CN113234361A - Pigment paste for ink-jet printing and preparation method thereof - Google Patents
Pigment paste for ink-jet printing and preparation method thereof Download PDFInfo
- Publication number
- CN113234361A CN113234361A CN202110536480.3A CN202110536480A CN113234361A CN 113234361 A CN113234361 A CN 113234361A CN 202110536480 A CN202110536480 A CN 202110536480A CN 113234361 A CN113234361 A CN 113234361A
- Authority
- CN
- China
- Prior art keywords
- parts
- carbon black
- weight
- pigment paste
- pigment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/001—Pigment pastes, e.g. for mixing in paints in aqueous medium
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/004—Pigment pastes, e.g. for mixing in paints containing an inorganic pigment
- C09D17/005—Carbon black
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/004—Pigment pastes, e.g. for mixing in paints containing an inorganic pigment
- C09D17/007—Metal oxide
- C09D17/008—Titanium dioxide
Abstract
The invention discloses a pigment color paste for ink-jet printing and a preparation method thereof, wherein the pigment color paste is prepared from the following raw materials in parts by weight: 30-45 parts of modified carbon black, 8-15 parts of dispersing agent, 1-3 parts of metal chloride, 0.8-1.5 parts of anti-settling agent, 0.5-1.2 parts of defoaming agent and 35-50 parts of deionized water. The pigment color paste for ink-jet printing has good stability and weather resistance; the modified carbon black is obtained by modifying the carbon black, the dispersibility, the stability and the light stability of the modified carbon black are obviously improved, the carbon black and the titanium dioxide are compounded, the titanium dioxide can be arranged between the carbon black and the light resistance is improved, the reflectivity of the titanium dioxide after film forming can be improved, the silicon-containing alumina sol is prepared by pseudo-boehmite and silicon dioxide, the silica-containing alumina sol is dripped into the suspension to obtain the modified carbon black with the envelope, and the light stability, the wettability and the stability are further improved.
Description
Technical Field
The invention relates to the technical field of pigment color paste, in particular to pigment color paste for ink-jet printing and a preparation method thereof.
Background
Digital printing is a technology in which digital ink is directly ejected through a printing nozzle to a textile to form a required pattern after being subjected to a force applied by a digital printing machine. The pigment ink digital printing has the advantages of wide applicability, simple pretreatment and post-treatment processes, energy conservation, no sewage discharge and the like, and is the development direction of the digital printing ink.
The preparation process of the ink comprises the steps of firstly grinding the pigment, the dispersing agent, the surfactant and the deionized water into pigment color paste, and then adding other auxiliary agents to prepare the pigment ink. The pigment color paste for preparing the pigment ink at present has the defect of stability.
Disclosure of Invention
The invention provides a pigment color paste for ink-jet printing and a preparation method thereof.
The invention adopts the following technical scheme for solving the technical problems:
a pigment paste for ink-jet printing is prepared from the following raw materials in parts by weight: 30-45 parts of modified carbon black, 8-15 parts of dispersing agent, 1-3 parts of metal chloride, 0.8-1.5 parts of anti-settling agent, 0.5-1.2 parts of defoaming agent and 35-50 parts of deionized water.
As a preferable scheme, the pigment paste for ink-jet printing is prepared from the following raw materials in parts by weight: 40 parts of modified carbon black, 12 parts of dispersing agent, 2.5 parts of metal chloride, 1 part of anti-settling agent, 0.9 part of defoaming agent and 43.6 parts of deionized water.
As a preferable scheme, the preparation method of the modified carbon black comprises the following steps:
s1, mixing carbon black and titanium dioxide according to the weight ratio of 1: 0.01-0.03, adding the mixture into a ball milling tank, and performing ball milling uniformly to obtain pigment powder;
s2, adding 6-10 parts by weight of pigment powder into 20-40 parts by weight of deionized water, adding 0.8-1.5 parts by weight of ammonium monoethanol, and uniformly stirring to obtain a suspension;
s3, adding 0.4-1 part by weight of pseudo-boehmite and 0.2-0.8 part by weight of silicon dioxide into 10-20 parts by weight of deionized water, uniformly dispersing, dripping 0.5-1 part by weight of hydrochloric acid solution, and performing ultrasonic treatment for 20-50 min to obtain a mixed solution;
s4, heating the suspension to 60-85 ℃, dripping the mixed solution into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s5, calcining the mixed powder at 750-850 ℃ for 1-5 h, cooling, and grinding until D95 is less than 0.2 mu m to obtain the modified carbon black.
