sodium laureth sulfate, 0.05% citric acid, 2.2% cocamide MEA, 0.22% allantoin, 0.25% polyquaternium-10, 0.31% betaine salicylate, 6.2% sodium lauroyl glutamate, 2.1% cocamide DEA, 4.3% lauryl sulfate TEA salt, 2.5% cocamidopropyl hydroxysultaine, 2% TRH-80, 1.1% polyquaternium-6, 0.2% preservative, 0.55% phytoncide, 0.3% essence, 0.3% Angelica SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, 0.25% brown algae (PHYLLACANTHA FIBROSA) extract, 0.2% CAMELLIA (Camellia JAPONICA) leaf extract, 0.25% COPTIS CHINENSIS (Coptis CHINENSIS) extract, 0.155% lemon yellow 19140 and 0.005% red 1603 40;
the sodium laureth sulfate is prepared by compounding 30% of water and 70% of sodium laureth sulfate in percentage by weight;
according to the weight percentage, the cocamidopropyl hydroxysultaine is specifically prepared by compounding 29.5 percent of cocamidopropyl hydroxysultaine, 4.5 percent of sodium chloride, 0.5 percent of sodium benzoate and 65.5 percent of water;
the TRH-80 comprises the components of 70 percent of water, 20 percent of oleamidopropyl PG-dimethyl ammonium chloride, 8.5 percent of sodium lactate and 1.5 percent of sodium isostearoyl lactylate in percentage by weight;
the preservative comprises the components of 94% of water, 2.5% of methylisothiazolinone and 3.5% of 2-bromo-2-nitropropane-1, 3-diol in percentage by weight;
the plant antipruritic comprises (by weight percentage) radix Gentianae Macrophyllae (GENTIANA MACROPHYLLA) extract 0.135%, SWERTIA BIMACULATA (SWERTIA BIMACULATA) extract 0.75%, GENTIANA SCABRA (GENTIANA SCABRA) extract 0.135%, 59.98% water and 39% propylene glycol;
the ANGELICA SINENSIS (ANGELICA POLYMORPHA SINENSIS) root extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of ANGELICA SINENSIS (ANGELICA POLYMORPHA SINENSIS) root extract according to weight percentage;
the brown algae (PHYLLACANTHA FIBROSA) extract is specifically composed of 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of brown algae (PHYLLACANTHA FIBROSA) extract in percentage by weight;
the CAMELLIA (CAMELLIA JAPONICA) leaf extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of CAMELLIA (CAMELLIA JAPONICA) leaf extract in percentage by weight;
the COPTIS CHINENSIS (coptidis CHINENSIS) extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of COPTIS CHINENSIS (coptidis CHINENSIS) extract in percentage by weight;
the essence is freesia; the pigments are lemon yellow CI19140 and red 40CI 16035.
Example 1-example 3 deoiling shampoos were prepared as follows, including:
s1, heating an emulsification pot filled with pure water according to the corresponding weight percentage to 85 ℃, adding sodium lauryl polyether sulfate according to the corresponding weight percentage into the emulsification pot, homogenizing and stirring at the rotating speed of 400r/min, and fully dissolving to obtain a first mixture;
s2, sequentially adding citric acid, cocamide MEA and allantoin in corresponding weight percentages into the first mixture obtained in the step S1, and homogenizing and stirring for 5min to obtain a second mixture;
s3, slowly adding polyquaternium-10 into cold pure water according to the formula amount, uniformly mixing to obtain polyquaternium-10 dispersion liquid, adding the polyquaternium-10 dispersion liquid into the second mixture obtained in the step S2, continuously and uniformly stirring for 5min in an emulsifying pot, fully mixing, keeping the temperature at 85 ℃ for 10min, and cooling to 50 ℃ to obtain a third mixture;
s4, adding the betaine salicylate and the sodium lauroyl glutamate with corresponding weight percentages into the emulsifying pot filled with the third mixture in the step S3, and homogenizing and stirring for 5min to obtain a fourth mixture;
s5, adding cocamide DEA, lauryl sulfate TEA salt, cocamidopropyl hydroxysulfobetaine, TRH-80, polyquaternium-6, antiseptic, phytoalexin, essence, radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, brown algae (PHYLLACANTHA FIBROSA) extract, herba Camelliae Japonicae (Camellia JAPONICA) leaf extract, rhizoma Coptidis (Coptis CHINENSIS) extract, lemon yellow CI19140 and red 40CI 5 in sequence with corresponding weight percentage to the fourth mixture obtained in step S4, homogenizing and stirring for 10min, sampling and inspecting to obtain the deoiling shampoo.
