CN112479591A - Sacrificial red glaze and preparation method thereof - Google Patents
Sacrificial red glaze and preparation method thereof Download PDFInfo
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- CN112479591A CN112479591A CN202011544313.5A CN202011544313A CN112479591A CN 112479591 A CN112479591 A CN 112479591A CN 202011544313 A CN202011544313 A CN 202011544313A CN 112479591 A CN112479591 A CN 112479591A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/14—Glass frit mixtures having non-frit additions, e.g. opacifiers, colorants, mill-additions
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C8/00—Enamels; Glazes; Fusion seal compositions being frit compositions having non-frit additions
- C03C8/02—Frit compositions, i.e. in a powdered or comminuted form
- C03C8/10—Frit compositions, i.e. in a powdered or comminuted form containing lead
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
- C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
- C04B41/85—Coating or impregnation with inorganic materials
- C04B41/86—Glazes; Cold glazes
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- Geochemistry & Mineralogy (AREA)
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Abstract
The invention relates to a worship red glaze which comprises the following components in parts by weight: 16 parts of a frit, 8-12 parts of cryolite, 0.3-0.8 part of malachite, 2-5 parts of yellow paraffin, 1.2-1.6 parts of copperflower, 13-19 parts of half-slope soil, 5-9 parts of red mud, 6-10 parts of dolomite and 3-7 parts of serpentine, wherein the frit comprises the following components in parts by weight: 10-15 parts of pyrophyllite, 9-13 parts of rhyolite, 0.1-0.4 part of galena, 8-13 parts of quartz and 0.5-0.7 part of manganese dioxide. The invention also relates to a preparation method of the sacrificial red glaze, and a product prepared by the sacrificial red glaze has the advantages that the glaze is sacrificial red, the color is delicate but not gorgeous, the red is transparent and purple, the color is stable, and the glaze has no crack, floating light and flowing phenomenon and elegant atmosphere; and the sintering rate reaches 82 percent.
Description
Technical Field
The invention relates to the field of ceramic glaze, in particular to a worship red glaze and a preparation method thereof.
Background
The best sacrificial pearl is the outstanding traditional ceramic product in China, and is a bright pearl in high-temperature colored glaze. Since ancient times, worship with red wine is one of the most difficult varieties to burn. The literature states that: the fact that the bright generation made bright red is not true. Although successful worship and worship are good in the early stages of Ming dynasty, the worship and worship cannot be brought out frequently by the third generation of Zheng De, Jiajing and Longqing. The pottery books were loaded: ' scarlet soil is not in detail in where, burning and making red ware, and is just absolutely Jiajing, so Jiajing 26 years (Gongyuan 1571 year), Zhao Shanli and Xianhong porcelain, all defended from Shixu Tu to change the case of alum red. So it is also a common practice that ancient palace cannot successfully make high-temperature copper red but only needs to make low-temperature iron red by burning, so that it can also be seen why the worship red is so famous and precious. And the ancient people prepares the worship red, which means that the original is not to be wonderful, and the formulas like coral, agate, gypsum rubrum, beads and burnt material … … are even really mixed with gold, but the burning rate is still very low, so that one or two worship red can be obtained by the folk law, namely the kiln fire of hundreds of furnaces. Even today with the development of science and technology, the fiesta glaze still has many problems to be researched and solved by people.
Disclosure of Invention
The invention aims to solve the problems and provides a sacrificial red glaze and a preparation method thereof.
The purpose of the invention is realized by the following technical scheme:
the provided sacrificial red glaze comprises the following components in parts by weight: 16 parts of frit, 8-12 parts of cryolite, 0.3-0.8 part of malachite, 2-5 parts of yellow paraffin, 1.2-1.6 parts of copperflower, 13-19 parts of half-slope soil, 5-9 parts of red mud, 6-10 parts of dolomite and 3-7 parts of serpentine, wherein the frit comprises the following components in parts by weight: 10-15 parts of pyrophyllite, 9-13 parts of rhyolite, 0.1-0.4 part of galena, 8-13 parts of quartz and 0.5-0.7 part of manganese dioxide.
