CN114181614A - 一种mof基光热除冰涂层及其制备方法 - Google Patents
一种mof基光热除冰涂层及其制备方法 Download PDFInfo
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- CN114181614A CN114181614A CN202111432352.0A CN202111432352A CN114181614A CN 114181614 A CN114181614 A CN 114181614A CN 202111432352 A CN202111432352 A CN 202111432352A CN 114181614 A CN114181614 A CN 114181614A
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- 238000000576 coating method Methods 0.000 title claims abstract description 49
- 239000011248 coating agent Substances 0.000 title claims abstract description 46
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 239000000463 material Substances 0.000 claims abstract description 42
- 239000000843 powder Substances 0.000 claims abstract description 28
- 239000004205 dimethyl polysiloxane Substances 0.000 claims abstract description 20
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims abstract description 20
- 239000013078 crystal Substances 0.000 claims abstract description 14
- 238000001035 drying Methods 0.000 claims abstract description 13
- JIDMEYQIXXJQCC-UHFFFAOYSA-L copper;2,2,2-trifluoroacetate Chemical compound [Cu+2].[O-]C(=O)C(F)(F)F.[O-]C(=O)C(F)(F)F JIDMEYQIXXJQCC-UHFFFAOYSA-L 0.000 claims abstract description 11
- YJTKZCDBKVTVBY-UHFFFAOYSA-N 1,3-Diphenylbenzene Chemical group C1=CC=CC=C1C1=CC=CC(C=2C=CC=CC=2)=C1 YJTKZCDBKVTVBY-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000004729 solvothermal method Methods 0.000 claims abstract description 10
- 238000006243 chemical reaction Methods 0.000 claims abstract description 8
- 238000001027 hydrothermal synthesis Methods 0.000 claims abstract description 7
- 239000002904 solvent Substances 0.000 claims abstract description 7
- 238000004140 cleaning Methods 0.000 claims abstract description 6
- 238000005507 spraying Methods 0.000 claims abstract description 6
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 claims abstract description 3
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 12
- 238000000034 method Methods 0.000 claims description 11
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 6
- -1 polydimethylsiloxane Polymers 0.000 claims description 5
- 125000005375 organosiloxane group Chemical group 0.000 claims description 4
- 230000035484 reaction time Effects 0.000 claims description 4
- WHQSYGRFZMUQGQ-UHFFFAOYSA-N n,n-dimethylformamide;hydrate Chemical compound O.CN(C)C=O WHQSYGRFZMUQGQ-UHFFFAOYSA-N 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 5
- 239000012621 metal-organic framework Substances 0.000 abstract 3
- 239000000654 additive Substances 0.000 abstract 2
- 230000000996 additive effect Effects 0.000 abstract 2
- 235000013870 dimethyl polysiloxane Nutrition 0.000 abstract 1
- CXQXSVUQTKDNFP-UHFFFAOYSA-N octamethyltrisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)O[Si](C)(C)C CXQXSVUQTKDNFP-UHFFFAOYSA-N 0.000 abstract 1
- 238000004987 plasma desorption mass spectroscopy Methods 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 8
- 229910052782 aluminium Inorganic materials 0.000 description 8
- 238000005286 illumination Methods 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 229910001220 stainless steel Inorganic materials 0.000 description 3
- 239000010935 stainless steel Substances 0.000 description 3
- 230000003075 superhydrophobic effect Effects 0.000 description 3
- 238000009825 accumulation Methods 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 230000008014 freezing Effects 0.000 description 2
- 238000007710 freezing Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 239000012212 insulator Substances 0.000 description 1
- 239000003446 ligand Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 238000010248 power generation Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000009736 wetting Methods 0.000 description 1
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D183/00—Coating compositions based on macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon, with or without sulfur, nitrogen, oxygen, or carbon only; Coating compositions based on derivatives of such polymers
