CN113213755A - 一种中性硼硅玻璃组合物、中性硼硅玻璃制品及其制备方法和应用 - Google Patents
一种中性硼硅玻璃组合物、中性硼硅玻璃制品及其制备方法和应用 Download PDFInfo
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- CN113213755A CN113213755A CN202110553932.9A CN202110553932A CN113213755A CN 113213755 A CN113213755 A CN 113213755A CN 202110553932 A CN202110553932 A CN 202110553932A CN 113213755 A CN113213755 A CN 113213755A
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- China
- Prior art keywords
- borosilicate glass
- weight
- neutral borosilicate
- composition
- glass
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000005388 borosilicate glass Substances 0.000 title claims abstract description 80
- 230000007935 neutral effect Effects 0.000 title claims abstract description 77
- 239000000203 mixture Substances 0.000 title claims abstract description 64
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 11
- 238000002360 preparation method Methods 0.000 title description 3
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims abstract description 25
- 229910052593 corundum Inorganic materials 0.000 claims abstract description 25
- 229910001845 yogo sapphire Inorganic materials 0.000 claims abstract description 25
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 24
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 21
- KKCBUQHMOMHUOY-UHFFFAOYSA-N Na2O Inorganic materials [O-2].[Na+].[Na+] KKCBUQHMOMHUOY-UHFFFAOYSA-N 0.000 claims abstract description 20
- 229910052681 coesite Inorganic materials 0.000 claims abstract description 20
- 229910052906 cristobalite Inorganic materials 0.000 claims abstract description 20
- 229910052682 stishovite Inorganic materials 0.000 claims abstract description 20
- 229910052905 tridymite Inorganic materials 0.000 claims abstract description 20
- MCMNRKCIXSYSNV-UHFFFAOYSA-N ZrO2 Inorganic materials O=[Zr]=O MCMNRKCIXSYSNV-UHFFFAOYSA-N 0.000 claims abstract description 11
- 229910000422 cerium(IV) oxide Inorganic materials 0.000 claims abstract description 10
- CETPSERCERDGAM-UHFFFAOYSA-N ceric oxide Chemical compound O=[Ce]=O CETPSERCERDGAM-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000011521 glass Substances 0.000 claims description 80
- 238000000034 method Methods 0.000 claims description 36
- 239000008395 clarifying agent Substances 0.000 claims description 18
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical group [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 16
- 238000002844 melting Methods 0.000 claims description 14
- 230000008018 melting Effects 0.000 claims description 14
- 150000003841 chloride salts Chemical class 0.000 claims description 9
- 150000004673 fluoride salts Chemical class 0.000 claims description 9
- 239000007832 Na2SO4 Substances 0.000 claims description 8
- 239000011780 sodium chloride Substances 0.000 claims description 8
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 8
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 7
- 229910001634 calcium fluoride Inorganic materials 0.000 claims description 7
- 239000000155 melt Substances 0.000 claims description 7
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical group [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 6
- 229910004883 Na2SiF6 Inorganic materials 0.000 claims description 5
- 229910052925 anhydrite Inorganic materials 0.000 claims description 5
- 238000000137 annealing Methods 0.000 claims description 5
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Inorganic materials [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 claims description 5
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical group [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 5
- 229910052796 boron Inorganic materials 0.000 claims description 4
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 3
- 238000007670 refining Methods 0.000 claims 1
- 238000007493 shaping process Methods 0.000 claims 1
- 239000003814 drug Substances 0.000 abstract description 13
- 239000000126 substance Substances 0.000 abstract description 10