Preferably, the red glaze for sacrificial rites consists of the following components in parts by weight: 16 parts of frit, 10 parts of cryolite, 0.5 part of malachite, 3 parts of yellow paraffin, 1.4 parts of copperflower, 17 parts of half-slope soil, 7 parts of red mud, 8 parts of dolomite and 6 parts of serpentine, wherein the frit comprises the following components in parts by weight: 12 parts of pyrophyllite, 11 parts of rhyolite, 0.3 part of galena, 10 parts of quartz and 0.6 part of manganese dioxide.
The invention also provides a preparation method of the sacrificial red glaze, which comprises the following steps:
s1, weighing according to a frit formula, uniformly mixing, melting at 1380-1450 ℃, and performing water quenching to obtain a frit for later use;
s2, weighing according to the sacrificial red glaze formula, and mixing the following materials: ball: water = 1: 2: grinding for 3h by using a 0.7 ball mill, and after the ground product is discharged, sieving the product with a 300-mesh sieve to obtain glaze slurry, wherein the sieved residue is 0.1 percent;
and S3, glazing the green body twice, glazing in a glaze dipping mode for the first time, wherein the glazing thickness is 0.2mm, naturally drying after glaze dipping, glazing in a glaze spraying mode for the second time, and firing in a tunnel kiln to obtain the red sacrificial glaze, wherein the glazing thickness is 0.1 mm.
Further, the firing process described in S3 is as follows: gradually raising the temperature from room temperature to 800 ℃ and preserving the temperature for 20 minutes in an oxidizing atmosphere when the temperature is 2 hours; then the mixture is transferred to reducing atmosphere and is gradually heated to 1300 ℃, the use time is 5 hours, and the heat preservation is carried out for 1 hour; gradually cooling to 400 deg.C, taking 3 hr, keeping the temperature for 30 min, and naturally cooling to room temperature.
Compared with the prior art, the invention has the following beneficial effects:
the invention provides a sacrificial red glaze, and a product prepared from the sacrificial red glaze, wherein the glaze is sacrificial red, has delicate and not gorgeous color, is transparent purple in red, has stable color and luster, and is free from cracks, floating light and flowing phenomena, thereby being elegant; and the sintering rate reaches 82 percent.
Detailed Description
The present invention will be further described with reference to the following examples.
Example 1
The embodiment discloses a sacrificial red glaze, which comprises the following preparation steps:
s1, weighing according to a frit formula: 12 parts of pyrophyllite, 11 parts of rhyolite, 0.3 part of galena, 10 parts of quartz and 0.6 part of manganese dioxide, uniformly mixing, melting at 1400 ℃, and performing water quenching to obtain a fusion cake for later use;
s2, weighing according to the formula of the worship red glaze: 16 parts of frit, 10 parts of cryolite, 0.5 part of malachite, 3 parts of yellow paraffin, 1.4 parts of copperflower, 17 parts of half-slope soil, 7 parts of red mud, 8 parts of dolomite and 6 parts of serpentine, and the method comprises the following steps: ball: water = 1: 2: grinding for 3h by using a 0.7 ball mill, and after the ground product is discharged, sieving the product with a 300-mesh sieve to obtain glaze slurry, wherein the sieved residue is 0.1 percent;
s3, glazing the green body twice, glazing in a glaze dipping mode for the first time, wherein the glazing thickness is 0.2mm, naturally drying after glaze dipping, glazing in a glaze spraying mode for the second time, and the glazing thickness is 0.1mm, and then firing in a tunnel kiln: the firing process of S3 is as follows: gradually raising the temperature from room temperature to 800 ℃ and preserving the temperature for 20 minutes in an oxidizing atmosphere when the temperature is 2 hours; then the mixture is transferred to reducing atmosphere and is gradually heated to 1300 ℃, the use time is 5 hours, and the heat preservation is carried out for 1 hour; gradually cooling to 400 ℃, taking 3 hours, preserving the heat for 30 minutes, and naturally cooling to room temperature to obtain the red glaze for the sacrifice. The yield is 85.2%.