The modified carbon black is obtained by modifying the carbon black, the dispersibility, the stability and the light stability (weather resistance) of the modified carbon black are obviously improved, the carbon black and the titanium dioxide are compounded, the titanium dioxide can be filled in gaps among the carbon black, the light resistance is improved, meanwhile, the reflectivity after film forming can be improved, the silicon-containing alumina sol is prepared by the pseudo-boehmite and the silicon dioxide and is dripped into the suspension to obtain the modified carbon black with the coating, the light stability, the wettability and the stability are further improved, and the carbon black and the titanium dioxide cannot be agglomerated, so that the flocculation and agglomeration phenomena in storage cannot be caused.
Preferably, the ball milling speed in the step S1 is 100 to 200rpm, and the ball milling time is 1.5 to 3 hours.
As a preferable scheme, the ultrasonic treatment power of the step S3 is 200-600W.
As a preferable scheme, the metal chloride is prepared from magnesium chloride and zinc chloride according to the weight ratio of 1: 0.5 to 2.
Under the formula system of the invention, the metal chloride composed of magnesium chloride and zinc chloride can reduce the Zeta potential on the surface of the modified carbon black, reduce the electrostatic repulsion among particles, reduce the steric hindrance, prevent the modified carbon black from settling and improve the stability.
Meanwhile, the inventors found that magnesium chloride and zinc chloride have better effects than other metal chlorides, and if the addition amount of the metal chloride is too large (greater than the upper limit value of 3), the electrostatic repulsion force and steric hindrance of the modified carbon black are too small, and the stability is rather deteriorated.
As a preferable scheme, the dispersant is a BYK-190 dispersant.
Preferably, the anti-settling agent is bentonite.
As a preferred scheme, the defoaming agent is a defoaming agent BYK-024.
The invention also provides a preparation method of the pigment paste for ink-jet printing, which comprises the following steps:
s11, adding deionized water, a dispersing agent and an anti-settling agent into a mixer, and stirring at the rotating speed of 500-800 rpm for 15-30 min to obtain a premixed solution;
s12, adding the modified carbon black and the metal chloride into the premixed liquid, and stirring at the rotating speed of 400-700 rpm for 15-30 min to obtain a pigment premixed liquid;
and S13, adding a defoaming agent, stirring at the rotating speed of 200-500 rpm for 8-20 min, and grinding until the D95 is less than 0.2 mu m to obtain the pigment paste for ink-jet printing.
The invention has the beneficial effects that: the pigment color paste for ink-jet printing has good stability and weather resistance; the modified carbon black is obtained by modifying the carbon black, the dispersibility, the stability and the light stability (weather resistance) of the modified carbon black are obviously improved, the carbon black and the titanium dioxide are compounded, the titanium dioxide can be filled in gaps among the carbon black, the light resistance is improved, meanwhile, the reflectivity after film forming can be improved, the silicon-containing alumina sol is prepared by the pseudo-boehmite and the silicon dioxide and is dripped into the suspension to obtain the modified carbon black with the coating, the light stability, the wettability and the stability are further improved, and the carbon black and the titanium dioxide cannot be agglomerated, so that the flocculation and agglomeration phenomena cannot be caused in storage.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below, and it is obvious that the described embodiments are a part of the embodiments of the present invention, but not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the present invention, the parts are all parts by weight unless otherwise specified.
Example 1
The pigment paste for the ink-jet printing is prepared from the following raw materials in parts by weight: 40 parts of modified carbon black, 12 parts of dispersing agent, 2.5 parts of metal chloride, 1 part of anti-settling agent, 0.9 part of defoaming agent and 43.6 parts of deionized water.
