CN111887464B - Preparation method and application of coffee aroma style coating thick paste slice - Google Patents
Preparation method and application of coffee aroma style coating thick paste slice Download PDFInfo
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- CN111887464B CN111887464B CN202010735184.1A CN202010735184A CN111887464B CN 111887464 B CN111887464 B CN 111887464B CN 202010735184 A CN202010735184 A CN 202010735184A CN 111887464 B CN111887464 B CN 111887464B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/90—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in food processing or handling, e.g. food conservation
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Abstract
A preparation method of a thick pulp sheet coated with coffee aroma style comprises the steps of soaking plant fibers in warm water, then carrying out enzyme treatment, dehydrating, drying and mechanically defibering; pulverizing the roasted coffee beans into coffee powder; uniformly mixing the defibered plant fibers with coffee powder, and then paving the mixture on a forming net to form a fiber thin layer; spraying an aqueous solution of an adhesive on the surface of the fiber thin layer, and drying to obtain a substrate; uniformly stirring the edible spice, the smoke agent and the coffee powder to form a base material; and placing the substrate on a stainless steel strip, uniformly coating the substrate with a base material, drying the substrate for the first time by using hot steam, demolding and turning over the substrate after the first drying, uniformly coating the base material on one surface which is not coated with the base material, and drying for the second time to obtain the coating thick paste sheet. The smoke generated after the sheet is heated does not generate substances such as nicotine and the like which are addicted and harmful to health, the smoke amount is large, the smoke amount is stable, and the smoking sense organ comfort degree is good.
Description
Technical Field
The invention belongs to the field of a preparation method of a novel heating non-combustion tobacco product.
Background
Because the traditional burning and sucking type cigarette generates a large amount of harmful components such as carbon monoxide, tar and the like which are harmful to human health when the tobacco is burnt, people research novel tobacco products, such as electronic cigarettes, which replace the traditional burning and sucking type cigarette. When people smoke the electronic cigarette, atomized liquid of cigarette oil of the electronic cigarette is inhaled into a human body instead of cracking products generated by burning of the traditional cigarette, so that the harmfulness can be reduced to a certain degree. However, the electronic cigarette needs to adopt liquid tobacco tar, the heating temperature of the electronic cigarette needs to be as high as 600 ℃ to generate a good atomization effect, and the high heating temperature inevitably causes some organic matters in the tobacco tar to crack to generate hazardous substances.
With the transformation of tobacco market, tobacco products (also called low-temperature cigarettes) which are not combusted by heating are gradually popularized. The tobacco products which are not burnt by heating are characterized in that tobacco shreds are heated by a special heating source, nicotine and flavor substances in the tobacco shreds are volatilized to generate smoke to meet the requirements of smokers during heating, the heating temperature is generally not more than 400 ℃, and IQOS (electric heating smokeless tobacco product) which is a representative product in the tobacco products which are not burnt by heating is more and more widely used. Ordinary electronic cigarettes provide a feeling of being close to a real cigarette by heating the tobacco tar, while IQOS provides a feeling of being close to a real cigarette by heating the cartridge. When the two cigarettes are the same as the smoke inhaled by smokers, the main components of the smoke are less nicotine and spice generated in the heating process, the smoke does not contain tar, but the IQOS can provide the real taste which is closest to the traditional cigarette compared with the electronic cigarette with heated tobacco tar. IQOS cartridges are specially treated tobacco and are heated after insertion into a heating rod, the heating temperature is controlled at about 350 ℃, the tobacco material in the cartridge is heated to a temperature sufficient to evaporate nicotine and flavor smoke without burning, thereby avoiding the release of tar, releasing less chemicals, but having the same taste as real tobacco.
However, because tobacco is still used as a heating material in the IQOS cartridge, nicotine which is addictive to people still exists in the smoke, so that people cannot really quit smoking; moreover, the IQOS has less smoke, too few sucking mouths and unstable aerosol quantity, the mouth feel is obviously inferior to the mouth feels of the former mouths after the last mouth is sucked, the 'paste' taste is improved, the fragrance is reduced, the aerosol has no thickness and satisfaction, and the suction feeling is not good.
Disclosure of Invention
The invention aims to solve the defects of the prior art and provides a preparation method of a coffee aroma style coating thick pulp sheet which does not contain raw material components harmful to human health, does not generate nicotine and other substances harmful to health after heating smoke, has the smoke amount close to that of the traditional cigarette, stable aerosol amount and good smoking sensory comfort, and an application of the sheet.
