CN112245382A - Skin-smoothing scrub essence and preparation method thereof - Google Patents
Skin-smoothing scrub essence and preparation method thereof Download PDFInfo
- Publication number
- CN112245382A CN112245382A CN201910595502.6A CN201910595502A CN112245382A CN 112245382 A CN112245382 A CN 112245382A CN 201910595502 A CN201910595502 A CN 201910595502A CN 112245382 A CN112245382 A CN 112245382A
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- China
- Prior art keywords
- essence
- skin
- scrub
- parts
- frosted
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention relates to the technical field of skin care products, and particularly relates to a skin smoothing frosted essence and a preparation method thereof, wherein the skin smoothing frosted essence comprises the following raw materials in parts by weight: 10-15 parts of snail essence, 0.1-1 part of scrub particles, 0.5-1 part of polypeptide composition, 1-5 parts of natural scrub agent, 1-5 parts of auxiliary scrub agent, 0.1-3 parts of lactobacillus acidophilus, 1-5 parts of centella asiatica extract, 5-10 parts of mother chrysanthemum extract, 5-10 parts of aloe extract, 20-30 parts of deionized water, 0.01-0.5 part of preservative, 0.01-1 part of chelating agent and 10-15 parts of humectant. The frosted essence disclosed by the invention is simple in raw materials, mild and non-irritant, and has the effects of promoting blood circulation, improving skin metabolism, removing free radicals, repairing damaged cells, expanding skin pores, supplementing cell nutrients, improving cellular immunity, fading fine wrinkles, improving skin brightness and enabling skin to be tender, smooth and elastic by adopting multiple plant extracts, frosted particles and a natural frosting agent in a synergistic manner.
Description
Technical Field
The invention relates to the technical field of skin care products, and particularly relates to a polishing essence for smoothing skin and a preparation method thereof.
Background
With aging, prolonged exposure to adverse environmental factors or malnutrition, changes in the visual appearance, physical characteristics and physiological functions of the skin, which are clinically manifested by rough skin, dryness, increased sensitivity and fragility, loose skin, decreased elasticity, increased wrinkles, atrophy of the skin, increased dermal transparency, and lightening of the skin, but generally maintain its overall geometric appearance, often in a grayish white color. These are closely related to aging, hypometabolism, long-term exposure to adverse environmental factors or malnutrition. In order to improve the phenomena of rough skin, water shortage and hard skin, the cutin removing product is used for removing the bad cells in the old cortical agent cortex on the skin in a massaging way, promoting the growth of new cells, removing impurities and increasing the absorption of subsequent care products.
Disclosure of Invention
In order to overcome the defects and shortcomings in the prior art, the invention aims to provide the scrub essence for smoothing the skin, the phase structure of the essence is stable, the pH value is within the range of 6.0-7.5, the scrub essence is close to the weak acid environment of the skin, the scrub essence has no stimulation to the skin, the added scrub particles and the natural scrub can effectively clean the skin, and the scrub essence is matched with various extracts and humectants to effectively enable the skin to be moisturized, moistened and elastic, so that the scrub essence has the effects of smoothing and tendering the skin.
The invention also aims to provide a preparation method of the scrub essence for smoothing skin, the preparation method is easy to operate, convenient to control and low in production cost, and can be used for large-scale production, and the prepared scrub essence can effectively moisturize, moisten and have elasticity to skin and has the effect of smoothing and tendering skin.
The purpose of the invention is realized by the following technical scheme: the skin-smoothing scrub essence comprises the following raw materials in parts by weight:
the conductivity of the deionized water is less than 0.32 mu S/cm, and the pH value is 6-7.
The essence is prepared by adopting the raw materials, the prepared essence is stable in phase structure, the pH value is in the range of 6.0-7.5, the pH value is close to the weak acid environment of skin, the skin is not stimulated, the added frosted particles and natural frosting agent can effectively clean the skin, and the skin can be effectively moisturized, moistened and elastic by matching with various extracts and humectants, so that the skin is smooth and tender; the centella asiatica extract can promote skin collagen regeneration, enhance cell basal layer cell activity, keep skin elasticity, compactness and oxidation resistance, inhibit free radical activity, regulate skin immunity, lighten melanin pigmentation and renew skin cell regeneration; the moisture retention of the skin is increased, and skin cells are activated and renewed; anti-allergy and protection function, and skin protection from external damage; the chamomile extract has biological activities of antibiosis, antioxidation, anti-inflammation, relieving, anti-allergy and the like, can intensively replenish water, deeply purify, eliminate fine wrinkles, make skin moist and enjoy, and has attractive luster; in addition, the aloe extract can make the essence astringe, soften, moisturize, diminish inflammation, bleach, relieve sclerosis and keratinization, improve scar, prevent wrinkle, pouch and skin laxity, and keep skin moist and tender when applied to skin.
Preferably, each part of the polypeptide composition comprises the following raw materials in parts by weight:
1-5 parts of hexapeptide
6-10 parts of rice peptide
8-12 parts of oat peptide.
The oat peptide is prepared by the following method:
a1, washing oat with clear water and drying, weighing dried oat, grinding, sieving to remove impurities, adding water and homogenizing, and adjusting pH to 2-4 to obtain a homogeneous solution A for later use;
a2, adding acid protease into the step A1 for enzymolysis, adjusting the pH value to 7-8 after enzymolysis, and adding trypsin for enzymolysis to obtain an enzymolysis liquid B for later use;
a3, centrifuging the enzymolysis liquid B obtained in the step A2, taking supernate for filtration, performing ultrafiltration on filtrate by using a hollow fiber membrane, and collecting the filtrate, namely the oat peptide.
