CN113801354A - 一种耐高温的透明玻璃纤维绝缘板及其制备方法 - Google Patents
一种耐高温的透明玻璃纤维绝缘板及其制备方法 Download PDFInfo
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- CN113801354A CN113801354A CN202111167608.XA CN202111167608A CN113801354A CN 113801354 A CN113801354 A CN 113801354A CN 202111167608 A CN202111167608 A CN 202111167608A CN 113801354 A CN113801354 A CN 113801354A
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- glass fiber
- flame
- stirring
- mixing
- fiber cloth
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- 239000003365 glass fiber Substances 0.000 title claims abstract description 71
- 238000002360 preparation method Methods 0.000 title claims abstract description 25
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 claims abstract description 80
- 239000003063 flame retardant Substances 0.000 claims abstract description 80
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- 229920005989 resin Polymers 0.000 claims abstract description 37
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- CMLFRMDBDNHMRA-UHFFFAOYSA-N 2h-1,2-benzoxazine Chemical compound C1=CC=C2C=CNOC2=C1 CMLFRMDBDNHMRA-UHFFFAOYSA-N 0.000 claims abstract description 36
- 239000000463 material Substances 0.000 claims abstract description 30
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- 238000013329 compounding Methods 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 11
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical compound C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims description 96
- 238000002156 mixing Methods 0.000 claims description 79
- 238000003756 stirring Methods 0.000 claims description 71
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 49
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- YLQBMQCUIZJEEH-UHFFFAOYSA-N tetrahydrofuran Natural products C=1C=COC=1 YLQBMQCUIZJEEH-UHFFFAOYSA-N 0.000 claims description 48
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- UBIJTWDKTYCPMQ-UHFFFAOYSA-N hexachlorophosphazene Chemical compound ClP1(Cl)=NP(Cl)(Cl)=NP(Cl)(Cl)=N1 UBIJTWDKTYCPMQ-UHFFFAOYSA-N 0.000 claims description 37
- ARXJGSRGQADJSQ-UHFFFAOYSA-N 1-methoxypropan-2-ol Chemical compound COCC(C)O ARXJGSRGQADJSQ-UHFFFAOYSA-N 0.000 claims description 36
- 238000001914 filtration Methods 0.000 claims description 36
- LVJZCPNIJXVIAT-UHFFFAOYSA-N 1-ethenyl-2,3,4,5,6-pentafluorobenzene Chemical compound FC1=C(F)C(F)=C(C=C)C(F)=C1F LVJZCPNIJXVIAT-UHFFFAOYSA-N 0.000 claims description 35
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- WYTZZXDRDKSJID-UHFFFAOYSA-N (3-aminopropyl)triethoxysilane Chemical compound CCO[Si](OCC)(OCC)CCCN WYTZZXDRDKSJID-UHFFFAOYSA-N 0.000 claims description 20
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- 229910000033 sodium borohydride Inorganic materials 0.000 claims description 16
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- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 11
- 238000004321 preservation Methods 0.000 claims description 11
- PKTOVQRKCNPVKY-UHFFFAOYSA-N dimethoxy(methyl)silicon Chemical compound CO[Si](C)OC PKTOVQRKCNPVKY-UHFFFAOYSA-N 0.000 claims description 10
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- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 description 1
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- YUWBVKYVJWNVLE-UHFFFAOYSA-N [N].[P] Chemical compound [N].[P] YUWBVKYVJWNVLE-UHFFFAOYSA-N 0.000 description 1
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- 229910052731 fluorine Inorganic materials 0.000 description 1
- 239000011737 fluorine Substances 0.000 description 1
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- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
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Classifications
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Abstract
Description
项目 | 实施例1 | 实施例2 | 实施例3 |
吸水率/% | 0.05 | 0.05 | 0.04 |
阻燃等级 | V-0 | V-0 | V-0 |
玻璃化转变温度℃ | 203 | 207 | 217 |
拉伸强度/MPa | 442 | 448 | 456 |
项目 | 实施例3 | 对比例1 | 对比例2 | 对比例3 | 对比例4 |
吸水率/% | 0.04 | 0.08 | 0.06 | 0.10 | 0.14 |
阻燃等级 | V-0 | V-1 | V-0 | V-1 | V-0 |
玻璃化转变温度℃ | 217 | 208 | 211 | 196 | 201 |
拉伸强度/MPa | 456 | 447 | 450 | 431 | 438 |
Claims (9)
Priority Applications (1)
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CN202111167608.XA CN113801354B (zh) | 2021-10-07 | 2021-10-07 | 一种耐高温的透明玻璃纤维绝缘板及其制备方法 |
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CN202111167608.XA CN113801354B (zh) | 2021-10-07 | 2021-10-07 | 一种耐高温的透明玻璃纤维绝缘板及其制备方法 |
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Publication Number | Publication Date |
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CN113801354A true CN113801354A (zh) | 2021-12-17 |
CN113801354B CN113801354B (zh) | 2022-07-08 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114702783A (zh) * | 2022-03-28 | 2022-07-05 | 惠州市纵胜电子材料有限公司 | 一种透明玻璃纤维手机盖板及其制备方法 |
CN115850912A (zh) * | 2022-12-02 | 2023-03-28 | 山东莱蔚特复合材料有限责任公司 | 一种板簧用玻璃纤维树脂复合材料的制备方法 |
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CN114702783A (zh) * | 2022-03-28 | 2022-07-05 | 惠州市纵胜电子材料有限公司 | 一种透明玻璃纤维手机盖板及其制备方法 |
CN114702783B (zh) * | 2022-03-28 | 2024-02-20 | 广东纵胜新材料股份有限公司 | 一种透明玻璃纤维手机盖板及其制备方法 |
CN115850912A (zh) * | 2022-12-02 | 2023-03-28 | 山东莱蔚特复合材料有限责任公司 | 一种板簧用玻璃纤维树脂复合材料的制备方法 |
CN115850912B (zh) * | 2022-12-02 | 2024-04-16 | 山东莱蔚特复合材料有限责任公司 | 一种板簧用玻璃纤维树脂复合材料的制备方法 |
CN116515276A (zh) * | 2023-05-05 | 2023-08-01 | 惠州市纵胜电子材料有限公司 | 一种基于玻纤聚氨酯复合材料的手机壳及其成型工艺 |
CN116515276B (zh) * | 2023-05-05 | 2024-02-20 | 广东纵胜新材料股份有限公司 | 一种基于玻纤聚氨酯复合材料的手机壳及其成型工艺 |
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