CN112921662A - Finishing process of pure cotton non-ironing soil-release fabric - Google Patents
Finishing process of pure cotton non-ironing soil-release fabric Download PDFInfo
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- CN112921662A CN112921662A CN202110141426.9A CN202110141426A CN112921662A CN 112921662 A CN112921662 A CN 112921662A CN 202110141426 A CN202110141426 A CN 202110141426A CN 112921662 A CN112921662 A CN 112921662A
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- fabric
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- 239000004744 fabric Substances 0.000 title claims abstract description 117
- 239000002689 soil Substances 0.000 title claims abstract description 44
- 238000010409 ironing Methods 0.000 title claims abstract description 25
- 229920000742 Cotton Polymers 0.000 title claims abstract description 24
- 238000007730 finishing process Methods 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 60
- 238000009990 desizing Methods 0.000 claims abstract description 28
- 238000005096 rolling process Methods 0.000 claims abstract description 26
- 238000005406 washing Methods 0.000 claims abstract description 23
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 21
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000009999 singeing Methods 0.000 claims abstract description 11
- 238000002791 soaking Methods 0.000 claims abstract description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 18
- 229920005989 resin Polymers 0.000 claims description 15
- 239000011347 resin Substances 0.000 claims description 15
- 239000000835 fiber Substances 0.000 claims description 11
- 239000003513 alkali Substances 0.000 claims description 10
- 230000000149 penetrating effect Effects 0.000 claims description 7
- 102000004190 Enzymes Human genes 0.000 claims description 6
- 108090000790 Enzymes Proteins 0.000 claims description 6
- 239000003054 catalyst Substances 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 239000003223 protective agent Substances 0.000 claims description 6
- 239000002516 radical scavenger Substances 0.000 claims description 6
- 238000007670 refining Methods 0.000 claims description 6
- 238000007598 dipping method Methods 0.000 claims description 5
- 238000001035 drying Methods 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 5
- 238000010025 steaming Methods 0.000 claims description 5
- 230000003670 easy-to-clean Effects 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 7
- 238000009988 textile finishing Methods 0.000 abstract description 2
- 230000000052 comparative effect Effects 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 6
- 238000013461 design Methods 0.000 description 4
- 239000010410 layer Substances 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- 238000004132 cross linking Methods 0.000 description 3
- 239000012847 fine chemical Substances 0.000 description 3
- 239000004814 polyurethane Substances 0.000 description 3
- 229920002635 polyurethane Polymers 0.000 description 3
- 239000004753 textile Substances 0.000 description 3
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 238000013329 compounding Methods 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 229910052731 fluorine Inorganic materials 0.000 description 2
- 239000011737 fluorine Substances 0.000 description 2
- 238000007710 freezing Methods 0.000 description 2
- 230000008014 freezing Effects 0.000 description 2
- 230000002209 hydrophobic effect Effects 0.000 description 2
- 229920001225 polyester resin Polymers 0.000 description 2
- 239000004645 polyester resin Substances 0.000 description 2
- 238000007493 shaping process Methods 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 230000037303 wrinkles Effects 0.000 description 2
- 229920001131 Pulp (paper) Polymers 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000003889 chemical engineering Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000007334 copolymerization reaction Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000005202 decontamination Methods 0.000 description 1
- 230000003588 decontaminative effect Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000007590 electrostatic spraying Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 150000002191 fatty alcohols Chemical class 0.000 description 1
- 238000004108 freeze drying Methods 0.000 description 1
- 239000011499 joint compound Substances 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000002346 layers by function Substances 0.000 description 1
- 239000010721 machine oil Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 229940051841 polyoxyethylene ether Drugs 0.000 description 1
- 229920000056 polyoxyethylene ether Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- QQONPFPTGQHPMA-UHFFFAOYSA-N propylene Natural products CC=C QQONPFPTGQHPMA-UHFFFAOYSA-N 0.000 description 1
- 239000010499 rapseed oil Substances 0.000 description 1