The preparation method of the modified carbon black comprises the following steps:
s1, mixing carbon black and titanium dioxide according to the weight ratio of 1: 0.02, adding the mixture into a ball milling tank, and carrying out ball milling for 2 hours at the rotating speed of 150 to obtain pigment powder;
s2, adding 9 parts by weight of pigment powder into 29.8 parts by weight of deionized water, adding 1.2 parts by weight of ammonium monoethanol, and uniformly stirring to obtain a suspension;
s3, adding 0.8 weight part of pseudo-boehmite and 0.5 weight part of silicon dioxide into 12 weight parts of deionized water, uniformly dispersing, dripping 0.8 weight part of 2mol/L hydrochloric acid solution, and performing 400W ultrasonic treatment for 30min to obtain a mixed solution;
s4, heating the suspension to 70 ℃, dripping the mixed solution into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s5, calcining the mixed powder at 820 ℃ for 2h, cooling, and grinding until D95 is less than 0.2 mu m to obtain the modified carbon black.
The metal chloride is prepared from magnesium chloride and zinc chloride according to a weight ratio of 1: 1.
The dispersant is BYK-190 dispersant.
The anti-settling agent is bentonite.
The defoaming agent is a defoaming agent BYK-024.
The preparation method of the pigment paste for ink-jet printing comprises the following steps:
s11, adding deionized water, a dispersing agent and an anti-settling agent into a mixer, and stirring at 700rpm for 25min to obtain a premixed solution;
s12, adding the modified carbon black and the metal chloride into the premix, and stirring at the rotating speed of 500rpm for 20min to obtain a pigment premix;
and S13, adding a defoaming agent, stirring at the rotating speed of 400rpm for 15min, and grinding until the D95 is less than 0.2 mu m to obtain the pigment paste for ink-jet printing.
Example 2
The pigment paste for the ink-jet printing is prepared from the following raw materials in parts by weight: 30 parts of modified carbon black, 8 parts of dispersing agent, 1.5 parts of metal chloride, 0.8 part of anti-settling agent, 0.5 part of defoaming agent and 35 parts of deionized water.
The preparation method of the modified carbon black comprises the following steps:
s1, mixing carbon black and titanium dioxide according to the weight ratio of 1: 0.02, adding the mixture into a ball milling tank, and carrying out ball milling for 2 hours at the rotating speed of 150 to obtain pigment powder;
s2, adding 9 parts by weight of pigment powder into 29.8 parts by weight of deionized water, adding 1.2 parts by weight of ammonium monoethanol, and uniformly stirring to obtain a suspension;
s3, adding 0.8 weight part of pseudo-boehmite and 0.5 weight part of silicon dioxide into 12 weight parts of deionized water, uniformly dispersing, dripping 0.8 weight part of 2mol/L hydrochloric acid solution, and performing 400W ultrasonic treatment for 30min to obtain a mixed solution;
s4, heating the suspension to 70 ℃, dripping the mixed solution into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s5, calcining the mixed powder at 820 ℃ for 2h, cooling, and grinding until D95 is less than 0.2 mu m to obtain the modified carbon black.
The metal chloride is prepared from magnesium chloride and zinc chloride according to a weight ratio of 1: 1.
The dispersant is BYK-190 dispersant.
The anti-settling agent is bentonite.
The defoaming agent is a defoaming agent BYK-024.
The preparation method of the pigment paste for ink-jet printing comprises the following steps:
s11, adding deionized water, a dispersing agent and an anti-settling agent into a mixer, and stirring at 700rpm for 25min to obtain a premixed solution;
s12, adding the modified carbon black and the metal chloride into the premix, and stirring at the rotating speed of 500rpm for 20min to obtain a pigment premix;
and S13, adding a defoaming agent, stirring at the rotating speed of 400rpm for 15min, and grinding until the D95 is less than 0.2 mu m to obtain the pigment paste for ink-jet printing.
Example 3
The pigment paste for the ink-jet printing is prepared from the following raw materials in parts by weight: 40 parts of modified carbon black, 15 parts of dispersing agent, 2 parts of metal chloride, 1.5 parts of anti-settling agent, 1.2 parts of defoaming agent and 50 parts of deionized water.