The hexapeptide adopted by the polypeptide composition in the raw materials can avoid muscle contraction, reduce the occurrence of dynamic lines, eliminate wrinkles, effectively reorganize collagen elasticity, strengthen the activity of elastin, relax facial lines, smooth wrinkles and improve relaxation; the added rice peptide consists of dipeptide and tripeptide, the molecular weight is less than 1400 daltons, and the rice peptide has the effects of anti-aging, cell regeneration, collagen and ATP synthesis and skin elasticity improvement when added into the essence; in addition, the oat peptide is very similar to Epidermal Growth Factor (EGF), is easy to be absorbed by skin, can accelerate cell proliferation, promote skin metabolism, activate skin, reduce skin roughness, promote collagen synthesis, increase skin elasticity and make skin glowing and beautiful. The prepared oat peptide has good small molecule peptide permeability, enters the skin, plays the role of a moisturizing factor, can soften the skin, lock skin moisture, moisten the skin, and has the effects of removing wrinkles, reducing skin roughness, activating the skin, accelerating cell proliferation and metabolism, keeping the skin in a young state, increasing the content of collagen in the skin, increasing the skin elasticity and having a better moisturizing effect; the pH value of enzymolysis in the step 2) is strictly controlled to be 7-8 in the preparation process, if the pH value is too high, the activity of trypsin is reduced, and if the pH value also inhibits the activity of trypsin.
Preferably, the frosted particles are a mixture of silicone microspheres, polyurethane particles and polyethylene frosted particles in a weight ratio of 0.8-1.2:1.0: 0.8-1.0. More preferably, the silicone microspheres have a particle average particle size of 3 to 15u m and an average oil absorption in the range of 60 to 300mL/100 g.
The organic silicon microspheres adopted by the frosted particles in the raw materials can effectively adsorb redundant grease on the surface layer of the skin, so that the skin can be kept fresh and clean for a long time; the polyethylene abrasive particles can effectively remove aged cutin and deeply clean dirt of skin and pores, and the prepared essence can better remove the aged cutin, relieve sclerosis and keratinization, improve scars and keep the skin moist and tender by coordinating the excellent performances of the three.
Preferably, the natural scrub agent is a mixture consisting of lotus extract, common lophatherum herb extract and water lily extract according to a weight ratio of 0.8:1.0-1.2: 1.0; the auxiliary abrasive is abrasive particles with the particle size of 80-100 meshes, which are prepared by mixing and grinding purslane and fresh bamboo juice according to the weight ratio of 0.8: 1.0-1.2.
The lotus extract and the water lily extract in the natural abrasive disclosed by the invention have very excellent antacid effect, and the addition of the lotus extract and the water lily extract in the essence can reduce harmful active oxygen for skin aging, effectively protect skin cells and ensure healthy and glossy skin; the purslane has the effects of resisting allergy, inflammation and various external irritations to the skin and also has a certain acne removing effect; in addition, fresh bamboo juice can effectively relieve and inhibit forehead raising lines, eye fish tail fine lines and the contraction and activity of peripheral muscles, help muscles relax, and recover the effects of smooth and soft skin elastic tissues.
Preferably, the chelating agent is a mixture of EDTA-2Na and citric acid in a weight ratio of 0.8-1.2: 1.0; the humectant is a mixture of glycerol, sodium hyaluronate and propylene glycol in a weight ratio of 0.8:1.0-1.2: 1.0.
The EDTA-2Na in the chelating agent can adjust the pH value of the frosted essence, namely, the pH value of the essence can be automatically adjusted within a range suitable for a user, so that the skin of the user is protected from strong stimulation; the citric acid can accelerate the renewal of cutin in the using process of the essence, and the renewal of the cutin is beneficial to the falling off of melanin in the skin, the shrinking of pores, the dissolution of blackheads and the like.
A preparation method of a skin-smoothing scrub essence comprises the following steps:
1) weighing snail essence, the polypeptide composition, the humectant and lactobacillus acidophilus according to the weight parts, adding into deionized water, mixing and stirring uniformly, heating to 40-60 ℃, and keeping the temperature for 30-60min to obtain a mixed solution C for later use;
2) weighing the centella extract, the chamomile extract, the aloe extract, the natural scrub agent and the chelating agent according to the weight parts, mixing, heating to 60-80 ℃, stirring, adding the auxiliary scrub agent, uniformly stirring, and then performing ultrasonic treatment for 10-20min under the condition that the frequency is 20000-25000Hz to obtain a mixed solution D for later use;
3) adding the mixed liquor C obtained in the step 1) and the mixed liquor D obtained in the step 2) into an emulsifier, heating to 60-70 ℃, and carrying out homogeneous micro-emulsification reaction for 10-15min to obtain micro-emulsion for later use;
4) adding the frosted particles and the preservative into the microemulsion obtained in the step 3), and uniformly stirring to obtain a frosted essence primary product;
5) sterilizing the primary frosted essence obtained in the step 4) for 40-60min under the ultraviolet ray with the wavelength of 200-250nm to obtain a finished frosted essence.
