CN113546594A - Solid-liquid ratio increasing reaction precipitation assembly for hydrothermal synthesis of special glass - Google Patents
Solid-liquid ratio increasing reaction precipitation assembly for hydrothermal synthesis of special glass Download PDFInfo
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- CN113546594A CN113546594A CN202110740327.2A CN202110740327A CN113546594A CN 113546594 A CN113546594 A CN 113546594A CN 202110740327 A CN202110740327 A CN 202110740327A CN 113546594 A CN113546594 A CN 113546594A
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B35/00—Boron; Compounds thereof
- C01B35/08—Compounds containing boron and nitrogen, phosphorus, oxygen, sulfur, selenium or tellurium
- C01B35/10—Compounds containing boron and oxygen
- C01B35/12—Borates
- C01B35/126—Borates of alkaline-earth metals, beryllium, aluminium or magnesium
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C1/00—Ingredients generally applicable to manufacture of glasses, glazes, or vitreous enamels
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Abstract
The invention relates to the technical field of special glass hydro-thermal synthesis, and discloses a solid-liquid ratio increasing reaction precipitation assembly for special glass hydro-thermal synthesis. This special glass hydrothermal synthesis is with increasing solid-to-liquid ratio reaction and is appeared subassembly, drive through external power source, and then make external power source drive the drive chain and rotate, thereby make the drive chain drive the promotion platform motion, and then make the promotion platform move under the cooperation of arc piece and bottom arc groove, thereby make the promotion platform drive swing piece and the motion of transmission dead slot, and then make the motion of transmission dead slot drive promotion stopper, thereby make the promotion stopper extrude interior soft piece motion, and then make the inside borate of interior soft piece transmitted the inside of mediation storehouse, and then make the hinge post under stirring, pushed the inside of appearing the storehouse, and then make high boron oxygen complex anion increase, thereby make special glass's quality improved.
Description
Technical Field
The invention relates to the technical field of special glass hydro-thermal synthesis, in particular to a solid-liquid ratio increasing reaction precipitation assembly for special glass hydro-thermal synthesis.
Background
In the development process of special glass in the current society, more and more special glass appears in the life and work of people, so in order to meet the increasing demand of the special glass, the hydro-thermal synthesis special glass is produced, the special glass is not only transparent and clean, but also has high strength and hardness, and is an indispensable material in daily production and life.
One of the main uses of the alkaline earth metal borate is as the important raw material of the alkali-free glass and ceramic industry, along with the development of special glass and ceramic, new requirements are provided for boron-containing materials, a magnesium borate raw material with special composition is needed, the special glass and ceramic have high limitation requirements for various impurities of the novel magnesium borate, the content of boron and magnesium is also in a special limited range, free magnesium oxide is not contained, and the synthesized magnesium borate is required to be crystalline hydrated magnesium borate, but the existing hydrothermal synthesis process equipment has the influence on the impurity content of the special glass by reaction time and batching solid-liquid ratio, wherein the higher the molar ratio of the raw material boron and magnesium is, the smaller the liquid-solid ratio is, high boron-oxygen complex anions are favorably formed, a magnesium borate product with high boron content is obtained, and simultaneously when the reaction temperature is lower and the reaction time is shorter, because the magnesium oxide and the boric acid are incompletely reacted, free magnesium oxide exists in the product, so that the special glass contains impurities.
Aiming at the problems, the invention provides a solid-liquid ratio increasing reaction precipitation component for hydrothermal synthesis of special glass, which has the advantages of accurate reaction time and small burdening solid-liquid ratio.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides the solid-liquid ratio increasing reaction precipitation component for the hydrothermal synthesis of the special glass, which has the advantages of accurate reaction time and small burdening solid-liquid ratio and solves the problems of inaccurate reaction time and large burdening solid-liquid ratio.
(II) technical scheme
In order to solve the technical problems, the invention provides the following technical scheme:
the utility model provides a special glass hydrothermal synthesis is with increasing solid-to-liquid ratio reaction and appearing subassembly, is including appearing reaction mechanism, the top swing joint who appears in the middle of the reaction mechanism has the top capping piece, and the bottom swing joint of top capping piece has the rotation groove, and the bottom of rotating the groove is rotated and is connected with the rotation post, and the outside swing joint who rotates the post has the harmonic plate, and the inside of harmonic plate evenly is equipped with the whirl mouth, and the bottom swing joint of whirl mouth has the lagging.
