CN114732768A

CN114732768A - Anti-dandruff shampoo

Info

Publication number: CN114732768A
Application number: CN202210423506.8A
Authority: CN
Inventors: 黄广文
Original assignee: Guangzhou Dichen Biotechnology Co ltd
Current assignee: Guangzhou Dichen Biotechnology Co ltd
Priority date: 2022-04-21
Filing date: 2022-04-21
Publication date: 2022-07-12

Abstract

The invention discloses an anti-dandruff shampoo, which comprises the components of pure water, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium laureth sulfate, TEA (lauryl sulfate), behenamidopropyl dimethylamine, guar gum hydroxypropyl trimethyl ammonium chloride, sodium glutamate, cocamidopropyl hydroxy sulfobetaine, citric acid, cocamido MEA (MEA), hydroxyphenylpropionamidobenzoic acid, oxidized polyethylene, hydroxyethyl urea, cyclopentadecyldimethyl siloxane, polydimethylsiloxane, dimethiconol, hydroxyethyl diphosphate, polyoxyethylene glycol,

Description

Anti-dandruff shampoo

Technical Field

The invention belongs to the technical field of daily washing and chemical products, and particularly relates to an anti-dandruff shampoo.

Background

The shampoo is also called shampoo, shampoo and the like, and has various markets, various effects, large quality difference and improper use, which can cause dry hair and lack of luster.

In addition, people often use hair gel to shape hair, but if the hair is not cleaned, residues are accumulated on the scalp, and dandruff is easy to grow.

At present, the dandruff removing shampoo on the market is difficult to clean residues in pores of the scalp and cannot play a good dandruff removing effect.

Disclosure of Invention

The invention mainly solves the technical problem of providing the anti-dandruff shampoo which has good cleaning and nursing effects, has the functions of long-acting anti-dandruff, oil control, itching relief, scalp soothing and the like, and reduces the irritation of the shampoo while ensuring the anti-dandruff effect.

In order to solve the technical problems, the invention adopts a technical scheme that:

an antidandruff shampoo is prepared from pure water, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium laureth sulfate, TEA lauryl sulfate, behenamidopropyl dimethylamine, guar hydroxypropyl trimethyl ammonium chloride, sodium glutamate, cocamidopropyl hydroxysultaine, citric acid, cocamide MEA, hydroxyphenylpropionamide benzoic acid, oxidized polyethylene, hydroxyethyl urea, cyclopentadecyldimethyl siloxane, dimethyl siloxane, dimethiconol, hydroxyethyl diphosphate, citric acid, sodium glutamate, sodium cocoamidopropyl hydroxysultaine, sodium lauryl sulfate,

ADS, preservative, essence,Radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) extract, Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, brown algae (PHYLLACANTHA FIBROSA) extract, Chinese arborvitae (Platycladus ORIENTALIS) leaf extract, Mentholum and pigment by mixing, heating, emulsifying, and homogenizing.

Further, the anti-dandruff shampoo comprises the following components in percentage by weight: 45-80% pure water, 0.1-0.5% acrylic acid/C10-30 alkanol acrylate crosspolymer, 10-17% sodium laureth sulfate, 1-3% lauryl sulfate TEA salt, 0.1-0.5% behenamidopropyl dimethylamine, 0.1-1.0% guar hydroxypropyltrimonium chloride, 0.5-2% sodium glutamate, 1-8% cocamidopropyl hydroxysultaine, 0.1-0.5% citric acid, 0.5-3% cocamidoMEA, 0.005-0.1% hydroxyphenylpropionamide benzoic acid, 0.01-0.1% oxidized polyethylene, 1-3% hydroxyethyl urea, 0.5-3% cyclopentademethicone, 0.5-3% dimethicone, 1-3% dimethiconol, 0.05-0.5% hydroxyethyl diphosphate, 0.5% hydroxyethyl alcohol,

ADS, 0.1-0.3% antiseptic, 0.1-0.5% essence, 0.1-0.3% radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, 0.1-0.3% Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, 0.1-0.3% brown algae (Phyllacantha) extract, 0.1-0.3% cacumen Platycladi (Platytrunk IEORNTALIS) extract, 0.1-0.3% menthol and 0.0001-0.0005% pigment.