- 238000005057 refrigeration Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000009489 vacuum treatment Methods 0.000 description 1
- 239000002759 woven fabric Substances 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/564—Polyureas, polyurethanes or other polymers having ureide or urethane links; Precondensation products forming them
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/58—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides
- D06M11/59—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with nitrogen or compounds thereof, e.g. with nitrides with ammonia; with complexes of organic amines with inorganic substances
- D06M11/61—Liquid ammonia
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Treatment Of Fiber Materials (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention relates to the technical field of textile finishing, in particular to a finishing process of pure cotton non-ironing easy-to-clean fabric, which comprises the working procedures of singeing → desizing → mercerizing → liquid ammonia → post-baking → pre-shrinking and rolling, wherein the fabric is subjected to secondary soaking and secondary rolling treatment by a fluorine-free finishing auxiliary agent in the post-baking working procedure, is dried, and is baked after being made into ready-made clothes. The pure cotton non-ironing soil release fabric obtained by the invention has wide soil release performance, has soil release effect on water-soluble and fat-soluble dirt, and can achieve the effects of 3/4 grade before soil release and washing, 4 grade after 10 times of washing (JIS L1919B method), 3 grade before soil release and washing and 3 grade after 10 times of washing (JIS L1919C-3 method); meanwhile, the fabric is made into ready-made clothes, and the non-ironing property of the fabric of the ready-made clothes is detected to be above grade 3.0.
Description
Technical Field
The invention relates to the technical field of textile finishing, in particular to a finishing process of pure cotton non-ironing soil-release fabric.
Background
Pure cotton fabric is always the preferred fabric of high-grade shirts, but because the common pure cotton fabric is easy to wrinkle, stiff and non-conformal, after washing for several times, the fabric wrinkles seriously and is not easy to be managed, and the fabric can be leveled only after ironing, which brings inconvenience to daily life of people; in addition, the clothes of the fabric are inevitably stained in the wearing process, such as water stains like dust and mud, and oil stains like rape oil and machine oil. At present, many researches have been made on the post-finishing of fabrics with soil release finishing agents to impart soil release function to the fabrics.
Chinese patent CN111434847A discloses a hydrophilic soil release fabric, which adopts hydrophilic polyester resin to form a resin layer on the surface of a single fiber to prevent oil stains from entering the interior of the fiber, the hydrophilic group of the hydrophilic polyester resin endows the fabric with hydrophilicity, and fatty alcohol polyoxyethylene ether dissolves the oil stains to enable the oil stains to fall off from the surface of the fiber.
Chinese patent CN210390320U discloses a soil release functional textile which is formed by compounding a plurality of fiber layers and functional layers, the process of the textile is complex, and the hand feeling of the textile inevitably becomes thick and hard due to the compounding process.
Chinese patent CN105133294A discloses a method for producing a clean-up easy-care full-face shirt, which comprises the steps of firstly carrying out liquid ammonia and preshrinking finishing on an all-cotton fabric, then carrying out electrostatic spraying of a first clean-up finishing agent, then carrying out microwave treatment, carrying out vacuum treatment on the treated fabric, then using wood pulp liquid after microwave treatment to cook, spin-drying, putting into a freezing chamber for freeze drying, then putting the fabric into a steeping liquor containing a second clean-up finishing agent and hydrophilic easy-care, carrying out padding treatment on the treated fabric, freezing, drying, cutting, making clothes, and carrying out finish-care shaping on a baking shaping machine to obtain a finished product. The whole production flow of this patent is complicated, and conventional enterprise does not have surface fabric microwave treatment and evacuation equipment, because need the cooling refrigeration, the production energy consumption also can corresponding improvement, and is with high costs.
Chinese patent CN106381701A discloses a processing method suitable for light-colored or white pure cotton fabric, the used auxiliary agent is perfluoroalkyl propylene copolymerization product, and the problem of fluorine-containing substance release exists in the production or wearing process.
