CN114409373A - She-family-element-containing celadon and preparation method thereof - Google Patents
She-family-element-containing celadon and preparation method thereof Download PDFInfo
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- CN114409373A CN114409373A CN202210003955.7A CN202210003955A CN114409373A CN 114409373 A CN114409373 A CN 114409373A CN 202210003955 A CN202210003955 A CN 202210003955A CN 114409373 A CN114409373 A CN 114409373A
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- 238000002360 preparation method Methods 0.000 title abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 46
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 239000000654 additive Substances 0.000 claims abstract description 23
- 239000002689 soil Substances 0.000 claims abstract description 22
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 19
- 239000000843 powder Substances 0.000 claims abstract description 19
- 239000002002 slurry Substances 0.000 claims abstract description 15
- 235000015895 biscuits Nutrition 0.000 claims abstract description 13
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims abstract description 12
- 239000010433 feldspar Substances 0.000 claims abstract description 12
- 239000000463 material Substances 0.000 claims abstract description 11
- 230000000996 additive effect Effects 0.000 claims abstract description 10
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 claims abstract description 7
- 229910052737 gold Inorganic materials 0.000 claims abstract description 7
- 239000010931 gold Substances 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 235000019738 Limestone Nutrition 0.000 claims abstract description 6
- 229910052599 brucite Inorganic materials 0.000 claims abstract description 6
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000006028 limestone Substances 0.000 claims abstract description 6
- 239000000203 mixture Substances 0.000 claims abstract description 6
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 6
- 229910000029 sodium carbonate Inorganic materials 0.000 claims abstract description 6
- 235000017550 sodium carbonate Nutrition 0.000 claims abstract description 6
- 229940036811 bone meal Drugs 0.000 claims abstract description 5
- 239000002374 bone meal Substances 0.000 claims abstract description 5
- 238000010304 firing Methods 0.000 claims description 25
- 238000001035 drying Methods 0.000 claims description 20
- 239000011505 plaster Substances 0.000 claims description 15
- 238000005507 spraying Methods 0.000 claims description 15
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 10
- XLOMVQKBTHCTTD-UHFFFAOYSA-N Zinc monoxide Chemical compound [Zn]=O XLOMVQKBTHCTTD-UHFFFAOYSA-N 0.000 claims description 10
- 238000000498 ball milling Methods 0.000 claims description 10
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 10
- 230000005484 gravity Effects 0.000 claims description 10
- 238000000227 grinding Methods 0.000 claims description 10
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 10
- 239000010453 quartz Substances 0.000 claims description 7
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 6
- NQNBVCBUOCNRFZ-UHFFFAOYSA-N nickel ferrite Chemical compound [Ni]=O.O=[Fe]O[Fe]=O NQNBVCBUOCNRFZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000005995 Aluminium silicate Substances 0.000 claims description 5
- 239000004115 Sodium Silicate Substances 0.000 claims description 5
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims description 5
- 235000012211 aluminium silicate Nutrition 0.000 claims description 5
- 229910002114 biscuit porcelain Inorganic materials 0.000 claims description 5
- 229910021538 borax Inorganic materials 0.000 claims description 5
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 239000004927 clay Substances 0.000 claims description 5
- 229910052570 clay Inorganic materials 0.000 claims description 5
- 239000011248 coating agent Substances 0.000 claims description 5
- 238000000576 coating method Methods 0.000 claims description 5
- YGANSGVIUGARFR-UHFFFAOYSA-N dipotassium dioxosilane oxo(oxoalumanyloxy)alumane oxygen(2-) Chemical compound [O--].[K+].[K+].O=[Si]=O.O=[Al]O[Al]=O YGANSGVIUGARFR-UHFFFAOYSA-N 0.000 claims description 5
- 238000007598 dipping method Methods 0.000 claims description 5
- 239000000428 dust Substances 0.000 claims description 5
- 239000010440 gypsum Substances 0.000 claims description 5
- 229910052602 gypsum Inorganic materials 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 238000000465 moulding Methods 0.000 claims description 5
- 229910052627 muscovite Inorganic materials 0.000 claims description 5
- 229910000027 potassium carbonate Inorganic materials 0.000 claims description 5
- 238000004513 sizing Methods 0.000 claims description 5
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 claims description 5
- 229910052911 sodium silicate Inorganic materials 0.000 claims description 5
- 239000004328 sodium tetraborate Substances 0.000 claims description 5
- 235000010339 sodium tetraborate Nutrition 0.000 claims description 5
- 238000003756 stirring Methods 0.000 claims description 5
- 230000001502 supplementing effect Effects 0.000 claims description 5
- 239000010456 wollastonite Substances 0.000 claims description 5