Preferably, the outer side swing joint of lagging has the screw thread post, and the upper and lower both sides of screw thread post all are equipped with presss from both sides the recess, and the outer side swing joint who presss from both sides the recess has the connecting plate, and the outer end swing joint of connecting plate has the flexible piece.
Preferably, the outer end of flexible piece is equipped with hollow post, and the outside fixedly connected with dysmorphism piece of hollow post, the bottom swing joint in dysmorphism piece outside has movable bottom plate, and movable bottom plate's the outside is equipped with the spring, and the figure of spring is less than movable bottom plate.
Preferably, the upper side and the lower side of the spring are movably connected with clamping plates, the outer sides of the clamping plates are provided with blending bins, the inner sides of the blending bins are movably connected with hinged columns, and the upper side and the lower side of each hinged column are movably connected with transmission mechanisms.
Preferably, the outer end of the transmission mechanism is movably connected with an inner soft block, the outer side of the inner soft block is movably connected with a pushing plug, the outer end of the pushing plug is movably connected with a limiting hook frame, and the middle part of the outer side of the limiting hook frame is movably connected with a transmission empty groove, so that the limiting hook frame is convenient to limit the pushing plug.
Preferably, the inner side of the transmission empty groove is movably connected with a swinging block, the top of the swinging block is movably connected with a reinforced connecting column, and the top of the reinforced connecting column is movably connected with a pushing table.
Preferably, the bottom ends of the upper side and the lower side of the pushing platform are movably connected with arc blocks, the outer sides of the arc blocks are movably connected with bottom arc grooves, and the outer ends of the pushing platform are movably connected with character folding rods.
(III) advantageous effects
Compared with the prior art, the invention provides a solid-liquid ratio increasing reaction precipitation component for hydrothermal synthesis of special glass, which has the following beneficial effects:
1. this special glass hydrothermal synthesis is with increasing solid-to-liquid ratio reaction and is appeared subassembly, drive through external power source, and then make external power source drive the drive chain and rotate, thereby make the drive chain drive the promotion platform motion, and then make the promotion platform move under the cooperation of arc piece and bottom arc groove, thereby make the promotion platform drive swing piece and the motion of transmission dead slot, and then make the motion of transmission dead slot drive promotion stopper, thereby make the promotion stopper extrude interior soft piece motion, and then make the inside borate of interior soft piece transmitted the inside of mediation storehouse, and then make the hinge post under stirring, pushed the inside of appearing the storehouse, and then make high boron oxygen complex anion increase, thereby make special glass's quality improved.
2. This special glass hydrothermal synthesis is with increasing solid-to-liquid ratio reaction and is appeared subassembly, through boron and the inside of installing the reaction mechanism that appears additional with magnesium that needs to handle, and then make the external power source drive the rotation post and rotate, and then make the rotation post drive the mediation board and rotate, and then when making the mediation board rotate, can be under the effect of whirl mouth, make the inside of appearing the reaction storehouse produce trickle, and then under the transmission of lagging, make the screw thread post rotate, and then make the screw thread post rotate the outside and move, thereby make the telescopic block drive the hollow post and move to the outside, and then make the spring in the hollow post outside when rotating, produce and rotate elasticity, and then make the inside boron of appearing the storehouse, the magnesium fully reacts, and then reduce boron and magnesium reaction time inadequately, the impurity that does not fully produce.
Drawings
FIG. 1 is a schematic view showing the connection of the precipitation reaction mechanism of the present invention.
Fig. 2 is an enlarged view of a mark a in fig. 1.
Fig. 3 is an enlarged view of the mark B in fig. 1.
Fig. 4 is an enlarged view of the C mark in fig. 1.
In the figure: 1. a precipitation reaction mechanism; 2. a top cover block; 3. a rotating groove; 4. rotating the column; 5. a harmonic plate; 6. a swirl port; 7. sheathing; 8. a threaded post; 9. clamping a groove; 10. a connecting plate; 11. a telescopic block; 12. a hollow column; 13. a shaped block; 14. a movable bottom plate; 15. a spring; 16. a splint; 17. a blending bin; 18. hinging the column; 19. a transmission mechanism; 20. an inner soft block; 21. pushing the plug; 22. a limit hook frame; 23. a transmission empty slot; 24. a swing block; 25. reinforcing the connecting column; 26. a pushing table; 27. an arc block; 28. a bottom arc groove; 29. folding the character rod; 30. a drive chain.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-4, a solid-liquid ratio increasing reaction precipitation assembly for hydrothermal synthesis of special glass comprises a precipitation reaction mechanism 1, wherein the top of the middle of the precipitation reaction mechanism 1 is movably connected with a top cover block 2, the bottom of the top cover block 2 is movably connected with a rotating groove 3, the bottom of the rotating groove 3 is rotatably connected with a rotating column 4, the outer side of the rotating column 4 is movably connected with a mixing plate 5, swirl ports 6 are uniformly arranged in the mixing plate 5, and the bottom of the swirl ports 6 is movably connected with a sleeve plate 7.
