CN114586847B - 一种鲜奶级母乳化牛乳蛋白基料及其制备方法 - Google Patents
一种鲜奶级母乳化牛乳蛋白基料及其制备方法 Download PDFInfo
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- CN114586847B CN114586847B CN202210271906.1A CN202210271906A CN114586847B CN 114586847 B CN114586847 B CN 114586847B CN 202210271906 A CN202210271906 A CN 202210271906A CN 114586847 B CN114586847 B CN 114586847B
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- milk
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- 239000000463 material Substances 0.000 title claims abstract description 22
- 102000014171 Milk Proteins Human genes 0.000 title claims abstract description 21
- 108010011756 Milk Proteins Proteins 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 18
- 235000021239 milk protein Nutrition 0.000 title claims abstract description 13
- 210000000481 breast Anatomy 0.000 title description 2
- 108010046377 Whey Proteins Proteins 0.000 claims abstract description 85
- 102000007544 Whey Proteins Human genes 0.000 claims abstract description 78
- 239000012528 membrane Substances 0.000 claims abstract description 71
- 238000001914 filtration Methods 0.000 claims abstract description 41
- 235000021119 whey protein Nutrition 0.000 claims abstract description 38
- 235000013350 formula milk Nutrition 0.000 claims abstract description 31
- 102000011632 Caseins Human genes 0.000 claims abstract description 30
- 108010076119 Caseins Proteins 0.000 claims abstract description 30
- 239000005018 casein Substances 0.000 claims abstract description 28
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 claims abstract description 28
- 235000021240 caseins Nutrition 0.000 claims abstract description 28
- 235000013336 milk Nutrition 0.000 claims abstract description 27
- 210000004080 milk Anatomy 0.000 claims abstract description 27
- 239000008267 milk Substances 0.000 claims abstract description 27
- 235000020256 human milk Nutrition 0.000 claims abstract description 22
- 210000004251 human milk Anatomy 0.000 claims abstract description 22
- 235000020247 cow milk Nutrition 0.000 claims abstract description 20
- 238000005238 degreasing Methods 0.000 claims abstract description 15
- 230000001954 sterilising effect Effects 0.000 claims abstract description 15
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- 239000007788 liquid Substances 0.000 claims description 29
- 239000000919 ceramic Substances 0.000 claims description 28
- 238000001471 micro-filtration Methods 0.000 claims description 27
- 238000000034 method Methods 0.000 claims description 18
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- 238000001816 cooling Methods 0.000 claims description 10
- 241000894006 Bacteria Species 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000009210 therapy by ultrasound Methods 0.000 claims description 3
- 239000005862 Whey Substances 0.000 abstract description 48
- 239000012466 permeate Substances 0.000 abstract description 44
- 239000000843 powder Substances 0.000 abstract description 30
- 238000000926 separation method Methods 0.000 abstract description 24
- 235000018102 proteins Nutrition 0.000 abstract description 19
- 102000004169 proteins and genes Human genes 0.000 abstract description 19
- 108090000623 proteins and genes Proteins 0.000 abstract description 19
- 239000002994 raw material Substances 0.000 abstract description 6
- 235000013351 cheese Nutrition 0.000 abstract description 4
- 238000012545 processing Methods 0.000 abstract description 4
- 235000013365 dairy product Nutrition 0.000 abstract description 3
- 239000000706 filtrate Substances 0.000 abstract description 3
- 238000001694 spray drying Methods 0.000 abstract description 3
- 239000004615 ingredient Substances 0.000 abstract description 2
- 230000004807 localization Effects 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 36
- 235000020185 raw untreated milk Nutrition 0.000 description 23
- 230000000052 comparative effect Effects 0.000 description 16
- 239000011148 porous material Substances 0.000 description 16
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- 239000002585 base Substances 0.000 description 10
- 239000012530 fluid Substances 0.000 description 10
- 238000001223 reverse osmosis Methods 0.000 description 10