- 229910052882 wollastonite Inorganic materials 0.000 claims description 5
- 239000011787 zinc oxide Substances 0.000 claims description 5
- 239000007767 bonding agent Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 5
- 235000017166 Bambusa arundinacea Nutrition 0.000 abstract description 4
- 235000017491 Bambusa tulda Nutrition 0.000 abstract description 4
- 241001330002 Bambuseae Species 0.000 abstract description 4
- 235000015334 Phyllostachys viridis Nutrition 0.000 abstract description 4
- 239000011425 bamboo Substances 0.000 abstract description 4
- 239000000126 substance Substances 0.000 abstract description 2
- 239000000725 suspension Substances 0.000 abstract description 2
- 229910052573 porcelain Inorganic materials 0.000 description 4
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 3
- 230000000630 rising effect Effects 0.000 description 3
- 230000008901 benefit Effects 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 229910001570 bauxite Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000000988 bone and bone Anatomy 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000010977 jade Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000003746 solid phase reaction Methods 0.000 description 1
Classifications
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- C—CHEMISTRY; METALLURGY
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- C04B33/00—Clay-wares
- C04B33/02—Preparing or treating the raw materials individually or as batches
- C04B33/04—Clay; Kaolin
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- C04B33/00—Clay-wares
- C04B33/24—Manufacture of porcelain or white ware
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- C04B33/00—Clay-wares
- C04B33/32—Burning methods
- C04B33/34—Burning methods combined with glazing
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3205—Alkaline earth oxides or oxide forming salts thereof, e.g. beryllium oxide
- C04B2235/3206—Magnesium oxides or oxide-forming salts thereof
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/327—Iron group oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3272—Iron oxides or oxide forming salts thereof, e.g. hematite, magnetite
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- C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/327—Iron group oxides, their mixed metal oxides, or oxide-forming salts thereof
- C04B2235/3279—Nickel oxides, nickalates, or oxide-forming salts thereof
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- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3284—Zinc oxides, zincates, cadmium oxides, cadmiates, mercury oxides, mercurates or oxide forming salts thereof
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- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3409—Boron oxide, borates, boric acids, or oxide forming salts thereof, e.g. borax
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- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
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- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/3427—Silicates other than clay, e.g. water glass
- C04B2235/3463—Alumino-silicates other than clay, e.g. mullite
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- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
- C04B2235/349—Clays, e.g. bentonites, smectites such as montmorillonite, vermiculites or kaolines, e.g. illite, talc or sepiolite
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- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
- C04B2235/442—Carbonates
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- C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
- C04B2235/30—Constituents and secondary phases not being of a fibrous nature
- C04B2235/44—Metal salt constituents or additives chosen for the nature of the anions, e.g. hydrides or acetylacetonate
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- C04B2235/60—Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
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Abstract
The invention discloses a she-nationality-element-containing celadon and a preparation method thereof, and aims to solve the problems that the elements are single and cannot be popularized in a large range. The key points of the technical scheme are as follows: the additive comprises raw materials, water and additives, wherein the weight percentage is 45-55: 35-45: 1-5, the raw materials comprise 25-35 parts of yellow glaze soil, 8-5 parts of purple gold soil, 35-25 parts of feldspar powder, 3-6 parts of talcum powder, 14-19 parts of limestone, 15-10 parts of bamboo village glaze soil, 11 parts of bone meal, 11 parts of fluxing materials, 8 parts of brucite and 7 parts of sericite, and the additive comprises 20-40 parts of silica powder, 6-12 parts of soda ash and 10-18 parts of feldspar powder. According to the invention, she-family elements are blended in the celadon preparation process, the slurry has good suspension property and dispersibility, high chemical stability and good rheological property through the mixture ratio of raw materials, and the biscuit glaze after glazing has good associativity, high porcelain-forming strength, strong stereoscopic impression and fine and smooth glaze tone without color difference through multi-stage heat treatment of the biscuit.
Description
Technical Field
The invention relates to the technical field of porcelain, in particular to a she-nationality-element-containing celadon and a preparation method thereof.
Background
The Longquan celadon is a traditional porcelain treasure with Chinese characteristics, and in the period of the south to the north, the Longquan in Zhejiang utilizes local superior natural conditions to manufacture the celadon, and the Longquan celadon is known as a bright pearl of the porcelain garden by the green color of the Longquan celadon, such as jade, light mirror and sound, and is popular with all national celadon enthusiasts.
The Longquan celadon is ever famous for countless and splendid color with a shape and has larger market demand. However, the popularization and application of the Longquan celadon are hindered by factors such as high raw material cost, insufficient celadon strength and color development strength, the market of the celadon can be widened by using the Long quan porcelain clay as a raw material to manufacture a celadon product containing she nationality culture, and the she nationality element is blended into the celadon product by combining the traditional Longquan celadon art with the she nationality culture, so that the she nationality element has remarkable social benefit and economic benefit.
There is therefore a need to propose a solution to this problem.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide the she-nationality element-containing celadon and the preparation method thereof.
The technical purpose of the invention is realized by the following technical scheme: the she-family element-containing celadon comprises raw materials, water and additives, wherein the weight percentage is 45-55: 35-45: 1-5, the raw materials comprise 25-35 parts of yellow glaze soil, 5-8 parts of purple gold soil, 25-35 parts of feldspar powder, 3-6 parts of talcum powder, 14-19 parts of limestone, 10-15 parts of bamboo-rural glaze soil, 11 parts of bone meal, 11 parts of fluxing materials, 8 parts of brucite and 7 parts of sericite, and the additive comprises 20-40 parts of silica powder, 6-12 parts of soda ash, 10-18 parts of feldspar powder, 10-15 parts of aluminum hydroxide, 5-8 parts of zinc oxide, 8-12 parts of calcium carbonate, 6-8 parts of borax, 2-6 parts of potassium carbonate, 6-10 parts of barium sulfate, 2-6 parts of a bonding agent and 8-15 parts of magnetic ordered mesoporous nickel ferrite.
The technical purpose of the invention is also realized by the following technical scheme: a preparation method of a she-family element-containing celadon comprises the following steps: (1) preparing raw materials, water and additives;
(2) preparing a sizing agent of the blank;
(3) selecting representative she-nationality elements and articles, and performing three-dimensional scanning on the representative she-nationality elements and the articles to obtain product appearance information and she-nationality element patterns;
(4) modeling according to the body by using three-dimensional modeling software according to the product appearance information and the she-family element pattern, and integrating the product appearance information and the she-family element design into three-dimensional modeling in the three-dimensional modeling software;
(5) carving the plaster model by using a five-axis carving machine according to the three-dimensional modeling data information after the design is finished;
(6) observing the processed plaster model in detail, checking and repairing the detail parts until she-nationality elements can be perfectly fused with the green body, and turning the adjusted plaster model to obtain a mold;
(7) forming a blank body: carrying out gypsum mold grouting molding on the slurry prepared in the step (2) to prepare a blank, controlling the grouting time to be 20-30s, placing the blank in a ventilated environment, and airing for 4-6 days, wherein the temperature is kept at 20-28 degrees;
(8) biscuit firing: the bisque firing comprises a first stage, a second stage and a third stage; the temperature interval of the second stage is 200-600 degrees, the temperature rise speed is 1-2 degrees/min, the air pressure in the kiln is kept at 0.2-0.3MPa, and the temperature is kept for 20-30 minutes when the temperature rises to 600 degrees;
(9) preparing glaze slip of glaze;
(10) glazing;
(11) glaze firing: the glaze firing comprises a first stage, a second stage, a third stage, a fourth stage and a fifth stage, wherein the temperature interval of the third stage is 950-1000 degrees, the temperature rise speed is 0.5-1 degree/min, the air pressure in the kiln is 0.3-0.5MPa, and the temperature is kept for 1.5-2 hours when the temperature rises to 1000 degrees.