Wherein, the outside swing joint of lagging 7 has screw thread post 8, and the upper and lower both sides of screw thread post 8 all are equipped with and press from both sides recess 9, and the outside swing joint that presss from both sides recess 9 has connecting plate 10, and the outer end swing joint of connecting plate 10 has flexible piece 11 to be convenient for screw thread post 8 presss from both sides the internal motion of recess 9 from top to bottom.
The outer end of the telescopic block 11 is provided with a hollow column 12, the outer side of the hollow column 12 is fixedly connected with a special-shaped block 13, the bottom end of the outer side of the special-shaped block 13 is movably connected with a movable bottom plate 14, the outer side of the movable bottom plate 14 is provided with springs 15, and the number of the springs 15 is less than that of the movable bottom plate 14.
Wherein, the upper and lower both sides of spring 15 are connected with splint 16 movably, and the outside of splint 16 is equipped with mediation storehouse 17, and the inboard swing joint of mediation storehouse 17 has hinge post 18, and the upper and lower both sides of hinge post 18 all swing joint have drive mechanism 19, and hinge post 18 stirs and produces the trickle.
The outer end of the transmission mechanism 19 is movably connected with an inner soft block 20, the outer side of the inner soft block 20 is movably connected with a pushing plug 21, the outer end of the pushing plug 21 is movably connected with a limiting hook frame 22, and the middle part of the outer side of the limiting hook frame 22 is movably connected with a transmission empty groove 23, so that the limiting hook frame 22 is convenient to limit the pushing plug 21.
Wherein, the inner side of the transmission empty groove 23 is movably connected with a swinging block 24, the top of the swinging block 24 is movably connected with a reinforced connecting column 25, and the top of the reinforced connecting column 25 is movably connected with a pushing platform 26.
The bottom ends of the upper side and the lower side of the pushing platform 26 are movably connected with arc blocks 27, the outer sides of the arc blocks 27 are movably connected with bottom arc grooves 28, the outer end of the pushing platform 26 is movably connected with a character folding rod 29, and the top of the character folding rod 29 is movably connected with a transmission chain 30.
When the device is used, firstly, boron and magnesium to be treated are additionally arranged inside the precipitation reaction mechanism 1, then an external power source drives the rotating column 4 to rotate, then the rotating column 4 drives the mixing plate 5 to rotate, and further when the mixing plate 5 rotates, the interior of the precipitation reaction bin produces trickle under the action of the cyclone port 6, further under the transmission of the sleeve plate 7, the threaded column 8 rotates, further the threaded column 8 rotates to move outwards, further the telescopic block 11 drives the hollow column 12 to move outwards, further the spring 15 outside the hollow column 12 produces rotating elastic force when rotating, further the boron and the magnesium inside the precipitation bin fully react, and further the defects of insufficient reaction time and insufficient production of the boron and the magnesium are reduced.
Through the drive of external power supply, and then make external power supply drive chain 30 rotate, thereby make drive chain 30 drive and promote the platform 26 motion, and then make and promote platform 26 and move under the cooperation of arc piece 27 and bottom arc groove 28, thereby make and promote platform 26 drive swing piece 24 and drive dead slot 23 motion, and then make drive dead slot 23 drive and promote stopper 21 motion, thereby make and promote stopper 21 extrusion inner soft piece 20 motion, and then make the inside borate of inner soft piece 20 transmitted to the inside of mediation storehouse 17, and then make hinge post 18 under stirring, pushed the inside of appearing the storehouse, and then make the high boron oxygen anion that matches increase, thereby make special glass's quality improved.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. The utility model provides a special glass hydrothermal synthesis is with increasing solid-to-liquid ratio reaction and educing subassembly, includes to educe reaction mechanism (1), its characterized in that: the top swing joint in the middle of the precipitation reaction mechanism (1) is provided with a top cover block (2), the bottom swing joint of the top cover block (2) is provided with a rotating groove (3), the bottom of the rotating groove (3) is connected with a rotating column (4), the outer side of the rotating column (4) is movably connected with a mixing plate (5), the inside of the mixing plate (5) is uniformly provided with a rotational flow port (6), and the bottom of the rotational flow port (6) is movably connected with a sleeve plate (7).