Chinese patent CN101942752A discloses a finishing method of a non-ironing moisture-absorbing soil-release fabric, which comprises the process routes of fabric preparation → pre-softening → moisture crosslinking → rolling moisture-absorbing soil-release assistant → high-temperature baking → tentering → preshrinking. This patent adopts the moisture cross-linking technology to make the loss of feeling of surface fabric great, and the clothing factory is difficult to press the fold according to the design on the clothing, and adds the process of the easy decontamination auxiliary agent of the independent padding in moisture cross-linking and tentering, has prolonged surface fabric process time greatly, has reduced production efficiency, and increases the energy consumption, and manufacturing cost is also corresponding improvement a lot.
Disclosure of Invention
The invention aims to provide a finishing process of pure cotton non-ironing and easy-to-clean fabric, which adopts a post-baking process to effectively realize the simultaneous existence of the non-ironing and easy-to-clean functions, the fabric finished by the process has the easy-to-clean function and the non-ironing effect of more than 3 grade, and the easy-to-clean auxiliary agent is a fluorine-free auxiliary agent and is environment-friendly.
The technical scheme adopted by the invention for solving the technical problems is as follows:
the finishing process of the pure cotton non-ironing soil-release fabric comprises the working procedures of singeing → desizing → mercerizing → liquid ammonia → post-baking → pre-shrinking and rolling, wherein the fabric is subjected to two-dipping and two-rolling treatment by using a fluorine-free finishing auxiliary agent in the post-baking working procedure, and is dried, and the fabric is baked after being made into a garment.
Wherein:
the fluorine-free finishing auxiliary agent in the post-baking procedure consists of the following components in concentration: non-ironing resin ERF-N: 40-160g/L, resin catalyst 530: 40-150g/L, formaldehyde scavenger CFF: 20-30g/L, fiber protective agent HDP: 5-30g/L, soil release finishing agent FR-100: 60-80g/L, penetrant WR-03: 5-30g/L, and the balance of water.
The easy-care resin ERF-N, the resin catalyst 530, the formaldehyde scavenger CFF, the fiber protective agent HDP and the easy-cleaning finishing agent FR-100 are all selected from products of Ziboli fine chemical industry Co., Ltd, and the penetrating agent WR-03 is selected from products of Ono Si Industrial Co., Ltd, Qingdao.
The rolling residual rate of the fabric after the two-dipping and two-rolling treatment in the post-baking process is 60-80%.
The drying temperature in the post-baking process is 110-130 ℃, and the drying time is 1-3 min; the baking temperature is 140-.
In the singeing procedure, the vehicle speed is 80-95m/min, and the flame intensity is 12-15 grades.
In the desizing procedure, the stacking time is 5-10min, the stacking temperature is 90-100 ℃, the washing temperature is 90-95 ℃, the temperature of a steam box is 90-100 ℃, the desizing speed is 85-95m/min, and the temperature of a material groove is 35-40 ℃; the desizing liquid contains desizing enzyme 5-10g/L, refining agent 5-10g/L, penetrating agent 1-5g/L and water for the rest.
The desizing enzyme is DS-HT which is a product of Ziboli fine chemical engineering Co.Ltd;
the refining agent is selected from XC-J which is a product of Ziplorui fine chemical engineering Co., Ltd;
the penetrant is WR-03 of Ono Si Industrial and trade company Limited in Qingdao.
In the mercerizing procedure, the alkali concentration is 18-22Be, the alkali liquor temperature is 30-40 ℃, the water washing temperature is 65-75 ℃, the spraying temperature is 65-75 ℃, the vehicle speed is 60-80m/min, the pH value of the cropping cloth cover is 5.5-7.5, and the width of the cloth cover is 1 inch less than that of the blank.
In the liquid ammonia process, the speed is 35-60m/min, the cloth cover tension range is 100-450N, the temperature of the treatment chamber is 60-70 ℃, the temperature of the steaming chamber is 110-120 ℃, the washing temperature is 50-55 ℃, and the pH value of the cloth cover is 5.5-7.5.
The speed in the pre-shrinking and rolling process is 50-70m/min, and the breadth falling and the shrinkage rate are controlled according to corresponding standards.