Example 2
The embodiment discloses a sacrificial red glaze, which comprises the following preparation steps:
s1, weighing according to a frit formula: 10 parts of pyrophyllite, 10 parts of rhyolite, 0.2 part of galena, 12 parts of quartz and 0.5 part of manganese dioxide, uniformly mixing, melting at 1380 ℃, and performing water quenching to obtain a fusion cake for later use;
s2, weighing according to the formula of the worship red glaze: 16 parts of frit, 8 parts of cryolite, 0.3 part of malachite, 5 parts of yellow paraffin, 1.2 parts of copperflower, 19 parts of half-slope soil, 5 parts of red mud, 10 parts of dolomite and 5 parts of serpentine, and the weight parts are as follows: ball: water = 1: 2: grinding for 3h by using a 0.7 ball mill, and after the ground product is discharged, sieving the product with a 300-mesh sieve to obtain glaze slurry, wherein the sieved residue is 0.1 percent;
s3, glazing the green body twice, glazing in a glaze dipping mode for the first time, wherein the glazing thickness is 0.2mm, naturally drying after glaze dipping, glazing in a glaze spraying mode for the second time, and the glazing thickness is 0.1mm, and then firing in a tunnel kiln: the firing process of S3 is as follows: gradually raising the temperature from room temperature to 800 ℃ and preserving the temperature for 20 minutes in an oxidizing atmosphere when the temperature is 2 hours; then the mixture is transferred to reducing atmosphere and is gradually heated to 1300 ℃, the use time is 5 hours, and the heat preservation is carried out for 1 hour; gradually cooling to 400 ℃, taking 3 hours, preserving the heat for 30 minutes, and naturally cooling to room temperature to obtain the red glaze for the sacrifice. The yield is 82.6%.
Example 3
The embodiment discloses a sacrificial red glaze, which comprises the following preparation steps:
s1, weighing according to a frit formula: 15 parts of pyrophyllite, 13 parts of rhyolite, 0.4 part of galena, 9 parts of quartz and 0.7 part of manganese dioxide, uniformly mixing, melting at 1450 ℃, and performing water quenching to obtain a fusion cake for later use;
s2, weighing according to the formula of the worship red glaze: 16 parts of frit, 12 parts of cryolite, 0.6 part of malachite, 4 parts of yellow paraffin, 1.5 parts of copperleaf, 16 parts of half-slope soil, 8 parts of red mud, 9 parts of dolomite and 5 parts of serpentine, and the weight parts are as follows: ball: water = 1: 2: grinding for 3h by using a 0.7 ball mill, and after the ground product is discharged, sieving the product with a 300-mesh sieve to obtain glaze slurry, wherein the sieved residue is 0.1 percent;
s3, glazing the green body twice, glazing in a glaze dipping mode for the first time, wherein the glazing thickness is 0.2mm, naturally drying after glaze dipping, glazing in a glaze spraying mode for the second time, and the glazing thickness is 0.1mm, and then firing in a tunnel kiln: the firing process of S3 is as follows: gradually raising the temperature from room temperature to 800 ℃ and preserving the temperature for 20 minutes in an oxidizing atmosphere when the temperature is 2 hours; then the mixture is transferred to reducing atmosphere and is gradually heated to 1300 ℃, the use time is 5 hours, and the heat preservation is carried out for 1 hour; gradually cooling to 400 ℃, taking 3 hours, preserving the heat for 30 minutes, and naturally cooling to room temperature to obtain the red glaze for the sacrifice. The yield is 82.8%.
