CN113234361B - Pigment paste for ink-jet printing and preparation method thereof - Google Patents
Pigment paste for ink-jet printing and preparation method thereof Download PDFInfo
- Publication number
- CN113234361B CN113234361B CN202110536480.3A CN202110536480A CN113234361B CN 113234361 B CN113234361 B CN 113234361B CN 202110536480 A CN202110536480 A CN 202110536480A CN 113234361 B CN113234361 B CN 113234361B
- Authority
- CN
- China
- Prior art keywords
- parts
- carbon black
- weight
- pigment
- inkjet printing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/001—Pigment pastes, e.g. for mixing in paints in aqueous medium
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/004—Pigment pastes, e.g. for mixing in paints containing an inorganic pigment
- C09D17/005—Carbon black
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/004—Pigment pastes, e.g. for mixing in paints containing an inorganic pigment
- C09D17/007—Metal oxide
- C09D17/008—Titanium dioxide
Abstract
The invention discloses pigment paste for inkjet printing and a preparation method thereof, wherein the pigment paste is prepared from the following raw materials in parts by weight: 30-45 parts of modified carbon black, 8-15 parts of dispersing agent, 1-3 parts of metal chloride, 0.8-1.5 parts of anti-settling agent, 0.5-1.2 parts of defoaming agent and 35-50 parts of deionized water. The pigment paste for ink-jet printing has good stability and weather resistance; the modified carbon black is obtained by modifying the carbon black, the dispersibility, the stability and the light stability of the modified carbon black are obviously improved, the carbon black and the titanium dioxide are compounded, the light resistance of the titanium dioxide can be improved between gaps between the carbon black, the reflectivity of the titanium dioxide after film formation can be improved, the silica-containing alumina sol is prepared by pseudo-boehmite and silicon dioxide, and the silica-containing alumina sol is dripped into a suspension to obtain the modified carbon black with a coating, so that the light stability, the wettability and the stability are further improved.
Description
Technical Field
The invention relates to the technical field of pigment color paste, in particular to pigment color paste for inkjet printing and a preparation method thereof.
Background
Digital printing is a technology that after the digital ink is subjected to the acting force applied by a digital printing machine, one drop of ink is directly sprayed onto textiles through a printing nozzle to form a required pattern. The pigment ink digital printing has the advantages of wide applicability, simple pretreatment and post-treatment processes, energy conservation, no sewage discharge and the like, and is the development direction of digital printing ink.
The preparation process of the ink comprises the steps of firstly grinding pigment, dispersing agent, surfactant and deionized water into pigment color paste, and then adding other auxiliary agents to prepare the pigment ink. The pigment paste for preparing pigment ink at present has the defect of stability.
Disclosure of Invention
The invention provides a pigment paste for ink-jet printing and a preparation method thereof.
The invention solves the technical problems by adopting the following technical scheme:
a pigment paste for ink-jet printing is prepared from the following raw materials in parts by weight: 30-45 parts of modified carbon black, 8-15 parts of dispersing agent, 1-3 parts of metal chloride, 0.8-1.5 parts of anti-settling agent, 0.5-1.2 parts of defoaming agent and 35-50 parts of deionized water.
As a preferable scheme, the pigment paste for ink-jet printing is prepared from the following raw materials in parts by weight: 40 parts of modified carbon black, 12 parts of dispersing agent, 2.5 parts of metal chloride, 1 part of anti-settling agent, 0.9 part of defoaming agent and 43.6 parts of deionized water.
As a preferred scheme, the preparation method of the modified carbon black comprises the following steps:
s1, carbon black and titanium dioxide are mixed according to the weight ratio of 1: adding 0.01-0.03 into a ball milling tank, and uniformly ball milling to obtain pigment powder;
s2, adding 6-10 parts by weight of pigment powder into 20-40 parts by weight of deionized water, adding 0.8-1.5 parts by weight of monoethanolamine, and uniformly stirring to obtain a suspension;
s3, adding 0.4-1 part by weight of pseudo-boehmite and 0.2-0.8 part by weight of silicon dioxide into 10-20 parts by weight of deionized water, uniformly dispersing, dripping 0.5-1 part by weight of hydrochloric acid solution, and carrying out ultrasonic treatment for 20-50 min to obtain a mixed solution;
s4, heating the suspension to 60-85 ℃, dripping the mixed liquid into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
and S5, calcining the mixed powder for 1-5 hours at 750-850 ℃, cooling, and grinding until D95 is less than 0.2 mu m, thus obtaining the modified carbon black.