Further, the sodium laureth sulfate is specifically prepared by compounding 30% of water and 70% of sodium laureth sulfate in percentage by weight;

according to the weight percentage, the cocamidopropyl hydroxysultaine is specifically prepared by compounding 29.5 percent of cocamidopropyl hydroxysultaine, 4.5 percent of sodium chloride, 0.5 percent of sodium benzoate and 65.5 percent of water;

in percentage by weight, the

The ADS is prepared from 40% phenoxyethanol, 40%The chlorbazole is compounded by 15 percent of decanediol and 5 percent of 1, 2-hexanediol;

the preservative comprises 94% of water, 2.5% of methylisothiazolinone and 3.5% of 2-bromo-2-nitropropane-1, 3-diol in percentage by weight.

Further, the ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract in percentage by weight;

the hamamelis virginiana (HAMAMELIS VIRGINIANA) extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of hamamelis virginiana (HAMAMELIS VIRGINIANA) extract in percentage by weight;

the brown algae (PHYLLACANTHA FIBROSA) extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of brown algae (PHYLLACANTHA FIBROSA) extract according to weight percentage;

the Chinese arborvitae (PLATYCLADUS ORIENTALIS) leaf extract is prepared from 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of Chinese arborvitae (PLATYCLADUS ORIENTALIS) leaf extract by mixing.

Further, the pigments are lemon yellow CI19140 and brilliant blue No. 1 CI 42090.

The preparation method of the anti-dandruff shampoo comprises the following steps:

s1, soaking acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer in corresponding weight percentage into pure water in corresponding weight percentage according to formula amount to obtain acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer dispersion solution; adding pure water with corresponding weight percentage into an emulsifying pot, heating to 75-85 ℃, adding the acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer dispersion solution into the emulsifying pot, emulsifying and homogenizing at the rotating speed of 20r/min for 0.5-1h to obtain a first mixture;

s2, adding sodium laureth sulfate and TEA lauryl sulfate in corresponding weight percentages into the emulsifying pot filled with the first mixture in the step S1, emulsifying and homogenizing at 75-85 ℃ and 20r/min for 3-8min to obtain a second mixture;

s3, adding the behenamidopropyl dimethylamine in a corresponding weight percentage into the emulsifying pot filled with the second mixture in the step S2, emulsifying and homogenizing at 75-85 ℃ and at a rotating speed of 20r/min for 1-3min, and uniformly mixing to obtain a third mixture;

s4, dispersing guar hydroxypropyl trimethyl ammonium chloride in cold pure water according to the formula amount to obtain a guar hydroxypropyl trimethyl ammonium chloride aqueous solution; adding the guar hydroxypropyl trimethyl ammonium chloride aqueous solution into an emulsifying pot filled with the third mixture in the step S3, emulsifying and homogenizing at 75-85 ℃ and 20r/min rotation speed for 2-5min, and mixing uniformly to obtain a fourth mixture;

s5, adding sodium glutamate, cocamidopropyl hydroxysultaine and citric acid in corresponding weight percentages into the emulsifying pot filled with the fourth mixture in the step S4, emulsifying and homogenizing at 75-85 ℃ and 20r/min rotation speed for 1-2min, then continuously adding cocamidoMEA and hydroxyphenylpropionamide benzoic acid in corresponding weight percentages, emulsifying and homogenizing, vacuumizing the emulsifying pot to-0.05 MPa and 15r/min rotation speed, and preserving heat for 10-20min for defoaming to obtain a fifth mixture;

s6, cooling the emulsification pot filled with the fifth mixture in the step S5 to 40-50 ℃, sequentially adding oxidized polyethylene, water and hydroxyethyl urea in corresponding weight percentages into the cooled emulsification pot, continuing to emulsify and homogenize, and uniformly stirring to obtain a sixth mixture;

s7, discharging 35-45kg of sixth mixture from the emulsification pot filled with the sixth mixture in the step S6, transferring the sixth mixture to a vacuum homogenizing and emulsifying machine, and sequentially adding cyclopentadecyldimethyl siloxane, polydimethylsiloxane, dimethiconol, hydroxyethyl diphosphate, methyl ethyl diphosphate, ethyl propyl diphosphate, ethyl diphosphate, etc,