The technical scheme adopted by the invention is as follows:
the preparation method of the coffee aroma style coating thick paste slice comprises the following steps:
(1) preparing roasted coffee beans, a smoke agent, an adhesive, an edible spice, plant fibers, biological enzyme and warm water;
(2) soaking plant fibers in warm water 4-5 times the weight of the plant fibers, keeping the water temperature at 35-40 ℃, soaking for 2-2.5 hours, performing enzyme treatment on the soaked plant fibers for 2.5-3 hours by using a biological enzyme preparation, and then dehydrating and drying to obtain dried plant fibers after the enzyme treatment;
(3) crushing coffee beans into 300-400-mesh coffee powder;
(4) mechanically defibering the plant fiber after enzyme treatment and drying, and then uniformly mixing the plant fiber with coffee powder, wherein the mass percentage of the plant fiber to the coffee powder is 80-60%: 20% -40%, and then laying the mixed material on a forming net to form a fiber thin layer;
(5) spraying an aqueous solution of an adhesive on the surface of the fiber thin layer, and drying to obtain a substrate; the aqueous solution of the adhesive is prepared by adding water into the adhesive, and has the mass concentration of 1-12%, and the mass ratio of the aqueous solution of the adhesive to the fiber thin layer is 3-4%;
(6) according to the mass percentage, 15-20% of edible spice, 15-25% of smoke agent and 70-55% of coffee powder prepared in the step (3) are poured into a material barrel and are uniformly stirred to form a base material;
(7) placing the substrate prepared in the step (5) on a stainless steel strip, and uniformly coating the base material prepared in the step (6) on the substrate; the coating amount of the base material is 30-40% of the mass of the substrate;
(8) introducing hot steam penetrating through the stainless steel strip along the vertical direction, carrying out primary drying on the substrate on the stainless steel strip, and demolding the substrate after primary drying to obtain a semi-finished substrate;
(9) turning over the demolded semi-finished substrate, and uniformly coating the base material on the surface which is not coated with the base material;
(10) drying the substrate for the second time by adopting drying equipment to obtain a thick slurry coating sheet;
(11) and removing wrinkles of the thick paste coated thin sheet, shaping and rolling to obtain a finished product.
Further, the plant fiber is a compound product of bagasse fiber and bamboo fiber, and the bagasse fiber accounts for 20-80% by weight, and the balance is bamboo fiber.
Further, the biological enzyme is one or a mixture of more of pectinase, cellulase, hemicellulase, alpha-L-arabinofuranosidase and amylase.
Further, in the step (2), when the soaked plant fiber is subjected to enzyme treatment by using the biological enzyme preparation, the addition amount of the biological enzyme is 0.3 to 0.5 percent of the weight of the plant fiber before soaking.
Further, the smoke agent is one or a mixture of more of propylene glycol, glycerol, sorbitol and diamine hydrogen phosphate.
Further, the adhesive is one or more of modified starch glue, sodium carboxymethyl cellulose, guar gum and chitosan.
Further, in the step (7), the substrate is placed on the stainless steel strip, and the base material is uniformly coated on the substrate, wherein the anti-sticking agent is coated on the stainless steel strip, and the base material is coated on the upper surface of the substrate by adopting a single-die head or double-die head screw extruder.
Further, the water content of the semi-finished substrate after the first drying in the step (8) when the steel strip is demoulded is 12% -18%, and the water content of the thick slurry coating sheet obtained by the second drying in the step (10) is 8% -15%.
Further, the base material obtained by pulp blending in the step (6) is ground into pulp by a double-screw kneading machine, the grinding temperature is 50-55 ℃, and the grinding flow is 20-25L/min.
The coffee aroma slice prepared by the method is applied to preparing tobacco products which can not burn by heating.
The prepared sheet does not contain addictive components such as tobacco and nicotine which are harmful to human health, the heated smoke does not generate substances which are addictive such as nicotine and harmful to health, the smoke particles can be smoked when being heated to 300-350 ℃, the smoke amount is close to that of the traditional cigarette, the smoke amount is stable, and the smoking sense comfort is good.