The preparation method of the modified carbon black comprises the following steps:
s1, mixing carbon black and titanium dioxide according to the weight ratio of 1: 0.02, adding the mixture into a ball milling tank, and carrying out ball milling for 2 hours at the rotating speed of 150 to obtain pigment powder;
s2, adding 9 parts by weight of pigment powder into 29.8 parts by weight of deionized water, adding 1.2 parts by weight of ammonium monoethanol, and uniformly stirring to obtain a suspension;
s3, adding 0.8 weight part of pseudo-boehmite and 0.5 weight part of silicon dioxide into 12 weight parts of deionized water, uniformly dispersing, dripping 0.8 weight part of 2mol/L hydrochloric acid solution, and performing 400W ultrasonic treatment for 30min to obtain a mixed solution;
s4, heating the suspension to 70 ℃, dripping the mixed solution into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s5, calcining the mixed powder at 820 ℃ for 2h, cooling, and grinding until D95 is less than 0.2 mu m to obtain the modified carbon black.
The metal chloride is prepared from magnesium chloride and zinc chloride according to a weight ratio of 1: 1.
The dispersant is BYK-190 dispersant.
The anti-settling agent is bentonite.
The defoaming agent is a defoaming agent BYK-024.
The preparation method of the pigment paste for ink-jet printing comprises the following steps:
s11, adding deionized water, a dispersing agent and an anti-settling agent into a mixer, and stirring at 700rpm for 25min to obtain a premixed solution;
s12, adding the modified carbon black and the metal chloride into the premix, and stirring at the rotating speed of 500rpm for 20min to obtain a pigment premix;
and S13, adding a defoaming agent, stirring at the rotating speed of 400rpm for 15min, and grinding until the D95 is less than 0.2 mu m to obtain the pigment paste for ink-jet printing.
Comparative example 1
Comparative example 1 differs from example 1 in that comparative example 1 uses carbon black instead of modified carbon black, and the other things are the same.
Comparative example 2
Comparative example 2 differs from example 1 in that the modified carbon black described in comparative example 2 was prepared by a method different from that of example 1, and in this comparative example, carbon black and titanium dioxide were not mixed, but the other examples were the same.
The preparation method of the modified carbon black comprises the following steps:
s1, adding 9 parts by weight of carbon black into 29.8 parts by weight of deionized water, adding 1.2 parts by weight of ammonium monoethanol, and uniformly stirring to obtain a suspension;
s2, adding 0.8 weight part of pseudo-boehmite and 0.5 weight part of silicon dioxide into 12 weight parts of deionized water, uniformly dispersing, dripping 0.8 weight part of 2mol/L hydrochloric acid solution, and performing 400W ultrasonic treatment for 30min to obtain a mixed solution;
s3, heating the suspension to 70 ℃, dripping the mixed solution into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s4, calcining the mixed powder at 820 ℃ for 2h, cooling, and grinding until D95 is less than 0.2 mu m to obtain the modified carbon black.
Comparative example 3
Comparative example 3 is different from example 1 in that the modified carbon black described in comparative example 3 is prepared by a method different from example 1, and in this comparative example, aluminum sol is used instead of the mixed solution, and the other is the same.
The preparation method of the modified carbon black comprises the following steps:
s1, mixing carbon black and titanium dioxide according to the weight ratio of 1: 0.02, adding the mixture into a ball milling tank, and carrying out ball milling for 2 hours at the rotating speed of 150 to obtain pigment powder;
s2, adding 9 parts by weight of pigment powder into 29.8 parts by weight of deionized water, adding 1.2 parts by weight of ammonium monoethanol, and uniformly stirring to obtain a suspension;
s3, heating the suspension to 70 ℃, dripping 13.1 parts by weight of alumina sol into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s4, calcining the mixed powder at 820 ℃ for 2h, cooling, and grinding until D95 is less than 0.2 mu m to obtain the modified carbon black.
The alumina sol of this comparative example was purchased from new materials ltd, ritol, mountains.
Comparative example 4
Comparative example 4 is different from example 1 in that the pigment paste raw material ratio for ink-jet printing described in comparative example 4 is different from that of example 1, and the rest is the same.
The pigment paste for the ink-jet printing is prepared from the following raw materials in parts by weight: 40 parts of modified carbon black, 12 parts of dispersing agent, 4 parts of metal chloride, 1 part of anti-settling agent, 0.9 part of defoaming agent and 43.6 parts of deionized water.
Comparative example 5
Comparative example 5 differs from example 1 in that the composition of the metal chloride described in comparative example 5 differs from example 1, all else being the same.
The metal chloride is prepared from aluminum chloride and ferric chloride according to a weight ratio of 1: 1.