According to the invention, the modified carbon black is obtained by modifying the carbon black, the dispersibility, the stability and the light stability (weather resistance) of the modified carbon black are obviously improved, the carbon black and the titanium dioxide are compounded, the titanium dioxide can be filled between gaps among the carbon black, the light resistance is improved, meanwhile, the reflectivity of the titanium dioxide after film formation is also improved, the silica-containing alumina sol is prepared by pseudo-boehmite and silicon dioxide, and is dripped into a suspension liquid, so that the modified carbon black with a coating is obtained, the light stability, the wettability and the stability are further improved, and the carbon black and the titanium dioxide are not agglomerated, so that flocculation and agglomeration phenomena in storage are not caused.
As a preferable scheme, the ball milling speed in the step S1 is 100-200 rpm, and the ball milling time is 1.5-3 h.
As a preferable scheme, the ultrasonic treatment power in the step S3 is 200-600W.
As a preferable scheme, the metal chloride is prepared from magnesium chloride and zinc chloride according to the weight ratio of 1: 0.5-2.
Under the formula system, the metal chloride composed of magnesium chloride and zinc chloride can reduce the Zeta potential on the surface of the modified carbon black, reduce electrostatic repulsive force among particles, reduce steric hindrance, prevent the modified carbon black from settling and improve the stability.
Meanwhile, the inventor finds that magnesium chloride and zinc chloride have better effects than other metal chlorides, and if the addition amount of the metal chloride is too large (more than the upper limit value 3), the electrostatic repulsive force and the steric hindrance of the modified carbon black are too small, and the stability is deteriorated instead.
As a preferred scheme, the dispersant is BYK-190 dispersant.
As a preferable scheme, the anti-settling agent is bentonite.
As a preferred scheme, the defoaming agent is a defoaming agent BYK-024.
The invention also provides a preparation method of the pigment paste for ink-jet printing, which comprises the following steps:
s11, adding deionized water, a dispersing agent and an anti-settling agent into a mixer, and stirring at a rotation speed of 500-800 rpm for 15-30 min to obtain a premix;
s12, adding the modified carbon black and the metal chloride into the premix, and stirring at 400-700 rpm for 15-30 min to obtain a pigment premix;
s13, adding a defoaming agent, stirring for 8-20 min at a rotation speed of 200-500 rpm, and grinding until D95 is less than 0.2 mu m to obtain the pigment color paste for inkjet printing.
The invention has the beneficial effects that: the pigment paste for ink-jet printing has good stability and weather resistance; the modified carbon black is obtained by modifying the carbon black, the dispersibility, the stability and the light stability (weather resistance) of the modified carbon black are obviously improved, the carbon black and the titanium dioxide are compounded, the titanium dioxide can be filled between gaps of the carbon black, the light resistance is improved, meanwhile, the titanium dioxide can also improve the reflectivity after film formation, silica-containing alumina sol is prepared by pseudo-boehmite and silica, and is dripped into suspension, so that the modified carbon black with the coating is obtained, the light stability, the wettability and the stability are further improved, and the carbon black and the titanium dioxide are not agglomerated, so that flocculation and caking phenomena can not occur in storage.
Detailed Description
For the purpose of making the objects, technical solutions and advantages of the embodiments of the present invention more apparent, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is apparent that the described embodiments are some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
In the present invention, the parts are parts by weight unless specifically stated otherwise.