Mixing and homogenizing ADS and pure water for 15-20min to obtain seventh mixture; inserting a ruler into the seventh mixture and taking up the ruler, detecting whether the ruler has particles with uneven size distribution, and if not, detecting the ruler is qualified; if yes, continuously mixing and homogenizing until the detection is qualified;

s8, adding antiseptic, essence, radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, brown algae (PHYLLACANTHA FIBROSA) extract, Platycladus ORIENTALIS (Platycladus ORIENTALIS) leaf extract, menthol, cocamidopropyl hydroxysultaine, lemon yellow CI19140 and Brilliant blue No. 1 CI42090 in corresponding weight percentage into the vacuum homogenizing emulsifying machine filled with the seventh mixture qualified in detection in the step S7, homogenizing for 15min, vacuumizing for 2min, detecting the sample, filtering and discharging by using a 100-mesh filter screen after the detection is qualified, and obtaining the anti-dandruff shampoo.

Further, the ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract, the hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, the brown algae (PHYLLACANTHA FIBROSA) extract and the biota ORIENTALIS (PLATYCLADUS ORIENTALIS) leaf extract are prepared based on the following extraction process steps, and specifically comprise the following steps:

s1, removing impurities in the plant raw materials, cleaning the plant raw materials with water, and then placing the plant raw materials in an air-blast drying oven at 50-55 ℃ for drying treatment to obtain the purified plant raw materials;

s2, putting the plant raw material cleaned in the step S1 into a high-speed grinder for grinding, and sieving the ground plant raw material through a sieve of 50-60 meshes to obtain plant raw material powder;

s3, placing the plant raw material powder obtained in the step S2 in an ultrasonic extraction device at room temperature, and carrying out ultrasonic extraction according to the following steps of 1: adding 80-100% ethanol water solution at a ratio of 15-30, and performing ultrasonic-assisted extraction for 30-50min to obtain plant material extractive solution;

s4, placing the plant material extracting solution obtained in the step S3 in a rotary evaporator for vacuum concentration, and then transferring the plant material extracting solution into a vacuum drying oven for drying at 40-50 ℃ to obtain the plant material extract.

Further, in the process of preparing the anti-dandruff shampoo, a plurality of ultrasonic heating devices are arranged on a stirring paddle of the emulsifying pot;

the ultrasonic heating device includes:

a housing;

a first sealing cavity, a second sealing cavity and a third sealing cavity are arranged in the shell;

the ultrasonic generator is arranged in the first sealing cavity, so that the shampoo raw material liquid in the emulsifying pot generates vibration, the liquid in the emulsifying pot is further promoted to be emulsified, and the dissolvability of various material raw materials is improved; the collision effect among liquid particles not only improves the temperature of the shampoo raw material liquid, assists in heating, but also accelerates the rising of bubbles in the insulation emulsification process of the shampoo raw material, thereby achieving the defoaming effect;

a heater is arranged in the second sealing cavity, and the uniformity of heating inside the liquid is ensured in the process of stirring the liquid shampoo raw material liquid by the stirring paddle;

a temperature sensor is arranged on the inner wall of the third sealed cavity, the temperature sensor displays the internal temperature of the shampoo raw material liquid in the stirring process, and the frequency of the ultrasonic generator and the heating temperature of the heater are further controlled based on the internal temperature;

the ultrasonic heating device is connected with the PLC control system of the emulsifying pot.

