CN114085711B - Plant essence for electronic atomized liquid and preparation method thereof - Google Patents
Plant essence for electronic atomized liquid and preparation method thereof Download PDFInfo
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- CN114085711B CN114085711B CN202111390167.XA CN202111390167A CN114085711B CN 114085711 B CN114085711 B CN 114085711B CN 202111390167 A CN202111390167 A CN 202111390167A CN 114085711 B CN114085711 B CN 114085711B
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- 239000007788 liquid Substances 0.000 title claims abstract description 50
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000000341 volatile oil Substances 0.000 claims abstract description 175
- 241000196324 Embryophyta Species 0.000 claims abstract description 51
- 239000002994 raw material Substances 0.000 claims abstract description 49
- 244000284012 Vetiveria zizanioides Species 0.000 claims abstract description 28
- 235000007769 Vetiveria zizanioides Nutrition 0.000 claims abstract description 28
- 235000007866 Chamaemelum nobile Nutrition 0.000 claims abstract description 18
- 241000208152 Geranium Species 0.000 claims abstract description 18
- 244000042664 Matricaria chamomilla Species 0.000 claims abstract description 18
- 235000007232 Matricaria chamomilla Nutrition 0.000 claims abstract description 18
- 244000179970 Monarda didyma Species 0.000 claims abstract description 18
- 235000010672 Monarda didyma Nutrition 0.000 claims abstract description 18
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- 238000000034 method Methods 0.000 claims abstract description 11
- 238000000889 atomisation Methods 0.000 claims abstract description 10
- 238000003756 stirring Methods 0.000 claims description 20
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- 238000010298 pulverizing process Methods 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 11
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- 239000000843 powder Substances 0.000 claims description 10
- 238000001256 steam distillation Methods 0.000 claims description 10
- 239000012530 fluid Substances 0.000 claims description 8
- 238000002791 soaking Methods 0.000 claims description 8
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- 229960002715 nicotine Drugs 0.000 description 9
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- 239000003571 electronic cigarette Substances 0.000 description 7
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 description 6
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 5
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- 210000004204 blood vessel Anatomy 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- QMVPMAAFGQKVCJ-UHFFFAOYSA-N citronellol Chemical compound OCCC(C)CCC=C(C)C QMVPMAAFGQKVCJ-UHFFFAOYSA-N 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 239000008369 fruit flavor Substances 0.000 description 2
- 235000011187 glycerol Nutrition 0.000 description 2
- UWKAYLJWKGQEPM-LBPRGKRZSA-N linalyl acetate Chemical compound CC(C)=CCC[C@](C)(C=C)OC(C)=O UWKAYLJWKGQEPM-LBPRGKRZSA-N 0.000 description 2
- 210000002751 lymph Anatomy 0.000 description 2
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- 239000007858 starting material Substances 0.000 description 2
- FQTLCLSUCSAZDY-UHFFFAOYSA-N (+) E(S) nerolidol Natural products CC(C)=CCCC(C)=CCCC(C)(O)C=C FQTLCLSUCSAZDY-UHFFFAOYSA-N 0.000 description 1
- OPFTUNCRGUEPRZ-UHFFFAOYSA-N (+)-beta-Elemen Natural products CC(=C)C1CCC(C)(C=C)C(C(C)=C)C1 OPFTUNCRGUEPRZ-UHFFFAOYSA-N 0.000 description 1
- OPFTUNCRGUEPRZ-QLFBSQMISA-N (-)-beta-elemene Chemical compound CC(=C)[C@@H]1CC[C@@](C)(C=C)[C@H](C(C)=C)C1 OPFTUNCRGUEPRZ-QLFBSQMISA-N 0.000 description 1
- QMVPMAAFGQKVCJ-SNVBAGLBSA-N (R)-(+)-citronellol Natural products OCC[C@H](C)CCC=C(C)C QMVPMAAFGQKVCJ-SNVBAGLBSA-N 0.000 description 1
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- GLZPCOQZEFWAFX-YFHOEESVSA-N Geraniol Natural products CC(C)=CCC\C(C)=C/CO GLZPCOQZEFWAFX-YFHOEESVSA-N 0.000 description 1
- 239000005792 Geraniol Substances 0.000 description 1
- 206010019233 Headaches Diseases 0.000 description 1
- 244000246386 Mentha pulegium Species 0.000 description 1
- 235000016257 Mentha pulegium Nutrition 0.000 description 1