Example 1
The pigment color paste for ink-jet printing is prepared from the following raw materials in parts by weight: 40 parts of modified carbon black, 12 parts of dispersing agent, 2.5 parts of metal chloride, 1 part of anti-settling agent, 0.9 part of defoaming agent and 43.6 parts of deionized water.
The preparation method of the modified carbon black comprises the following steps:
s1, carbon black and titanium dioxide are mixed according to the weight ratio of 1:0.02 is added into a ball milling tank, ball milling is carried out for 2 hours at a rotating speed of 150, and pigment powder is obtained;
s2, adding 9 parts by weight of pigment powder into 29.8 parts by weight of deionized water, adding 1.2 parts by weight of monoethanolamine, and uniformly stirring to obtain a suspension;
s3, adding 0.8 part by weight of pseudo-boehmite and 0.5 part by weight of silicon dioxide into 12 parts by weight of deionized water, uniformly dispersing, dripping 0.8 part by weight of 2mol/L hydrochloric acid solution, and performing 400W ultrasonic treatment for 30min to obtain a mixed solution;
s4, heating the suspension to 70 ℃, dripping the mixed liquid into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s5, calcining the mixed powder for 2 hours at the temperature of 820 ℃, cooling, and grinding until D95 is less than 0.2 mu m, thus obtaining the modified carbon black.
The metal chloride is prepared from magnesium chloride and zinc chloride according to the weight ratio of 1: 1.
The dispersing agent is BYK-190 dispersing agent.
The anti-settling agent is bentonite.
The defoaming agent is a defoaming agent BYK-024.
The preparation method of the pigment paste for ink-jet printing comprises the following steps:
s11, adding deionized water, a dispersing agent and an anti-settling agent into a mixer, and stirring at 700rpm for 25min to obtain a premix;
s12, adding the modified carbon black and the metal chloride into the premix, and stirring for 20min at a rotation speed of 500rpm to obtain pigment premix;
s13, adding a defoaming agent, stirring for 15min at 400rpm, and grinding until D95 is less than 0.2 mu m to obtain the pigment color paste for inkjet printing.
Example 2
The pigment color paste for ink-jet printing is prepared from the following raw materials in parts by weight: 30 parts of modified carbon black, 8 parts of dispersing agent, 1.5 parts of metal chloride, 0.8 part of anti-settling agent, 0.5 part of defoaming agent and 35 parts of deionized water.
The preparation method of the modified carbon black comprises the following steps:
s1, carbon black and titanium dioxide are mixed according to the weight ratio of 1:0.02 is added into a ball milling tank, ball milling is carried out for 2 hours at a rotating speed of 150, and pigment powder is obtained;
s2, adding 9 parts by weight of pigment powder into 29.8 parts by weight of deionized water, adding 1.2 parts by weight of monoethanolamine, and uniformly stirring to obtain a suspension;
s3, adding 0.8 part by weight of pseudo-boehmite and 0.5 part by weight of silicon dioxide into 12 parts by weight of deionized water, uniformly dispersing, dripping 0.8 part by weight of 2mol/L hydrochloric acid solution, and performing 400W ultrasonic treatment for 30min to obtain a mixed solution;
s4, heating the suspension to 70 ℃, dripping the mixed liquid into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s5, calcining the mixed powder for 2 hours at the temperature of 820 ℃, cooling, and grinding until D95 is less than 0.2 mu m, thus obtaining the modified carbon black.
The metal chloride is prepared from magnesium chloride and zinc chloride according to the weight ratio of 1: 1.
The dispersing agent is BYK-190 dispersing agent.
The anti-settling agent is bentonite.
The defoaming agent is a defoaming agent BYK-024.
The preparation method of the pigment paste for ink-jet printing comprises the following steps:
s11, adding deionized water, a dispersing agent and an anti-settling agent into a mixer, and stirring at 700rpm for 25min to obtain a premix;
s12, adding the modified carbon black and the metal chloride into the premix, and stirring for 20min at a rotation speed of 500rpm to obtain pigment premix;
s13, adding a defoaming agent, stirring for 15min at 400rpm, and grinding until D95 is less than 0.2 mu m to obtain the pigment color paste for inkjet printing.