- 235000020183 skimmed milk Nutrition 0.000 description 9
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 8
- 239000012465 retentate Substances 0.000 description 7
- 239000008367 deionised water Substances 0.000 description 6
- 229910021641 deionized water Inorganic materials 0.000 description 6
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- 239000000203 mixture Substances 0.000 description 6
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 description 5
- 239000008101 lactose Substances 0.000 description 5
- 239000002253 acid Substances 0.000 description 4
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- 238000005516 engineering process Methods 0.000 description 4
- 238000005374 membrane filtration Methods 0.000 description 4
- 238000001728 nano-filtration Methods 0.000 description 4
- 238000004140 cleaning Methods 0.000 description 3
- 230000001186 cumulative effect Effects 0.000 description 3
- 238000005265 energy consumption Methods 0.000 description 3
- 229910052500 inorganic mineral Inorganic materials 0.000 description 3
- 239000011344 liquid material Substances 0.000 description 3
- 239000011707 mineral Substances 0.000 description 3
- 235000010755 mineral Nutrition 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000011084 recovery Methods 0.000 description 3
- 238000001179 sorption measurement Methods 0.000 description 3
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 239000003153 chemical reaction reagent Substances 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 238000009776 industrial production Methods 0.000 description 2
- 235000021243 milk fat Nutrition 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000009740 moulding (composite fabrication) Methods 0.000 description 2
- 229910017604 nitric acid Inorganic materials 0.000 description 2
- 239000012474 protein marker Substances 0.000 description 2
- 238000004064 recycling Methods 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 238000012216 screening Methods 0.000 description 2
- 235000020254 sheep milk Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000011782 vitamin Substances 0.000 description 2
- 235000013343 vitamin Nutrition 0.000 description 2
- 229940088594 vitamin Drugs 0.000 description 2
- 229930003231 vitamin Natural products 0.000 description 2
- 235000021247 β-casein Nutrition 0.000 description 2
- 241000283690 Bos taurus Species 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 description 1
- PHOQVHQSTUBQQK-SQOUGZDYSA-N D-glucono-1,5-lactone Chemical compound OC[C@H]1OC(=O)[C@H](O)[C@@H](O)[C@@H]1O PHOQVHQSTUBQQK-SQOUGZDYSA-N 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 239000004695 Polyether sulfone Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 150000001720 carbohydrates Chemical class 0.000 description 1
- 235000014633 carbohydrates Nutrition 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
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- 238000002474 experimental method Methods 0.000 description 1
- 235000019197 fats Nutrition 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000012209 glucono delta-lactone Nutrition 0.000 description 1
- 239000000182 glucono-delta-lactone Substances 0.000 description 1
- 229960003681 gluconolactone Drugs 0.000 description 1
- 230000008676 import Effects 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 230000003278 mimic effect Effects 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 229920006393 polyether sulfone Polymers 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000000717 retained effect Effects 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 238000000108 ultra-filtration Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/14—Milk preparations; Milk powder or milk powder preparations in which the chemical composition of the milk is modified by non-chemical treatment
- A23C9/142—Milk preparations; Milk powder or milk powder preparations in which the chemical composition of the milk is modified by non-chemical treatment by dialysis, reverse osmosis or ultrafiltration
- A23C9/1422—Milk preparations; Milk powder or milk powder preparations in which the chemical composition of the milk is modified by non-chemical treatment by dialysis, reverse osmosis or ultrafiltration by ultrafiltration, microfiltration or diafiltration of milk, e.g. for separating protein and lactose; Treatment of the UF permeate