- 235000004357 Mentha x piperita Nutrition 0.000 description 1
- GLZPCOQZEFWAFX-JXMROGBWSA-N Nerol Natural products CC(C)=CCC\C(C)=C\CO GLZPCOQZEFWAFX-JXMROGBWSA-N 0.000 description 1
- FQTLCLSUCSAZDY-ATGUSINASA-N Nerolidol Chemical compound CC(C)=CCC\C(C)=C\CC[C@](C)(O)C=C FQTLCLSUCSAZDY-ATGUSINASA-N 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 241000109329 Rosa xanthina Species 0.000 description 1
- 235000004789 Rosa xanthina Nutrition 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- WUOACPNHFRMFPN-UHFFFAOYSA-N alpha-terpineol Chemical compound CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 description 1
- 239000003242 anti bacterial agent Substances 0.000 description 1
- 239000003429 antifungal agent Substances 0.000 description 1
- 229940121375 antifungal agent Drugs 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- JGQFVRIQXUFPAH-UHFFFAOYSA-N beta-citronellol Natural products OCCC(C)CCCC(C)=C JGQFVRIQXUFPAH-UHFFFAOYSA-N 0.000 description 1
- 230000036772 blood pressure Effects 0.000 description 1
- 229940043350 citral Drugs 0.000 description 1
- 235000000484 citronellol Nutrition 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 150000004292 cyclic ethers Chemical class 0.000 description 1
- SQIFACVGCPWBQZ-UHFFFAOYSA-N delta-terpineol Natural products CC(C)(O)C1CCC(=C)CC1 SQIFACVGCPWBQZ-UHFFFAOYSA-N 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- -1 ester alcohols Chemical class 0.000 description 1
- 235000019441 ethanol Nutrition 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 238000011010 flushing procedure Methods 0.000 description 1
- 230000004927 fusion Effects 0.000 description 1
- WTEVQBCEXWBHNA-JXMROGBWSA-N geranial Chemical compound CC(C)=CCC\C(C)=C\C=O WTEVQBCEXWBHNA-JXMROGBWSA-N 0.000 description 1
- 229940113087 geraniol Drugs 0.000 description 1
- 238000009499 grossing Methods 0.000 description 1
- 231100000869 headache Toxicity 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 235000001050 hortel pimenta Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 210000004877 mucosa Anatomy 0.000 description 1
- WASNIKZYIWZQIP-AWEZNQCLSA-N nerolidol Natural products CC(=CCCC(=CCC[C@@H](O)C=C)C)C WASNIKZYIWZQIP-AWEZNQCLSA-N 0.000 description 1
- 231100000344 non-irritating Toxicity 0.000 description 1
- 235000019645 odor Nutrition 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 150000007965 phenolic acids Chemical class 0.000 description 1
- 235000009048 phenolic acids Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 230000002633 protecting effect Effects 0.000 description 1
- 230000001624 sedative effect Effects 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 230000009967 tasteless effect Effects 0.000 description 1
- 150000003505 terpenes Chemical class 0.000 description 1
- 235000007586 terpenes Nutrition 0.000 description 1
- 229940116411 terpineol Drugs 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 231100000167 toxic agent Toxicity 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
- Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
Abstract
The invention belongs to the technical field of essence and spice, and particularly relates to a plant essence for electronic atomized liquid and a preparation method thereof. The plant essence raw material components for the electronic atomized liquid comprise: 5-12 parts of peony petal essential oil, 2.5-4 parts of chamomile essential oil, 0.8-3 parts of vetiver essential oil, 0.5-2 parts of madder essential oil, 8-15 parts of bergamot essential oil, 0.2-1.5 parts of rose essential oil, 3-7 parts of geranium essential oil, 1.5-3 parts of brandy leaf essential oil and 10-20 parts of ethanol; the vetiver essential oil is added into the raw material components, so that the volatilization of the low-boiling plant extract can be slowed down, the volatilization process is uniform and slow, the electronic atomization liquid has longer lasting taste, does not rush nose, and is aromatic and long-lasting; the Texas cypress wood oil is added to blur the fragrance limit among all the fragrance raw materials, so that the fragrance of the essence is finer and softer; the components are cooperatively blended, so that the electronic atomized liquid is rich in fragrance and durable, and provides a good experience for users.