The shampoos prepared in examples 1-3 were compared for their relevant properties and the results are shown in the following table:
appearance of the product | Fragrance | pH value | Consistency (25 ℃ C.) | |
Example 1 | Yellow liquid | C188 | 5.8 | 13470CPS |
Example 2 | Yellow liquid | C188 | 5.9 | 13892CPS |
Example 3 | Yellow liquid | C188 | 6.1 | 13544CPS |
As can be seen from the data in the table, the deoiling shampoo prepared by the embodiment of the invention is weakly acidic, has no irritation to hair and scalp, and has the effects of being mild, not damaging hair, deeply cleaning greasy dirt, nourishing and repairing hair and strengthening hair root; the appearance, fragrance and consistency of the deoiling shampoo of the invention meet the acceptance and liking degree of the public consumers.
Example 4
The ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract, the brown algae (PHYLLACANTHA FIBROSA) extract, the CAMELLIA (CAMELLIA JAPONICA) leaf extract, and the COPTIS (coptidis CHINENSIS) extract described in example 1-example 3 are prepared based on the following extraction process steps, and specifically include:
s1, removing impurities in the plant raw materials, cleaning the plant raw materials with water, and then placing the plant raw materials in a forced air drying oven for drying treatment at 50 ℃ to obtain the cleaned plant raw materials;
s2, placing the plant raw material cleaned in the step S1 into a flash extractor at room temperature, and extracting the plant raw material according to the proportion of 1: adding 100% ethanol water solution into 20 of the feed liquid ratio, extracting the cleaned plant raw material by using a flash extractor under the conditions of 220V voltage and 8000r/min of rotation speed for 75s, sieving the prepared extracting solution by using a 60-mesh sieve, and collecting to obtain filtered plant raw material extracting solution;
s3, placing the plant material extracting solution obtained in the step S2 in a rotary evaporator for vacuum concentration, and then transferring the plant material extracting solution into a vacuum drying oven to be dried at the temperature of 45 ℃ to obtain the plant material extract.
The working principle and the beneficial effects of the embodiment are as follows: in the invention, the effective components in ANGELICA (ANGELICA POLYMORPHA SINENSIS) root, brown algae (PHYLLACANTHA FIBROSA), CAMELLIA (CAMELLIA JAPONICA) leaf and COPTIS (coptidis CHINENSIS) are prepared into the extract to the maximum extent by a flash extraction technology, so that the invention has the advantages of high extraction efficiency, short extraction time and the like, and effectively enhances the nourishing and protecting effects on hair when the ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract, the brown algae (PHYLLACANTHA FIBROSA) extract, the CAMELLIA (CAMELLIA JAPONICA) leaf extract and the COPTIS (coptidis CHINENSIS) extract are applied to the oil-removing shampoo.
Example 5
Examples 1-3 de-oiling shampoos were prepared, with a separate feed device on the lid of the emulsification pan:
the feeding device comprises a feeding cylinder, a liquid feeding pipeline and a powder feeding pipeline;
a cylinder cover is arranged above the feeding cylinder, and an annular sealing ring is arranged on the inner side of the cylinder cover, so that the feeding cylinder is in a sealed environment after the cylinder cover is arranged on the feeding cylinder cover;
a rotary table is fixedly connected below the feeding cylinder, and the feeding cylinder is connected with the liquid feeding pipeline and the powder feeding pipeline through the rotary table; one or more small holes are formed in the rotary table, and the diameter of each small hole is the same as that of the liquid feeding pipeline or the powder feeding pipeline; the feed cylinder is selected to be communicated with the liquid feed pipeline or the powder feed pipeline through the rotation of the turntable, and liquid or powder raw materials are conveyed;
the rotation of the rotary disc is controlled by a PLC control system of the emulsifying pot;
the liquid feeding pipeline penetrates through the pot cover and extends into the emulsifying pot;
the liquid feeding pipeline positioned outside the pot cover is provided with a pressure regulating valve, the pressure regulating valve is connected with a booster pump through a pipeline, and the liquid feeding pipeline realizes the rapid conveying of liquid raw materials in the pipeline by virtue of the pressurization of the booster pump;
the tail end of a liquid feeding pipe which is positioned at the inner side of the pot cover and extends into the emulsifying pot is provided with a hollow cone nozzle which is used for generating raw material liquid drops with uniform size and falling into mixed liquid in the emulsifying pot so as to increase the contact area of each liquid raw material and accelerate emulsification;
the powder feeding pipeline penetrates through the pot cover and extends into the emulsifying pot;
and an air exhaust regulating valve is arranged on the powder feeding pipeline positioned outside the pot cover and is connected with the micro vacuum pump through a pipeline, and air flow in the pipeline is formed in the powder feeding pipeline by means of air pressure difference, so that the powder raw materials are driven to move, and the purpose of conveying the powder raw materials is achieved.
The working principle and the beneficial effects of the embodiment are as follows: in the process of preparing the deoiling shampoo, the independent feeding device is arranged on the pot cover of the emulsifying pot, the operation is simple and easy, the cost is low, the complex operation that the pot cover needs to be opened repeatedly in the process of emulsifying the homogenized deoiling shampoo raw material in the emulsifying pot is reduced, the working efficiency of the equipment is improved, and the emulsification effect of the deoiling shampoo mixed raw material is enhanced in an auxiliary manner; also ensures the stability of the environment in the emulsifying pot in the preparation process and avoids the condition that the quality of the deoiling shampoo product is not stable due to the preparation environment.
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all equivalent structural changes made by using the contents of the present specification, or any other related technical fields directly or indirectly, are included in the scope of the present invention.
Claims (10)
1. A de-oiling shampoo is characterized in that: the deoiling shampoo is prepared by mixing, heating, emulsifying and homogenizing water, sodium laureth sulfate, citric acid, cocamide MEA, allantoin, polyquaternium-10, betaine salicylate, sodium lauroyl glutamate, cocamide DEA, lauryl sulfate TEA salt, cocamidopropyl hydroxysultaine, TRH-80, polyquaternium-6, antiseptic, plant antipruritic, essence, radix Angelicae SINENSIS ANGELICA POLYMORPHISINENSIS root extract, brown algae (PHYLLACANTHA FIBROSA) extract, herba Camelliae Japonicae (CAMELLIA JAPONICA) leaf extract, rhizoma Coptidis (Coptis CHINENSIS) extract and pigment.
2. A degreasing shampoo as in claim 1 wherein: the deoiling shampoo comprises the following components in percentage by weight: 54-69% of water, 14-18% of sodium laureth sulfate, 0.03-0.06% of citric acid, 1.5-2.5% of cocamide MEA, 0.1-0.3% of allantoin, 0.2-0.3% of polyquaternium-10, 0.3-0.35% of salicylic acid, 6-6.5% of sodium lauroyl glutamate, 1.5-2.5% of cocamide DEA, 3-5% of TEA lauryl sulfate, 1-3% of cocamidopropyl hydroxysultaine, 1-3% of TRH-80, 0.4-1.4% of polyquaternium-6, 0.1-0.3% of preservative, 0.3-0.7% of plant antipruritic, 0.1-1% of essence, 0.1-0.3% of radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, 0.1-0.3% of brown algae (PHYLLACANTHA FIBROSA) extract, 0.1-0.3% of CAMELLIA (Camellia JAPONICA) leaf extract, 0.1-0.3% of COPTIS CHINENSIS (Coptis CHINENSIS) extract and 0.1-0.2% of pigment.
3. A degreasing shampoo as in claim 1 wherein: the sodium laureth sulfate is prepared by compounding 30 percent of water and 70 percent of sodium laureth sulfate in percentage by weight;
the cocamidopropyl hydroxysultaine is prepared by compounding 29.5% of cocamidopropyl hydroxysultaine, 4.5% of sodium chloride, 0.5% of sodium benzoate and 65.5% of water in percentage by weight.
4. A degreasing shampoo as in claim 1 wherein: the TRH-80 comprises the components of 70 percent of water, 20 percent of oleamidopropyl PG-dimethyl ammonium chloride, 8.5 percent of sodium lactate and 1.5 percent of sodium isostearoyl lactylate in percentage by weight;
the preservative comprises 94% of water, 2.5% of methylisothiazolinone and 3.5% of 2-bromo-2-nitropropane-1, 3-diol in percentage by weight.