The preparation method of the scrub essence for smoothing skin of the invention has the advantages that the preparation method is simple in operation steps, convenient to control and high in production efficiency, the synergistic effect among the raw materials can be fully utilized by strictly controlling the adding sequence of the raw materials during preparation, the snail essence, the polypeptide composition, the humectant and the lactobacillus acidophilus are added into deionized water to be mixed, the four materials are fully dissolved with each other, the intersolubility of the four materials is improved, the activities of the polypeptide composition, the lactobacillus acidophilus and the mother chrysanthemum extract are activated on the premise of further mixing the centella asiatica extract, the mother chrysanthemum extract, the aloe extract, the natural scrub agent and the chelating agent, the scrub particles are added after the reaction of all the raw materials is finished to ensure that the scrub particles are uniformly dispersed, and finally the pH value of the essence is adjusted to be closer to the pH value of a human body and to be mildly and easily absorbed, can increase skin water-moistening property.
Wherein, the heating temperature is strictly controlled to be 40-60 ℃ in the step 1), the activities of the polypeptide composition, the humectant and the lactobacillus acidophilus can be effectively improved, so that the snail essence, the polypeptide composition, the humectant and the lactobacillus acidophilus are mutually dissolved, the heating temperature is not easy to be too high, if the heating temperature is too high, the lactobacillus acidophilus can be inactivated, and if the heating temperature is too low, the optimal activity of the lactobacillus acidophilus can not be achieved; and strictly controlling the temperature of the emulsification reaction in the step 3) to be 60-70 ℃, wherein if the temperature is too low, partial substances in the emulsification reaction volatilize, the demulsification phenomenon occurs, and if the temperature is too low, the emulsification is insufficient.
The invention has the beneficial effects that: the essence disclosed by the invention is simple in raw materials, mild and non-irritant, capable of cleaning and protecting skin, removing wrinkles and resisting aging, whitening and beautifying, and capable of protecting facial skin, and has the advantages that multiple plant extracts, frosted particles and natural frosting agents are adopted, so that the blood circulation is promoted, the metabolism of skin newcastle is improved, free radicals are removed, damaged cells are repaired, skin pores are expanded, cell nutrients are supplemented, the permeability of the essence is good, functional components can penetrate into the skin, the cellular immunity is improved, fine lines are reduced, the skin brightness is improved, the skin is tender, smooth and wrinkle-free, and the skin can be white, tender and elastic after long-term use.
The preparation method disclosed by the invention is simple to operate, convenient to control, high in production efficiency and low in production cost, and can be used for large-scale production.
Detailed Description
The present invention will be further described with reference to the following examples for facilitating understanding of those skilled in the art, and the description of the embodiments is not intended to limit the present invention.
Example 1
The skin-smoothing scrub essence comprises the following raw materials in parts by weight:
the conductivity of the deionized water is less than 0.32 mu S/cm, and the pH value is 6.
Each part of the polypeptide composition comprises the following raw materials in parts by weight:
1 portion of hexapeptide
6 portions of rice peptide
8 parts of oat peptide.
The oat peptide is prepared by the following method:
a1, washing oat with clear water and drying, weighing dried oat, grinding, sieving to remove impurities, adding water for homogenizing, and adjusting pH to 2 to obtain a homogeneous solution A for later use;
a2, adding acid protease in the step A1 for enzymolysis, adjusting the pH value to 7 after enzymolysis, and adding trypsin for enzymolysis to obtain an enzymolysis liquid B for later use;
a3, centrifuging the enzymolysis liquid B obtained in the step A2, taking supernate for filtration, performing ultrafiltration on filtrate by using a hollow fiber membrane, and collecting the filtrate, namely the oat peptide.
The frosted particles are a mixture of organosilicon microspheres, polyurethane particles and polyethylene frosted particles according to the weight ratio of 0.8:1.0: 0.8. More preferably, the silicone microspheres have a particle average particle size of 3u m and an average oil absorption in the range of 60mL/100 g.
The natural scrub agent is a mixture consisting of a lotus extract, a phyllostachys pubescens extract and a water lily extract according to a weight ratio of 0.8:1.0: 1.0; the auxiliary abrasive is abrasive particles with the particle size of 80 meshes, which are prepared by mixing and grinding purslane and fresh bamboo juice according to the weight ratio of 0.8: 1.0.
The chelating agent is a mixture of EDTA-2Na and citric acid according to the weight ratio of 0.8: 1.0; the humectant is a mixture of glycerol, sodium hyaluronate and propylene glycol in a weight ratio of 0.8:1.0: 1.0.
A preparation method of a skin-smoothing scrub essence comprises the following steps:
1) weighing snail essence, the polypeptide composition, the humectant and lactobacillus acidophilus according to the weight parts, adding into deionized water, mixing and stirring uniformly, heating to 40 ℃, and keeping the temperature for 30min to obtain a mixed solution C for later use;
2) weighing herba Centellae extract, flos Matricariae Chamomillae extract, Aloe extract, natural scrub agent and chelating agent according to weight parts, mixing, heating to 60 deg.C, stirring, adding auxiliary scrub agent, stirring, and performing ultrasound at 20000Hz for 10min to obtain mixed solution D;
3) adding the mixed liquor C obtained in the step 1) and the mixed liquor D obtained in the step 2) into an emulsifier, heating to 60 ℃, and carrying out homogeneous micro-emulsification reaction for 10min to obtain micro-emulsion for later use;
4) adding the frosted particles and the preservative into the microemulsion obtained in the step 3), and uniformly stirring to obtain a frosted essence primary product;
5) sterilizing the primary polishing essence obtained in the step 4) for 40min under the ultraviolet ray with the wavelength of 200nm to obtain a finished polishing essence.
