CN112379546A - 聚合物分散染料液晶材料、电致变色调光薄膜及制备方法 - Google Patents
聚合物分散染料液晶材料、电致变色调光薄膜及制备方法 Download PDFInfo
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- CN112379546A CN112379546A CN202011324289.4A CN202011324289A CN112379546A CN 112379546 A CN112379546 A CN 112379546A CN 202011324289 A CN202011324289 A CN 202011324289A CN 112379546 A CN112379546 A CN 112379546A
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- liquid crystal
- dye liquid
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- crystal material
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- 239000000463 material Substances 0.000 title claims abstract description 61
- 229920000642 polymer Polymers 0.000 title claims abstract description 52
- 239000000986 disperse dye Substances 0.000 title claims abstract description 32
- 238000002360 preparation method Methods 0.000 title claims abstract description 7
- 239000000975 dye Substances 0.000 claims abstract description 66
- 239000003292 glue Substances 0.000 claims abstract description 45
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 34
- RAXXELZNTBOGNW-UHFFFAOYSA-N imidazole Natural products C1=CNC=N1 RAXXELZNTBOGNW-UHFFFAOYSA-N 0.000 claims abstract description 33
- 229920001187 thermosetting polymer Polymers 0.000 claims abstract description 26
- 239000003822 epoxy resin Substances 0.000 claims abstract description 22
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- 238000001723 curing Methods 0.000 claims description 72
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- 238000000034 method Methods 0.000 claims description 17
- 238000001029 thermal curing Methods 0.000 claims description 16
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- ULKLGIFJWFIQFF-UHFFFAOYSA-N 5K8XI641G3 Chemical compound CCC1=NC=C(C)N1 ULKLGIFJWFIQFF-UHFFFAOYSA-N 0.000 claims description 7
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- 239000006087 Silane Coupling Agent Substances 0.000 claims description 4
- QGBSISYHAICWAH-UHFFFAOYSA-N dicyandiamide Chemical compound NC(N)=NC#N QGBSISYHAICWAH-UHFFFAOYSA-N 0.000 claims description 4
- UWFRVQVNYNPBEF-UHFFFAOYSA-N 1-(2,4-dimethylphenyl)propan-1-one Chemical compound CCC(=O)C1=CC=C(C)C=C1C UWFRVQVNYNPBEF-UHFFFAOYSA-N 0.000 claims description 3
- AHDSRXYHVZECER-UHFFFAOYSA-N 2,4,6-tris[(dimethylamino)methyl]phenol Chemical compound CN(C)CC1=CC(CN(C)C)=C(O)C(CN(C)C)=C1 AHDSRXYHVZECER-UHFFFAOYSA-N 0.000 claims description 3
- HPILSDOMLLYBQF-UHFFFAOYSA-N 2-[1-(oxiran-2-ylmethoxy)butoxymethyl]oxirane Chemical compound C1OC1COC(CCC)OCC1CO1 HPILSDOMLLYBQF-UHFFFAOYSA-N 0.000 claims description 3
- 125000002723 alicyclic group Chemical group 0.000 claims description 3
- 239000004841 bisphenol A epoxy resin Substances 0.000 claims description 3
- AOBIOSPNXBMOAT-UHFFFAOYSA-N 2-[2-(oxiran-2-ylmethoxy)ethoxymethyl]oxirane Chemical compound C1OC1COCCOCC1CO1 AOBIOSPNXBMOAT-UHFFFAOYSA-N 0.000 claims description 2
- LXBGSDVWAMZHDD-UHFFFAOYSA-N 2-methyl-1h-imidazole Chemical compound CC1=NC=CN1 LXBGSDVWAMZHDD-UHFFFAOYSA-N 0.000 claims description 2
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- 229910052724 xenon Inorganic materials 0.000 description 3
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- 238000012546 transfer Methods 0.000 description 2
- PSGCQDPCAWOCSH-UHFFFAOYSA-N (4,7,7-trimethyl-3-bicyclo[2.2.1]heptanyl) prop-2-enoate Chemical compound C1CC2(C)C(OC(=O)C=C)CC1C2(C)C PSGCQDPCAWOCSH-UHFFFAOYSA-N 0.000 description 1
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- WOBHKFSMXKNTIM-UHFFFAOYSA-N Hydroxyethyl methacrylate Chemical compound CC(=C)C(=O)OCCO WOBHKFSMXKNTIM-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 238000007259 addition reaction Methods 0.000 description 1