The invention carries out enzyme treatment on plant fiber which is an important component of the thin sheet substrate molding fiber by thick pulp coating method, and partially degrades the plant fiber, so that the fiber structure becomes loose, which is beneficial to fiber splitting in the later period; meanwhile, the content of pectin in the plant fiber is effectively reduced by utilizing the biological enzyme, the release amount of harmful substances such as methanol and the like after combustion is greatly reduced, and the effect is obvious. Meanwhile, a large amount of roasted coffee powder is added into the base materials formed by the substrate and the pulp, the woody smell of the slices is further covered by the roasted coffee aroma, and the strong coffee aroma style is realized, so that the quality of the slices is greatly improved. The plant fiber adopts a compound product of the bagasse fiber and the bamboo fiber, and has the advantages of uniform smoke release during smoking, no peculiar smell, strong adsorbability, self-burnt fragrance after baking, no adhesion on the surface, high tensile strength, good processing resistance and the like.
According to the invention, the coffee bean raw material is finely processed, and the integrated processes of extrusion forming, grading drying and the like are adopted, so that the prepared sheet material has the advantages of large smoke agent loading capacity, high coffee component proportion, large product smoke release amount, high release stability, good processing resistance and the like.
Detailed Description
The invention is further described below by means of specific examples.
Example 1
The preparation method of the coffee aroma style coating thick paste slice comprises the following steps:
(1) uniformly mixing 20% of bagasse fiber and 80% of bamboo fiber in percentage by weight, soaking in warm water 4 times of the weight of all the fibers, keeping the water temperature at 35-40 ℃, soaking for 2 hours, and performing enzyme treatment on the soaked fibers for 3 hours by using pectinase and cellulase preparation, wherein the addition amount of the biological enzyme is 0.4% of the weight of the fibers before soaking. Then dehydrating and drying to obtain dried plant fiber after enzyme treatment;
(2) crushing coffee beans into coffee powder of about 350 meshes;
(3) defibering the plant fiber after enzyme treatment and drying by using a defibering machine, and then uniformly mixing the plant fiber with coffee powder, wherein the mass percentage of the plant fiber to the coffee powder is 70%: 30 percent, then laying the mixed material on a forming net to form a fiber thin layer;
(4) spraying an aqueous solution of an adhesive on the surface of the fiber thin layer, and drying to obtain a substrate; the aqueous solution of the adhesive is prepared by adding water into modified starch glue, and has the mass concentration of 8%, and the mass ratio of the aqueous solution of the adhesive to the thin fiber layer is 3%;
(5) pouring 15% of edible spice, 15% of propylene glycol and 70% of the coffee powder prepared in the step (2) into a material barrel according to the mass percentage, and uniformly stirring to form a base material; and (3) grinding the base material into pulp by using a double-screw kneading machine, wherein the grinding temperature is 50-55 ℃, and the grinding flow is 20-25L/min. The edible spice can be various edible spices purchased from the market, such as jujube essence, dried orange peel, honey and the like;
(6) firstly, coating an anti-sticking agent on stainless steel strip steel, wherein the anti-sticking agent is propylene glycol, placing the substrate prepared in the step (4) on the stainless steel strip, and uniformly coating the base material prepared in the step (5) on the upper surface of the substrate by adopting a double-die-head screw extruder; the coating amount of the base material is 35 percent of the mass of the substrate;
(7) introducing hot steam penetrating through the stainless steel strip along the vertical direction, carrying out primary drying on the substrate on the stainless steel strip, and demolding the substrate after primary drying to obtain a semi-finished substrate; the water content of the semi-finished substrate when the steel strip is demoulded is 15%;
(8) turning over the demolded semi-finished substrate, and uniformly coating the base material on the surface which is not coated with the base material;
(9) drying the substrate for the second time by adopting drying equipment to obtain a coating thick paste slice with the water content of 10%;
(10) and removing wrinkles of the thick paste coated thin sheet, shaping and rolling to obtain a finished product.
The coffee aroma slice finished product prepared by the method is applied to preparing a tobacco product which is not combusted by heating.