2. The solid-to-liquid ratio increasing reaction precipitation assembly for special glass hydrothermal synthesis according to claim 1, wherein: the outer side of the sleeve plate (7) is movably connected with a threaded column (8), the upper side and the lower side of the threaded column (8) are both provided with clamping grooves (9), the outer side of each clamping groove (9) is movably connected with a connecting plate (10), and the outer end of each connecting plate (10) is movably connected with a telescopic block (11).
3. The solid-to-liquid ratio increasing reaction precipitation assembly for special glass hydrothermal synthesis according to claim 2, wherein: the outer end of flexible piece (11) is equipped with hollow column (12), the outside fixedly connected with dysmorphism piece (13) of hollow column (12), the bottom swing joint in dysmorphism piece (13) outside has movable bottom plate (14), and the outside of movable bottom plate (14) is equipped with spring (15).
4. The solid-to-liquid ratio increasing reaction precipitation assembly for special glass hydrothermal synthesis according to claim 3, wherein: the upper side and the lower side of the spring (15) are movably connected with clamping plates (16), the outer side of each clamping plate (16) is provided with a blending bin (17), the inner side of each blending bin (17) is movably connected with a hinged column (18), and the upper side and the lower side of each hinged column (18) are both movably connected with a transmission mechanism (19).
5. The solid-to-liquid ratio increasing reaction precipitation assembly for special glass hydrothermal synthesis according to claim 4, wherein: the outer end of the transmission mechanism (19) is movably connected with an inner soft block (20), the outer side of the inner soft block (20) is movably connected with a pushing plug (21), the outer end of the pushing plug (21) is movably connected with a limiting hook frame (22), and the middle part of the outer side of the limiting hook frame (22) is movably connected with a transmission empty groove (23).
6. The solid-to-liquid ratio increasing reaction precipitation assembly for special glass hydrothermal synthesis according to claim 5, wherein: the inner side of the transmission empty groove (23) is movably connected with a swinging block (24), the top of the swinging block (24) is movably connected with a reinforced connecting column (25), and the top of the reinforced connecting column (25) is movably connected with a pushing platform (26).
7. The solid-to-liquid ratio increasing reaction precipitation assembly for special glass hydrothermal synthesis according to claim 6, wherein: the bottom ends of the upper side and the lower side of the pushing platform (26) are movably connected with arc blocks (27), the outer side of each arc block (27) is movably connected with a bottom arc groove (28), and the outer end of the pushing platform (26) is movably connected with a folding rod (29).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110740327.2A CN113546594B (en) | 2021-07-01 | 2021-07-01 | Special glass hydrothermal synthesis is with increasing solid-to-liquid ratio reaction and separating subassembly |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110740327.2A CN113546594B (en) | 2021-07-01 | 2021-07-01 | Special glass hydrothermal synthesis is with increasing solid-to-liquid ratio reaction and separating subassembly |
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| Publication Number | Publication Date |
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| CN113546594A true CN113546594A (en) | 2021-10-26 |
| CN113546594B CN113546594B (en) | 2023-08-04 |
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2021
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| CN109012412A (en) * | 2018-08-21 | 2018-12-18 | 伍超群 | A kind of adjustable medicinal liquid medicament mixing apparatus of stirring range |
| CN110052236A (en) * | 2019-05-15 | 2019-07-26 | 林枫 | A kind of resins synthesis reaction kettle |
| US20200108419A1 (en) * | 2019-08-27 | 2020-04-09 | Caiqiao Chen | Maintenance device for Huanghuali bracelets |
| CN112279341A (en) * | 2020-11-27 | 2021-01-29 | 曹高永 | Marine increase air exchange subassembly of pollution treatment based on hydrochloric acid mediation |
| CN112890633A (en) * | 2021-01-13 | 2021-06-04 | 路文娟 | Broken wall machine food processing is with avoiding high rotational speed low moment of torsion subassembly |
| CN112808127A (en) * | 2021-01-25 | 2021-05-18 | 云和县新华涂料厂 | Water-soluble resin mixing ratio increasing assembly for water-based paint production |
| CN112876301A (en) * | 2021-01-27 | 2021-06-01 | 广州于达生物科技有限公司 | High-density quick-decomposing assembly for fermentation processing of biological fertilizer |
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