Example 2
The skin-smoothing scrub essence comprises the following raw materials in parts by weight:
the conductivity of the deionized water is less than 0.32 mu S/cm, and the pH value is 6.3.
Each part of the polypeptide composition comprises the following raw materials in parts by weight:
2 portions of hexapeptide
7 portions of rice peptide
And 9 parts of oat peptide.
The oat peptide is prepared by the following method:
a1, washing oat with clear water and drying, weighing dried oat, grinding, sieving to remove impurities, adding water for homogenizing, and adjusting pH to 2.9 to obtain a homogeneous solution A for later use;
a2, adding acid protease into the step A1 for enzymolysis, adjusting the pH value to 7.3 after enzymolysis, and adding trypsin for enzymolysis to obtain an enzymolysis liquid B for later use;
a3, centrifuging the enzymolysis liquid B obtained in the step A2, taking supernate for filtration, performing ultrafiltration on filtrate by using a hollow fiber membrane, and collecting the filtrate, namely the oat peptide.
The frosted particles are a mixture of organosilicon microspheres, polyurethane particles and polyethylene frosted particles according to the weight ratio of 0.9:1.0: 0.85. More preferably, the silicone microspheres have a particle average particle size of 6u m and an average oil absorption in the range of 100mL/100 g.
The natural scrub agent is a mixture consisting of a lotus extract, a phyllostachys pubescens extract and a water lily extract according to a weight ratio of 0.8:1.05: 1.0; the auxiliary abrasive is abrasive particles with the particle size of 85 meshes, which are prepared by mixing and grinding purslane and fresh bamboo juice according to the weight ratio of 0.8: 1.05.
The chelating agent is a mixture of EDTA-2Na and citric acid in a weight ratio of 0.9: 1.0; the humectant is a mixture of glycerol, sodium hyaluronate and propylene glycol in a weight ratio of 0.8:1.05: 1.0.
A preparation method of a skin-smoothing scrub essence comprises the following steps:
1) weighing snail essence, the polypeptide composition, the humectant and lactobacillus acidophilus according to the weight parts, adding into deionized water, mixing and stirring uniformly, heating to 45 ℃, and keeping the temperature for 38min to obtain a mixed solution C for later use;
2) weighing herba Centellae extract, flos Matricariae Chamomillae extract, Aloe extract, natural scrub agent and chelating agent according to weight parts, mixing, heating to 65 deg.C, stirring, adding auxiliary scrub agent, stirring, and performing ultrasonic treatment at 21750Hz for 13min to obtain mixed solution D;
3) adding the mixed liquor C obtained in the step 1) and the mixed liquor D obtained in the step 2) into an emulsifier, heating to 63 ℃, and carrying out homogeneous micro-emulsification reaction for 12min to obtain micro-emulsion for later use;
4) adding the frosted particles and the preservative into the microemulsion obtained in the step 3), and uniformly stirring to obtain a frosted essence primary product;
5) sterilizing the primary polishing essence obtained in the step 4) for 45min under ultraviolet rays with the wavelength of 215nm to obtain a finished polishing essence.
Example 3
The skin-smoothing scrub essence comprises the following raw materials in parts by weight:
the conductivity of the deionized water is less than 0.32 mu S/cm, and the pH value is 6.5.
Each part of the polypeptide composition comprises the following raw materials in parts by weight:
hexagon 3 portions
8 portions of rice peptide
10 parts of oat peptide.
The oat peptide is prepared by the following method:
a1, washing oat with clear water and drying, weighing dried oat, grinding, sieving to remove impurities, adding water for homogenizing, and adjusting pH to 3 to obtain a homogeneous solution A for later use;
a2, adding acid protease into the step A1 for enzymolysis, adjusting the pH value to 7.5 after enzymolysis, and adding trypsin for enzymolysis to obtain an enzymolysis liquid B for later use;
a3, centrifuging the enzymolysis liquid B obtained in the step A2, taking supernate for filtration, performing ultrafiltration on filtrate by using a hollow fiber membrane, and collecting the filtrate, namely the oat peptide.
The frosted particles are a mixture of organosilicon microspheres, polyurethane particles and polyethylene frosted particles according to the weight ratio of 1.0:1.0: 0.9. More preferably, the silicone microspheres have a particle average particle size of 9u m and an average oil absorption in the range of 180mL/100 g.
The natural scrub agent is a mixture consisting of a lotus extract, a phyllostachys pubescens extract and a water lily extract according to a weight ratio of 0.8:1.1: 1.0; the auxiliary abrasive is abrasive particles with the particle size of 90 meshes, which are prepared by mixing and grinding purslane and fresh bamboo juice according to the weight ratio of 0.8: 1.1.
The chelating agent is a mixture of EDTA-2Na and citric acid according to the weight ratio of 1.0: 1.0; the humectant is a mixture of glycerol, sodium hyaluronate and propylene glycol in a weight ratio of 0.8:1.1: 1.0.
A preparation method of a skin-smoothing scrub essence comprises the following steps:
1) weighing snail essence, the polypeptide composition, the humectant and lactobacillus acidophilus according to the weight parts, adding into deionized water, mixing and stirring uniformly, heating to 50 ℃, and keeping the temperature for 45min to obtain a mixed solution C for later use;
2) weighing herba Centellae extract, flos Matricariae Chamomillae extract, Aloe extract, natural scrub agent and chelating agent according to weight parts, mixing, heating to 70 deg.C, stirring, adding auxiliary scrub agent, stirring, and performing ultrasonic treatment at 22500Hz for 15min to obtain mixed solution D;
3) adding the mixed liquor C obtained in the step 1) and the mixed liquor D obtained in the step 2) into an emulsifier, heating to 65 ℃ to perform homogeneous micro-emulsification reaction for 13min to obtain micro-emulsion for later use;
4) adding the frosted particles and the preservative into the microemulsion obtained in the step 3), and uniformly stirring to obtain a frosted essence primary product;
5) sterilizing the primary polishing essence obtained in the step 4) for 50min under the ultraviolet ray with the wavelength of 225nm to obtain a finished polishing essence.
Example 4
The skin-smoothing scrub essence comprises the following raw materials in parts by weight:
the conductivity of the deionized water is less than 0.32 mu S/cm, and the pH value is 6.8.
Each part of the polypeptide composition comprises the following raw materials in parts by weight:
4 portions of hexapeptide
9 portions of rice peptide
11 parts of oat peptide.
The oat peptide is prepared by the following method:
a1, washing oat with clear water and drying, weighing dried oat, grinding, sieving to remove impurities, adding water for homogenizing, and adjusting pH to 3.5 to obtain a homogeneous solution A for later use;
a2, adding acid protease into the step A1 for enzymolysis, adjusting the pH value to 7.8 after enzymolysis, and adding trypsin for enzymolysis to obtain an enzymolysis liquid B for later use;
a3, centrifuging the enzymolysis liquid B obtained in the step A2, taking supernate for filtration, performing ultrafiltration on filtrate by using a hollow fiber membrane, and collecting the filtrate, namely the oat peptide.
The frosted particles are a mixture of organosilicon microspheres, polyurethane particles and polyethylene frosted particles according to the weight ratio of 1.1:1.0: 0.95. More preferably, the silicone microspheres have a particle average particle size of 12u m and an average oil absorption in the range of 240mL/100 g.
The natural scrub agent is a mixture consisting of a lotus extract, a phyllostachys pubescens extract and a water lily extract according to a weight ratio of 0.8:1.15: 1.0; the auxiliary abrasive is abrasive particles with the particle size of 95 meshes, which are prepared by mixing and grinding purslane and fresh bamboo juice according to the weight ratio of 0.8: 1.15.
The chelating agent is a mixture of EDTA-2Na and citric acid according to the weight ratio of 1.1: 1.0; the humectant is a mixture of glycerol, sodium hyaluronate and propylene glycol in a weight ratio of 0.8:1.15: 1.0.
A preparation method of a skin-smoothing scrub essence comprises the following steps:
1) weighing snail essence, the polypeptide composition, the humectant and lactobacillus acidophilus according to the weight parts, adding into deionized water, mixing and stirring uniformly, heating to 55 ℃, and keeping the temperature for 52min to obtain a mixed solution C for later use;
2) weighing herba Centellae extract, flos Matricariae Chamomillae extract, Aloe extract, natural scrub agent and chelating agent according to weight parts, mixing, heating to 75 deg.C, stirring, adding auxiliary scrub agent, stirring, and performing ultrasonic treatment at 237500Hz for 18min to obtain mixed solution D;
3) adding the mixed solution C obtained in the step 1) and the mixed solution D obtained in the step 2) into an emulsifier, heating to 68 ℃ to perform a homogeneous micro-emulsification reaction for 14min to obtain a micro-emulsion for later use;
4) adding the frosted particles and the preservative into the microemulsion obtained in the step 3), and uniformly stirring to obtain a frosted essence primary product;
5) sterilizing the primary polishing essence obtained in the step 4) for 55min under ultraviolet rays with the wavelength of 240nm to obtain a finished polishing essence.
Example 5
The skin-smoothing scrub essence comprises the following raw materials in parts by weight:
the conductivity of the deionized water is less than 0.32 mu S/cm, and the pH value is 7.
Each part of the polypeptide composition comprises the following raw materials in parts by weight:
hexagon 5 portions
10 portions of rice peptide
12 parts of oat peptide.
The oat peptide is prepared by the following method:
a1, washing oat with clear water and drying, weighing dried oat, grinding, sieving to remove impurities, adding water for homogenizing, and adjusting pH to 4 to obtain a homogeneous solution A for later use;
a2, adding acid protease in the step A1 for enzymolysis, adjusting the pH value to 8 after enzymolysis, and adding trypsin for enzymolysis to obtain an enzymolysis liquid B for later use;
a3, centrifuging the enzymolysis liquid B obtained in the step A2, taking supernate for filtration, performing ultrafiltration on filtrate by using a hollow fiber membrane, and collecting the filtrate, namely the oat peptide.
The frosted particles are a mixture of organosilicon microspheres, polyurethane particles and polyethylene frosted particles according to the weight ratio of 1.2:1.0: 1.0. More preferably, the silicone microspheres have a particle average particle size of 15u m and an average oil absorption in the range of 300mL/100 g.
The natural scrub agent is a mixture consisting of a lotus extract, a phyllostachys pubescens extract and a water lily extract according to a weight ratio of 0.8:1.2: 1.0; the auxiliary abrasive is abrasive particles with the particle size of 100 meshes, which are prepared by mixing and grinding purslane and fresh bamboo juice according to the weight ratio of 0.8: 1.2.
The chelating agent is a mixture of EDTA-2Na and citric acid according to the weight ratio of 1.2: 1.0; the humectant is a mixture of glycerol, sodium hyaluronate and propylene glycol in a weight ratio of 0.8:1.2: 1.0.
A preparation method of a skin-smoothing scrub essence comprises the following steps:
1) weighing snail essence, the polypeptide composition, the humectant and lactobacillus acidophilus according to the weight parts, adding into deionized water, mixing and stirring uniformly, and heating to 60 ℃ and keeping the temperature for 60min to obtain a mixed solution C for later use;
2) weighing herba Centellae extract, flos Matricariae Chamomillae extract, Aloe extract, natural scrub agent and chelating agent according to weight parts, mixing, heating to 80 deg.C, stirring, adding auxiliary scrub agent, stirring, and performing ultrasonic treatment at 25000Hz for 20min to obtain mixed solution D;
3) adding the mixed solution C obtained in the step 1) and the mixed solution D obtained in the step 2) into an emulsifier, heating to 70 ℃, and carrying out homogeneous micro-emulsification reaction for 15min to obtain micro-emulsion for later use;
4) adding the frosted particles and the preservative into the microemulsion obtained in the step 3), and uniformly stirring to obtain a frosted essence primary product;
5) sterilizing the primary polishing essence obtained in the step 4) for 60min under the ultraviolet ray with the wavelength of 250nm to obtain a finished polishing essence.
Comparative example 1
The skin-smoothing scrub essence comprises the following raw materials in parts by weight:
the conductivity of the deionized water is less than 0.32 mu S/cm, and the pH value is 6.
Each part of the polypeptide composition comprises the following raw materials in parts by weight:
1 portion of hexapeptide
6 portions of rice peptide
8 parts of oat peptide.
The oat peptide is prepared by the following method:
a1, washing oat with clear water and drying, weighing dried oat, grinding, sieving to remove impurities, adding water for homogenizing, and adjusting pH to 2 to obtain a homogeneous solution A for later use;
a2, adding acid protease in the step A1 for enzymolysis, adjusting the pH value to 7 after enzymolysis, and adding trypsin for enzymolysis to obtain an enzymolysis liquid B for later use;
a3, centrifuging the enzymolysis liquid B obtained in the step A2, taking supernate for filtration, performing ultrafiltration on filtrate by using a hollow fiber membrane, and collecting the filtrate, namely the oat peptide.
The natural scrub agent is a mixture consisting of a lotus extract, a phyllostachys pubescens extract and a water lily extract according to a weight ratio of 0.8:1.0: 1.0; the auxiliary abrasive is abrasive particles with the particle size of 80 meshes, which are prepared by mixing and grinding purslane and fresh bamboo juice according to the weight ratio of 0.8: 1.0.
The chelating agent is a mixture of EDTA-2Na and citric acid according to the weight ratio of 0.8: 1.0; the humectant is a mixture of glycerol, sodium hyaluronate and propylene glycol in a weight ratio of 0.8:1.0: 1.0.
A preparation method of a skin-smoothing scrub essence comprises the following steps:
1) weighing snail essence, the polypeptide composition, the humectant and lactobacillus acidophilus according to the weight parts, adding into deionized water, mixing and stirring uniformly, heating to 40 ℃, and keeping the temperature for 30min to obtain a mixed solution C for later use;
2) weighing herba Centellae extract, flos Matricariae Chamomillae extract, Aloe extract, natural scrub agent and chelating agent according to weight parts, mixing, heating to 60 deg.C, stirring, adding auxiliary scrub agent, stirring, and performing ultrasound at 20000Hz for 10min to obtain mixed solution D;
3) adding the mixed liquor C obtained in the step 1) and the mixed liquor D obtained in the step 2) into an emulsifier, heating to 60 ℃, and carrying out homogeneous micro-emulsification reaction for 10min to obtain micro-emulsion for later use;
4) sterilizing the microemulsion obtained in the step 3) for 40min under the ultraviolet ray with the wavelength of 200nm to obtain the finished product of the frosted essence.
Comparative example 2
The skin-smoothing scrub essence comprises the following raw materials in parts by weight:
the conductivity of the deionized water is less than 0.32 mu S/cm, and the pH value is 6.5.
The frosted particles are a mixture of organosilicon microspheres, polyurethane particles and polyethylene frosted particles according to the weight ratio of 1.0:1.0: 0.9. More preferably, the silicone microspheres have a particle average particle size of 9u m and an average oil absorption in the range of 180mL/100 g.
The natural scrub agent is a mixture consisting of a lotus extract, a phyllostachys pubescens extract and a water lily extract according to a weight ratio of 0.8:1.1: 1.0; the auxiliary abrasive is abrasive particles with the particle size of 90 meshes, which are prepared by mixing and grinding purslane and fresh bamboo juice according to the weight ratio of 0.8: 1.1.
The chelating agent is a mixture of EDTA-2Na and citric acid according to the weight ratio of 1.0: 1.0; the humectant is a mixture of glycerol, sodium hyaluronate and propylene glycol in a weight ratio of 0.8:1.1: 1.0.
A preparation method of a skin-smoothing scrub essence comprises the following steps:
1) weighing snail essence, a humectant and lactobacillus acidophilus according to the weight parts, adding into deionized water, mixing and stirring uniformly, heating to 50 ℃, and keeping the temperature for 45min to obtain a mixed solution C for later use;
2) weighing herba Centellae extract, flos Matricariae Chamomillae extract, Aloe extract, natural scrub agent and chelating agent according to weight parts, mixing, heating to 70 deg.C, stirring, adding auxiliary scrub agent, stirring, and performing ultrasonic treatment at 22500Hz for 15min to obtain mixed solution D;
3) adding the mixed liquor C obtained in the step 1) and the mixed liquor D obtained in the step 2) into an emulsifier, heating to 65 ℃ to perform homogeneous micro-emulsification reaction for 13min to obtain micro-emulsion for later use;
4) adding the frosted particles and the preservative into the microemulsion obtained in the step 3), and uniformly stirring to obtain a frosted essence primary product;
5) sterilizing the primary polishing essence obtained in the step 4) for 50min under the ultraviolet ray with the wavelength of 225nm to obtain a finished polishing essence.
Comparative example 3
The skin-smoothing scrub essence comprises the following raw materials in parts by weight:
the conductivity of the deionized water is less than 0.32 mu S/cm, and the pH value is 7.
Each part of the polypeptide composition comprises the following raw materials in parts by weight:
hexagon 5 portions
10 portions of rice peptide
12 parts of oat peptide.
The oat peptide is prepared by the following method:
a1, washing oat with clear water and drying, weighing dried oat, grinding, sieving to remove impurities, adding water for homogenizing, and adjusting pH to 4 to obtain a homogeneous solution A for later use;
a2, adding acid protease in the step A1 for enzymolysis, adjusting the pH value to 8 after enzymolysis, and adding trypsin for enzymolysis to obtain an enzymolysis liquid B for later use;
a3, centrifuging the enzymolysis liquid B obtained in the step A2, taking supernate for filtration, performing ultrafiltration on filtrate by using a hollow fiber membrane, and collecting the filtrate, namely the oat peptide.
The frosted particles are a mixture of organosilicon microspheres, polyurethane particles and polyethylene frosted particles according to the weight ratio of 1.2:1.0: 1.0. More preferably, the silicone microspheres have a particle average particle size of 15u m and an average oil absorption in the range of 300mL/100 g.
The chelating agent is a mixture of EDTA-2Na and citric acid according to the weight ratio of 1.2: 1.0; the humectant is a mixture of glycerol, sodium hyaluronate and propylene glycol in a weight ratio of 0.8:1.2: 1.0.
A preparation method of a skin-smoothing scrub essence comprises the following steps:
1) weighing snail essence, the polypeptide composition, the humectant and lactobacillus acidophilus according to the weight parts, adding into deionized water, mixing and stirring uniformly, and heating to 60 ℃ and keeping the temperature for 60min to obtain a mixed solution C for later use;
2) weighing herba Centellae extract, flos Matricariae Chamomillae extract, Aloe extract and chelating agent according to weight parts, mixing, heating to 80 deg.C, stirring, adding auxiliary scrub agent, stirring, and performing ultrasonic treatment at 25000Hz for 20min to obtain mixed solution D;
3) adding the mixed solution C obtained in the step 1) and the mixed solution D obtained in the step 2) into an emulsifier, heating to 70 ℃, and carrying out homogeneous micro-emulsification reaction for 15min to obtain micro-emulsion for later use;
4) adding the frosted particles and the preservative into the microemulsion obtained in the step 3), and uniformly stirring to obtain a frosted essence primary product;
5) sterilizing the primary polishing essence obtained in the step 4) for 60min under the ultraviolet ray with the wavelength of 250nm to obtain a finished polishing essence.
The essences prepared in examples 1 to 5 and comparative examples 1 to 3 were subjected to a performance test. First, 80 female subjects with healthy skin were selected and divided into 4 groups of 20 persons, and the test group consisted of subjects with the lotions prepared in examples 1 to 5 and comparative examples 1 to 3 applied to the left half face of each subject and a blank group consisted of subjects with no substance applied to the right half face. The experiment period is 8 weeks, and the skin of the subject was examined and analyzed by various instruments at 8 weeks to evaluate the effect of the lotions on the improvement of the moisture content of the skin, the elasticity of the skin, the fine wrinkles, the roughness of the skin and the number of coarse and large pores, and the results are shown in table 1 below.
TABLE 1
Note: wherein "+" is an increase and "-" is a decrease
From the above results, it can be seen that the essence of examples 1 to 5 of the present invention has the effects of improving skin elasticity, eliminating fine lines, skin roughness and coarse and large hair hole number, and also has the effects of brightening skin and brightening skin color. The essence in example 3 has the best effects of improving skin elasticity and eliminating fine wrinkles, skin roughness and coarse and large pore numbers.
Compared with the example 1, the raw materials of the essence of the comparative example 1 are not added with the abrasive particles, and the skin moisture content, skin elasticity, fine lines, skin roughness and coarse pore number improvement effect tests are carried out on the essence prepared from the raw materials, and the analysis shows that the effect of the essence on skin elasticity increase is reduced, the effects of fine line elimination, skin roughness elimination and coarse pore number elimination are obviously reduced, so that the prepared essence has poor effects on skin elasticity increase, fine line elimination, skin roughness elimination and coarse pore number elimination; the invention shows that the addition of the frosted particles into the raw materials can improve the effects of improving the skin elasticity, eliminating fine lines, skin roughness and coarse and large hair hole number of the prepared essence, and simultaneously has the effects of brightening the skin and brightening the skin color.
Compared with the example 3, the raw materials of the essence of the comparative example 2 are not added with the polypeptide composition, and the effect tests of improving the skin moisture content, the skin elasticity, the fine lines, the skin roughness and the number of coarse pores are carried out on the essence prepared from the raw materials, and the analysis shows that the effect of the essence on increasing the skin elasticity and the skin moisture content is relatively reduced, the fine lines are eliminated, the skin roughness is obviously reduced, so that the prepared essence has poor effects on increasing the skin elasticity, eliminating the fine lines, the skin roughness and the number of coarse pores; the polypeptide composition is added into the raw materials, so that the prepared essence can be improved, the skin elasticity is improved, fine lines, the skin roughness and the number of coarse and large pores are eliminated, and the effects of brightening the skin and brightening the skin color are achieved.
Compared with the example 5, the natural abrasive is not added into the raw materials of the essence of the comparative example 3, the skin moisture content, skin elasticity, fine lines, skin roughness and coarse and large pore number improvement effect tests are carried out on the abrasive essence prepared by using the raw materials, and the analysis shows that the effects of the essence on skin elasticity increase, fine line elimination, skin roughness and large pore number elimination are remarkably reduced, so that the prepared essence has poor effects on skin elasticity increase, fine line elimination, skin roughness elimination and large pore number elimination; the natural abrasive is added into the raw materials, so that the prepared essence can be improved, the effects of improving skin elasticity, eliminating fine lines, skin roughness and the number of coarse and large pores are achieved, and the effects of enabling the skin to be bright and white and brightening the skin color are achieved.
The above-described embodiments are preferred implementations of the present invention, and the present invention may be implemented in other ways without departing from the spirit of the present invention.
Claims (10)
1. The skin-smoothing scrub essence is characterized in that: the feed comprises the following raw materials in parts by weight:
2. the skin smoothing scrub essence of claim 1, wherein: each part of the polypeptide composition comprises the following raw materials in parts by weight:
1-5 parts of hexapeptide
6-10 parts of rice peptide
8-12 parts of oat peptide.
3. The skin smoothing scrub essence of claim 2, wherein: the oat peptide is prepared by the following method:
a1, washing oat with clear water and drying, weighing dried oat, grinding, sieving to remove impurities, adding water and homogenizing, and adjusting pH to 2-4 to obtain a homogeneous solution A for later use;
a2, adding acid protease into the step A1 for enzymolysis, adjusting the pH value to 7-8 after enzymolysis, and adding trypsin for enzymolysis to obtain an enzymolysis liquid B for later use;
a3, centrifuging the enzymolysis liquid B obtained in the step A2, taking supernate for filtration, performing ultrafiltration on filtrate by using a hollow fiber membrane, and collecting the filtrate, namely the oat peptide.
4. The skin smoothing scrub essence of claim 1, wherein: the frosted particles are a mixture of organosilicon microspheres, polyurethane particles and polyethylene frosted particles according to the weight ratio of 0.8-1.2:1.0: 0.8-1.0.
5. The skin smoothing scrub essence of claim 1, wherein: the natural scrub agent is a mixture consisting of a lotus extract, a phyllostachys pubescens extract and a water lily extract according to a weight ratio of 0.8:1.0-1.2: 1.0.
6. The skin smoothing scrub essence of claim 1, wherein: the auxiliary frosting agent is frosted particles prepared by mixing and grinding purslane and fresh bamboo juice according to the weight ratio of 0.8: 1.0-1.2.
7. The skin smoothing scrub essence of claim 6, wherein: the grain diameter of the abrasive particles is 80-100 meshes.
8. The skin smoothing scrub essence of claim 1, wherein: the chelating agent is a mixture of EDTA-2Na and citric acid according to the weight ratio of 0.8-1.2: 1.0; the humectant is a mixture of glycerol, sodium hyaluronate and propylene glycol in a weight ratio of 0.8:1.0-1.2: 1.0.
9. A method of making the skin smoothing scrub serum of claims 1-8, wherein: the method comprises the following steps:
1) weighing snail essence, the polypeptide composition, the humectant and lactobacillus acidophilus according to the weight parts, adding the mixture into deionized water, mixing and stirring uniformly, and heating and preserving heat to obtain a mixed solution C for later use;
2) weighing and mixing the centella extract, the chamomile extract, the aloe extract, the natural scrub agent and the chelating agent according to the weight parts, heating and stirring, adding the auxiliary scrub agent, uniformly stirring, and performing ultrasonic treatment to obtain a mixed solution D for later use;
3) adding the mixed liquor C obtained in the step 1) and the mixed liquor D obtained in the step 2) into an emulsifier, and carrying out homogeneous micro-emulsification reaction to obtain micro-emulsion for later use;
4) adding the frosted particles and the preservative into the microemulsion obtained in the step 3), and uniformly stirring to obtain a frosted essence primary product;
5) sterilizing the primary frosted essence obtained in the step 4) under ultraviolet rays to obtain a finished frosted essence.
10. The skin smoothing scrub essence of claim 1, wherein: in the step 1), the heating and heat preservation temperature is 40-60 ℃, and the heat preservation time is 30-60 min; in the step 2), the temperature is raised to 60-80 ℃, the ultrasonic frequency is 20000-; the temperature of the micro-emulsification reaction in the step 3) is 60-70 ℃, and the reaction time is 10-15 min; the wavelength of the ultraviolet rays in the step 5) is 200-250nm, and the sterilization time is 40-60 min.
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