- 238000004806 packaging method and process Methods 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 229940079593 drug Drugs 0.000 description 7
- 239000003513 alkali Substances 0.000 description 6
- 238000012360 testing method Methods 0.000 description 6
- 229910000272 alkali metal oxide Inorganic materials 0.000 description 5
- 238000005352 clarification Methods 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 4
- 230000007547 defect Effects 0.000 description 4
- 239000000243 solution Substances 0.000 description 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 238000002425 crystallisation Methods 0.000 description 3
- 230000008025 crystallization Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- UGTZHPSKYRIGRJ-YUMQZZPRSA-N Lys-Glu Chemical compound NCCCC[C@H](N)C(=O)N[C@H](C(O)=O)CCC(O)=O UGTZHPSKYRIGRJ-YUMQZZPRSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000011049 filling Methods 0.000 description 2
- 238000000265 homogenisation Methods 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- 108010009298 lysylglutamic acid Proteins 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000009512 pharmaceutical packaging Methods 0.000 description 2
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 1
- 208000007536 Thrombosis Diseases 0.000 description 1
- XGCTUKUCGUNZDN-UHFFFAOYSA-N [B].O=O Chemical compound [B].O=O XGCTUKUCGUNZDN-UHFFFAOYSA-N 0.000 description 1
- OBNDGIHQAIXEAO-UHFFFAOYSA-N [O].[Si] Chemical compound [O].[Si] OBNDGIHQAIXEAO-UHFFFAOYSA-N 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 229910001413 alkali metal ion Inorganic materials 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000003708 ampul Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 230000001066 destructive effect Effects 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 238000005429 filling process Methods 0.000 description 1
- 238000007496 glass forming Methods 0.000 description 1
- 238000001802 infusion Methods 0.000 description 1
- 229910001387 inorganic aluminate Inorganic materials 0.000 description 1
- 238000010253 intravenous injection Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000005022 packaging material Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 229910052697 platinum Inorganic materials 0.000 description 1
- 229910001414 potassium ion Inorganic materials 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000001954 sterilising effect Effects 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229960005486 vaccine Drugs 0.000 description 1
- 230000006441 vascular event Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/089—Glass compositions containing silica with 40% to 90% silica, by weight containing boron
- C03C3/091—Glass compositions containing silica with 40% to 90% silica, by weight containing boron containing aluminium
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61J—CONTAINERS SPECIALLY ADAPTED FOR MEDICAL OR PHARMACEUTICAL PURPOSES; DEVICES OR METHODS SPECIALLY ADAPTED FOR BRINGING PHARMACEUTICAL PRODUCTS INTO PARTICULAR PHYSICAL OR ADMINISTERING FORMS; DEVICES FOR ADMINISTERING FOOD OR MEDICINES ORALLY; BABY COMFORTERS; DEVICES FOR RECEIVING SPITTLE
- A61J1/00—Containers specially adapted for medical or pharmaceutical purposes
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B15/00—Drawing glass upwardly from the melt
- C03B15/14—Drawing tubes, cylinders, or rods from the melt
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/089—Glass compositions containing silica with 40% to 90% silica, by weight containing boron
- C03C3/091—Glass compositions containing silica with 40% to 90% silica, by weight containing boron containing aluminium
- C03C3/093—Glass compositions containing silica with 40% to 90% silica, by weight containing boron containing aluminium containing zinc or zirconium
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/50—Glass production, e.g. reusing waste heat during processing or shaping
- Y02P40/57—Improving the yield, e-g- reduction of reject rates
Landscapes
- Chemical & Material Sciences (AREA)
- Materials Engineering (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Geochemistry & Mineralogy (AREA)