The invention is further configured to: and (3) drying and crushing the raw materials according to the weight ratio, then putting the raw materials into a ball mill for ball milling until the raw materials pass through a 500-mesh sieve to obtain a finished raw material, uniformly mixing the finished raw material, water and an additive according to the weight ratio, adding a proper amount of sodium silicate, putting the mixture into a stirrer for stirring and heating, and thus obtaining the slurry of the blank.
The invention is further configured to: and (3) the glaze slip of the glaze in the step (9) is prepared by respectively grinding the dried kaolin, clay, quartz, wollastonite, muscovite and glaze ash, then putting the ground materials together into a ball mill, adding water for ball milling, and grinding until the ground paste passes through a 400-mesh sieve to obtain the glaze slip.
The invention is further configured to: the glazing in the step (10) comprises inner glazing: adjusting the glaze slip to the specific gravity of 55 baume degrees, pouring the glaze slip into a biscuit firing blank by using a measuring cup, standing for 8-10 s, pouring out the excess glaze slip, and then putting the product with the inner glaze in a drying room for drying for 12-24 h; coating an outer glaze: taking out the dried product, removing dust, supplementing water, glazing the outer glaze by using a glaze dipping method, setting the glazing time to be 8-10 s and the specific gravity of the glaze slip to be 55 baume degrees, and placing the glazed product in a drying room to be dried for 12-24 h; glaze spraying: and taking out the dried product, and placing the dried product on an automatic glaze spraying machine for uniformly spraying glaze on the inner side and the outer side.
In conclusion, the invention has the following beneficial effects:
according to the invention, the she-nationality elements are blended in the celadon preparation process, part of common quartz and bauxite generally adopted in the prior art are replaced by yellow glaze soil, purple gold soil and bamboo-country glaze soil, the characteristic that quartz and alumina in Longquan porcelain soil can fully react with blank raw materials is utilized, so that solid-phase reaction is more complete, the improvement of the celadon ceramic forming strength and stable glaze color are facilitated, the celadon yield is higher through the good catalytic effect of the magnetic ordered mesoporous nickel ferrite, the slurry has good suspension property and dispersibility, the chemical stability is high, the rheological property is good, and the biscuit is fired through five-stage heat treatment after glazing, so that the glaze blank is good in associativity, high in ceramic forming strength, strong in stereoscopic impression, fine and smooth in hue and free of chromatic aberration;
Detailed Description
In order to make those skilled in the art better understand the technical solution of the present invention, the present invention is further described in detail with reference to specific embodiments, and it should be noted that the embodiments and features of the embodiments of the present application can be combined with each other without conflict.
In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "sleeved/connected," "connected," and the like are to be construed broadly, e.g., "connected," which may be fixedly connected, detachably connected, or integrally connected; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
The present invention is described in detail below.
The first embodiment is as follows: the she-family element-containing celadon comprises raw materials, water and additives, and the weight percentage is 54: 45: the raw materials comprise 25 parts of yellow glaze soil, 5 parts of purple gold soil, 25 parts of feldspar powder, 3 parts of talcum powder, 14 parts of limestone, 10 parts of bamboo soil, 11 parts of bone powder, 11 parts of fluxing materials, 8 parts of brucite and 7 parts of sericite, and the additives comprise 20 parts of silica powder, 6 parts of soda ash, 10 parts of feldspar powder, 10 parts of aluminum hydroxide, 5 parts of zinc oxide, 8 parts of calcium carbonate, 6 parts of borax, 2 parts of potassium carbonate, 6 parts of barium sulfate, 2 parts of adhesives and 8 parts of magnetic ordered mesoporous nickel ferrite.
A preparation method of a she-family element-containing celadon comprises the following steps: (1) preparing raw materials, water and additives;
(2) preparing a sizing agent of the blank;
(3) selecting representative she-nationality elements and articles, and performing three-dimensional scanning on the representative she-nationality elements and the articles to obtain product appearance information and she-nationality element patterns;
(4) modeling according to the body by using three-dimensional modeling software according to the product appearance information and the she-family element pattern, and integrating the product appearance information and the she-family element design into three-dimensional modeling in the three-dimensional modeling software;
(5) carving the plaster model by using a five-axis carving machine according to the three-dimensional modeling data information after the design is finished;
(6) observing the processed plaster model in detail, checking and repairing the detail parts until she-nationality elements can be perfectly fused with the green body, and turning the adjusted plaster model to obtain a mold;
(7) forming a blank body: carrying out gypsum mold grouting molding on the slurry prepared in the step (2) to prepare a blank, controlling the grouting time at 20s, placing the blank in a ventilated environment, and airing for 4 days, wherein the temperature is kept at 20 degrees;
(8) biscuit firing: the bisque firing comprises a first stage, a second stage and a third stage; the temperature interval of the second stage is 200-600 degrees, the temperature rise speed is 1-2 degrees/min, the air pressure in the kiln is kept at 0.2-0.3MPa, and the temperature is kept for 20 minutes when the temperature rises to 600 degrees;
(9) preparing glaze slip of glaze;
(10) glazing;
(11) glaze firing: the glaze firing comprises a first stage, a second stage, a third stage, a fourth stage and a fifth stage, wherein the temperature interval of the third stage is 950-1000 degrees, the temperature rising speed is 0.5-1 degree/min, the air pressure in the kiln is 0.3-0.5MPa, and the temperature is preserved for 1.5 hours when the temperature rises to 1000 degrees.
And (3) drying and crushing the raw materials according to the weight ratio, then putting the raw materials into a ball mill for ball milling until the raw materials pass through a 500-mesh sieve to obtain finished raw materials, uniformly mixing the finished raw materials, water and the additive according to the weight ratio, adding a proper amount of sodium silicate, putting the mixture into a stirrer for stirring and heating, and thus obtaining the slurry of the blank.
And (3) preparing glaze slip of the glaze in the step (9), wherein the preparation method comprises the steps of respectively grinding the dried kaolin, clay, quartz, wollastonite, muscovite and glaze ash, then putting the ground materials together into a ball mill, adding water for ball milling, grinding until slurry is sieved by a 400-mesh sieve, and thus obtaining the glaze slip.
The glazing in the step (10) comprises inner glazing: adjusting the glaze slip to the specific gravity of 55 baume degrees, pouring the glaze slip into a biscuit firing blank by using a measuring cup, standing for 8-10 s, pouring out the excess glaze slip, and then putting the product with the inner glaze in a drying room for drying for 12-24 h; coating an outer glaze: taking out the dried product, removing dust, supplementing water, glazing the outer glaze by using a glaze dipping method, setting the glazing time to be 8-10 s and the specific gravity of the glaze slip to be 55 baume degrees, and placing the glazed product in a drying room to be dried for 12-24 h; glaze spraying: and taking out the dried product, and placing the dried product on an automatic glaze spraying machine for uniformly spraying glaze on the inner side and the outer side.
Example two: the she-family element-containing celadon comprises raw materials, water and additives, and the weight percentage is 50: 45: 5, the raw materials comprise 31 parts of yellow glaze soil, 6 parts of purple gold soil, 27 parts of feldspar powder, 5 parts of talcum powder, 16 parts of limestone, 12 parts of bamboo soil, 11 parts of bone meal, 11 parts of fluxing materials, 8 parts of brucite and 7 parts of sericite, and the additive comprises 30 parts of silica powder, 11 parts of soda ash, 15 parts of feldspar powder, 12 parts of aluminum hydroxide, 6 parts of zinc oxide, 10 parts of calcium carbonate, 7 parts of borax, 3 parts of potassium carbonate, 9 parts of barium sulfate, 4 parts of adhesive and 13 parts of magnetic ordered mesoporous nickel ferrite.