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C7/00—Other dairy technology
- A23C7/04—Removing unwanted substances other than lactose or milk proteins from milk
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C7/00—Other dairy technology
- A23C7/04—Removing unwanted substances other than lactose or milk proteins from milk
- A23C7/046—Removing unwanted substances other than lactose or milk proteins from milk by centrifugation without using chemicals, e.g. bactofugation; re-use of bactofugate
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23C—DAIRY PRODUCTS, e.g. MILK, BUTTER OR CHEESE; MILK OR CHEESE SUBSTITUTES; MAKING THEREOF
- A23C9/00—Milk preparations; Milk powder or milk powder preparations
- A23C9/14—Milk preparations; Milk powder or milk powder preparations in which the chemical composition of the milk is modified by non-chemical treatment
Landscapes
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Water Supply & Treatment (AREA)
- Dairy Products (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
Description
Claims (6)
Priority Applications (1)
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CN202210271906.1A CN114586847B (zh) | 2022-03-18 | 2022-03-18 | 一种鲜奶级母乳化牛乳蛋白基料及其制备方法 |
Applications Claiming Priority (1)
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CN202210271906.1A CN114586847B (zh) | 2022-03-18 | 2022-03-18 | 一种鲜奶级母乳化牛乳蛋白基料及其制备方法 |
Publications (2)
Publication Number | Publication Date |
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CN114586847A CN114586847A (zh) | 2022-06-07 |
CN114586847B true CN114586847B (zh) | 2024-04-26 |
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CN202210271906.1A Active CN114586847B (zh) | 2022-03-18 | 2022-03-18 | 一种鲜奶级母乳化牛乳蛋白基料及其制备方法 |
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Families Citing this family (1)
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CN118271424A (zh) * | 2024-06-03 | 2024-07-02 | 中国农业科学院农产品加工研究所 | 一种鲜奶级高纯度α-乳白蛋白的分离制备方法 |
Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102630803A (zh) * | 2012-05-15 | 2012-08-15 | 东北农业大学 | 母乳化牛乳蛋白及其制备方法 |
CN106417888A (zh) * | 2016-09-27 | 2017-02-22 | 江南大学 | 一种低温微滤分离牛乳β‑酪蛋白和乳清蛋白以模拟人乳蛋白组成的方法 |
CN109788771A (zh) * | 2016-08-08 | 2019-05-21 | 达能日尔维公司 | 生产婴儿配方产品和乳制品的方法 |
CN110367339A (zh) * | 2019-08-07 | 2019-10-25 | 大连工业大学 | 一种富含κ-酪蛋白乳清粉及其制备方法和应用 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20080206415A1 (en) * | 2004-10-07 | 2008-08-28 | Next Proteins, Inc. | Protein beverage and method of making the same |
WO2009059266A1 (en) * | 2007-11-02 | 2009-05-07 | Select Milk Producers, Inc. | Methods for casein production |
CA3028529A1 (en) * | 2016-06-21 | 2017-12-28 | Arla Foods Amba | Process for production of improved nutritional products containing milk protein and milk saccharides, and products obtained by the process |
-
2022
- 2022-03-18 CN CN202210271906.1A patent/CN114586847B/zh active Active
Patent Citations (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102630803A (zh) * | 2012-05-15 | 2012-08-15 | 东北农业大学 | 母乳化牛乳蛋白及其制备方法 |
CN109788771A (zh) * | 2016-08-08 | 2019-05-21 | 达能日尔维公司 | 生产婴儿配方产品和乳制品的方法 |
CN106417888A (zh) * | 2016-09-27 | 2017-02-22 | 江南大学 | 一种低温微滤分离牛乳β‑酪蛋白和乳清蛋白以模拟人乳蛋白组成的方法 |
CN110367339A (zh) * | 2019-08-07 | 2019-10-25 | 大连工业大学 | 一种富含κ-酪蛋白乳清粉及其制备方法和应用 |
Non-Patent Citations (5)
Title |
---|
Ceramic membrane filtration of skim milk for the production of a casein-enriched permeate;Bo Song et al;《International Dairy Journal》;第1-6页 * |
Optimization of protein fractionation by skim milk microfiltration: Choice of ceramic membrane pore size and filtration temperature;Camilla Elise Jørgensen et al;《Journal of Dairy Science》;第6164-6179页 * |
Process efficiency of casein separation from milk using polymeric spiral-wound microfiltration membranes;D. Mercier-Bouchard et al;《Journal of Dairy Science》;第8838-8848页 * |
冯春宇.《固液分离原理与工业水处理装置》.西安电子科技大学出版社,2017,第97页. * |
陶瓷膜对脱脂乳中酪蛋白与其他组分的高效分离;张瑞华等;《食品科学》;第38卷(第10期);236-243页 * |
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CN114586847A (zh) | 2022-06-07 |
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