Example 3
The pigment color paste for ink-jet printing is prepared from the following raw materials in parts by weight: 40 parts of modified carbon black, 15 parts of dispersing agent, 2 parts of metal chloride, 1.5 parts of anti-settling agent, 1.2 parts of defoaming agent and 50 parts of deionized water.
The preparation method of the modified carbon black comprises the following steps:
s1, carbon black and titanium dioxide are mixed according to the weight ratio of 1:0.02 is added into a ball milling tank, ball milling is carried out for 2 hours at a rotating speed of 150, and pigment powder is obtained;
s2, adding 9 parts by weight of pigment powder into 29.8 parts by weight of deionized water, adding 1.2 parts by weight of monoethanolamine, and uniformly stirring to obtain a suspension;
s3, adding 0.8 part by weight of pseudo-boehmite and 0.5 part by weight of silicon dioxide into 12 parts by weight of deionized water, uniformly dispersing, dripping 0.8 part by weight of 2mol/L hydrochloric acid solution, and performing 400W ultrasonic treatment for 30min to obtain a mixed solution;
s4, heating the suspension to 70 ℃, dripping the mixed liquid into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s5, calcining the mixed powder for 2 hours at the temperature of 820 ℃, cooling, and grinding until D95 is less than 0.2 mu m, thus obtaining the modified carbon black.
The metal chloride is prepared from magnesium chloride and zinc chloride according to the weight ratio of 1: 1.
The dispersing agent is BYK-190 dispersing agent.
The anti-settling agent is bentonite.
The defoaming agent is a defoaming agent BYK-024.
The preparation method of the pigment paste for ink-jet printing comprises the following steps:
s11, adding deionized water, a dispersing agent and an anti-settling agent into a mixer, and stirring at 700rpm for 25min to obtain a premix;
s12, adding the modified carbon black and the metal chloride into the premix, and stirring for 20min at a rotation speed of 500rpm to obtain pigment premix;
s13, adding a defoaming agent, stirring for 15min at 400rpm, and grinding until D95 is less than 0.2 mu m to obtain the pigment color paste for inkjet printing.
Comparative example 1
Comparative example 1 differs from example 1 in that comparative example 1 uses carbon black instead of modified carbon black, all of which are identical.
Comparative example 2
Comparative example 2 differs from example 1 in that the modified carbon black described in comparative example 2 was prepared by a method different from example 1 in that carbon black and titanium pigment were not mixed in this comparative example, and the other were the same.
The preparation method of the modified carbon black comprises the following steps:
s1, adding 9 parts by weight of carbon black into 29.8 parts by weight of deionized water, adding 1.2 parts by weight of monoethanolamine, and uniformly stirring to obtain a suspension;
s2, adding 0.8 part by weight of pseudo-boehmite and 0.5 part by weight of silicon dioxide into 12 parts by weight of deionized water, uniformly dispersing, dripping 0.8 part by weight of 2mol/L hydrochloric acid solution, and performing 400W ultrasonic treatment for 30min to obtain a mixed solution;
s3, heating the suspension to 70 ℃, dripping the mixed liquid into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s4, calcining the mixed powder for 2 hours at the temperature of 820 ℃, cooling, and grinding until D95 is less than 0.2 mu m, thus obtaining the modified carbon black.
Comparative example 3
Comparative example 3 is different from example 1 in that the modified carbon black described in comparative example 3 is produced by a method different from example 1 in that in this comparative example, an aluminum sol is used instead of the mixed solution, and all others are the same.
The preparation method of the modified carbon black comprises the following steps:
s1, carbon black and titanium dioxide are mixed according to the weight ratio of 1:0.02 is added into a ball milling tank, ball milling is carried out for 2 hours at a rotating speed of 150, and pigment powder is obtained;
s2, adding 9 parts by weight of pigment powder into 29.8 parts by weight of deionized water, adding 1.2 parts by weight of monoethanolamine, and uniformly stirring to obtain a suspension;
s3, heating the suspension to 70 ℃, dripping 13.1 parts by weight of aluminum sol into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s4, calcining the mixed powder for 2 hours at the temperature of 820 ℃, cooling, and grinding until D95 is less than 0.2 mu m, thus obtaining the modified carbon black.