A preparation method of a she-family element-containing celadon comprises the following steps: (1) preparing raw materials, water and additives;
(2) preparing a sizing agent of the blank;
(3) selecting representative she-nationality elements and articles, and performing three-dimensional scanning on the representative she-nationality elements and the articles to obtain product appearance information and she-nationality element patterns;
(4) modeling according to the body by using three-dimensional modeling software according to the product appearance information and the she-family element pattern, and integrating the product appearance information and the she-family element design into three-dimensional modeling in the three-dimensional modeling software;
(5) carving the plaster model by using a five-axis carving machine according to the three-dimensional modeling data information after the design is finished;
(6) observing the processed plaster model in detail, checking and repairing the detail parts until she-nationality elements can be perfectly fused with the green body, and turning the adjusted plaster model to obtain a mold;
(7) forming a blank body: carrying out gypsum mold grouting molding on the slurry prepared in the step (2) to prepare a blank, controlling the grouting time to be 20-30s, placing the blank in a ventilated environment, and airing for 4-6 days, wherein the temperature is kept at 20-28 degrees;
(8) biscuit firing: the bisque firing comprises a first stage, a second stage and a third stage; the temperature interval of the second stage is 200-600 degrees, the temperature rise speed is 1-2 degrees/min, the air pressure in the kiln is kept at 0.2-0.3MPa, and the temperature is kept for 25 minutes when the temperature rises to 600 degrees;
(9) preparing glaze slip of glaze;
(10) glazing;
(11) glaze firing: the glaze firing comprises a first stage, a second stage, a third stage, a fourth stage and a fifth stage, wherein the temperature interval of the third stage is 950-1000 degrees, the temperature rising speed is 0.5-1 degree/min, the air pressure in the kiln is 0.3-0.5MPa, and the temperature is preserved for 1.8 hours when the temperature rises to 1000 degrees.
And (3) drying and crushing the raw materials according to the weight ratio, then putting the raw materials into a ball mill for ball milling until the raw materials pass through a 500-mesh sieve to obtain finished raw materials, uniformly mixing the finished raw materials, water and the additive according to the weight ratio, adding a proper amount of sodium silicate, putting the mixture into a stirrer for stirring and heating, and thus obtaining the slurry of the blank.
And (3) preparing glaze slip of the glaze in the step (9), wherein the preparation method comprises the steps of respectively grinding the dried kaolin, clay, quartz, wollastonite, muscovite and glaze ash, then putting the ground materials together into a ball mill, adding water for ball milling, grinding until slurry is sieved by a 400-mesh sieve, and thus obtaining the glaze slip.
The glazing in the step (10) comprises inner glazing: adjusting the glaze slip to the specific gravity of 55 baume degrees, pouring the glaze slip into a biscuit firing blank by using a measuring cup, standing for 8-10 s, pouring out the excess glaze slip, and then putting the product with the inner glaze in a drying room for drying for 12-24 h; coating an outer glaze: taking out the dried product, removing dust, supplementing water, glazing the outer glaze by using a glaze dipping method, setting the glazing time to be 8-10 s and the specific gravity of the glaze slip to be 55 baume degrees, and placing the glazed product in a drying room to be dried for 12-24 h; glaze spraying: and taking out the dried product, and placing the dried product on an automatic glaze spraying machine for uniformly spraying glaze on the inner side and the outer side.
Example three: the she-family element-containing celadon comprises raw materials, water and additives, and the weight percentage is 55: 40: 5, the raw materials comprise 35 parts of yellow glaze soil, 8 parts of purple gold soil, 35 parts of feldspar powder, 6 parts of talcum powder, 19 parts of limestone, 15 parts of bamboo soil, 11 parts of bone meal, 11 parts of fluxing materials, 8 parts of brucite and 7 parts of sericite, and the additives comprise 40 parts of silica powder, 12 parts of soda ash, 18 parts of feldspar powder, 15 parts of aluminum hydroxide, 8 parts of zinc oxide, 12 parts of calcium carbonate, 8 parts of borax, 6 parts of potassium carbonate, 10 parts of barium sulfate, 6 parts of adhesives and 15 parts of magnetic ordered mesoporous nickel ferrite.
A preparation method of a she-family element-containing celadon comprises the following steps: (1) preparing raw materials, water and additives;
(2) preparing a sizing agent of the blank;
(3) selecting representative she-nationality elements and articles, and performing three-dimensional scanning on the representative she-nationality elements and the articles to obtain product appearance information and she-nationality element patterns;
(4) modeling according to the body by using three-dimensional modeling software according to the product appearance information and the she-family element pattern, and integrating the product appearance information and the she-family element design into three-dimensional modeling in the three-dimensional modeling software;
(5) carving the plaster model by using a five-axis carving machine according to the three-dimensional modeling data information after the design is finished;
(6) observing the processed plaster model in detail, checking and repairing the detail parts until she-nationality elements can be perfectly fused with the green body, and turning the adjusted plaster model to obtain a mold;
(7) forming a blank body: carrying out gypsum mold grouting molding on the slurry prepared in the step (2) to prepare a blank, controlling the grouting time to be 20-30s, placing the blank in a ventilated environment, and airing for 4-6 days, wherein the temperature is kept at 20-28 degrees;
(8) biscuit firing: the bisque firing comprises a first stage, a second stage and a third stage; the temperature interval of the second stage is 200-600 degrees, the temperature rise speed is 1-2 degrees/min, the air pressure in the kiln is kept at 0.2-0.3MPa, and the temperature is kept for 30 minutes when the temperature rises to 600 degrees;
(9) preparing glaze slip of glaze;
(10) glazing;
(11) glaze firing: the glaze firing comprises a first stage, a second stage, a third stage, a fourth stage and a fifth stage, wherein the temperature interval of the third stage is 950-1000 degrees, the temperature rising speed is 0.5-1 degree/min, the air pressure in the kiln is 0.3-0.5MPa, and the temperature is preserved for 2 hours when the temperature rises to 1000 degrees.
And (3) drying and crushing the raw materials according to the weight ratio, then putting the raw materials into a ball mill for ball milling until the raw materials pass through a 500-mesh sieve to obtain finished raw materials, uniformly mixing the finished raw materials, water and the additive according to the weight ratio, adding a proper amount of sodium silicate, putting the mixture into a stirrer for stirring and heating, and thus obtaining the slurry of the blank.
And (3) preparing glaze slip of the glaze in the step (9), wherein the preparation method comprises the steps of respectively grinding the dried kaolin, clay, quartz, wollastonite, muscovite and glaze ash, then putting the ground materials together into a ball mill, adding water for ball milling, grinding until slurry is sieved by a 400-mesh sieve, and thus obtaining the glaze slip.
The glazing in the step (10) comprises inner glazing: adjusting the glaze slip to the specific gravity of 55 baume degrees, pouring the glaze slip into a biscuit firing blank by using a measuring cup, standing for 8-10 s, pouring out the excess glaze slip, and then putting the product with the inner glaze in a drying room for drying for 12-24 h; coating an outer glaze: taking out the dried product, removing dust, supplementing water, glazing the outer glaze by using a glaze dipping method, setting the glazing time to be 8-10 s and the specific gravity of the glaze slip to be 55 baume degrees, and placing the glazed product in a drying room to be dried for 12-24 h; glaze spraying: and taking out the dried product, and placing the dried product on an automatic glaze spraying machine for uniformly spraying glaze on the inner side and the outer side.
The above description is only a preferred embodiment of the present invention, and the protection scope of the present invention is not limited to the above embodiments, and all technical solutions belonging to the idea of the present invention belong to the protection scope of the present invention. It should be noted that modifications and embellishments within the scope of the invention may occur to those skilled in the art without departing from the principle of the invention, and are considered to be within the scope of the invention.
Claims (5)
1. The she-family element-containing celadon comprises raw materials, water and additives, and is characterized in that: the weight percentage is 45-55: 35-45: 1-5, the raw materials comprise 25-35 parts of yellow glaze soil, 5-8 parts of purple gold soil, 25-35 parts of feldspar powder, 3-6 parts of talcum powder, 14-19 parts of limestone, 10-15 parts of bamboo-rural glaze soil, 11 parts of bone meal, 11 parts of fluxing materials, 8 parts of brucite and 7 parts of sericite, and the additive comprises 20-40 parts of silica powder, 6-12 parts of soda ash, 10-18 parts of feldspar powder, 10-15 parts of aluminum hydroxide, 5-8 parts of zinc oxide, 8-12 parts of calcium carbonate, 6-8 parts of borax, 2-6 parts of potassium carbonate, 6-10 parts of barium sulfate, 2-6 parts of a bonding agent and 8-15 parts of magnetic ordered mesoporous nickel ferrite.