Description
Technical Field
The invention belongs to the technical field of essence and spice, and particularly relates to a plant essence for electronic atomized liquid and a preparation method thereof.
Background
Electronic atomized liquid is also called atomized liquid, electronic cigarette liquid, tobacco tar and the like, is the most core technology in the whole electronic cigarette industry chain, and determines the safety of products and visual feeling of obtaining mouthfeel by consumers. The electronic atomized liquid is a liquid prepared by extracting essence from plants, adding propylene glycol, glycerol and the like, heating by an atomizer of the electronic cigarette, and gasifying into mist to be absorbed by a human body.
The essence is used as an important component of the electronic atomized liquid for adjusting the taste so as to meet the sensory requirements of consumers, and the essence for the electronic atomized liquid at present mainly depends on two ways of natural plant extraction and chemical synthesis. The essence synthesized by chemistry has a safety dispute, so that the environment-friendly ecological environment space is created for further meeting the scientific and healthy living needs of people, the living quality of people is improved, and the development of essence plant resources to a greater extent becomes a necessary trend.
The main stream of plant essence for electronic atomized liquid in the market at present has tobacco flavor essence, cool mint flavor essence and various fruit flavor essences, and the tobacco flavor essence has high simulation degree but strong irritation to throat; the mint flavor can cover up the heavy astringent taste of nicotine in the electronic atomized liquid, but has strong and durable cool feeling, and is not suitable for people with cold and cool constitution; the fruit flavor essence is fresh, but the heavy astringency of nicotine in the electronic atomized liquid is difficult to mask, and the lasting fragrance is poor. In addition, the essence with the main stream taste is easy to volatilize at room temperature, the atomization bullet cannot be completely sealed, smell of volatile substances can be smelled from the periphery of the atomization bullet even when the electronic cigarette does not work, particularly atomized liquid in a liquid storage bin can be conducted and heated by a heating atomization core when the electronic cigarette works, so that the volatile substances in the atomized liquid are accelerated to escape and lose, the concentration of the volatile substances is lower and lower, the electronic cigarette is even tasteless when being sucked to the middle and later stages, and the user experience is seriously reduced.
Disclosure of Invention
The invention aims at solving the problems in the prior art and provides the environment-friendly plant essence for the electronic atomized liquid, which is not easy to volatilize and is capable of lasting fragrance, and the sucking quality of the electronic atomized liquid is greatly improved.
The above object of the present invention can be achieved by the following technical solutions: the plant essence for the electronic atomized liquid comprises the following raw material components:
peony petal essential oil 5-12 parts
2.5-4 parts of chamomile essential oil
0.8-3 parts of vetiver essential oil
0.5-2 parts of madder essential oil
8-15 parts of bergamot essential oil
0.2-1.5 parts of herba rosae rugosae essential oil
3-7 parts of geranium essential oil
1.5-3 parts of white orchid leaf essential oil
10-20 parts of ethanol.
The plant essence is prepared from the plant essential oil, is safe, has no stimulation, has rich and pleasant aroma, has smaller extract molecules, is easy to diffuse, can be rapidly diffused into blood vessels and lymph when the electronic atomized liquid is pumped, promotes blood circulation, takes away carbon dioxide and deposited metabolic substances in the body, and reduces the harm of nicotine in the electronic atomized liquid to the body. According to the invention, the vetiver essential oil is added into the plant essence, so that on one hand, the vetiver essential oil has excellent adsorption capacity, volatilization of low-boiling plant extracts can be slowed down, the volatilization process is uniform and slow, and the electronic atomized liquid has longer lasting taste, does not rush nose and is aromatic and long; on the other hand, the vetiver essential oil and the components of different aroma raw materials are in synergistic effect, so that the original equilibrium state is broken, and the volatilization characteristics of the aroma components are changed.