The finishing process of the pure cotton non-ironing soil release fabric is mainly suitable for pure cotton yarn dyed woven fabrics.
The invention has the following beneficial effects:
(1) according to the invention, the polyurethane type soil release auxiliary FR-100 is used in the finishing auxiliary, the FR-100 is organic silicon modified polyurethane, the organic silicon group can form a layer of hydrophobic film on the surface of the yarn to prevent the soil from permeating into the fiber, the hydrophilic group carried by the polyurethane enables the soil to be removed more easily in a water bath environment, and the excellent soil release performance of the fabric is realized through the double effects of preventing the soil from entering the interior and easily removing the soil. In the invention, the finishing auxiliary agent is also used by WR-03, and the surface tension of the fabric can be increased by the WR-03, so that the auxiliary agents such as the easy-to-clean auxiliary agent FR-100 and the easy-care resin ERF-N can more easily enter the fabric; a layer of hydrophobic film can be formed on the surface of the yarn in the fabric, so that the soil release effect of the fabric is further enhanced. The auxiliary agents adopted in the post-baking process are all fluorine-free auxiliary agents, so that the problem of fluorine release is avoided, and the method is green and environment-friendly.
The invention adopts the post-baking process, the fabric is treated by two-dipping and two-rolling, the non-ironing resin ERF-N enters the yarn and is dried at the temperature of 110-; after the fabric is cut into ready-made clothes, ironing and flattening the ready-made clothes into needed pleats or creases, baking the ready-made clothes for 3-5min at the temperature of 140-. The invention adopts the post-baking process, and after the fabric is made into ready-made clothes, the non-ironing property of the fabric is above grade 3.0.
(2) The pure cotton non-ironing soil release fabric obtained by the invention has wide soil release performance, has soil release effect on water-soluble and fat-soluble dirt, and can achieve the effects of 3/4 grade before soil release and washing, 4 grade after 10 times of washing (JIS L1919B method), 3 grade before soil release and 3 grade after 10 times of washing (JIS L1919C-3 method); meanwhile, the fabric is made into ready-made clothes, and the non-ironing property of the fabric of the ready-made clothes is detected to be above grade 3.0.
(3) The finishing process can be realized on conventional finishing equipment, is simple in process and low in cost, and is suitable for large-scale production.
Detailed Description
The present invention is further described below with reference to examples.
Example 1
The yarn-dyed 3/2 square plain blank (CJSW04042-2001765-1-D) with the design specification of 60/61 × CPT60XCPT100/2 × 160 × 110 sequentially goes through the working procedures of singeing → desizing → mercerizing → liquid ammonia → post-baking → preshrinking and rolling to obtain the finished fabric. The method specifically comprises the following steps:
(1) in the singeing process, the vehicle speed is 80m/min, and the flame intensity is 12 grades.
(2) In the desizing procedure, the stacking time is 10min, the stacking temperature is 90 ℃, the washing temperature is 95 ℃, the steam box temperature is 100 ℃, the desizing speed is 85m/min, the material groove temperature is 35 ℃, the adopted desizing liquid contains desizing enzyme DS-HT 5g/L, refining agent XC-J5 g/L, penetrating agent WR-031 g/L and the balance of water.
(3) In the mercerizing process, the alkali concentration is 22Be, the alkali liquor temperature is 40 ℃, the water washing temperature is 75 ℃, the spraying temperature is 75 ℃, the vehicle speed is 60m/min, the pH value of the cloth cover of the cropping cloth is 5.5, and the width of the cloth cover is 1 inch less than that of the blank.
(4) In the liquid ammonia process, the speed of the liquid ammonia is 60m/min, the tension range of the cloth cover is 100N, the temperature of a treatment chamber is 60 ℃, the temperature of a steaming chamber is 110 ℃, the temperature of water washing is 50 ℃, and the pH value of the cloth cover of the cropping cloth is 6.0, so that the semi-finished grey cloth is obtained.