2. The method for preparing the celadon containing the she-nationality element according to claim 1, characterized in that: the method comprises the following steps: (1) preparing raw materials, water and additives;
(2) preparing a sizing agent of the blank;
(3) selecting representative she-nationality elements and articles, and performing three-dimensional scanning on the representative she-nationality elements and the articles to obtain product appearance information and she-nationality element patterns;
(4) modeling according to the body by using three-dimensional modeling software according to the product appearance information and the she-family element pattern, and integrating the product appearance information and the she-family element design into three-dimensional modeling in the three-dimensional modeling software;
(5) carving the plaster model by using a five-axis carving machine according to the three-dimensional modeling data information after the design is finished;
(6) observing the processed plaster model in detail, checking and repairing the detail parts until she-nationality elements can be perfectly fused with the green body, and turning the adjusted plaster model to obtain a mold;
(7) forming a blank body: carrying out gypsum mold grouting molding on the slurry prepared in the step (2) to prepare a blank, controlling the grouting time to be 20-30s, placing the blank in a ventilated environment, and airing for 4-6 days, wherein the temperature is kept at 20-28 degrees;
(8) biscuit firing: the bisque firing comprises a first stage, a second stage and a third stage; the temperature interval of the second stage is 200-600 degrees, the temperature rise speed is 1-2 degrees/min, the air pressure in the kiln is kept at 0.2-0.3MPa, and the temperature is kept for 20-30 minutes when the temperature rises to 600 degrees;
(9) preparing glaze slip of glaze;
(10) glazing;
(11) glaze firing: the glaze firing comprises a first stage, a second stage, a third stage, a fourth stage and a fifth stage, wherein the temperature interval of the third stage is 950-1000 degrees, the temperature rise speed is 0.5-1 degree/min, the air pressure in the kiln is 0.3-0.5MPa, and the temperature is kept for 1.5-2 hours when the temperature rises to 1000 degrees.
3. The method for preparing the celadon containing the she-nationality element according to claim 2, characterized in that: and (3) drying and crushing the raw materials according to the weight ratio, then putting the raw materials into a ball mill for ball milling until the raw materials pass through a 500-mesh sieve to obtain a finished raw material, uniformly mixing the finished raw material, water and an additive according to the weight ratio, adding a proper amount of sodium silicate, putting the mixture into a stirrer for stirring and heating, and thus obtaining the slurry of the blank.
4. The method for preparing the celadon containing the she-nationality element according to claim 2, characterized in that: and (3) the glaze slip of the glaze in the step (9) is prepared by respectively grinding the dried kaolin, clay, quartz, wollastonite, muscovite and glaze ash, then putting the ground materials together into a ball mill, adding water for ball milling, and grinding until the ground paste passes through a 400-mesh sieve to obtain the glaze slip.
5. The method for preparing the celadon containing the she-nationality element according to claim 2, characterized in that: the glazing in the step (10) comprises inner glazing: adjusting the glaze slip to the specific gravity of 55 baume degrees, pouring the glaze slip into a biscuit firing blank by using a measuring cup, standing for 8-10 s, pouring out the excess glaze slip, and then putting the product with the inner glaze in a drying room for drying for 12-24 h; coating an outer glaze: taking out the dried product, removing dust, supplementing water, glazing the outer glaze by using a glaze dipping method, setting the glazing time to be 8-10 s and the specific gravity of the glaze slip to be 55 baume degrees, and placing the glazed product in a drying room to be dried for 12-24 h; glaze spraying: and taking out the dried product, and placing the dried product on an automatic glaze spraying machine for uniformly spraying glaze on the inner side and the outer side.
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Application publication date: 20220429 |