The invention has at least the following advantages:

(1) the anti-dandruff shampoo has good deep cleaning and nursing effects, and also has the effects of removing dandruff for a long time, controlling oil, relieving itching and relieving scalp, and the washed hair is smooth and glossy;

(2) the anti-dandruff shampoo is mild and does not damage hair, and reduces the irritation of the shampoo to the scalp while ensuring the anti-dandruff effect;

(3) the dandruff removing shampoo is prepared by preparing an ANGELICA (Angelica POLYMORPHA SINENSIS) root extract, a Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, a brown algae (Phyllacantha fortosa) extract and a Chinese arborvitae (Platylabus ORIENTALIS) leaf extract through an ultrasonic auxiliary leaching technology, effectively improves the utilization of active ingredients in the extracts, enhances the application of the ANGELICA (Angelica POLYMORPHA SINENSIS) root extract, the Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, the brown algae (PHYLLACANTHA FIBROSA) extract and the Chinese arborvitae (Platylabus ORIENTALIS) leaf extract in the dandruff removing shampoo, and relieves the functions of scalp and nourishing hair roots;

(4) in the process of preparing the anti-dandruff shampoo, the plurality of ultrasonic heating devices are arranged on the stirring paddle of the emulsifying pot, so that the heating uniformity of the shampoo raw material liquid in the emulsifying pot is improved, the emulsification of the shampoo raw material liquid in the emulsifying pot is further promoted, and the dissolubility of various material raw materials is improved; in addition, the defoaming effect of the shampoo raw material in the heat-preservation emulsification process is assisted to be enhanced, so that the quality of the anti-dandruff shampoo is improved.

Detailed Description

The following detailed description of the preferred embodiments of the present invention is provided to enable those skilled in the art to more readily understand the advantages and features of the present invention, and to clearly and unequivocally define the scope of the present invention.

Example 1

Anti-dandruff shampoo

The anti-dandruff shampoo comprises the following components in percentage by weight: 64.78964% pure water, 0.2% acrylic acid/C10-30 alkanol acrylate crosspolymer, 15% sodium laureth sulfate, 2% lauryl sulfate TEA salt, 0.3% behenamidopropyl dimethylamine, 0.5% guar hydroxypropyltrimonium chloride, 1% sodium glutamate, 6% cocamidopropyl hydroxysultaine, 0.15% citric acid, 1% cocamidoMEA, 0.01% hydroxyphenylpropionamidobenzoic acid, 0.05% oxidized polyethylene, 2% hydroxyethyl urea, 1% cyclopentadimethylsiloxane, 1% polydimethylsiloxane, 1.5% dimethiconol, 0.1% hydroxyethyl diphosphate, 0.30% ethylene glycol diphosphate, propylene glycol, and propylene glycol, propylene,

ADS, 0.2% antiseptic, 0.4% essence, 0.2% radix Angelicae sinensis (Angelica polymorpha)A SINENSIS) root extract, 0.2% witch hazel (HAMAMELIS VIRGINIANA) extract, 0.2% brown algae (PHYLLACANTHA FIBROSA) extract, 0.2% biota ORIENTALIS (PLATYCLADUS ORIENTALIS) leaf extract, 0.2% menthol, 0.00021% lemon yellow CI19140, and 0.00015% brilliant blue No. 1 CI 42090.

The sodium laureth sulfate is prepared by compounding 30% of water and 70% of sodium laureth sulfate in percentage by weight;

the cocamidopropyl hydroxysultaine is prepared by compounding 29.5% of cocamidopropyl hydroxysultaine, 4.5% of sodium chloride, 0.5% of sodium benzoate and 65.5% of water in percentage by weight;

in percentage by weight, the

The ADS is specifically prepared by compounding 40% of phenoxyethanol, 40% of climbazole, 15% of decanediol and 5% of 1, 2-hexanediol;

the preservative comprises 94% of water, 2.5% of methylisothiazolinone and 3.5% of 2-bromo-2-nitropropane-1, 3-diol by weight percent.

The ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract in percentage by weight;

Example 2

Anti-dandruff shampoo

The difference from the embodiment 1 is that the anti-dandruff shampoo comprises the following components in percentage by weight: 63.40963% pure water, 0.15% acrylic acid/C10-30 alkanol acrylate crosspolymer, 16% sodium laureth sulfate, 2.5% TEA lauryl sulfate, 0.25% behenamidopropyl dimethylamine, 0.55% guar hydroxypropyltrimonium chloride, 1% sodium glutamate, 6% cocamidopropyl hydroxysultaine, 0.17% citric acid, 1% cocamidoMEA, 0.01% hydroxyphenylpropionamide benzoic acid, 0.06% oxidized polyethylene, 1.8% hydroxyethyl urea, 1% cyclopentadimethylsiloxane, 1% polydimethylsiloxane, 1.8% dimethiconol, 0.1% hydroxyethyl diphosphate, 0.1% ethylene glycol diphosphate, propylene glycol, and propylene glycol, propylene glycol,

ADS, 0.2% preservative, 0.4% essence, 0.25% ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract, 0.2% hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, 0.15% brown algae (PHYLLACANTHA FIBROSA) extract, 0.3% biota ORIENTALIS (PLATYCLADUS ORIENTALIS) leaf extract, 0.2% menthol, 0.00025% lemon yellow CI19140, and 0.00012% brilliant blue No. 1 CI 42090.

in percentage by weight, the

ADS is prepared from 40% phenoxyEthanol, 40 percent of climbazole, 15 percent of decanediol and 5 percent of 1, 2-hexanediol;

The ANGELICA SINENSIS (ANGELICA POLYMORPHA SINENSIS) root extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of ANGELICA SINENSIS (ANGELICA POLYMORPHA SINENSIS) root extract according to weight percentage;

Example 3

Anti-dandruff shampoo

The anti-dandruff shampoo is different from the anti-dandruff shampoo in example 1 in that the anti-dandruff shampoo comprises the following components in percentage by weight: 62.21964% pure water, 0.25% acrylic acid/C10-30 alkanol acrylate crosspolymer, 16% sodium laureth sulfate, 2% TEA lauryl sulfate, 0.3% behenamidopropyl dimethylamine, 0.7% guar hydroxypropyltrimonium chloride, 1% sodium glutamate, 7% cocamidopropyl hydroxysultaine, 0.13% citric acid, 1.2% cocamidoMEA, 0.01% hydroxyphenylpropionamide benzoic acid, 0.04% oxidized polyethylene, 2% hydroxyethyl urea, 1%Cyclopentadimethylsiloxane, 1% polydimethylsiloxane, 1.5% dimethiconol, 0.15% hydroxyethyldiphosphonic acid,

ADS, 0.2% antiseptic, 0.4% essence, 0.3% radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, 0.25% Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, 0.15% brown algae (PHYLLACANTHA FIBROSA) extract, 0.2% cacumen Platycladi (Platycladus ORIENTALIS) leaf extract, 0.2% menthol, 0.00022% lemon yellow CI19140, and 0.00014% Brilliant blue No. 1 CI 42090.

in percentage by weight, the

Example 1-example 3 an anti-dandruff shampoo was prepared by the following steps comprising:

s1, soaking acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer in corresponding weight percentage into pure water in corresponding weight percentage according to formula amount to obtain acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer dispersion solution; adding pure water with corresponding weight percentage into an emulsifying pot, heating to 80 ℃, adding the acrylic acid (ester)/C10-30 alkanol acrylate crosslinked polymer dispersion solution into the emulsifying pot, and emulsifying and homogenizing at the rotating speed of 20r/min for 1h to obtain a first mixture;

s2, adding sodium laureth sulfate and TEA lauryl sulfate in corresponding weight percentages into the emulsifying pot filled with the first mixture in the step S1, emulsifying and homogenizing at 80 ℃ and 20r/min for 5min to obtain a second mixture;

s3, adding behenamide propyl dimethylamine in a corresponding weight percentage into the emulsifying pot filled with the second mixture in the step S2, emulsifying and homogenizing at 80 ℃ and 20r/min of rotation speed for 1min, and mixing uniformly to obtain a third mixture;

s4, dispersing guar hydroxypropyl trimethyl ammonium chloride in cold pure water according to the formula amount to obtain a guar hydroxypropyl trimethyl ammonium chloride aqueous solution; adding the guar hydroxypropyl trimethyl ammonium chloride aqueous solution into an emulsifying pot filled with the third mixture in the step S3, emulsifying and homogenizing at 80 ℃ and 20r/min rotation speed for 3min, and mixing uniformly to obtain a fourth mixture;