(5) In the post-baking process, the semi-finished grey cloth is subjected to two-dipping and two-rolling treatment by using a fluorine-free finishing auxiliary agent, the rolling residual rate is 60 percent, the semi-finished grey cloth is dried for 1min at 120 ℃, and the semi-finished grey cloth is baked for 1min at 170 ℃ after the fabric is made into a garment; wherein the fluorine-free finishing auxiliary agent consists of the following components in concentration: non-ironing resin ERF-N: 160g/L, resin catalyst 530: 150g/L, formaldehyde scavenger CFF: 30g/L, fiber protective agent HDP: 30g/L, soil release finishing agent FR-100: 80g/L, penetrant WR-03: 30g/L and the balance of water.
(6) And the speed in the pre-shrinking and rolling process is 50m/min, so that the finished fabric is obtained.
Example 2
The yarn-dyed plain grey fabric (CJKSW04453-2000418-1-D) with the design specification of 53/54 × CPT100/2 XFT 40(40D) 140 × 76 sequentially undergoes the working procedures of singeing → desizing → mercerizing → liquid ammonia → post-baking → preshrinking and rolling to obtain the finished fabric. The method specifically comprises the following steps:
(1) in the singeing process, the vehicle speed is 90m/min, and the flame intensity is 14 grades.
(2) In the desizing procedure, the stacking time is 8min, the stacking temperature is 95 ℃, the water washing temperature is 93 ℃, the steam box temperature is 95 ℃, the desizing speed is 90m/min, the material groove temperature is 38 ℃, the adopted desizing liquid contains desizing enzyme DS-HT 8g/L, refining agent XC-J8 g/L, penetrating agent WR-033 g/L and the balance of water.
(3) In the mercerizing process, the alkali concentration is 20Be, the alkali liquor temperature is 35 ℃, the water washing temperature is 70 ℃, the spraying temperature is 70 ℃, the vehicle speed is 70m/min, the pH value of the cloth cover of the cropping cloth is 6.0, and the width of the cloth cover is 1 inch less than that of the blank.
(4) In the liquid ammonia process, the liquid ammonia speed is 55m/min, the cloth cover tension range is 250N, the temperature of a treatment chamber is 65 ℃, the temperature of a steaming chamber is 115 ℃, the water washing temperature is 53 ℃, and the pH value of the cloth cover of the cropping cloth is 7.5, so that the semi-finished grey cloth is obtained.
(5) In the post-baking process, the semi-finished grey cloth is subjected to secondary soaking and secondary rolling treatment by using a fluorine-free finishing auxiliary agent, the rolling residual rate is 70 percent, the semi-finished grey cloth is dried for 2min at 120 ℃, and the semi-finished grey cloth is baked for 2min at 160 ℃ after the fabric is made into a garment; wherein the fluorine-free finishing auxiliary agent consists of the following components in concentration: non-ironing resin ERF-N: 100g/L, resin catalyst 530: 100g/L, formaldehyde scavenger CFF: 25g/L, fiber protective agent HDP: 20g/L, soil release finishing agent FR-100: 70g/L, penetrant WR-03: 20g/L, and the balance of water.
(6) And the speed in the pre-shrinking and rolling process is 60m/min, so that the finished fabric is obtained.
Example 3
The yarn-dyed plain grey fabric with the design specification of 57/58 CPT40 CPT40 130 100 sequentially undergoes the working procedures of singeing → desizing → mercerizing → liquid ammonia → post baking → pre-shrinking and rolling to obtain the finished fabric. The method specifically comprises the following steps:
(1) in the singeing procedure, the vehicle speed is 95m/min, and the flame intensity is 15 grades.
(2) In the desizing procedure, the stacking time is 5min, the stacking temperature is 100 ℃, the water washing temperature is 90 ℃, the steam box temperature is 90 ℃, the desizing speed is 95m/min, the material groove temperature is 40 ℃, and the adopted desizing liquid contains desizing enzyme DS-HT 10g/L, refining agent XC-J10 g/L, penetrating agent WR-035 g/L and the balance of water.