- General Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Glass Compositions (AREA)
Abstract
Description
实施例 | 1 | 2 | 3 | 4 | 5 |
SiO<sub>2</sub>(wt%) | 73.5 | 74 | 73 | 75 | 72 |
Al<sub>2</sub>O<sub>3</sub>(wt%) | 10.5 | 8 | 11 | 8 | 8 |
B<sub>2</sub>O<sub>3</sub>(wt%) | 9 | 10 | 9 | 10 | 12 |
Na<sub>2</sub>O(wt%) | 5.4 | 5 | 4 | 5 | 6 |
K<sub>2</sub>O(wt%) | 0 | 0 | 1.5 | 0.2 | 0 |
CaO(wt%) | 1 | 1.1 | 0 | 1 | 1.2 |
BaO(wt%) | 0 | 1 | 0.8 | 0.2 | 0 |
ZrO<sub>2</sub>(wt%) | 0 | 0.2 | 0 | 0 | 0.3 |
CeO<sub>2</sub>(wt%) | 0 | 0.3 | 0.3 | 0.1 | 0 |
SiO<sub>2</sub>+Al<sub>2</sub>O<sub>3</sub> | 84.00 | 82.00 | 84.00 | 83.00 | 80.00 |
(Na<sub>2</sub>O+K<sub>2</sub>O)/(Al<sub>2</sub>O<sub>3</sub>+B<sub>2</sub>O<sub>3</sub>) | 0.28 | 0.28 | 0.28 | 0.29 | 0.30 |
澄清剂NaCl(wt%) | 0.3 | 0 | 0 | 0.4 | 0.4 |
澄清剂CaF(wt%) | 0.3 | 0 | 0.3 | 0 | 0.1 |
澄清剂Na<sub>2</sub>SO<sub>4</sub>(wt%) | 0 | 0.4 | 0.1 | 0.1 | 0 |
粘度10<sup>2.3</sup>泊对应温度(℃) | 1668 | 1654 | 1660 | 1648 | 1645 |
粘度10<sup>4</sup>泊对应温度(℃) | 1275 | 1254 | 1268 | 1235 | 1233 |
粘度10<sup>4.5</sup>泊对应温度(℃) | 1175 | 1158 | 1165 | 1156 | 1162 |
析晶上限温度(℃) | 1058 | 1010 | 1020 | 1022 | 1040 |
软化点(℃) | 846 | 835 | 852 | 847 | 832 |
98℃耐水性 | HGB1级 | HGB1级 | HGB1级 | HGB1级 | HGB1级 |
121℃耐水性 | 1级 | 1级 | 1级 | 1级 | 1级 |
耐酸性 | 1级 | 1级 | 1级 | 1级 | 1级 |
耐碱性 | 1级 | 1级 | 1级 | 1级 | 1级 |
破坏压力(N) | 1485 | 1455 | 1522 | 1466 | 1299 |
熔融温度(℃) | 1660 | 1645 | 1650 | 1640 | 1635 |
澄清温度(℃) | 1670 | 1655 | 1660 | 1650 | 1645 |
退火温度(℃) | 585 | 575 | 580 | 570 | 565 |
Claims (10)
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CN202110553932.9A CN113213755B (zh) | 2021-05-20 | 2021-05-20 | 一种中性硼硅玻璃组合物、中性硼硅玻璃制品及其制备方法和应用 |
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CN113213755A true CN113213755A (zh) | 2021-08-06 |
CN113213755B CN113213755B (zh) | 2023-06-20 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN114195382A (zh) * | 2021-12-29 | 2022-03-18 | 湖南旗滨医药材料科技有限公司 | 硼硅酸盐玻璃组合物、硼硅酸盐玻璃制备方法和药用玻璃 |
CN115368013A (zh) * | 2022-09-02 | 2022-11-22 | 中南大学 | 一种着色医用中性硼硅玻璃及其制备方法 |
CN117263519A (zh) * | 2023-09-15 | 2023-12-22 | 凯盛君恒药玻(重庆)有限公司 | 一种无氯根无亚硝酸盐的拉管用中硼硅玻璃及其制备方法 |
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DE3722130A1 (de) * | 1987-07-02 | 1989-01-12 | Schott Glaswerke | Borosilikatglas |
DE10027699A1 (de) * | 2000-06-03 | 2002-04-18 | Schott Rohrglas Gmbh | Borosilicatglas hoher chemischer Beständigkeit |
CN1495141A (zh) * | 2002-08-24 | 2004-05-12 | 肖特玻璃制造厂 | 具有高水解稳定性的硼硅酸盐玻璃 |
CN104261676A (zh) * | 2014-09-04 | 2015-01-07 | 东莞市长安东阳光铝业研发有限公司 | 一种中性硼硅玻璃及其应用 |
CN110128011A (zh) * | 2013-04-26 | 2019-08-16 | 肖特股份有限公司 | 优选用于医药领域的具有改良的抗水解性的硼硅玻璃 |
US20190382303A1 (en) * | 2018-06-18 | 2019-12-19 | Schott Ag | Borosilicate glass article with low boron content |
CN111977972A (zh) * | 2020-09-01 | 2020-11-24 | 湖南旗滨医药材料科技有限公司 | 硼硅酸盐玻璃及其制备方法 |
CN112624607A (zh) * | 2021-01-05 | 2021-04-09 | 河北光兴半导体技术有限公司 | 复合澄清剂、中性硼硅药用玻璃用组合物及其制备的玻璃和应用 |
CN112694254A (zh) * | 2021-01-04 | 2021-04-23 | 河北光兴半导体技术有限公司 | 一种中硼硅玻璃组合物、中硼硅玻璃及其制备方法和应用 |
CN112811813A (zh) * | 2021-01-15 | 2021-05-18 | 河北光兴半导体技术有限公司 | 一种硼硅玻璃组合物、硼硅玻璃及其制备方法和应用 |
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2021
- 2021-05-20 CN CN202110553932.9A patent/CN113213755B/zh active Active
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DE3722130A1 (de) * | 1987-07-02 | 1989-01-12 | Schott Glaswerke | Borosilikatglas |
DE10027699A1 (de) * | 2000-06-03 | 2002-04-18 | Schott Rohrglas Gmbh | Borosilicatglas hoher chemischer Beständigkeit |
CN1495141A (zh) * | 2002-08-24 | 2004-05-12 | 肖特玻璃制造厂 | 具有高水解稳定性的硼硅酸盐玻璃 |
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CN111977972A (zh) * | 2020-09-01 | 2020-11-24 | 湖南旗滨医药材料科技有限公司 | 硼硅酸盐玻璃及其制备方法 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN114195382A (zh) * | 2021-12-29 | 2022-03-18 | 湖南旗滨医药材料科技有限公司 | 硼硅酸盐玻璃组合物、硼硅酸盐玻璃制备方法和药用玻璃 |
CN115368013A (zh) * | 2022-09-02 | 2022-11-22 | 中南大学 | 一种着色医用中性硼硅玻璃及其制备方法 |
CN117263519A (zh) * | 2023-09-15 | 2023-12-22 | 凯盛君恒药玻(重庆)有限公司 | 一种无氯根无亚硝酸盐的拉管用中硼硅玻璃及其制备方法 |
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