s5, adding sodium glutamate, cocamidopropyl hydroxysultaine and citric acid in corresponding weight percentage into an emulsifying pot filled with the fourth mixture in the step S4, emulsifying and homogenizing at 80 ℃ and 20r/min rotating speed for 2min, then continuously adding cocamidoMEA and hydroxyphenylpropionamide benzoic acid in corresponding weight percentage, emulsifying and homogenizing, vacuumizing the emulsifying pot to-0.05 MPa and 15r/min rotating speed, preserving heat for 15min, and defoaming to obtain a fifth mixture;

s6, cooling the emulsification pot filled with the fifth mixture in the step S5 to 40 ℃, sequentially adding oxidized polyethylene, water and hydroxyethyl urea in corresponding weight percentages into the cooled emulsification pot, continuing to emulsify and homogenize, and uniformly stirring to obtain a sixth mixture;

Mixing and homogenizing ADS and pure water for 15-20min to obtain a seventh mixture; inserting a ruler into the seventh mixture and taking up, detecting whether particles with uneven size distribution exist on the ruler, and if not, detecting to be qualified; if yes, continuously mixing and homogenizing until the detection is qualified;

s8, adding antiseptic, essence, radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, brown algae (PHYLLACANTHA FIBROSA) extract, cacumen Platycladi (Platycladus ORIENTALIS) leaf extract, Mentholum, cocamidopropyl hydroxysultaine, lemon yellow CI19140, and Brilliant blue No. 1 CI42090 into vacuum homogenizing and emulsifying machine filled with seventh mixture qualified by detection in step S7, homogenizing for 15min, vacuumizing for 2min, detecting sample, filtering with 100 mesh filter screen, and making into dandruff removing shampoo.

The results of comparisons of the properties of the shampoos prepared in examples 1-3 are shown in the following table:

as can be seen from the table, the anti-dandruff shampoo prepared in the embodiment of the invention is weakly acidic, the irritation of the shampoo to hair and scalp is reduced, and the anti-dandruff shampoo prepared in the invention has good cleaning and nursing effects, and has the functions of long-acting anti-dandruff, oil control, itching relieving, scalp soothing and the like.

Example 4

The ANGELICA (ANGELICA POLYMORPHA SINENSIS) root extract, hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, brown algae (PHYLLACANTHA FIBROSA) extract, and biota ORIENTALIS (PLATYCLADUS ORIENTALIS) leaf extract described in example 1-example 3 were prepared based on the following extraction process steps, including:

s1, removing impurities in the plant raw materials, cleaning the plant raw materials with water, and then placing the plant raw materials in an air-blast drying oven for drying treatment at 55 ℃ to obtain the cleaned plant raw materials;

s2, putting the plant raw material cleaned in the step S1 into a high-speed grinder for grinding, and sieving the ground plant raw material through a 60-mesh sieve to obtain plant raw material powder;

s3, placing the plant raw material powder obtained in the step S2 in an ultrasonic extraction device at room temperature, and carrying out ultrasonic extraction according to the following steps of 1: 15, adding 90% ethanol water solution into the mixture, and performing ultrasonic-assisted extraction for 45min to obtain plant material extract;

s4, placing the plant material extracting solution obtained in the step S3 in a rotary evaporator for vacuum concentration, and then transferring the plant material extracting solution into a vacuum drying oven for drying at 50 ℃ to obtain the plant material extract.

The working principle and the beneficial effects of the embodiment are as follows: in the invention, the ANGELICA (Angelica POLYMORPHA SINENSIS) root extract, the hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, the brown algae (PHYLLACANTHA FIBROSA) extract and the biota ORIENTALIS (PLATYCLADUS ORIENTALIS) leaf extract are prepared by an ultrasonic auxiliary extraction technology, so that the utilization of active ingredients in the extracts is effectively improved, and the effects of relieving the scalp and nourishing hair roots when the ANGELICA (Angelica POLYMORPHA SINENSIS) root extract, the hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, the brown algae (PHYLLACANTHA FIBROSA) extract and the biota ORIENTALIS (PLATYCLADUS ORIENTALIS) leaf extract are applied to the dandruff removing shampoo are enhanced.