The peony petal essential oil contains various active ingredients such as ester alcohols, terpenes, phenolic acids, unsaturated hydrocarbons and the like, and the ingredients are safe, rich and various in fragrance and have an antioxidant effect.
The chamomile essential oil contains rich cyclic ethers, flavonoids and other components, has good antibacterial, anti-inflammatory and sedative effects, and protects the sensitive physique user.
The electronic atomized liquid contains nicotine, which is known to be a highly toxic substance, and the nicotine is required to be detoxified through the liver after being inhaled into human body, so that the liver of people with dependency on the nicotine bears a large detoxication load, and the liver is inevitably damaged by long-term high-pressure work, thereby affecting the health of the people. For this reason, the inventors have added madder essential oil to the essential raw materials, which has liver protecting effect.
The bergamot essential oil mainly contains linalyl acetate, linalool, terpineol, nerol, dihydrodill alcohol, citral, bergamot phenol and the like, has the effects of refreshing, helping memory, improving working efficiency, reducing blood pressure, smoothing blood flow, treating headache and the like, and enables a user under high-pressure and high-load work to feel refreshing and relaxed after sucking electronic atomized liquid.
The herba Rosmarini officinalis essential oil has flos Rosae Rugosae fragrance, is excellent antibacterial and antifungal agent, is mild and non-irritating to airway mucosa, and has antiinflammatory effect.
The geranium essential oil mainly comprises geraniol, citronellol, linalool and other components, has excellent oxidation resistance and antibacterial property, is synergistic with the geranium essential oil and the chamomile essential oil, has pleasant aroma and has various odors such as roses, oranges, peppermint and the like.
The white orchid leaf essential oil mainly contains the faint scent in the clear and nourishing scent, the faint scent is sweet and is more and more elegant than linalool in scent, the white orchid essential oil is slightly provided with white orchid scent, the scent is transparent and does not remain long, the essential oil contains linalool, linalool acetate, dihydrolinalool, elemene, nerolidol and the like, the smoke can be refined, and the fusion of nicotine in the smoke and the flower scent of various raw material essential oils can be promoted.
Preferably, the plant essence raw material component for the electronic atomization liquid also comprises 1-4 parts of Texas cypress wood oil.
By adding the Texas cypress wood oil, the main adjustment of the essence is more outstanding, and other outstanding fragrance raw materials in the essence are coordinated, so that the original and stimulated fragrance becomes soft, the fragrance limit among the fragrance raw materials is blurred, and the fragrance of the essence is softer.
The second object of the present invention is to provide a preparation method of the plant essence, comprising the following steps:
s1: weighing the raw materials in parts by weight for later use;
s2: sequentially placing the weighed peony petal essential oil, chamomile essential oil, madder essential oil, bergamot essential oil, rose essential oil, geranium essential oil and brandy leaf essential oil into a stirring container, and stirring at normal temperature to fully and uniformly mix the raw materials;
s3: adding vetiver essential oil, texas cedar wood oil and ethanol, continuously stirring, and fully fusing to obtain the plant essence for the electronic atomization liquid.
Preferably, the preparation methods of the peony essential oil and the chamomile essential oil are as follows:
(1) Pulverizing plant materials to 30-45 mesh, adding 1-2 times of pure water into plant powder, and mixing;
(2) Placing the mixture in dry distillation equipment, and obtaining distillate gas by a temperature programming mode;
(3) Collecting distillate gas, and condensing at 3-10deg.C to obtain corresponding raw material essential oil.
Further preferably, the temperature programming is specifically that the temperature is firstly increased to 80-110 ℃ at 3-8 ℃/min, the temperature is kept for 1-2h, then the temperature is increased to 300-450 ℃ at the temperature increasing rate of 5-10 ℃/min, and the temperature is kept for 1-2h.