(3) In the mercerizing process, the alkali concentration is 18Be, the alkali liquor temperature is 30 ℃, the water washing temperature is 65 ℃, the spraying temperature is 65 ℃, the vehicle speed is 80m/min, the pH value of the cloth cover of the cropping cloth is 7.5, and the width of the cloth cover is 1 inch less than the width of the blank.
(4) In the liquid ammonia process, the liquid ammonia speed is 60m/min, the cloth cover tension range is 450N, the temperature of a treatment chamber is 70 ℃, the temperature of a steaming chamber is 120 ℃, the water washing temperature is 55 ℃, and the pH value of the cloth cover of the cropping cloth is 5.5, so that the semi-finished grey cloth is obtained.
(5) In the post-baking process, the semi-finished grey cloth is subjected to secondary soaking and secondary rolling treatment by using a fluorine-free finishing aid, the rolling retention rate is 80 percent, the semi-finished grey cloth is dried for 3min at 110 ℃, and the semi-finished grey cloth is baked for 3min at 140 ℃ after the fabric is made into a garment; wherein the fluorine-free finishing auxiliary agent consists of the following components in concentration: non-ironing resin ERF-N: 40g/L, resin catalyst 530: 40g/L, formaldehyde scavenger CFF: 20g/L, fiber protective agent HDP: 5g/L, soil release finishing agent FR-100: 60g/L, penetrant WR-03: 5g/L, and the balance of water.
(6) And the speed in the pre-shrinking and rolling process is 70m/min, so that the finished fabric is obtained.
Index tests were performed on the finished fabrics obtained in examples 1-3, and the data are shown in table 1.
TABLE 1 index data Table of the finished fabrics of examples 1-3
The finished fabrics obtained in the examples 1-3 are made into ready-made clothes, and the ready-made clothes are baked for 3-5min at the temperature of 140 ℃ and 170 ℃, and the non-ironing data of the ready-made clothes fabrics are shown in Table 2.
TABLE 2 Table of easy-care data for garments made from the fabrics obtained in examples 1-3
Comparative example 1
In the post-baking process, no easy-to-clean finishing agent FR-100 is added into the fluorine-free finishing auxiliary agent, and the rest steps are the same as in example 1.
Comparative example 2
No penetrating agent WR-03 is added into the fluorine-free finishing auxiliary agent in the post-baking process, and the rest steps are the same as the steps in the example 1.
Comparative example 3
In the post-baking step, a soil release finish HSD selected from products of Tpinorui Fine chemical Co., Ltd is added to the fluorine-free finish assistant, and the rest steps are the same as in example 1.
Comparative example 4
In the post-baking step, a penetrant MAG-L selected from products of Ziboluri Fine chemical Co., Ltd is added to the fluorine-free finishing assistant, and the rest steps are the same as in example 1.
Index tests are carried out on the finished fabrics obtained in the comparative examples 1-4, and the data are shown in Table 3.
TABLE 3 index data table of the finished fabrics of comparative examples 1-4
The finished fabrics obtained in the comparative examples 1-4 are made into ready-made clothes, the ready-made clothes are baked for 3-5min at the temperature of 140-.
TABLE 4 Table of easy care data for garments made from the face fabrics obtained in comparative examples 1-4
Claims (10)
1. A finishing process of pure cotton non-ironing soil release fabric comprises the working procedures of singeing → desizing → mercerizing → liquid ammonia → post baking → preshrinking and rolling, and is characterized in that: and in the post-baking process, the fabric is subjected to secondary soaking and secondary rolling treatment by using the fluorine-free finishing auxiliary agent, is dried and is baked.
2. The finishing process of the pure cotton easy-care and soil-release fabric according to claim 1, which is characterized in that: the fluorine-free finishing auxiliary agent consists of the following components in concentration: non-ironing resin ERF-N: 40-160g/L, resin catalyst 530: 40-150g/L, formaldehyde scavenger CFF: 20-30g/L, fiber protective agent HDP: 5-30g/L, soil release finishing agent FR-100: 60-80g/L, penetrant WR-03: 5-30g/L, and the balance of water.
3. The finishing process of the pure cotton easy-care and soil-release fabric according to claim 1, which is characterized in that: the rolling allowance rate of the fabric after the two-dipping and two-rolling treatment is 60-80%.
4. The finishing process of the pure cotton easy-care and soil-release fabric according to claim 1, which is characterized in that: the drying temperature is 110-; the baking temperature is 140-.
5. The finishing process of the pure cotton easy-care and soil-release fabric according to claim 1, which is characterized in that: in the singeing procedure, the vehicle speed is 80-95m/min, and the flame intensity is 12-15 grades.
6. The finishing process of the pure cotton easy-care and soil-release fabric according to claim 1, which is characterized in that: in the desizing procedure, the stacking time is 5-10min, the stacking temperature is 90-100 ℃, the washing temperature is 90-95 ℃, the steam box temperature is 90-100 ℃, the desizing speed is 85-95m/min, and the material tank temperature is 35-40 ℃.
7. The finishing process of the pure cotton easy-care and soil-release fabric according to claim 6, which is characterized in that: the desizing liquid adopted in the desizing procedure contains 5-10g/L of desizing enzyme, 5-10g/L of refining agent, 1-5g/L of penetrating agent and the balance of water.
8. The finishing process of the pure cotton easy-care and soil-release fabric according to claim 1, which is characterized in that: in the mercerizing procedure, the alkali concentration is 18-22Be, the alkali liquor temperature is 30-40 ℃, the water washing temperature is 65-75 ℃, the spraying temperature is 65-75 ℃, the vehicle speed is 60-80m/min, the pH value of the cropping cloth cover is 5.5-7.5, and the width of the cloth cover is 1 inch less than that of the blank.
9. The finishing process of the pure cotton easy-care and soil-release fabric according to claim 1, which is characterized in that: in the liquid ammonia process, the speed is 35-60m/min, the cloth cover tension range is 100-450N, the temperature of the treatment chamber is 60-70 ℃, the temperature of the steaming chamber is 110-120 ℃, the washing temperature is 50-55 ℃, and the pH value of the cloth cover is 5.5-7.5.
10. The finishing process of the pure cotton easy-care and soil-release fabric according to claim 1, which is characterized in that: the speed of the pre-shrinking and rolling process is 50-70 m/min.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113235292A (en) * | 2021-06-28 | 2021-08-10 | 江南大学 | Delayed baking non-ironing finishing process for cotton fabric |
| CN113981685A (en) * | 2021-10-18 | 2022-01-28 | 鲁丰织染有限公司 | Processing method of non-ironing waterproof sanded fabric |
| CN114045670A (en) * | 2021-11-17 | 2022-02-15 | 鲁丰织染有限公司 | Short-flow processing technology for environment-friendly fluorine-free easy-to-clean non-ironing finishing |
| CN114411316A (en) * | 2021-12-17 | 2022-04-29 | 鲁泰纺织股份有限公司 | Preparation method of cotton/spandex single jersey knitted shirt fabric |
| CN114808450A (en) * | 2022-03-22 | 2022-07-29 | 鲁丰织染有限公司 | Environment-friendly processing technology for improving easy-to-decontaminate performance of resin finishing |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004017617A (en) * | 2002-06-20 | 2004-01-22 | Toppan Printing Co Ltd | Stainproofing decorative material |
| CN102041685A (en) * | 2010-11-19 | 2011-05-04 | 鲁泰纺织股份有限公司 | Finishing method of fiber product free of cleaning by detergent |