Comparative example 1
The formula of the raw materials is adjusted, the preparation process is consistent with that of the example 1, and the steps are as follows:
s1, weighing according to a frit formula: 18 parts of pyrophyllite, 8 parts of rhyolite, 0.5 part of galena, 5 parts of quartz and 0.1 part of manganese dioxide, uniformly mixing, melting at 1400 ℃, and performing water quenching to obtain a fusion cake for later use;
s2, weighing according to the formula of the worship red glaze: 16 parts of frit, 6 parts of cryolite, 0.3 part of malachite, 10 parts of yellow paraffin, 1 part of copperleaf, 22 parts of half-slope soil, 12 parts of red mud, 12 parts of dolomite and 2 parts of serpentine, and the preparation method comprises the following steps: ball: water = 1: 2: grinding for 3h by using a 0.7 ball mill, and after the ground product is discharged, sieving the product with a 300-mesh sieve to obtain glaze slurry, wherein the sieved residue is 0.1 percent;
s3, glazing the green body twice, glazing in a glaze dipping mode for the first time, wherein the glazing thickness is 0.2mm, naturally drying after glaze dipping, glazing in a glaze spraying mode for the second time, and the glazing thickness is 0.1mm, and then firing in a tunnel kiln: the firing process of S3 is as follows: gradually raising the temperature from room temperature to 800 ℃ and preserving the temperature for 20 minutes in an oxidizing atmosphere when the temperature is 2 hours; then the mixture is transferred to reducing atmosphere and is gradually heated to 1300 ℃, the use time is 5 hours, and the heat preservation is carried out for 1 hour; gradually cooling to 400 deg.C, taking 3 hr, keeping the temperature for 30 min, and naturally cooling to room temperature.
Comparative example 2
Adjusting the formula and the preparation process of the raw materials, and comprising the following steps:
s1, weighing according to a frit formula: 10 parts of pyrophyllite, 9 parts of rhyolite, 14 parts of quartz and 0.7 part of manganese dioxide, uniformly mixing, melting at 1200 ℃, and performing water quenching to obtain a fusion cake for later use;
s2, weighing according to the formula of the worship red glaze: 16 parts of clinker, 15 parts of cryolite, 2 parts of yellow wax stone, 1.5 parts of copper flower, 18 parts of half slope soil, 10 parts of red mud, 6 parts of dolomite and 4 parts of serpentine, and the weight parts are as follows: ball: water = 1: 2: grinding for 3h by using a 0.65 ball mill, and after the ground product is discharged, sieving the residue by using a 250-mesh sieve to obtain glaze slurry;
s3, glazing the green body twice, glazing in a glaze dipping mode for the first time, wherein the glazing thickness is 0.2mm, naturally drying after glaze dipping, glazing in a glaze spraying mode for the second time, and the glazing thickness is 0.1mm, and then firing in a tunnel kiln: the firing process of S3 is as follows: gradually increasing the temperature from the room temperature to 600 ℃, taking 3 hours, and preserving the heat for 20 minutes; transferring to reducing atmosphere and gradually heating to 1300 ℃, wherein the use time is 5 hours; gradually cooling to 400 deg.C, taking 3 hr, keeping the temperature for 30 min, and naturally cooling to room temperature.
Comparative example 3
Adjusting the formula and the preparation process of the raw materials, and comprising the following steps:
s1, weighing according to a frit formula: 10 parts of pyrophyllite, 15 parts of rhyolite, 0.1 part of galena and 14 parts of quartz, uniformly mixing, melting at the temperature of 1480 ℃, and performing water quenching to obtain a fusion cake for later use;
s2, weighing according to the formula of the worship red glaze: 16 parts of frit, 16 parts of cryolite, 1 part of malachite, 4 parts of yellow paraffin, 0.8 part of copperflower, 12 parts of half-slope soil, 5 parts of red mud, 12 parts of dolomite and 6 parts of serpentine, and the preparation method comprises the following steps: ball: water = 1: 2: grinding for 3h by using a ball mill at 0.8, and sieving with a 300-mesh sieve to obtain glaze slurry, wherein the sieved residue is 0.08 percent after the glaze slurry is discharged;
s3, glazing the green body in a glaze dipping mode, wherein the glazing thickness is 0.3mm, and then firing in a tunnel kiln: the firing process of S3 is as follows: gradually increasing the temperature from room temperature to 800 ℃ for 2 hours, gradually increasing the temperature to 1200 ℃ in the oxidation atmosphere, and keeping the temperature for 1 hour for 5 hours; gradually cooling to 300 deg.C, taking 6 hr, and naturally cooling to room temperature.