The aluminum sol of this comparative example was purchased from Shandong Lier New Material Co., ltd.
Comparative example 4
Comparative example 4 is different from example 1 in that the pigment paste raw material ratio for inkjet printing described in comparative example 4 is different from example 1, and the other are the same.
The pigment color paste for ink-jet printing is prepared from the following raw materials in parts by weight: 40 parts of modified carbon black, 12 parts of dispersing agent, 4 parts of metal chloride, 1 part of anti-settling agent, 0.9 part of defoaming agent and 43.6 parts of deionized water.
Comparative example 5
Comparative example 5 differs from example 1 in that the composition of the metal chloride described in comparative example 5 is different from example 1, and the other are the same.
The metal chloride is prepared from aluminum chloride and ferric chloride according to the weight ratio of 1: 1.
To further demonstrate the effect of the present invention, the following test methods were provided:
1. stability test: the pigment paste for inkjet printing prepared in examples 1 to 3 and comparative examples 1 to 5 was left at 25 ℃ for 180 days, and the stability of the pigment paste was judged by visually observing whether or not the apparent pigment particle precipitation, flocculation, delamination, and caking stability occurred.
2. The weatherability of the pigment color paste for ink-jet printing is tested by adopting a QUV (ultraviolet lamp) manual accelerated aging method, and the color difference (delta E) before and after accelerated aging irradiation is measured by an X-rite portable spectrocolorimeter, and the QUV (ultraviolet lamp) is accelerated aged for 1000 hours.
Table 1 test results
As can be seen from Table 1, the pigment paste for inkjet printing according to the present invention has good stability and weather resistance.
Comparative examples 1 to 3 show that different raw material ratios for inkjet printing pigment paste can affect stability and weather resistance in a certain range.
Comparative example 1 and comparative example 1 show that the present invention significantly improves the stability and weather resistance by modifying the carbon black.
As is clear from comparative examples 1 and 2, the carbon black and titanium pigment were mixed and modified to improve stability and weather resistance.
As is clear from comparative examples 1 and 3, the mixed solution according to the present invention can improve stability and weather resistance more than the aluminum sol.
As is clear from comparative examples 1 and 4, when the amount of the metal chloride added is too large, caking phenomenon occurs to affect stability and weather resistance.
Comparative examples 1 and 5 show that the stability and weather resistance of the metal chloride of example 1 of the present invention are reduced if other substances are substituted.
With the above-described preferred embodiments according to the present invention as an illustration, the above-described descriptions can be used by persons skilled in the relevant art to make various changes and modifications without departing from the scope of the technical idea of the present invention. The technical scope of the present invention is not limited to the description, but must be determined according to the scope of the claims.
Claims (8)
1. The pigment color paste for ink-jet printing is characterized by being prepared from the following raw materials in parts by weight: 30-45 parts of modified carbon black, 8-15 parts of dispersing agent, 1-3 parts of metal chloride, 0.8-1.5 parts of anti-settling agent, 0.5-1.2 parts of defoaming agent and 35-50 parts of deionized water;
the preparation method of the modified carbon black comprises the following steps:
s1, carbon black and titanium dioxide are mixed according to the weight ratio of 1: adding 0.01-0.03 into a ball milling tank, and uniformly ball milling to obtain pigment powder;
s2, adding 6-10 parts by weight of pigment powder into 20-40 parts by weight of deionized water, adding 0.8-1.5 parts by weight of monoethanolamine, and uniformly stirring to obtain a suspension;
s3, adding 0.4-1 part by weight of pseudo-boehmite and 0.2-0.8 part by weight of silicon dioxide into 10-20 parts by weight of deionized water, uniformly dispersing, dripping 0.5-1 part by weight of hydrochloric acid solution, and carrying out ultrasonic treatment for 20-50 min to obtain a mixed solution;
s4, heating the suspension to 60-85 ℃, dripping the mixed liquid into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s5, calcining the mixed powder for 1-5 hours at 750-850 ℃, cooling, and grinding until D95 is less than 0.2 mu m to obtain modified carbon black;
the metal chloride is prepared from magnesium chloride and zinc chloride according to the weight ratio of 1: 0.5-2.