| CN102585145A (en) * | 2012-02-21 | 2012-07-18 | 黑龙江泰纳科技发展有限责任公司 | Three-protection anti-microbial finishing agent and preparation method thereof |
| CN105113210A (en) * | 2015-09-07 | 2015-12-02 | 江苏阳光股份有限公司 | Method for treating fragrant easy-care shirt easy to decontaminate |
| CN105133294A (en) * | 2015-09-07 | 2015-12-09 | 江苏阳光股份有限公司 | Soil-release non-ironing all cotton shirt processing method |
| CN108547152A (en) * | 2018-04-27 | 2018-09-18 | 东华大学 | The preparation method of the easy decontamination flexibility cotton textile of wash resistant moisturizing |
| CN111434847A (en) * | 2019-01-11 | 2020-07-21 | 东丽纤维研究所（中国）有限公司 | Hydrophilic soil release fabric |
-
2021
- 2021-02-02 CN CN202110141426.9A patent/CN112921662A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004017617A (en) * | 2002-06-20 | 2004-01-22 | Toppan Printing Co Ltd | Stainproofing decorative material |
| CN102041685A (en) * | 2010-11-19 | 2011-05-04 | 鲁泰纺织股份有限公司 | Finishing method of fiber product free of cleaning by detergent |
| CN102585145A (en) * | 2012-02-21 | 2012-07-18 | 黑龙江泰纳科技发展有限责任公司 | Three-protection anti-microbial finishing agent and preparation method thereof |
| CN105113210A (en) * | 2015-09-07 | 2015-12-02 | 江苏阳光股份有限公司 | Method for treating fragrant easy-care shirt easy to decontaminate |
| CN105133294A (en) * | 2015-09-07 | 2015-12-09 | 江苏阳光股份有限公司 | Soil-release non-ironing all cotton shirt processing method |
| CN108547152A (en) * | 2018-04-27 | 2018-09-18 | 东华大学 | The preparation method of the easy decontamination flexibility cotton textile of wash resistant moisturizing |
| CN111434847A (en) * | 2019-01-11 | 2020-07-21 | 东丽纤维研究所（中国）有限公司 | Hydrophilic soil release fabric |
Non-Patent Citations (5)
| Title |
|---|
| 强涛涛: "《合成革化学品》", 31 July 2016, 中国轻工业出版社 * |
| 王国建 等: "《功能高分子材料》", 31 January 2010, 同济大学出版社 * |
| 王际平: "《中国纺织品整理及进展（第二卷）》", 31 May 2015, 中国轻工业出版社 * |
| 纪惠军: "《印染技术》", 31 July 2012, 东华大学出版社 * |
| 马世昌: "《化学物质辞典》", 30 April 1999, 陕西科学技术出版社 * |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113235292A (en) * | 2021-06-28 | 2021-08-10 | 江南大学 | Delayed baking non-ironing finishing process for cotton fabric |
| WO2023273800A1 (en) * | 2021-06-28 | 2023-01-05 | 江南大学 | Delayed baking-based non-ironing finishing process for cotton fabric |
| US11718942B2 (en) | 2021-06-28 | 2023-08-08 | Jiangnan University | Delayed-cure durable press finishing technology for cotton fabrics |
| CN113981685A (en) * | 2021-10-18 | 2022-01-28 | 鲁丰织染有限公司 | Processing method of non-ironing waterproof sanded fabric |
| CN114045670A (en) * | 2021-11-17 | 2022-02-15 | 鲁丰织染有限公司 | Short-flow processing technology for environment-friendly fluorine-free easy-to-clean non-ironing finishing |
| CN114045670B (en) * | 2021-11-17 | 2023-08-04 | 鲁丰织染有限公司 | Short-process processing technology for environment-friendly fluorine-free easy-to-decontaminate wash-and-wear finishing |
| CN114411316A (en) * | 2021-12-17 | 2022-04-29 | 鲁泰纺织股份有限公司 | Preparation method of cotton/spandex single jersey knitted shirt fabric |
| CN114411316B (en) * | 2021-12-17 | 2023-11-24 | 鲁泰纺织股份有限公司 | Preparation method of cotton/spandex jersey knitted shirt fabric |
| CN114808450A (en) * | 2022-03-22 | 2022-07-29 | 鲁丰织染有限公司 | Environment-friendly processing technology for improving easy-to-decontaminate performance of resin finishing |
| CN114808450B (en) * | 2022-03-22 | 2023-08-18 | 鲁丰织染有限公司 | Environment-friendly processing technology for improving soil release performance of resin finishing |
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