5. A degreasing shampoo as in claim 1 wherein: the plant antipruritic comprises (by weight) radix Gentianae Macrophyllae (GENTIANA MACROPHYLLA) extract 0.135%, SWERTIA BIMACULATA (SWERTIA BIMACULATA) extract 0.75%, GENTIANA SCABRA (GENTIANA SCABRA) extract 0.135%, 59.98% water and 39% propylene glycol.
6. A degreasing shampoo as in claim 1 wherein: the ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract in percentage by weight;
the brown algae (PHYLLACANTHA FIBROSA) extract is specifically composed of 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of brown algae (PHYLLACANTHA FIBROSA) extract in percentage by weight;
the CAMELLIA (CAMELLIA JAPONICA) leaf extract is prepared by compounding 93 percent of water, 0.45 percent of phenoxyethanol, 0.05 percent of ethylhexyl glycerol, 0.2 percent of p-hydroxyacetophenone, 1 percent of butanediol and 5.3 percent of CAMELLIA (CAMELLIA JAPONICA) leaf extract according to weight percentage;
the COPTIS CHINENSIS (coptidis CHINENSIS) extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of COPTIS CHINENSIS (coptidis CHINENSIS) extract in percentage by weight.
7. A degreasing shampoo as in claim 1 wherein: the essence is freesia; the pigments are lemon yellow CI19140 and red 40CI 16035.
8. A process for the preparation of a degreasing shampoo as claimed in any of claims 1 to 7 wherein: the method comprises the following steps:
s1, heating an emulsification pot filled with pure water with the corresponding weight percentage to 80-90 ℃, adding sodium laureth sulfate with the corresponding weight percentage into the emulsification pot, homogenizing and stirring at the rotating speed of 400r/min, and fully dissolving to obtain a first mixture;
s2, sequentially adding citric acid, cocamide MEA and allantoin in corresponding weight percentages into the first mixture obtained in the step S1, and homogenizing and stirring for 3-8min to obtain a second mixture;
s3, slowly adding polyquaternium-10 into cold pure water according to the formula amount, uniformly mixing to obtain polyquaternium-10 dispersion liquid, adding the polyquaternium-10 dispersion liquid into the second mixture obtained in the step S2, continuously and uniformly stirring for 3-8min in an emulsifying pot, fully mixing, keeping the temperature at 80-85 ℃ for 5-15min, and cooling to 40-60 ℃ to obtain a third mixture;
s4, adding betaine salicylate and sodium lauroyl glutamate with corresponding weight percentage into the emulsifying pot filled with the third mixture in the step S3, and homogenizing and stirring for 3-8min to obtain a fourth mixture;
s5, adding cocamide DEA, lauryl sulfate TEA salt, cocamidopropyl hydroxysulfobetaine, TRH-80, polyquaternium-6, antiseptic, phytoalexin, essence, radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, brown algae (PHYLLACANTHA FIBROSA) extract, herba Camelliae Japonicae (Camellia JAPONICA) leaf extract, rhizoma Coptidis (Coptis CHINENSIS) extract, lemon yellow CI19140 and red 40CI 5 in sequence with corresponding weight percentage to the fourth mixture obtained in step S4, homogenizing and stirring for 5-15min, sampling and inspecting to obtain deoiling shampoo.
9. A degreasing shampoo as in claim 6 wherein: the radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, brown algae (PHYLLACANTHA FIBROSA) extract, folium Camelliae SINENSIS (Camellia JAPONICA) extract and rhizoma Coptidis (Coptis CHINENSIS) extract are prepared by the following extraction process steps, and specifically comprise:
s1, removing impurities in the plant raw materials, cleaning the plant raw materials with water, and then placing the plant raw materials in an air-blast drying oven at 50-55 ℃ for drying treatment to obtain the purified plant raw materials;
s2, placing the plant raw material cleaned in the step S1 into a flash extractor at room temperature, and extracting the plant raw material according to the proportion of 1: adding 80-100% ethanol water solution into 10-30 of the material-liquid ratio, extracting the cleaned plant raw material by using a flash extractor under the conditions of 200-230V voltage and 7500-10000r/min rotating speed for 50-100s, sieving the prepared extracting solution by using a 50-60 mesh sieve, and collecting to obtain the filtered plant raw material extracting solution;
s3, placing the plant material extracting solution obtained in the step S2 in a rotary evaporator for vacuum concentration, and then transferring the plant material extracting solution into a vacuum drying oven to be dried at 40-50 ℃ to obtain the plant material extract.