2. Pigment paste for inkjet printing according to claim 1, characterized in that the pigment paste for inkjet printing is made of the following raw materials in parts by weight: 40 parts of modified carbon black, 12 parts of dispersing agent, 2.5 parts of metal chloride, 1 part of anti-settling agent, 0.9 part of defoaming agent and 43.6 parts of deionized water.
3. The pigment paste for inkjet printing according to claim 1, wherein the ball milling rate in the step S1 is 100-200 rpm, and the ball milling time is 1.5-3 hours.
4. The pigment paste for inkjet printing according to claim 1, wherein the ultrasonic treatment power in the step S3 is 200 to 600w.
5. Pigment paste for inkjet printing according to claim 1, characterized in that the dispersant is a BYK-190 dispersant.
6. Pigment paste for inkjet printing according to claim 1, wherein the anti-settling agent is bentonite.
7. Pigment paste for inkjet printing according to claim 1, characterized in that the defoamer is defoamer BYK-024.
8. A method for preparing pigment paste for inkjet printing, which is characterized by preparing the pigment paste for inkjet printing according to any one of claims 1 to 7, comprising the following steps:
s11, adding deionized water, a dispersing agent and an anti-settling agent into a mixer, and stirring at a rotation speed of 500-800 rpm for 15-30 min to obtain a premix;
s12, adding the modified carbon black and the metal chloride into the premix, and stirring at 400-700 rpm for 15-30 min to obtain a pigment premix;
s13, adding a defoaming agent, stirring for 8-20 min at a rotation speed of 200-500 rpm, and grinding until D95 is less than 0.2 mu m to obtain the pigment color paste for inkjet printing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110536480.3A CN113234361B (en) | 2021-05-17 | 2021-05-17 | Pigment paste for ink-jet printing and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110536480.3A CN113234361B (en) | 2021-05-17 | 2021-05-17 | Pigment paste for ink-jet printing and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN113234361A CN113234361A (en) | 2021-08-10 |
| CN113234361B true CN113234361B (en) | 2023-05-02 |
Family
ID=77134788
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202110536480.3A Active CN113234361B (en) | 2021-05-17 | 2021-05-17 | Pigment paste for ink-jet printing and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN113234361B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115748001B (en) * | 2022-10-25 | 2023-12-22 | 桐乡市励志特种纤维股份有限公司 | Stock solution coloring regenerated environment-friendly antibacterial polyester special-shaped filament yarn and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB674832A (en) * | 1944-05-08 | 1952-07-02 | Goodrich Co B F | Improvements in and relating to surface active agents and in pigment compositions and pigmented rubber compositions prepared therewith |
| DE19929845A1 (en) * | 1999-06-29 | 2001-01-11 | Degussa | Surface-modified pyrogenic titanium dioxide, used in cosmetics e.g. sun-protection agents, is treated with ammonium-functional silane |
| CN105482659A (en) * | 2015-12-17 | 2016-04-13 | 芜湖市宝艺游乐科技设备有限公司 | Wear-resistant and fire-resistant polyester powder coating and preparing method thereof |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL182737C (en) * | 1979-12-29 | 1988-05-02 | Kansai Paint Co Ltd | PIGMENT DISPERSION, CONTAINING A PIGMENT, A DISPENSANT AND AN ORGANIC DISPENSING MEDIUM. |
| JP3654413B2 (en) * | 1997-10-31 | 2005-06-02 | 戸田工業株式会社 | Iron-based black composite particle powder and method for producing the same, paint using the iron-based black composite particle powder, and rubber / resin composition colored with the iron-based black composite particle powder |
| JP4407789B2 (en) * | 2002-03-04 | 2010-02-03 | 戸田工業株式会社 | Modified carbon black particle powder and method for producing the same, paint and resin composition containing the modified carbon black particle powder |