- 125000000129 anionic group Chemical group 0.000 description 1
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- 125000000524 functional group Chemical group 0.000 description 1
- LNEPOXFFQSENCJ-UHFFFAOYSA-N haloperidol Chemical compound C1CC(O)(C=2C=CC(Cl)=CC=2)CCN1CCCC(=O)C1=CC=C(F)C=C1 LNEPOXFFQSENCJ-UHFFFAOYSA-N 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
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- 125000006850 spacer group Chemical group 0.000 description 1
- 238000009281 ultraviolet germicidal irradiation Methods 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/13—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on liquid crystals, e.g. single liquid crystal display cells
- G02F1/133—Constructional arrangements; Operation of liquid crystal cells; Circuit arrangements
- G02F1/1333—Constructional arrangements; Manufacturing methods
- G02F1/1334—Constructional arrangements; Manufacturing methods based on polymer dispersed liquid crystals, e.g. microencapsulated liquid crystals
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K19/00—Liquid crystal materials
- C09K19/04—Liquid crystal materials characterised by the chemical structure of the liquid crystal components, e.g. by a specific unit
- C09K19/38—Polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K9/00—Tenebrescent materials, i.e. materials for which the range of wavelengths for energy absorption is changed as a result of excitation by some form of energy
- C09K9/02—Organic tenebrescent materials
-
- G—PHYSICS
- G02—OPTICS
- G02F—OPTICAL DEVICES OR ARRANGEMENTS FOR THE CONTROL OF LIGHT BY MODIFICATION OF THE OPTICAL PROPERTIES OF THE MEDIA OF THE ELEMENTS INVOLVED THEREIN; NON-LINEAR OPTICS; FREQUENCY-CHANGING OF LIGHT; OPTICAL LOGIC ELEMENTS; OPTICAL ANALOGUE/DIGITAL CONVERTERS
- G02F1/00—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics
- G02F1/01—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour
- G02F1/15—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect
- G02F1/1514—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect characterised by the electrochromic material, e.g. by the electrodeposited material
- G02F1/1516—Devices or arrangements for the control of the intensity, colour, phase, polarisation or direction of light arriving from an independent light source, e.g. switching, gating or modulating; Non-linear optics for the control of the intensity, phase, polarisation or colour based on an electrochromic effect characterised by the electrochromic material, e.g. by the electrodeposited material comprising organic material
- G02F1/15165—Polymers
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K2211/00—Chemical nature of organic luminescent or tenebrescent compounds
- C09K2211/14—Macromolecular compounds
- C09K2211/1441—Heterocyclic
- C09K2211/145—Heterocyclic containing oxygen as the only heteroatom
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- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Nonlinear Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Dispersion Chemistry (AREA)
- Mathematical Physics (AREA)
- Liquid Crystal (AREA)
- Electrochromic Elements, Electrophoresis, Or Variable Reflection Or Absorption Elements (AREA)
Abstract
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CN202011324289.4A CN112379546B (zh) | 2020-11-23 | 2020-11-23 | 聚合物分散染料液晶材料、电致变色调光薄膜及制备方法 |
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CN202011324289.4A CN112379546B (zh) | 2020-11-23 | 2020-11-23 | 聚合物分散染料液晶材料、电致变色调光薄膜及制备方法 |
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CN112379546A true CN112379546A (zh) | 2021-02-19 |
CN112379546B CN112379546B (zh) | 2022-08-19 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113265219A (zh) * | 2021-06-16 | 2021-08-17 | 深圳市撒比斯科技有限公司 | 一种pdlc电致变色薄膜用uv胶黏剂及其制备方法 |
CN114654846A (zh) * | 2022-02-23 | 2022-06-24 | 深圳天珑无线科技有限公司 | 一种复合材料及其制作方法、电子设备 |
CN114871081A (zh) * | 2022-06-02 | 2022-08-09 | 福耀玻璃工业集团股份有限公司 | 导电胶层的制备方法、调光组件的制备方法和调光玻璃的制备方法 |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1985004262A1 (en) * | 1984-03-19 | 1985-09-26 | Kent State University | Light modulating material comprising a liquid crystal dispersion in a synthetic resin matrix |
WO2004005426A1 (ja) * | 2002-07-05 | 2004-01-15 | Asahi Glass Company, Limited | 調光素子およびその製造方法 |
CN101735564A (zh) * | 2009-12-22 | 2010-06-16 | 上海康达化工有限公司 | 一种风力发电叶片用真空灌注树脂及其制备方法 |
CN101776819A (zh) * | 2009-01-14 | 2010-07-14 | 北京众智同辉科技有限公司 | 一种高清亮点的电致液晶雾化玻璃 |
CN103885233A (zh) * | 2012-12-21 | 2014-06-25 | 北京众智同辉科技有限公司 | 一种彩色聚合物分散型液晶薄膜的制备方法 |
CN104395371A (zh) * | 2012-06-07 | 2015-03-04 | 日本化药株式会社 | 环氧树脂组合物及其固化物、以及固化性树脂组合物 |
CN106019681A (zh) * | 2016-07-15 | 2016-10-12 | 深圳市华星光电技术有限公司 | 透明液晶显示装置及其制作方法 |
CN107703667A (zh) * | 2017-09-29 | 2018-02-16 | 西京学院 | 一种彩色聚合物分散液晶薄膜及其制备方法 |
-
2020
- 2020-11-23 CN CN202011324289.4A patent/CN112379546B/zh active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO1985004262A1 (en) * | 1984-03-19 | 1985-09-26 | Kent State University | Light modulating material comprising a liquid crystal dispersion in a synthetic resin matrix |
WO2004005426A1 (ja) * | 2002-07-05 | 2004-01-15 | Asahi Glass Company, Limited | 調光素子およびその製造方法 |
CN101776819A (zh) * | 2009-01-14 | 2010-07-14 | 北京众智同辉科技有限公司 | 一种高清亮点的电致液晶雾化玻璃 |
CN101735564A (zh) * | 2009-12-22 | 2010-06-16 | 上海康达化工有限公司 | 一种风力发电叶片用真空灌注树脂及其制备方法 |
CN104395371A (zh) * | 2012-06-07 | 2015-03-04 | 日本化药株式会社 | 环氧树脂组合物及其固化物、以及固化性树脂组合物 |
CN103885233A (zh) * | 2012-12-21 | 2014-06-25 | 北京众智同辉科技有限公司 | 一种彩色聚合物分散型液晶薄膜的制备方法 |
CN106019681A (zh) * | 2016-07-15 | 2016-10-12 | 深圳市华星光电技术有限公司 | 透明液晶显示装置及其制作方法 |
CN107703667A (zh) * | 2017-09-29 | 2018-02-16 | 西京学院 | 一种彩色聚合物分散液晶薄膜及其制备方法 |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN113265219A (zh) * | 2021-06-16 | 2021-08-17 | 深圳市撒比斯科技有限公司 | 一种pdlc电致变色薄膜用uv胶黏剂及其制备方法 |
CN113265219B (zh) * | 2021-06-16 | 2023-03-14 | 深圳市撒比斯科技有限公司 | 一种pdlc电致变色薄膜用uv胶黏剂及其制备方法 |
CN114654846A (zh) * | 2022-02-23 | 2022-06-24 | 深圳天珑无线科技有限公司 | 一种复合材料及其制作方法、电子设备 |
CN114871081A (zh) * | 2022-06-02 | 2022-08-09 | 福耀玻璃工业集团股份有限公司 | 导电胶层的制备方法、调光组件的制备方法和调光玻璃的制备方法 |
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Effective date of registration: 20221130 Address after: 519000 room 111, 1st floor, No.6 workshop, No.9 Jinzhu Road, Tangjiawan Town, Zhuhai City, Guangdong Province Patentee after: ZHUHAI SINGYES NEW MATERIALS TECHNOLOGY Co.,Ltd. Patentee after: Shuifa Xingye energy (Zhuhai) Co.,Ltd. Address before: 519085 room 111, 1st floor, No.6 workshop, No.9 Jinzhu Road, Tangjiawan Town, Xiangzhou District, Zhuhai City, Guangdong Province Patentee before: ZHUHAI SINGYES NEW MATERIALS TECHNOLOGY Co.,Ltd. |
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CP03 | Change of name, title or address |
Address after: 519000 room 111, 1st floor, No.6 workshop, No.9 Jinzhu Road, Tangjiawan Town, Zhuhai City, Guangdong Province Patentee after: Zhuhai Shuifa Xingye New Materials Technology Co.,Ltd. Country or region after: China Patentee after: Shuifa Xingye energy (Zhuhai) Co.,Ltd. Address before: 519000 room 111, 1st floor, No.6 workshop, No.9 Jinzhu Road, Tangjiawan Town, Zhuhai City, Guangdong Province Patentee before: ZHUHAI SINGYES NEW MATERIALS TECHNOLOGY Co.,Ltd. Country or region before: China Patentee before: Shuifa Xingye energy (Zhuhai) Co.,Ltd. |