To further demonstrate the effect of the present invention, the following test methods were provided:
1. and (3) stability testing: the pigment paste for ink-jet printing prepared in examples 1 to 3 and comparative examples 1 to 5 was left at 25 ℃ for 180 days, and the stability of the pigment paste was judged by visually observing the presence or absence of significant precipitation, flocculation, delamination and caking stability of the pigment particles.
2. The weather resistance of the prepared pigment color paste for ink-jet printing is tested by adopting a QUV (ultraviolet lamp) artificial accelerated aging method, the color difference (delta E) before and after accelerated aging irradiation is measured by an X-rite portable spectrocolorimeter, and the QUV (ultraviolet lamp) accelerated aging is 1000 h.
TABLE 1 test results
As can be seen from Table 1, the pigment pastes for ink-jet printing according to the present invention have good stability and weatherability.
As can be seen from comparison of examples 1-3, the stability and weather resistance can be affected within a certain range by the raw material ratio of different pigment pastes for ink-jet printing.
Comparing example 1 with comparative example 1, it can be seen that the stability and weather resistance are significantly improved by modifying carbon black according to the present invention.
As can be seen from the comparison of example 1 and comparative example 2, the stability and weather resistance can be improved by mixing carbon black and titanium dioxide and then performing modification treatment.
It is understood from comparative example 1 and comparative example 3 that the stability and weather resistance can be improved more by using the mixed solution of the present invention than by using an aluminum sol.
It is understood from comparative example 1 and comparative example 4 that if the amount of the metal chloride added is too large, the blocking phenomenon occurs, which affects the stability and weather resistance.
It can be seen from the comparison between example 1 and comparative example 5 that the metal chloride of example 1 of the present invention is deteriorated in stability and weather resistance if replaced with other materials.
In light of the foregoing description of preferred embodiments according to the invention, it is clear that many changes and modifications can be made by the person skilled in the art without departing from the scope of the invention. The technical scope of the present invention is not limited to the contents of the specification, and must be determined according to the scope of the claims.
Claims (10)
1. The pigment paste for ink-jet printing is characterized by being prepared from the following raw materials in parts by weight: 30-45 parts of modified carbon black, 8-15 parts of dispersing agent, 1-3 parts of metal chloride, 0.8-1.5 parts of anti-settling agent, 0.5-1.2 parts of defoaming agent and 35-50 parts of deionized water.
2. The pigment paste for inkjet printing according to claim 1, wherein the pigment paste for inkjet printing is prepared from the following raw materials in parts by weight: 40 parts of modified carbon black, 12 parts of dispersing agent, 2.5 parts of metal chloride, 1 part of anti-settling agent, 0.9 part of defoaming agent and 43.6 parts of deionized water.
3. The pigment paste for inkjet printing according to claim 1, wherein the modified carbon black is prepared by the following steps:
s1, mixing carbon black and titanium dioxide according to the weight ratio of 1: 0.01-0.03, adding the mixture into a ball milling tank, and performing ball milling uniformly to obtain pigment powder;
s2, adding 6-10 parts by weight of pigment powder into 20-40 parts by weight of deionized water, adding 0.8-1.5 parts by weight of ammonium monoethanol, and uniformly stirring to obtain a suspension;
s3, adding 0.4-1 part by weight of pseudo-boehmite and 0.2-0.8 part by weight of silicon dioxide into 10-20 parts by weight of deionized water, uniformly dispersing, dripping 0.5-1 part by weight of hydrochloric acid solution, and performing ultrasonic treatment for 20-50 min to obtain a mixed solution;
s4, heating the suspension to 60-85 ℃, dripping the mixed solution into the suspension, uniformly stirring, filtering and drying to obtain mixed powder;
s5, calcining the mixed powder at 750-850 ℃ for 1-5 h, cooling, and grinding until D95 is less than 0.2 mu m to obtain the modified carbon black.
4. The pigment paste for inkjet printing according to claim 3, wherein the ball milling speed in the step S1 is 100-200 rpm, and the ball milling time is 1.5-3 h.
5. The pigment paste for inkjet printing according to claim 3, wherein the ultrasonic treatment power of the step S3 is 200-600W.
6. The pigment paste for inkjet printing according to claim 1 wherein the metal chloride is a mixture of magnesium chloride and zinc chloride in a weight ratio of 1: 0.5 to 2.