Example 5

Examples 1 to 3 in which an anti-dandruff shampoo was prepared, a plurality of ultrasonic heating devices were provided on a stirring blade of the emulsifying pot;

the ultrasonic heating device includes:

a housing;

an ultrasonic generator is arranged in the first sealing cavity;

a heater is arranged in the second sealing cavity;

a temperature sensor is arranged on the inner wall of the third sealing cavity;

The working principle and the beneficial effects of the embodiment are as follows: in the process of preparing the anti-dandruff shampoo, the plurality of ultrasonic heating devices are arranged on the stirring paddle of the emulsifying pot, so that the heating uniformity of the shampoo raw material liquid in the emulsifying pot is improved, the emulsification of the shampoo raw material liquid in the emulsifying pot is further promoted, and the dissolubility of various material raw materials is improved; in addition, the defoaming effect of the shampoo raw material in the heat-preservation emulsification process is assisted to be enhanced, so that the quality of the anti-dandruff shampoo is improved.

The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all equivalent structural changes made by using the contents of the present specification, or any other related technical fields directly or indirectly, are included in the scope of the present invention.

Claims

1. An anti-dandruff shampoo is characterized in that: the anti-dandruff shampoo is prepared from pure water, acrylic acid (ester)/C10-30 alkanol acrylateDipolymers, sodium laureth sulfate, TEA lauryl sulfate, behenamidopropyl dimethylamine, guar hydroxypropyltrimonium chloride, sodium glutamate, cocamidopropyl hydroxysultaine, citric acid, cocamide MEA, hydroxyphenylpropionamide benzoic acid, oxidized polyethylene, hydroxyethyl urea, cyclopentadimethylsiloxane, polydimethylsiloxane, dimethiconol, hydroxyethyldiphosphonic acid, Crini

ADS, antiseptic, essence, radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, brown algae (PHYLLACANTHA FIBROSA) extract, Chinese arborvitae (Platycladus ORIENTALIS) leaf extract, Mentholum and pigment by mixing, heating, emulsifying, and homogenizing.

2. An anti-dandruff shampoo according to claim 1, wherein: the anti-dandruff shampoo comprises the following components in percentage by weight: 45-80% pure water, 0.1-0.5% acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 10-17% sodium laureth sulfate, 1-3% TEA lauryl sulfate, 0.1-0.5% behenamidopropyl dimethylamine, 0.1-1.0% guar hydroxypropyltrimonium chloride, 0.5-2% sodium glutamate, 1-8% cocamidopropyl hydroxysultaine, 0.1-0.5% citric acid, 0.5-3% cocamide MEA, 0.005-0.1% hydroxyphenylpropionamide benzoic acid, 0.01-0.1% oxidized polyethylene, 1-3% hydroxyethyl urea, 0.5-3% cyclopentadecyl dimethyl siloxane, 0.5-3% dimethyl siloxane, 1-3% dimethyl siloxanol, 0.05-0.5% hydroxyethyl diphosphate, 0.5% hydroxyethyl urea, 1-0.5% ethylene glycol, 1-2% propylene glycol, 1-0.5% lauryl sulfate, 0.1-0.5% behenamidopropyl dimethylamine, 0.1-0.5% sodium hydroxide, 0.1-0.1% hydroxypropyl trimethyl ammonium chloride, 0.1-0.1% hydroxypropyl ammonium chloride, 0.1-0.1% sodium chloride, 0.1% hydroxyethyl urea, 0.1-0.1% hydroxyethyl urea, 0.1-0.5% hydroxyethyl urea, 0.5% of sodium chloride, 0.5% of a, 0.5-1.5% Crini

ADS, 0.1-0.3% antiseptic, 0.1-0.5% essence, 0.1-0.3% radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, 0.1-0.3% Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, 0.1-0.3% brown algae (PHYLLACANTHA FIBROSA) extract, 0.1-0.3% cacumen Platycladi (Platysacus ORIENTALIS) leafExtract, 0.1-0.3% of menthol and 0.0001-0.0005% of pigment.