10. The method according to claim 8, wherein said emulsifying pan is provided with a separate feeding device on the lid:
the feeding device comprises a feeding cylinder, a liquid feeding pipeline and a powder feeding pipeline;
a cylinder cover is arranged above the feeding cylinder, and an annular sealing ring is arranged on the inner side of the cylinder cover, so that the feeding cylinder is in a sealed environment after the cylinder cover is arranged on the feeding cylinder cover;
a rotary table is fixedly connected below the feeding cylinder, and the feeding cylinder is connected with the liquid feeding pipeline and the powder feeding pipeline through the rotary table; one or more small holes are formed in the rotary table, and the diameter of each small hole is the same as that of the liquid feeding pipeline or the powder feeding pipeline; the feed cylinder is selected to be communicated with the liquid feed pipeline or the powder feed pipeline through the rotation of the turntable, and liquid or powder raw materials are conveyed;
the rotation of the rotary disc is controlled by a PLC control system of the emulsifying pot;
the liquid feeding pipeline penetrates through the pot cover and extends into the emulsifying pot;
the liquid feeding pipeline positioned outside the pot cover is provided with a pressure regulating valve, the pressure regulating valve is connected with a booster pump through a pipeline, and the liquid feeding pipeline completes the rapid conveying of the liquid raw materials in the pipeline by virtue of the pressurization of the booster pump;
the tail end of a liquid feeding pipe which is positioned at the inner side of the pot cover and extends into the emulsifying pot is provided with a hollow cone nozzle which is used for generating raw material liquid drops with uniform size and falling into mixed liquid in the emulsifying pot;
the powder feeding pipeline penetrates through the pot cover and extends into the emulsifying pot;
and an air exhaust regulating valve is arranged on the powder feeding pipeline positioned outside the pot cover and is connected with the micro vacuum pump through a pipeline, and air flow in the pipeline is formed in the powder feeding pipeline by means of air pressure difference, so that the powder raw materials are driven to move, and the powder raw materials are conveyed.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115337224A (en) * | 2022-09-02 | 2022-11-15 | 深圳市菲茵尔化妆品贸易有限公司 | Shampoo liquid |
CN117017883A (en) * | 2023-08-25 | 2023-11-10 | 广州帝臣生物科技股份有限公司 | Deoiling shampoo and preparation method thereof |
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CN109846729A (en) * | 2019-04-10 | 2019-06-07 | 浙江养丝生物科技有限公司 | A kind of scalp cleaning condensation and its preparation process |
CN110123663A (en) * | 2019-05-16 | 2019-08-16 | 菏泽龙池生物科技有限公司 | A kind of shampoo and preparation method thereof cleaning scalp grease |
CN114146012A (en) * | 2021-07-30 | 2022-03-08 | 广东嘉丹婷日用品有限公司 | Antibacterial and anti-dandruff shampoo and preparation method thereof |
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CN109846729A (en) * | 2019-04-10 | 2019-06-07 | 浙江养丝生物科技有限公司 | A kind of scalp cleaning condensation and its preparation process |
CN110123663A (en) * | 2019-05-16 | 2019-08-16 | 菏泽龙池生物科技有限公司 | A kind of shampoo and preparation method thereof cleaning scalp grease |
CN114146012A (en) * | 2021-07-30 | 2022-03-08 | 广东嘉丹婷日用品有限公司 | Antibacterial and anti-dandruff shampoo and preparation method thereof |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN115337224A (en) * | 2022-09-02 | 2022-11-15 | 深圳市菲茵尔化妆品贸易有限公司 | Shampoo liquid |
CN117017883A (en) * | 2023-08-25 | 2023-11-10 | 广州帝臣生物科技股份有限公司 | Deoiling shampoo and preparation method thereof |
CN117017883B (en) * | 2023-08-25 | 2024-02-20 | 广州帝臣生物科技股份有限公司 | Deoiling shampoo and preparation method thereof |
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