7. The pigment paste for inkjet printing according to claim 1 wherein the dispersant is a BYK-190 dispersant.
8. The pigment paste for inkjet printing according to claim 1 wherein the anti-settling agent is bentonite.
9. The pigment paste for inkjet printing according to claim 1 wherein the defoamer is a defoamer BYK-024.
10. A preparation method of pigment paste for ink-jet printing is characterized in that the method is used for preparing the pigment paste for ink-jet printing according to any one of claims 1 to 9 and comprises the following steps:
s11, adding deionized water, a dispersing agent and an anti-settling agent into a mixer, and stirring at the rotating speed of 500-800 rpm for 15-30 min to obtain a premixed solution;
s12, adding the modified carbon black and the metal chloride into the premixed liquid, and stirring at the rotating speed of 400-700 rpm for 15-30 min to obtain a pigment premixed liquid;
and S13, adding a defoaming agent, stirring at the rotating speed of 200-500 rpm for 8-20 min, and grinding until the D95 is less than 0.2 mu m to obtain the pigment paste for ink-jet printing.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110536480.3A CN113234361B (en) | 2021-05-17 | 2021-05-17 | Pigment paste for ink-jet printing and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202110536480.3A CN113234361B (en) | 2021-05-17 | 2021-05-17 | Pigment paste for ink-jet printing and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN113234361A true CN113234361A (en) | 2021-08-10 |
| CN113234361B CN113234361B (en) | 2023-05-02 |
Family
ID=77134788
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202110536480.3A Active CN113234361B (en) | 2021-05-17 | 2021-05-17 | Pigment paste for ink-jet printing and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN113234361B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115748001A (en) * | 2022-10-25 | 2023-03-07 | 桐乡市励志特种纤维股份有限公司 | Stock solution coloring regenerated environment-friendly antibacterial polyester profiled filament and preparation method thereof |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB674832A (en) * | 1944-05-08 | 1952-07-02 | Goodrich Co B F | Improvements in and relating to surface active agents and in pigment compositions and pigmented rubber compositions prepared therewith |
| US4404318A (en) * | 1979-12-29 | 1983-09-13 | Kansai Paint Co., Ltd. | Pigment dispersion |
| JPH11323174A (en) * | 1997-10-31 | 1999-11-26 | Toda Kogyo Corp | Iron-based black composite particle powder and its production, coating material prepared by using the iron-based black composite particle powder, and rubber resin composition colored with the iron-based black composite particle powder |
| DE19929845A1 (en) * | 1999-06-29 | 2001-01-11 | Degussa | Surface-modified pyrogenic titanium dioxide, used in cosmetics e.g. sun-protection agents, is treated with ammonium-functional silane |
| JP2003327867A (en) * | 2002-03-04 | 2003-11-19 | Toda Kogyo Corp | Modified carbon block particle powder and method for producing the same, coating containing the modified carbon black particle powder and resin composition |
| CN104004416A (en) * | 2014-06-04 | 2014-08-27 | 福建省华普新材料有限公司 | Water-based colour paste for printing ink |
| CN104212286A (en) * | 2014-08-26 | 2014-12-17 | 中国建筑股份有限公司 | Gray solar reflective cooling coating and preparation method thereof |
| CN105482659A (en) * | 2015-12-17 | 2016-04-13 | 芜湖市宝艺游乐科技设备有限公司 | Wear-resistant and fire-resistant polyester powder coating and preparing method thereof |
| CN108084796A (en) * | 2017-12-15 | 2018-05-29 | 佛山市扬子颜料有限公司 | A kind of new package carbon black ceramics marking ink and preparation method thereof |
-
2021
- 2021-05-17 CN CN202110536480.3A patent/CN113234361B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB674832A (en) * | 1944-05-08 | 1952-07-02 | Goodrich Co B F | Improvements in and relating to surface active agents and in pigment compositions and pigmented rubber compositions prepared therewith |
| US4404318A (en) * | 1979-12-29 | 1983-09-13 | Kansai Paint Co., Ltd. | Pigment dispersion |
| JPH11323174A (en) * | 1997-10-31 | 1999-11-26 | Toda Kogyo Corp | Iron-based black composite particle powder and its production, coating material prepared by using the iron-based black composite particle powder, and rubber resin composition colored with the iron-based black composite particle powder |