3. An anti-dandruff shampoo according to claim 1, wherein: the sodium laureth sulfate is prepared by compounding 30 percent of water and 70 percent of sodium laureth sulfate in percentage by weight;

according to the weight percentage, the Crini

4. An anti-dandruff shampoo according to claim 1, wherein: the ANGELICA SINENSIS (ANGELICA POLYMORPHA SINENSIS) root extract is prepared by compounding 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of ANGELICA SINENSIS (ANGELICA POLYMORPHA SINENSIS) root extract according to weight percentage;

the Chinese arborvitae (Platycladus ORIENTALIS) leaf extract is prepared from 93% of water, 0.45% of phenoxyethanol, 0.05% of ethylhexyl glycerol, 0.2% of p-hydroxyacetophenone, 1% of butanediol and 5.3% of Platycladus ORIENTALIS (Platycladus ORIENTALIS) leaf extract by compounding according to weight percentage.

5. An anti-dandruff shampoo according to claim 1, wherein: the pigments are lemon yellow CI19140 and brilliant blue No. 1 CI 42090.

6. A process for the preparation of an anti-dandruff shampoo according to any of claims 1 to 5, characterized in that: the method comprises the following steps:

s5, adding sodium glutamate, cocamidopropyl hydroxysultaine and citric acid in corresponding weight percentage into an emulsifying pot filled with the fourth mixture in the step S4, emulsifying and homogenizing at 75-85 ℃ and 20r/min rotating speed for 1-2min, then continuing adding cocamide MEA and hydroxyphenylpropionamide benzoic acid in corresponding weight percentage, emulsifying and homogenizing, vacuumizing the emulsifying pot to-0.05 MPa and 15r/min rotating speed, preserving heat for 10-20min, and defoaming to obtain a fifth mixture;

s7, discharging 35-45kg of sixth mixture from the emulsifying pot filled with the sixth mixture in the step S6, transferring the sixth mixture to a vacuum homogenizing emulsifying machine, and sequentially adding cyclopentadecyldimethyl siloxane, polydimethylsiloxane, dimethiconol, hydroxyethyl diphosphate and Crini to the vacuum homogenizing emulsifying machine according to the corresponding weight percentage

Mixing and homogenizing ADS and pure water for 15-20min to obtain seventh mixture; inserting a ruler into the seventh mixture and taking up, detecting whether particles with uneven size distribution exist on the ruler, and if not, detecting to be qualified; if yes, continuously mixing and homogenizing until the detection is qualified;

s8, adding antiseptic, essence, radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, brown algae (PHYLLACANTHA FIBROSA) extract, cacumen Platycladi (Platycladus ORIENTALIS) leaf extract, Mentholum, cocamidopropyl hydroxysultaine, lemon yellow CI19140, and Brilliant blue No. 1 CI42090 into vacuum homogenizing emulsifying machine filled with the seventh mixture qualified by detection in step S7, homogenizing for 15min, vacuumizing for 2min to detect sample, filtering with 100 mesh filter screen to obtain dandruff removing shampoo.

7. An anti-dandruff shampoo according to claim 4, wherein: the radix Angelicae SINENSIS (Angelica POLYMORPHA SINENSIS) root extract, Hamamelis virginiana (HAMAMELIS VIRGINIANA) extract, brown algae (PHYLLACANTHA FIBROSA) extract and Chinese arborvitae (Platycladus ORIENTALIS) leaf extract are prepared based on the following extraction process steps, and specifically comprise:

s3, placing the plant raw material powder obtained in the step S2 in an ultrasonic extraction device at room temperature, and performing extraction according to the following steps of 1: adding 80-100% ethanol water solution at a ratio of 15-30, and performing ultrasonic-assisted extraction for 30-50min to obtain plant material extractive solution;

8. The method for preparing an anti-dandruff shampoo according to claim 6, wherein a plurality of ultrasonic heating devices are arranged on the stirring paddle of the emulsifying pot;

the ultrasonic heating device includes:

a housing;

an ultrasonic generator is arranged in the first sealing cavity;

a heater is arranged in the second sealing cavity;

a temperature sensor is arranged on the inner wall of the third sealing cavity;