By adopting sectional distillation, the aroma components with different volatility and boiling point can be better collected through specific heating rate and continuous heating time at specific temperature, and richer aroma types can be obtained.
Preferably, the preparation methods of the vetiver essential oil, the madder essential oil and the rose essential oil are subcritical extraction methods, and the subcritical fluid is petroleum ether.
Further preferably, the subcritical extraction conditions are: the pressure is 4.5-5MPa, the temperature is 120-150 ℃, the time is 20-30min, and the flow is 1-3L/h.
Preferably, the specific preparation steps of the bergamot essential oil, the geranium essential oil and the brandy leaf essential oil are as follows: pulverizing the raw materials into coarse powder, respectively, and soaking in 3-5 times of water for 3-5 hr; stirring, extracting by steam distillation for 2-4h, and collecting in an oil-water separator to obtain crude essential oil; centrifuging the crude essential oil at 3000r/min for 10min, and collecting supernatant to obtain the final product.
Compared with the prior art, the invention has the following beneficial effects:
1. the plant essence is prepared from the plant essential oil, is safe, has no stimulation, has rich and pleasant aroma, has smaller extract molecules, is easy to diffuse, can be rapidly diffused into blood vessels and lymph when the electronic atomized liquid is pumped, promotes blood circulation, takes away carbon dioxide and deposited metabolic substances in the body, and reduces the harm of nicotine in the electronic atomized liquid to the body.
2. According to the invention, the vetiver essential oil is added into the plant essence, so that on one hand, the vetiver essential oil has excellent adsorption capacity, volatilization of low-boiling plant extracts can be slowed down, the volatilization process is uniform and slow, and the electronic atomized liquid has longer lasting taste, does not rush nose and is aromatic and long; on the other hand, the vetiver essential oil and the components of different aroma raw materials are in synergistic effect, so that the original equilibrium state is broken, and the volatilization characteristics of the aroma components are changed.
3. According to the invention, according to the characteristics of different plant essential oils, the method is not used, the aroma substances in the plant raw materials can be fully extracted, and the obtained essential oil has pure aroma and does not contain any chemical smell.
Detailed Description
The following are specific examples of the present invention and illustrate the technical scheme of the present invention, but the present invention is not limited to these examples. The starting materials not separately prepared in the context of the present invention are all commercially available conventional starting materials, and the processes not mentioned are all conventional in the art.
Examples 1 to 5
The composition of the plant essence components in examples 1-5 are shown in Table 1 in parts by weight.
TABLE 1
Example 6
Adopts a mode of combining carbonization and steam distillation to respectively prepare peony essential oil and chamomile essential oil, and specifically comprises the following steps: pulverizing plant materials to 30 mesh, adding 1 times of pure water into plant powder, and mixing; placing the mixture in dry distillation equipment, heating to 80 ℃ at a speed of 3 ℃/min by adopting a temperature programming mode, preserving heat for 1h, heating to 300 ℃ at a heating rate of 5 ℃/min, and preserving heat for 1h; collecting fraction gas, and condensing at 3deg.C to obtain corresponding raw material essential oil.
The vetiver essential oil, the madder essential oil and the rose essential oil are respectively prepared by adopting a subcritical extraction method, and specifically comprise the following steps: pulverizing the raw materials, soaking and extracting in subcritical fluid petroleum ether, controlling the extraction pressure to 4.5MPa, the temperature to 120 ℃ and the time to 20min, and controlling the fluid flow to 1L/h.
Extracting bergamot essential oil, geranium essential oil and brandy leaf essential oil respectively by adopting a steam method, wherein the preparation method comprises the following specific steps: pulverizing the raw materials into coarse powder, respectively, and soaking in 3 times of water for 3 hr; stirring, extracting by steam distillation for 2 hours, and collecting in an oil-water separator to obtain crude essential oil; centrifuging the crude essential oil at 3000r/min for 10min, and collecting supernatant to obtain the final product.
Weighing the raw material components according to the weight parts of the example 1 for standby; sequentially placing the weighed peony petal essential oil, chamomile essential oil, madder essential oil, bergamot essential oil, rose essential oil, geranium essential oil and brandy leaf essential oil into a stirring container, and stirring at normal temperature to fully and uniformly mix the raw materials; adding vetiver essential oil, texas cedar wood oil and ethanol, continuously stirring, and fully fusing to obtain the plant essence for the electronic atomization liquid.
Example 7
Adopts a mode of combining carbonization and steam distillation to respectively prepare peony essential oil and chamomile essential oil, and specifically comprises the following steps: pulverizing plant materials to 40 mesh, adding 1.5 times of pure water into plant powder, and mixing; placing the mixture in dry distillation equipment, heating to 80 ℃ at a speed of 6 ℃/min by adopting a temperature programming mode, preserving heat for 1h, heating to 300 ℃ at a speed of 7 ℃/min, and preserving heat for 1.5h; collecting fraction gas, and condensing at 6deg.C to obtain corresponding raw material essential oil.
The vetiver essential oil, the madder essential oil and the rose essential oil are respectively prepared by adopting a subcritical extraction method, and specifically comprise the following steps: pulverizing the raw materials, soaking and extracting in subcritical fluid petroleum ether, controlling the extraction pressure to 4.8MPa, the temperature to 130 ℃ and the time to 25min, and controlling the fluid flow to 2L/h.
Extracting bergamot essential oil, geranium essential oil and brandy leaf essential oil respectively by adopting a steam method, wherein the preparation method comprises the following specific steps: pulverizing the raw materials into coarse powder, respectively, and soaking in 4 times of water for 4 hr; stirring, extracting by steam distillation for 3h, and collecting in an oil-water separator to obtain crude essential oil; centrifuging the crude essential oil at 3000r/min for 10min, and collecting supernatant to obtain the final product.
Weighing the raw material components according to the weight parts of the example 1 for standby; sequentially placing the weighed peony petal essential oil, chamomile essential oil, madder essential oil, bergamot essential oil, rose essential oil, geranium essential oil and brandy leaf essential oil into a stirring container, and stirring at normal temperature to fully and uniformly mix the raw materials; adding vetiver essential oil, texas cedar wood oil and ethanol, continuously stirring, and fully fusing to obtain the plant essence for the electronic atomization liquid.
Example 8
Adopts a mode of combining carbonization and steam distillation to respectively prepare peony essential oil and chamomile essential oil, and specifically comprises the following steps: pulverizing plant materials to 45 mesh, adding 2 times of pure water into plant powder, and mixing; placing the mixture in dry distillation equipment, heating to 80 ℃ at 8 ℃/min by adopting a temperature programming mode, preserving heat for 1h, heating to 300 ℃ at a heating rate of 10 ℃/min, and preserving heat for 2h; collecting fraction gas, and condensing at 10deg.C to obtain corresponding raw material essential oil.
The vetiver essential oil, the madder essential oil and the rose essential oil are respectively prepared by adopting a subcritical extraction method, and specifically comprise the following steps: pulverizing the raw materials, soaking and extracting in subcritical fluid petroleum ether, controlling the extraction pressure to 5MPa, the temperature to 150 ℃ and the time to 30min, and controlling the fluid flow to 3L/h.
Extracting bergamot essential oil, geranium essential oil and brandy leaf essential oil respectively by adopting a steam method, wherein the preparation method comprises the following specific steps: pulverizing the raw materials into coarse powder, respectively, and soaking in 5 times of water for 5 hr; stirring, extracting by steam distillation for 4 hours, and collecting in an oil-water separator to obtain crude essential oil; centrifuging the crude essential oil at 3000r/min for 10min, and collecting supernatant to obtain the final product.
Weighing the raw material components according to the weight parts of the example 1 for standby; sequentially placing the weighed peony petal essential oil, chamomile essential oil, madder essential oil, bergamot essential oil, rose essential oil, geranium essential oil and brandy leaf essential oil into a stirring container, and stirring at normal temperature to fully and uniformly mix the raw materials; adding vetiver essential oil, texas cedar wood oil and ethanol, continuously stirring, and fully fusing to obtain the plant essence for the electronic atomization liquid.
Example 9
The difference from example 8 is only that the raw material components are weighed according to the parts by weight of example 2.
Example 10
The difference from example 8 is only that the raw material components are weighed according to the parts by weight of example 3.
Example 11
The difference from example 8 is only that the raw material components are weighed according to the parts by weight of example 4.
Example 12
The difference from example 8 is only that the raw material components are weighed according to the parts by weight of example 5.
Comparative example 1
The only difference from example 8 is that the raw material component does not contain vetiver essential oil.
Comparative example 2
The raw material component does not contain Texas cypress oil.
Comparative example 3
The raw material components of peony petal essential oil, chamomile essential oil, vetiver essential oil, madder essential oil, bergamot essential oil, rose essential oil, geranium essential oil and brandy leaf essential oil are extracted by adopting a dry distillation and steam distillation combined mode.
Comparative example 4
The raw material components of peony petal essential oil, chamomile essential oil, vetiver essential oil, madder essential oil, bergamot essential oil, rose essential oil, geranium essential oil and brandy leaf essential oil are extracted by adopting a subcritical extraction method.
Comparative example 5
The raw material components of peony petal essential oil, chamomile essential oil, vetiver essential oil, madder essential oil, bergamot essential oil, rose essential oil, geranium essential oil and brandy leaf essential oil are all extracted by adopting a steam distillation mode.
Experiment
1. The plant essences obtained in examples 6 to 12 and comparative examples 1 to 5 were added in equal amounts to the electronic atomized liquid, and the sensory quality thereof was evaluated.
10g of the plant essence obtained in examples 6-12 and comparative examples 1-5, 1g of nicotine, 50g of glycerin and 58.5g of propylene glycol are respectively mixed and uniformly stirred to obtain 12 groups of corresponding electronic atomized liquid, the electronic atomized liquid is added into an electronic cigarette device, 120 smoking volunteers are extracted and divided into 12 groups of 10 people each, each group absorbs the same electronic atomized liquid, the smoking experience is scored, 4 evaluation indexes including aroma, harmony, irritation and aftertaste are set, the evaluation standards are shown in table 2, each smoker scores the sensory experience of smoking according to each evaluation index, the scoring result is collected, the average value is obtained, and the test result is shown in table 2.
TABLE 2
TABLE 3 Table 3
2. Fragrance durability evaluation, whether fragrance was felt after 1min, 2min, and 3min of suction, and evaluation results are shown in table 4.
TABLE 4 Table 4
As can be seen from the data in table 3, the electronic atomized liquid prepared from the plant essence of comparative example 1 without adding vetiver essential oil has significantly reduced fragrance and significantly increased irritation, and the electronic atomized liquid has no fragrance after the pumping time is prolonged to 2min in combination with table 4; the electronic atomized liquid prepared from the plant essence of the embodiment 6-12 added with the vetiver essential oil has rich fragrance, basically no stimulation, and has better fragrance along with the extension of the pumping time, and mainly benefits from the fact that the vetiver essential oil has excellent adsorption capacity, can slow down the volatilization of low-boiling plant extracts, enables the volatilization process to be uniform and slow, has longer lasting flavor without flushing nose, is aromatic and long-lasting, and simultaneously, the vetiver essential oil and different fragrance raw material components are synergistic, the original balance state is broken, and the volatilization characteristics of fragrance components are changed.
As can be seen from the data in table 3, the electronic atomized liquid prepared from the plant essence of comparative example 2 without the addition of texas cypress oil was not smooth and soft enough in harmony, and had a heavy aftertaste, which was uncomfortable; the electronic atomized liquid prepared by the plant essence of the embodiment 6-12 added with the Texas cypress wood oil has fine and soft suction feeling and pure aftertaste, so that people feel fresh and air, and the main adjustment of the essence is more prominent mainly by adding the Texas cypress wood oil, and other prominent perfume raw materials in the essence are coordinated, so that the original more stimulated perfume becomes soft, the perfume limit among the perfume raw materials is blurred, and the perfume of the essence is finer and softer.
Table 3 and Table 4 show that the plant essential oil extracted by the single extraction method of comparative examples 3-5 has various indexes reduced after being prepared into the electronic atomized liquid, and the plant essential oil obtained by matching different extraction methods has better sensory experience in the sucking process of the electronic atomized liquid according to plant characteristics, mainly characterized in that the fragrance substances in the plant raw materials can be fully extracted by adopting different extraction methods according to different plant essential oil characteristics, and the fragrance of the obtained essential oil is pure and durable and does not contain any chemical smell.
In view of the numerous embodiments of the present invention, the experimental data of each embodiment is huge and is not suitable for the one-by-one listing and explanation here, but the content of the verification needed by each embodiment and the obtained final conclusion are close. While the invention has been described in detail and with reference to specific embodiments thereof, it will be apparent to one skilled in the art that various changes and modifications can be made therein without departing from the spirit and scope thereof.
Claims (2)
1. A plant essence for an electronic atomized liquid, characterized in that the plant essence comprises the following raw material components:
peony petal essential oil 5-12 parts
2.5-4 parts of chamomile essential oil
0.8-3 parts of vetiver essential oil
0.5-2 parts of madder essential oil
8-15 parts of bergamot essential oil
0.2-1.5 parts of herba rosae rugosae essential oil
3-7 parts of geranium essential oil
1.5-3 parts of white orchid leaf essential oil
10-20 parts of ethanol; the plant essence also comprises 1-4 parts of Texas cypress oil;
the preparation method of the peony petal essential oil and the chamomile essential oil specifically comprises the following steps:
(1) Pulverizing plant materials to 30-45 mesh, adding 1-2 times of pure water into plant powder, and mixing;
(2) Placing the mixture in dry distillation equipment, and obtaining distillate gas by a temperature programming mode;
(3) Collecting distillate gas, and condensing at 3-10deg.C to obtain corresponding raw material essential oil;
the temperature programming is specifically that the temperature is firstly increased to 80-110 ℃ at 3-8 ℃/min, the temperature is kept for 1-2h, then the temperature is increased to 300-450 ℃ at the temperature increasing rate of 5-10 ℃/min, and the temperature is kept for 1-2h;
the preparation methods of the vetiver essential oil, the madder essential oil and the rose essential oil are subcritical extraction methods, and subcritical fluid is petroleum ether; the subcritical extraction conditions are as follows: the pressure is 4.5-5MPa, the temperature is 120-150 ℃, the time is 20-30min, and the flow is 1-3L/h;
the preparation method of the bergamot essential oil, the geranium essential oil and the brandy leaf essential oil comprises the following specific steps: pulverizing the raw materials into coarse powder, respectively, and soaking in 3-5 times of water for 3-5 hr; stirring, extracting by steam distillation for 2-4h, and collecting in an oil-water separator to obtain crude essential oil; centrifuging the crude essential oil at 3000r/min for 10min, and collecting supernatant to obtain the final product.
2. The method for preparing plant essence for electronic atomized liquid according to claim 1, characterized in that the preparation method comprises the following steps:
s1: weighing the raw materials according to claim 1 for later use;
s2: sequentially placing the weighed peony petal essential oil, chamomile essential oil, madder essential oil, bergamot essential oil, rose essential oil, geranium essential oil and brandy leaf essential oil into a stirring container, and stirring at normal temperature to fully and uniformly mix the raw materials;
s3: adding vetiver essential oil, texas cedar wood oil and ethanol, continuously stirring, and fully fusing to obtain the plant essence for the electronic atomization liquid.
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| JP6371927B1 (en) * | 2018-02-23 | 2018-08-08 | 株式会社 東亜産業 | Non-tobacco plant composition manufacturing method, electronic cigarette packing manufacturing method, electronic cigarette packing, and electronic cigarette cartridge using the same |
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| KR20120136269A (en) * | 2011-06-08 | 2012-12-18 | (주) 앤디 | Aroma essence using natural herbs and method of the same |
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