| DE19929845A1 (en) * | 1999-06-29 | 2001-01-11 | Degussa | Surface-modified pyrogenic titanium dioxide, used in cosmetics e.g. sun-protection agents, is treated with ammonium-functional silane |
| JP2003327867A (en) * | 2002-03-04 | 2003-11-19 | Toda Kogyo Corp | Modified carbon block particle powder and method for producing the same, coating containing the modified carbon black particle powder and resin composition |
| CN104004416A (en) * | 2014-06-04 | 2014-08-27 | 福建省华普新材料有限公司 | Water-based colour paste for printing ink |
| CN104212286A (en) * | 2014-08-26 | 2014-12-17 | 中国建筑股份有限公司 | Gray solar reflective cooling coating and preparation method thereof |
| CN105482659A (en) * | 2015-12-17 | 2016-04-13 | 芜湖市宝艺游乐科技设备有限公司 | Wear-resistant and fire-resistant polyester powder coating and preparing method thereof |
| CN108084796A (en) * | 2017-12-15 | 2018-05-29 | 佛山市扬子颜料有限公司 | A kind of new package carbon black ceramics marking ink and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 燕丰: "安徽确成硅化学开发出超高分散白炭黑制备新方法", 《橡塑技术与装备》 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115748001A (en) * | 2022-10-25 | 2023-03-07 | 桐乡市励志特种纤维股份有限公司 | Stock solution coloring regenerated environment-friendly antibacterial polyester profiled filament and preparation method thereof |
| CN115748001B (en) * | 2022-10-25 | 2023-12-22 | 桐乡市励志特种纤维股份有限公司 | Stock solution coloring regenerated environment-friendly antibacterial polyester special-shaped filament yarn and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN113234361B (en) | 2023-05-02 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP3948934B2 (en) | Aluminum pigment, method for producing the same, and resin composition | |
| CN110922878A (en) | Water-based high-gloss two-component acrylic polyurethane coating and preparation method thereof | |
| EP1086975A1 (en) | Aqueous pigment dispersion, process for producing the same, and water-based ink comprising the same | |
| WO2021237404A1 (en) | Aqueous epoxy anticorrosive coating and preparation method therefor | |
| CN109337536A (en) | A kind of water soluble acrylic acid -ol acid coating and preparation method thereof | |
| CN108276890B (en) | Water-based automobile intermediate coating composition and preparation method thereof | |
| CN113234361A (en) | Pigment paste for ink-jet printing and preparation method thereof | |
| CN101845254A (en) | Elastic aqueous fluorocarbon paint for external walls | |
| CN114213916B (en) | Water-based non-shading plain color finish paint for automobile and preparation method thereof | |
| CN111058310B (en) | Water-based white ink and preparation method thereof | |
| CN106147392A (en) | A kind of packaging for foodstuff printing water ink and preparation method thereof | |
| CN113355942B (en) | Color paste for internal coloring of paper pulp and preparation method thereof | |
| CN101641414A (en) | Method for producing transparent pigment violet 23 | |
| CN107793845A (en) | A kind of building coating aqueous color paste and preparation method thereof | |
| CN104974661A (en) | Polyethersulfone superfine micropowder and application thereof, paint containing polyethersulfone superfine micropowder and preparation method thereof | |
| CN112812634A (en) | Water-based vacuum cup baking paint and preparation method thereof | |
| CN106916491A (en) | High solids content, high-strength aqueous carbon black mill base preparation method | |
| CN111117463B (en) | Water-based spray coating two-component polyurethane coating and preparation method thereof | |
| CN107286802A (en) | Refitted car ultrafast dry one-component priming paint and preparation method | |
| CN105062220A (en) | Preparation method for cationic type for organic red water-based color paste | |
| CN110452568B (en) | Anticorrosive paint, preparation method thereof and anticorrosive coating | |
| CN115521673A (en) | Environment-friendly exterior wall texture coating not prone to blooming during spraying and preparation method thereof | |
| CN104893395B (en) | Cathode electrophoresis dope | |
| CN110003743A (en) | A kind of water-based stoving paint and its preparation process | |
| CN110452609A (en) | Coating and preparation method are applied in the low VOCs discharge of rail traffic |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |