CN113549499A - Sapindus saponin laundry detergent and preparation method thereof - Google Patents
Sapindus saponin laundry detergent and preparation method thereof Download PDFInfo
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- CN113549499A CN113549499A CN202110707143.6A CN202110707143A CN113549499A CN 113549499 A CN113549499 A CN 113549499A CN 202110707143 A CN202110707143 A CN 202110707143A CN 113549499 A CN113549499 A CN 113549499A
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- 239000003599 detergent Substances 0.000 title claims abstract description 50
- 239000001397 quillaja saponaria molina bark Substances 0.000 title claims abstract description 48
- 229930182490 saponin Natural products 0.000 title claims abstract description 48
- 150000007949 saponins Chemical class 0.000 title claims abstract description 48
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 241000580938 Sapindus Species 0.000 title description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 57
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 38
- 241000694414 Sapindus saponaria Species 0.000 claims abstract description 34
- 235000018324 Shepherdia canadensis Nutrition 0.000 claims abstract description 34
- 238000003756 stirring Methods 0.000 claims abstract description 24
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 20
- 150000002191 fatty alcohols Chemical class 0.000 claims abstract description 19
- 239000004088 foaming agent Substances 0.000 claims abstract description 19
- 239000011780 sodium chloride Substances 0.000 claims abstract description 19
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims abstract description 18
- 241000580955 Sapindus mukorossi Species 0.000 claims abstract description 15
- UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 claims abstract description 10
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 229910000030 sodium bicarbonate Inorganic materials 0.000 claims abstract description 9
- 235000017557 sodium bicarbonate Nutrition 0.000 claims abstract description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000008367 deionised water Substances 0.000 claims abstract description 5
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 5
- 238000011049 filling Methods 0.000 claims abstract description 5
- 238000001914 filtration Methods 0.000 claims abstract description 5
- 239000011259 mixed solution Substances 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 6
- 229920001285 xanthan gum Polymers 0.000 claims description 6
- 239000000230 xanthan gum Substances 0.000 claims description 6
- 229940082509 xanthan gum Drugs 0.000 claims description 6
- 235000010493 xanthan gum Nutrition 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 4
- 238000005303 weighing Methods 0.000 claims description 4
- CHHHXKFHOYLYRE-UHFFFAOYSA-M 2,4-Hexadienoic acid, potassium salt (1:1), (2E,4E)- Chemical compound [K+].CC=CC=CC([O-])=O CHHHXKFHOYLYRE-UHFFFAOYSA-M 0.000 claims description 3
- 239000004302 potassium sorbate Substances 0.000 claims description 3
- 229940069338 potassium sorbate Drugs 0.000 claims description 3
- 235000010241 potassium sorbate Nutrition 0.000 claims description 3
- 241000282414 Homo sapiens Species 0.000 abstract description 5
- 239000006260 foam Substances 0.000 abstract description 5
- 238000003912 environmental pollution Methods 0.000 abstract description 4
- 239000010865 sewage Substances 0.000 abstract description 3
- 239000000463 material Substances 0.000 abstract 1
- 230000000052 comparative effect Effects 0.000 description 11
- 238000005202 decontamination Methods 0.000 description 11
- 230000003588 decontaminative effect Effects 0.000 description 11
- 230000000694 effects Effects 0.000 description 8
- 238000005406 washing Methods 0.000 description 8
- 230000003385 bacteriostatic effect Effects 0.000 description 6
- 238000005187 foaming Methods 0.000 description 5
- 239000000126 substance Substances 0.000 description 5
- 239000004094 surface-active agent Substances 0.000 description 5
- 230000006378 damage Effects 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 102000004169 proteins and genes Human genes 0.000 description 3
- 108090000623 proteins and genes Proteins 0.000 description 3
- 238000012360 testing method Methods 0.000 description 3
- 230000000844 anti-bacterial effect Effects 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000006229 carbon black Substances 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 210000002374 sebum Anatomy 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 244000230012 Gleditsia triacanthos Species 0.000 description 1
- 235000013813 Gleditsia triacanthos Nutrition 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000003945 anionic surfactant Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000000686 essence Substances 0.000 description 1
- 238000012851 eutrophication Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000010685 fatty oil Substances 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 229930182470 glycoside Natural products 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000002736 nonionic surfactant Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 229930004725 sesquiterpene Natural products 0.000 description 1
- -1 sesquiterpene glycoside Chemical class 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 231100000331 toxic Toxicity 0.000 description 1
- 230000002588 toxic effect Effects 0.000 description 1
- 229930182493 triterpene saponin Natural products 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/825—Mixtures of compounds all of which are non-ionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2006—Monohydric alcohols
- C11D3/201—Monohydric alcohols linear
- C11D3/2013—Monohydric alcohols linear fatty or with at least 8 carbon atoms in the alkyl chain
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2079—Monocarboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2075—Carboxylic acids-salts thereof
- C11D3/2086—Hydroxy carboxylic acids-salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/662—Carbohydrates or derivatives
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Inorganic Chemistry (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
Abstract
The application provides a soapnut saponin laundry detergent and a preparation method thereof, and raw materials for preparing the soapnut saponin laundry detergent comprise 2-9 parts of soapnut saponin, 25-35 parts of citric acid, 20-28 parts of sodium bicarbonate, 1-4 parts of a foaming agent, 8-14 parts of sodium chloride, 28-33 parts of fatty alcohol and 0.1-0.2 part of an auxiliary agent. Uniformly stirring the soapberry saponin, the citric acid, the foaming agent, the fatty alcohol and the deionized water, adding the baking soda, the sodium chloride and the auxiliary agent while stirring, stirring until the materials are uniformly mixed, standing for defoaming for 8 hours, filtering, detecting, and filling into bags to obtain the finished product. The soapberry saponin laundry detergent provided by the application has less foam, is fine and smooth, and has super strong oil stain removal capability; when in use, the detergent does not irritate the skin of a human body, and the washed sewage is easy to decompose and can not cause environmental pollution after being discharged.
Description
Technical Field
The application relates to the field of fine chemical engineering, in particular to a soapberry saponin laundry detergent and a preparation method thereof.
Background
With the improvement of the living standard of human beings and the continuous improvement of the safety consciousness of people on washing daily necessities, the selection principle of the surfactant gradually tends to consider how to exert the best main effect and auxiliary effect of the surfactant under the premise of firstly meeting the normal state of protecting skin and hair and generating as little toxic and side effect as possible on the human body. In recent years, ecological civilization construction is highly regarded by the nation, and in order to meet the pursuit of people for life styles such as health, green and low carbon, people return to nature, and the use of novel all-natural surfactant tends to be great. At present, a large number of various laundry products exist in the market, such as washing powder, laundry detergent, washing soap, washing balls and the like, but most of the laundry products need to be added with a large amount of anionic surfactants and the like, the surfactants have strong permeability and are easy to irritate the skin, and the sewage discharge after washing can cause environmental pollution.
Therefore, the skilled person in the art provides a soapberry saponin laundry detergent and a preparation method thereof to solve the problems set forth in the background art.
Disclosure of Invention
Aiming at the defects of the prior art, the application aims to provide the soapberry saponin laundry detergent and the preparation method thereof, the soapberry saponin laundry detergent is prepared by processing soapberry saponin, citric acid, baking soda, a foaming agent, sodium chloride, fatty alcohol, essence, xanthan gum, potassium sorbate and the like serving as raw materials, the irritation of the laundry detergent is reduced through reasonable proportion, the laundry detergent is mild and does not damage skin, and compared with the traditional laundry detergent, the soapberry saponin laundry detergent has stronger decontamination capability and antibacterial capability, and has the characteristics of easiness in decomposition and no environmental pollution.
The technical scheme adopted by the application is as follows:
a soapnut saponin laundry detergent is prepared from the following raw materials: 2-9 parts of soapnut saponin, 25-35 parts of citric acid, 20-28 parts of baking soda, 1-4 parts of foaming agent, 8-14 parts of sodium chloride, 28-33 parts of fatty alcohol and 0.1-0.2 part of auxiliary agent.
Further, the soapnut saponin laundry detergent is prepared from the following raw materials: 5 parts of soapnut saponin, 31 parts of citric acid, 25 parts of baking soda, 2 parts of a foaming agent, 10 parts of sodium chloride, 30 parts of fatty alcohol and 0.12 part of an auxiliary agent.
Further, the soapnut saponin laundry detergent is prepared from the following raw materials: 6 parts of soapberry saponin, 28 parts of citric acid, 23 parts of baking soda, 2.6 parts of a foaming agent, 12 parts of sodium chloride, 32 parts of fatty alcohol and 0.15 part of an auxiliary agent.
Further, the soapberry saponin laundry detergent comprises 1% -3% of essence, 80% -90% of xanthan gum and 6% -15% of potassium sorbate.
Further, a preparation method of the soapberry saponin laundry detergent comprises the following steps:
(1) weighing soapberry saponin, citric acid, sodium bicarbonate, a foaming agent, sodium chloride, fatty alcohol and an auxiliary agent for later use;
(2) putting the soapberry saponin, the citric acid, the foaming agent and the fatty alcohol into a stirring tank, adding 1-3L of deionized water, stirring at the stirring speed of 50-70 r/min, and stirring for 10-15 min to obtain a mixed solution;
(3) adding sodium bicarbonate, sodium chloride and an auxiliary agent into the mixed solution obtained in the step (2), stirring while adding, standing for defoaming for 8 hours after uniformly mixing, filtering, detecting, and filling into bags to obtain the finished product.
The beneficial effect of this application lies in:
sapindus saponin is a natural nonionic surfactant, and its main surface active components are triterpene saponin (I), sesquiterpene glycoside (II), fatty oil and protein, besides it also contains many substances beneficial to human body; the surfactant has the advantages of less foam, fineness, strong oil stain removing capability, and mild property without damaging skin. The soapberry saponin can be rapidly decomposed in a sewer, has no three-waste pollution in the production process and the subsequent sewage discharge process, is environment-friendly, and does not bring negative problems of a fluorescent agent, chemical surface activity, environmental pollution, river eutrophication and the like. The soapberry laundry detergent disclosed by the application also comprises auxiliary components besides the soapberry saponin, so that the production cost is greatly reduced and the characteristics of mildness and no damage to the skin are ensured through reasonable proportioning.
Detailed Description
The technical solutions in the embodiments of the present application will be clearly and completely described below with reference to the embodiments of the present application, and it is obvious that the described embodiments are only a part of the embodiments of the present application, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present application.
Example 1
A soapberry saponin laundry detergent is prepared from the following raw materials in parts by weight: 5 parts of soapnut saponin, 31 parts of citric acid, 25 parts of baking soda, 2 parts of a foaming agent, 10 parts of sodium chloride, 30 parts of fatty alcohol and 0.12 part of an auxiliary agent. The preparation method comprises the following steps:
(1) weighing soapberry saponin, citric acid, sodium bicarbonate, a foaming agent, sodium chloride, fatty alcohol and an auxiliary agent for later use;
(2) putting the soapberry saponin, the citric acid, the foaming agent and the fatty alcohol into a stirring tank, adding 1-3L of deionized water, stirring at the stirring speed of 50-70 r/min, and stirring for 10-15 min to obtain a mixed solution;
(3) adding sodium bicarbonate, sodium chloride and an auxiliary agent into the mixed solution obtained in the step (2), stirring while adding, standing for defoaming for 8 hours after uniformly mixing, filtering, detecting, and filling into bags to obtain the finished product.
Example 2
A soapberry saponin laundry detergent is prepared from the following raw materials in parts by weight: 6 parts of soapberry saponin, 28 parts of citric acid, 23 parts of baking soda, 2.6 parts of a foaming agent, 12 parts of sodium chloride, 32 parts of fatty alcohol and 0.15 part of an auxiliary agent. The preparation method comprises the following steps:
(1) weighing soapberry saponin, citric acid, sodium bicarbonate, a foaming agent, sodium chloride, fatty alcohol and an auxiliary agent for later use;
(2) putting the soapberry saponin, the citric acid, the foaming agent and the fatty alcohol into a stirring tank, adding 1-3L of deionized water, stirring at the stirring speed of 50-70 r/min, and stirring for 10-15 min to obtain a mixed solution;
(3) adding sodium bicarbonate, sodium chloride and an auxiliary agent into the mixed solution obtained in the step (2), stirring while adding, standing for defoaming for 8 hours after uniformly mixing, filtering, detecting, and filling into bags to obtain the finished product.
Example 3
1. Measurement of physical and chemical properties of laundry detergent
1.1, subject: examples 1-2 and comparative examples commercial laundry detergents: soapberry laundry detergent.
1.2, experimental method:
1.2.1 viscosity: measured at 25 ℃ with a spindle viscometer type NDJ-1.
1.2.2 pH: and (3) adding 10g of the laundry detergent into 50g of water at room temperature, uniformly stirring, and measuring by using an electronic pH meter.
1.2.3 foam Properties: the test was carried out according to the method specified in GB/T7462-1994 "determination of surfactant-foaming power-modified Ross-Miles method".
1.3, experimental results: see table 1:
TABLE 1 results of physical and chemical property test of laundry detergent
As can be seen from table 1, the viscosity of the xanthan gum in examples 1 to 2 is high because the addition amount of the xanthan gum is increased, the viscosity is remarkably increased compared with the comparative ratio, the flow is slow, the xanthan gum cannot be poured out too much during use, and waste is not easily caused; the laundry detergents of examples 1-2 and the comparative examples are weakly acidic, and have the characteristics of no harm to human bodies and no pollution to water sources.
As can be seen from Table 1, the laundry detergents in the embodiments 1-2 of the present application have good foaming effect and good foam stability; comparative example 1 was poor in foaming ability and foam stability, mainly because the comparative example was decocted with soapberry and honeylocust alone without adding auxiliary ingredients. Therefore, it is found that the higher the amount of soapberry used is, the higher the foaming performance is, and the more suitable auxiliary agents need to be selected and mixed in a specific ratio to exert the most excellent foaming performance.
2. Determination of detergency
Referring to a detergency determination method in QB/T1224-; wherein the washing method comprises the steps of soaking the dirty cloth in clear water for 3 minutes, rubbing and washing the dirty cloth for 1 minute, and washing the dirty cloth by direct current water. See table 2 for results.
TABLE 2 detergency test results
| Group of | Carbon black (decontamination ratio) | Protein (decontamination ratio) | Sebum (stain removal ratio) |
| Standard laundry detergent | 1.00 | 1.00 | 1.00 |
| Comparative example | 1.15 | 1.12 | 1.08 |
| Example 1 | 1.24 | 1.22 | 1.15 |
| Example 2 | 1.26 | 1.21 | 1.13 |
Note: the standard laundry detergent is prepared according to GB/T13174-; the decontamination ratio is less than 1, which indicates that the decontamination capability of the laundry detergent is less than that of the standard laundry detergent, and the decontamination ratio is greater than 1, which indicates that the decontamination capability of the measured laundry detergent is greater than that of the standard laundry detergent; the greater the stain removal ratio, the greater the stain removal capacity of the tested composition.
As can be seen from table 2, the decontamination ratios of the laundry detergents prepared in embodiments 1 to 2 of the present invention to carbon black, protein and sebum are all at a high level, and a good decontamination effect is achieved; the decontamination effect of the comparative example is higher than that of the standard laundry detergent, but the decontamination effect of the comparative example is obviously poorer than that of the laundry detergent prepared in the examples 1-2.
3. Laundry detergent antibacterial performance determination
The bacteriostatic effects of the laundry liquids of the examples 1-2 and the comparative example are determined by referring to the QB/T2850-2007 standard, and the determination results are shown in Table 3.
TABLE 3 laundry detergent bacteriostatic property determination results
As can be seen from Table 3, the bacteriostatic performance of the laundry detergents of the embodiments 1-2 of the invention is significantly higher than that of the comparative example, the bacteriostatic rate is between 97% and 99.9%, and the bacteriostatic rate of the comparative example is between 91% and 95%; the applicant believes that the main reason is that the best bacteriostatic performance can be achieved only by adopting the soapberry saponin and other substances for compatibility and matching in a specific ratio in the examples.
The above description is only for the purpose of illustrating the preferred embodiments of the present application and is not to be construed as limiting the present application, and all equivalent variations and modifications within the scope of the present application are intended to be covered by the present application. Furthermore, it should be understood that although the present description refers to embodiments, not every embodiment may contain only a single embodiment, and such description is for clarity only, and those skilled in the art should integrate the description, and the embodiments may be combined as appropriate to form other embodiments understood by those skilled in the art.
Claims (5)
1. A soapberry saponin laundry detergent is characterized in that: the raw materials for preparing the soapnut saponin laundry detergent comprise 2-9 parts of soapnut saponin, 25-35 parts of citric acid, 20-28 parts of sodium bicarbonate, 1-4 parts of foaming agent, 8-14 parts of sodium chloride, 28-33 parts of fatty alcohol and 0.1-0.2 part of auxiliary agent.
2. The soapberry saponin laundry detergent of claim 1, wherein: the raw materials for preparing the soapnut saponin laundry detergent comprise 5 parts of soapnut saponin, 31 parts of citric acid, 25 parts of baking soda, 2 parts of foaming agent, 10 parts of sodium chloride, 30 parts of fatty alcohol and 0.12 part of auxiliary agent.
3. The soapberry saponin laundry detergent of claim 1, wherein: the raw materials for preparing the soapnut saponin laundry detergent comprise 6 parts of soapnut saponin, 28 parts of citric acid, 23 parts of baking soda, 2.6 parts of foaming agent, 12 parts of sodium chloride, 32 parts of fatty alcohol and 0.15 part of auxiliary agent.
4. The soapberry saponin laundry detergent of claim 1, wherein: the auxiliary agent comprises 1-3% of essence, 80-90% of xanthan gum and 6-15% of potassium sorbate.
5. The preparation method of the soapberry saponin laundry detergent as claimed in claim 1, wherein the preparation method comprises the following steps: the method comprises the following steps:
(1) weighing soapberry saponin, citric acid, sodium bicarbonate, a foaming agent, sodium chloride, fatty alcohol and an auxiliary agent for later use;
(2) putting the soapberry saponin, the citric acid, the foaming agent and the fatty alcohol into a stirring tank, adding 1-3L of deionized water, stirring at the stirring speed of 50-70 r/min, and stirring for 10-15 min to obtain a mixed solution;
(3) adding sodium bicarbonate, sodium chloride and an auxiliary agent into the mixed solution obtained in the step (2), stirring while adding, standing for defoaming for 8 hours after uniformly mixing, filtering, detecting, and filling into bags to obtain the finished product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110707143.6A CN113549499A (en) | 2021-06-24 | 2021-06-24 | Sapindus saponin laundry detergent and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110707143.6A CN113549499A (en) | 2021-06-24 | 2021-06-24 | Sapindus saponin laundry detergent and preparation method thereof |
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| Publication Number | Publication Date |
|---|---|
| CN113549499A true CN113549499A (en) | 2021-10-26 |
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| CN202110707143.6A Pending CN113549499A (en) | 2021-06-24 | 2021-06-24 | Sapindus saponin laundry detergent and preparation method thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103468419A (en) * | 2013-09-29 | 2013-12-25 | 浙江海洋学院 | Natural and environment-friendly solid clothes-washing magic cube and preparation method thereof |
| CN105316119A (en) * | 2015-10-20 | 2016-02-10 | 成都市三禾田生物技术有限公司 | Sapindoside infant laundry detergent and preparation method thereof |
| CN110591834A (en) * | 2019-09-23 | 2019-12-20 | 贵州山水生物科技有限公司 | Laundry detergent containing okra extract and raspberry enzyme and preparation method of laundry detergent |
-
2021
- 2021-06-24 CN CN202110707143.6A patent/CN113549499A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103468419A (en) * | 2013-09-29 | 2013-12-25 | 浙江海洋学院 | Natural and environment-friendly solid clothes-washing magic cube and preparation method thereof |
| CN105316119A (en) * | 2015-10-20 | 2016-02-10 | 成都市三禾田生物技术有限公司 | Sapindoside infant laundry detergent and preparation method thereof |
| CN110591834A (en) * | 2019-09-23 | 2019-12-20 | 贵州山水生物科技有限公司 | Laundry detergent containing okra extract and raspberry enzyme and preparation method of laundry detergent |
Non-Patent Citations (1)
| Title |
|---|
| 豆子: "无患子百变用途", 《中国保健营养》 * |
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