And (3) evaluating the effect:
the glaze effects obtained by respectively preparing the glaze materials in the embodiments 1 to 3 and the comparative examples 1 to 3 are shown in table 1:
TABLE 1
| Surface condition of glaze layer | Coloring effect of glaze | |
| Example 1 | No crack, floating light and flowing | Deep red worship and purple in red |
| Example 2 | No crack, floating light and flowing | The partial product was slightly darker in color than in example 1 |
| Example 3 | No crack, floating light and flowing | Part of the finished product is slightly brighter than the color of the product in example 1 |
| Comparative example 1 | No crack, floating light and flowing | Is turbid and dark red |
| Comparative example 2 | Slight crack was observed | Is bright purple and has impurities |
| Comparative example 3 | Phenomenon of glaze flow | Is greenish and has impurities |
Experiments show that the ratio of various raw materials, the firing process and the like have great influence on the glaze effect, and the glaze prepared in example 1 has the best effect, the purest color and the highest yield, and is the best example.
Claims (4)
1. The sacrificial red glaze is characterized by comprising the following components in percentage by weight: 16 parts of a frit, 8-12 parts of cryolite, 0.3-0.8 part of malachite, 2-5 parts of yellow paraffin, 1.2-1.6 parts of copperflower, 13-19 parts of half-slope soil, 5-9 parts of red mud, 6-10 parts of dolomite and 3-7 parts of serpentine, wherein the frit comprises the following components in parts by weight: 10-15 parts of pyrophyllite, 9-13 parts of rhyolite, 0.1-0.4 part of galena, 8-13 parts of quartz and 0.5-0.7 part of manganese dioxide.
2. The sacrificial red glaze as recited in claim 1, wherein the sacrificial red glaze comprises the following components in parts by weight: 16 parts of frit, 10 parts of cryolite, 0.5 part of malachite, 3 parts of yellow wax stone, 1.4 parts of copperflower, 17 parts of half-slope soil, 7 parts of red mud, 8 parts of dolomite and 6 parts of serpentine, wherein the frit consists of the following components in parts by weight: 12 parts of pyrophyllite, 11 parts of rhyolite, 0.3 part of galena, 10 parts of quartz and 0.6 part of manganese dioxide.
3. The method for preparing the sacrificial red glaze according to the claim 1 or 2, which is characterized by comprising the following steps:
s1, weighing according to a frit formula, uniformly mixing, melting at 1380-1450 ℃, and performing water quenching to obtain a frit for later use;
s2, weighing according to the sacrificial red glaze formula, and mixing the following materials: ball: water = 1: 2: grinding for 3h by using a 0.7 ball mill, and after the ground product is discharged, sieving the product with a 300-mesh sieve to obtain glaze slurry, wherein the sieved residue is 0.1 percent;
and S3, glazing the green body twice, glazing in a glaze dipping mode for the first time, wherein the glazing thickness is 0.2mm, naturally drying after glaze dipping, glazing in a glaze spraying mode for the second time, and firing in a tunnel kiln to obtain the red sacrificial glaze, wherein the glazing thickness is 0.1 mm.
4. The method for preparing sacrificial red glaze according to claim 1 or 2, wherein the firing process of S3 is as follows: gradually raising the temperature from room temperature to 800 ℃ and preserving the temperature for 20 minutes in an oxidizing atmosphere when the temperature is 2 hours; then the mixture is transferred to reducing atmosphere and is gradually heated to 1300 ℃, the use time is 5 hours, and the heat preservation is carried out for 1 hour; gradually cooling to 400 deg.C, taking 3 hr, keeping the temperature for 30 min, and naturally cooling to room temperature.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117383966A (en) * | 2023-10-18 | 2024-01-12 | 景德镇陶瓷大学 | Red glaze ceramic and its prepn process |
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