| CN104004416A (en) * | 2014-06-04 | 2014-08-27 | 福建省华普新材料有限公司 | Water-based colour paste for printing ink |
| CN104212286B (en) * | 2014-08-26 | 2017-02-01 | 中国建筑股份有限公司 | Gray solar reflective cooling coating and preparation method thereof |
| CN108084796A (en) * | 2017-12-15 | 2018-05-29 | 佛山市扬子颜料有限公司 | A kind of new package carbon black ceramics marking ink and preparation method thereof |
-
2021
- 2021-05-17 CN CN202110536480.3A patent/CN113234361B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB674832A (en) * | 1944-05-08 | 1952-07-02 | Goodrich Co B F | Improvements in and relating to surface active agents and in pigment compositions and pigmented rubber compositions prepared therewith |
| DE19929845A1 (en) * | 1999-06-29 | 2001-01-11 | Degussa | Surface-modified pyrogenic titanium dioxide, used in cosmetics e.g. sun-protection agents, is treated with ammonium-functional silane |
| CN105482659A (en) * | 2015-12-17 | 2016-04-13 | 芜湖市宝艺游乐科技设备有限公司 | Wear-resistant and fire-resistant polyester powder coating and preparing method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN113234361A (en) | 2021-08-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP4027938B2 (en) | Aluminum pigment, method for producing the same, and resin composition | |
| JP3948934B2 (en) | Aluminum pigment, method for producing the same, and resin composition | |
| CN111440496B (en) | Water-based UV silver powder coating and preparation method and application thereof | |
| CN113234361B (en) | Pigment paste for ink-jet printing and preparation method thereof | |
| EP2847283B1 (en) | Paint dispersion | |
| WO2018180936A1 (en) | Coated pigment | |
| WO2021237404A1 (en) | Aqueous epoxy anticorrosive coating and preparation method therefor | |
| EP1349809B1 (en) | Method of preparing a fumed metal oxide dispersion | |
| CN114213916B (en) | Water-based non-shading plain color finish paint for automobile and preparation method thereof | |
| CN104974661B (en) | Polyethersulfone ultra-fine micropowder, its purposes and the coating containing polyethersulfone ultra-fine micropowder and their preparation method | |
| CN101845254A (en) | Elastic aqueous fluorocarbon paint for external walls | |
| KR20160060913A (en) | Method for controlling aggregation of sol-gel nanoparticles by solvent relative permittivity, and fabrication of superhydrophobic surfaces using thereof | |
| CN112812634A (en) | Water-based vacuum cup baking paint and preparation method thereof | |
| CN107286802A (en) | Refitted car ultrafast dry one-component priming paint and preparation method | |
| CN110894385A (en) | Single-component aqueous environment-friendly industrial crack paint and preparation method thereof | |
| CN115521673A (en) | Environment-friendly exterior wall texture coating not prone to blooming during spraying and preparation method thereof | |
| CN110452568B (en) | Anticorrosive paint, preparation method thereof and anticorrosive coating | |
| JP6830526B2 (en) | A method for producing the pigment having improved alkali resistance by encapsulating the bismuth pigment with an ion blocking agent. | |
| CN108299932B (en) | Preparation method of modified carbon black slurry for black matte water-based metal anticorrosive paint | |
| CN115818740B (en) | Synthetic method of ruthenium dioxide nano powder | |
| CN116478582B (en) | Waterborne thermosetting ether FEVE fluorine coating, preparation method and aluminum metal substrate | |
| CN110452609A (en) | Coating and preparation method are applied in the low VOCs discharge of rail traffic | |
| CN115322633B (en) | Single-component blue-phase ultra-black automobile coating and preparation method thereof | |
| CN110003743A (en) | A kind of water-based stoving paint and its preparation process | |
| CN116478568B (en) | Amphiphilic nano silicon dioxide filler for improving water resistance of water-based paint and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |