CN111979430A - 一种通过冶金烧结从含铷物料中高效回收铷的方法 - Google Patents
一种通过冶金烧结从含铷物料中高效回收铷的方法 Download PDFInfo
- Publication number
- CN111979430A CN111979430A CN202010862680.3A CN202010862680A CN111979430A CN 111979430 A CN111979430 A CN 111979430A CN 202010862680 A CN202010862680 A CN 202010862680A CN 111979430 A CN111979430 A CN 111979430A
- Authority
- CN
- China
- Prior art keywords
- rubidium
- sintering
- efficiently recovering
- metallurgical
- dust
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229910052701 rubidium Inorganic materials 0.000 title claims abstract description 88
- IGLNJRXAVVLDKE-UHFFFAOYSA-N rubidium atom Chemical compound [Rb] IGLNJRXAVVLDKE-UHFFFAOYSA-N 0.000 title claims abstract description 88
- 238000005245 sintering Methods 0.000 title claims abstract description 54
- 239000000463 material Substances 0.000 title claims abstract description 48
- 238000000034 method Methods 0.000 title claims abstract description 25
- 239000000428 dust Substances 0.000 claims abstract description 29
- 239000002994 raw material Substances 0.000 claims abstract description 27
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 20
- 238000002156 mixing Methods 0.000 claims abstract description 17
- 239000004576 sand Substances 0.000 claims abstract description 16
- 239000002245 particle Substances 0.000 claims abstract description 13
- 239000008187 granular material Substances 0.000 claims abstract description 9
- 239000002910 solid waste Substances 0.000 claims abstract description 9
- 239000012320 chlorinating reagent Substances 0.000 claims abstract description 8
- 239000003245 coal Substances 0.000 claims abstract description 8
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 3
- 238000003756 stirring Methods 0.000 claims abstract description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 18
- 229910052742 iron Inorganic materials 0.000 claims description 9
- 238000012216 screening Methods 0.000 claims description 9
- 238000009628 steelmaking Methods 0.000 claims description 8
- 239000000203 mixture Substances 0.000 claims description 7
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 6
- 239000004615 ingredient Substances 0.000 claims description 6
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 claims description 5
- 239000001110 calcium chloride Substances 0.000 claims description 5
- 229910001628 calcium chloride Inorganic materials 0.000 claims description 5
- WUKWITHWXAAZEY-UHFFFAOYSA-L calcium difluoride Chemical compound [F-].[F-].[Ca+2] WUKWITHWXAAZEY-UHFFFAOYSA-L 0.000 claims description 5
- 239000010436 fluorite Substances 0.000 claims description 5
- 230000008569 process Effects 0.000 claims description 5
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 claims description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 4
- 239000000571 coke Substances 0.000 claims description 4
- 238000004064 recycling Methods 0.000 claims description 4
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 claims description 3
- 239000000292 calcium oxide Substances 0.000 claims description 3
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 239000011780 sodium chloride Substances 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 235000019270 ammonium chloride Nutrition 0.000 claims description 2
- RHZUVFJBSILHOK-UHFFFAOYSA-N anthracen-1-ylmethanolate Chemical compound C1=CC=C2C=C3C(C[O-])=CC=CC3=CC2=C1 RHZUVFJBSILHOK-UHFFFAOYSA-N 0.000 claims description 2
- 239000003830 anthracite Substances 0.000 claims description 2
- 239000002802 bituminous coal Substances 0.000 claims description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 2
- 238000002386 leaching Methods 0.000 abstract description 4
- 230000007613 environmental effect Effects 0.000 abstract description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 18
- 239000000779 smoke Substances 0.000 description 10
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 8
- 229910052783 alkali metal Inorganic materials 0.000 description 6
- 150000001340 alkali metals Chemical class 0.000 description 6
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 4
- 238000005660 chlorination reaction Methods 0.000 description 4
- 229910052804 chromium Inorganic materials 0.000 description 4
- 239000011651 chromium Substances 0.000 description 4
- 229910052500 inorganic mineral Inorganic materials 0.000 description 4
- 239000011707 mineral Substances 0.000 description 4
- 229910052759 nickel Inorganic materials 0.000 description 4
- 229910000831 Steel Inorganic materials 0.000 description 3
- 230000001276 controlling effect Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 230000001105 regulatory effect Effects 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- 235000012239 silicon dioxide Nutrition 0.000 description 3
- 239000010959 steel Substances 0.000 description 3
- 239000012141 concentrate Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 239000010445 mica Substances 0.000 description 2
- 229910052618 mica group Inorganic materials 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 239000002893 slag Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000010433 feldspar Substances 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 239000010438 granite Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 229910052629 lepidolite Inorganic materials 0.000 description 1
- 229910001744 pollucite Inorganic materials 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 238000009270 solid waste treatment Methods 0.000 description 1
- 230000001180 sulfating effect Effects 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
- C22B26/10—Obtaining alkali metals
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/14—Agglomerating; Briquetting; Binding; Granulating
- C22B1/16—Sintering; Agglomerating
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/14—Agglomerating; Briquetting; Binding; Granulating
- C22B1/24—Binding; Briquetting ; Granulating
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B7/00—Working up raw materials other than ores, e.g. scrap, to produce non-ferrous metals and compounds thereof; Methods of a general interest or applied to the winning of more than two metals
- C22B7/02—Working-up flue dust
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Environmental & Geological Engineering (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Geochemistry & Mineralogy (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Processing Of Solid Wastes (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202010862680.3A CN111979430B (zh) | 2020-08-25 | 2020-08-25 | 一种通过冶金烧结从含铷物料中高效回收铷的方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN202010862680.3A CN111979430B (zh) | 2020-08-25 | 2020-08-25 | 一种通过冶金烧结从含铷物料中高效回收铷的方法 |
Publications (2)
Publication Number | Publication Date |
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CN111979430A true CN111979430A (zh) | 2020-11-24 |
CN111979430B CN111979430B (zh) | 2022-05-20 |
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CN202010862680.3A Active CN111979430B (zh) | 2020-08-25 | 2020-08-25 | 一种通过冶金烧结从含铷物料中高效回收铷的方法 |
Country Status (1)
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CN (1) | CN111979430B (zh) |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5849063A (en) * | 1992-01-15 | 1998-12-15 | Metals Recycling Technologies Corp. | Production of direct reduced iron and/or pig iron from industrial waste streams |
CN101775505A (zh) * | 2010-02-08 | 2010-07-14 | 中南大学 | 氯化焙烧法从锂云母中提取锂的方法和设备 |
CN104178644A (zh) * | 2014-07-23 | 2014-12-03 | 湖南鑫生矿冶废弃物综合利用科技有限公司 | 从铁尾矿中回收铷的方法 |
CN107267777A (zh) * | 2017-06-09 | 2017-10-20 | 北京矿冶研究总院 | 一种含铷矿中提取铷的新方法 |
CN108624765A (zh) * | 2018-06-14 | 2018-10-09 | 中南大学 | 一种从低品位含铷尾矿高效回收铷的工艺 |
CN108676942A (zh) * | 2018-05-18 | 2018-10-19 | 廖辉明 | 一种含铁和或锌铅铜锡等物料与熔融钢渣协同处理回收方法 |
CN111020204A (zh) * | 2019-12-31 | 2020-04-17 | 耒阳市焱鑫有色金属有限公司 | 一种二次资源含砷配铁含稀散元素配氯化剂的富氧侧吹炉熔炼方法 |
CN111534704A (zh) * | 2020-06-28 | 2020-08-14 | 山西省岩矿测试应用研究所(山西省贵金属及珠宝玉石检测中心) | 一种含钾岩石中协同提取钾、铷的方法 |
-
2020
- 2020-08-25 CN CN202010862680.3A patent/CN111979430B/zh active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5849063A (en) * | 1992-01-15 | 1998-12-15 | Metals Recycling Technologies Corp. | Production of direct reduced iron and/or pig iron from industrial waste streams |
CN101775505A (zh) * | 2010-02-08 | 2010-07-14 | 中南大学 | 氯化焙烧法从锂云母中提取锂的方法和设备 |
CN104178644A (zh) * | 2014-07-23 | 2014-12-03 | 湖南鑫生矿冶废弃物综合利用科技有限公司 | 从铁尾矿中回收铷的方法 |
CN107267777A (zh) * | 2017-06-09 | 2017-10-20 | 北京矿冶研究总院 | 一种含铷矿中提取铷的新方法 |
CN108676942A (zh) * | 2018-05-18 | 2018-10-19 | 廖辉明 | 一种含铁和或锌铅铜锡等物料与熔融钢渣协同处理回收方法 |
CN108624765A (zh) * | 2018-06-14 | 2018-10-09 | 中南大学 | 一种从低品位含铷尾矿高效回收铷的工艺 |
CN111020204A (zh) * | 2019-12-31 | 2020-04-17 | 耒阳市焱鑫有色金属有限公司 | 一种二次资源含砷配铁含稀散元素配氯化剂的富氧侧吹炉熔炼方法 |
CN111534704A (zh) * | 2020-06-28 | 2020-08-14 | 山西省岩矿测试应用研究所(山西省贵金属及珠宝玉石检测中心) | 一种含钾岩石中协同提取钾、铷的方法 |
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CN111979430B (zh) | 2022-05-20 |
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Address after: 517000 Chuanlong group, Liangcun village, Huangtian Town, Dongyuan County, Heyuan City, Guangdong Province Applicant after: Guangdong Jinyu Environmental Technology Co.,Ltd. Address before: 517000 Chuanlong group, Liangcun village, Huangtian Town, Dongyuan County, Heyuan City, Guangdong Province Applicant before: GUANGDONG JINYU ENVIRONMENTAL TECHNOLOGY Co.,Ltd. |
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GR01 | Patent grant | ||
GR01 | Patent grant | ||
CB03 | Change of inventor or designer information |
Inventor after: Zhou Ji Inventor after: Li Xiang Inventor after: Xue Wentao Inventor after: Yang Yongming Inventor after: Hong Qingshou Inventor after: Wang Yanji Inventor after: Yang Qingxian Inventor before: Li Xiang Inventor before: Xue Wentao Inventor before: Yang Yongming Inventor before: Zhou Ji Inventor before: Hong Qingshou Inventor before: Wang Yanji Inventor before: Yang Qingxian |
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CB03 | Change of inventor or designer information | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A method for efficient recovery of rubidium from rubidium containing materials by metallurgical sintering Effective date of registration: 20220622 Granted publication date: 20220520 Pledgee: Industrial and Commercial Bank of China Limited Heyuan branch Pledgor: Guangdong Jinyu Environmental Technology Co.,Ltd. Registration number: Y2022980008482 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right |