- C09D183/04—Polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G83/00—Macromolecular compounds not provided for in groups C08G2/00 - C08G81/00
- C08G83/008—Supramolecular polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Paints Or Removers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Abstract
Description
0s | 10s | 20s | 30s | 40s | |
纯PDMS涂层 | 35.1℃ | 42.3℃ | 46.7℃ | 51.4℃ | 55.3℃ |
实施例1涂层 | 34.6℃ | 63.3℃ | 75.6℃ | 82.0℃ | 84.5℃ |
Claims (7)
Priority Applications (1)
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CN202111432352.0A CN114181614B (zh) | 2021-11-29 | 2021-11-29 | 一种mof基光热除冰涂层及其制备方法 |
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CN202111432352.0A CN114181614B (zh) | 2021-11-29 | 2021-11-29 | 一种mof基光热除冰涂层及其制备方法 |
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CN114181614A true CN114181614A (zh) | 2022-03-15 |
CN114181614B CN114181614B (zh) | 2022-05-13 |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115448400A (zh) * | 2022-08-26 | 2022-12-09 | 南京林业大学 | 一种负载金属有机骨架的木基蒸发器的制备方法 |
CN116535904A (zh) * | 2023-06-08 | 2023-08-04 | 福州大学 | 一种透明光热类液体防/除冰涂层及其制备方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106622142A (zh) * | 2015-11-03 | 2017-05-10 | 中国石油化工股份有限公司 | 一种金属有机骨架材料Cu3(BTC)2及其制备方法和应用 |
CN110183674A (zh) * | 2019-04-30 | 2019-08-30 | 华中科技大学 | 树状自相似性金属有机框架复合材料及其制备与应用 |
CN110204767A (zh) * | 2019-06-24 | 2019-09-06 | 中国科学院长春应用化学研究所 | 一种耐用型防冰材料及其制备方法 |
EP3586956A1 (en) * | 2018-06-22 | 2020-01-01 | ETH Zurich | Nanoreactors for the synthesis of porous crystalline materials |
WO2020034008A1 (en) * | 2018-08-16 | 2020-02-20 | Commonwealth Scientific And Industrial Research Organisation | Metal organic framework based water capture apparatus |
-
2021
- 2021-11-29 CN CN202111432352.0A patent/CN114181614B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106622142A (zh) * | 2015-11-03 | 2017-05-10 | 中国石油化工股份有限公司 | 一种金属有机骨架材料Cu3(BTC)2及其制备方法和应用 |
EP3586956A1 (en) * | 2018-06-22 | 2020-01-01 | ETH Zurich | Nanoreactors for the synthesis of porous crystalline materials |
WO2020034008A1 (en) * | 2018-08-16 | 2020-02-20 | Commonwealth Scientific And Industrial Research Organisation | Metal organic framework based water capture apparatus |
CN110183674A (zh) * | 2019-04-30 | 2019-08-30 | 华中科技大学 | 树状自相似性金属有机框架复合材料及其制备与应用 |
CN110204767A (zh) * | 2019-06-24 | 2019-09-06 | 中国科学院长春应用化学研究所 | 一种耐用型防冰材料及其制备方法 |
Non-Patent Citations (2)
Title |
---|
周胜: "金属有机骨架膜的制备与应用进展", 《化工进展》 * |
李路路: "共价有机框架材料研宄进展", 《物理化学学报》 * |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115448400A (zh) * | 2022-08-26 | 2022-12-09 | 南京林业大学 | 一种负载金属有机骨架的木基蒸发器的制备方法 |
CN115448400B (zh) * | 2022-08-26 | 2024-04-09 | 南京林业大学 | 一种负载金属有机骨架的木基蒸发器的制备方法 |
CN116535904A (zh) * | 2023-06-08 | 2023-08-04 | 福州大学 | 一种透明光热类液体防/除冰涂层及其制备方法 |
CN116535904B (zh) * | 2023-06-08 | 2024-06-04 | 福州大学 | 一种透明光热类液体防/除冰涂层及其制备方法 |
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CN114181614B (zh) | 2022-05-13 |
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Effective date of registration: 20231018 Address after: No. 132 Wufengshan Road, New District, Zhenjiang City, Jiangsu Province, 212000 Patentee after: Zhenjiang Fengtai Agricultural Technology Co.,Ltd. Address before: 213001 No. 1801 Wu Cheng Road, Changzhou, Jiangsu Patentee before: JIANGSU University OF TECHNOLOGY |
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Effective date of registration: 20240703 Address after: 224200, located in the China Europe Science and Technology Industrial Park, Jingba Road, Dongtai Economic Development Zone, Yancheng City, Jiangsu Province Patentee after: Yancheng Chentao Information Technology Co.,Ltd. Country or region after: China Address before: No. 132 Wufengshan Road, New District, Zhenjiang City, Jiangsu Province, 212000 Patentee before: Zhenjiang Fengtai Agricultural Technology Co.,Ltd. Country or region before: China |