Example 2
The preparation method of the coffee aroma style coating thick paste slice comprises the following steps:
(1) uniformly mixing 50% of bagasse fiber and 50% of bamboo fiber, soaking the mixture in warm water which is 5 times of the total weight of the fibers, keeping the water temperature at about 40 ℃, soaking for 2 hours, and performing enzyme treatment on the soaked fibers for 2.5 hours by using a hemicellulase preparation, wherein the addition amount of the biological enzyme is 0.5% of the weight of the fibers before soaking. Then dehydrating and drying to obtain dried plant fiber after enzyme treatment;
(2) crushing coffee beans into 400-mesh coffee powder;
(3) sending the plant fiber after enzyme treatment and drying into a forming head box by wind to break up and disintegrate the fiber, and then uniformly mixing the plant fiber and the coffee powder, wherein the mass percentage of the plant fiber to the coffee powder is 80%: 20 percent, then laying the mixed material on a forming net to form a fiber thin layer;
(4) spraying an aqueous solution of an adhesive on the surface of the fiber thin layer, and drying to obtain a substrate; the aqueous solution of the adhesive is prepared by mixing sodium carboxymethylcellulose and guar gum and then adding water, and the mass concentration of the aqueous solution of the adhesive is 12%, and the aqueous solution of the adhesive accounts for 4% of the mass ratio of the fiber thin layer;
(5) pouring 20% of edible spice, 20% of glycerol, 5% of sorbitol and 55% of the coffee powder prepared in the step (2) into a material barrel according to the mass percentage, and uniformly stirring to form a base material; grinding the base material with a double-screw kneading machine at 50-55 deg.C with a grinding flow of 20-25L/min;
(6) firstly, coating an anti-sticking agent on stainless steel strip steel, placing the substrate prepared in the step (4) on the stainless steel strip, and uniformly coating the base material prepared in the step (5) on the upper surface of the substrate by adopting a single-die screw extruder; the coating amount of the base material is 30 percent of the mass of the substrate;
(7) introducing hot steam penetrating through the stainless steel strip along the vertical direction, carrying out primary drying on the substrate on the stainless steel strip, and demolding the substrate after primary drying to obtain a semi-finished substrate; the water content of the semi-finished substrate when the steel strip is demoulded is 18%;
(8) turning over the demolded semi-finished substrate, and uniformly coating the base material on the surface which is not coated with the base material;
(9) drying the substrate for the second time by adopting drying equipment to obtain a coating thick paste slice with the water content of 15%;
(10) and removing wrinkles of the thick paste coated thin sheet, shaping and rolling to obtain a finished product.
The coffee aroma sheet finished product prepared by the method is applied to preparing a tobacco product which is not combusted by heating.
Example 3
The preparation method of the coffee aroma style coating thick paste slice comprises the following steps:
(1) uniformly mixing 80% of bagasse fiber and 20% of bamboo fiber, soaking in warm water with the weight of 4.5 times of the total fiber weight, keeping the water temperature at 35-40 ℃, soaking for 2-2.5 hours, and performing enzyme treatment on the soaked fiber for 2.5-3 hours by using a preparation of alpha-L-arabinofuranosidase and amylase, wherein the addition amount of the biological enzyme is 0.3% of the weight of the fiber before soaking. Then dehydrating and drying to obtain dried plant fiber after enzyme treatment;
(2) crushing coffee beans into 300-mesh coffee powder;
(3) sending the plant fiber after enzyme treatment and drying into a forming head box by wind to break up and disintegrate the fiber, and then uniformly mixing the plant fiber and the coffee powder, wherein the mass percentage of the plant fiber to the coffee powder is 60%: 40 percent, and then laying the mixed material on a forming net to form a fiber thin layer;
(4) spraying an aqueous solution of an adhesive on the surface of the fiber thin layer, and drying to obtain a substrate; the aqueous solution of the adhesive is prepared by adding water into chitosan, and has a mass concentration of 1%, and the mass ratio of the aqueous solution of the adhesive to the thin fiber layer is 4%;
(5) pouring 18% of edible spice, 18% of diammonium hydrogen phosphate and 64% of the coffee powder prepared in the step (2) into a material barrel by mass percent, and uniformly stirring to form a base material;
(6) firstly, coating an anti-sticking agent on stainless steel strip steel, placing the substrate prepared in the step (4) on the stainless steel strip, and uniformly coating the base material prepared in the step (5) on the upper surface of the substrate by adopting a single-die screw extruder; the coating amount of the base material is 40 percent of the mass of the substrate;
(7) introducing hot steam penetrating through the stainless steel strip along the vertical direction, carrying out primary drying on the substrate on the stainless steel strip, and demolding the substrate after primary drying to obtain a semi-finished substrate; the water content of the semi-finished substrate when the steel strip is demoulded is 12%;
(8) turning over the demolded semi-finished substrate, and uniformly coating the base material on the surface which is not coated with the base material;
(9) drying the substrate for the second time by adopting drying equipment to obtain a coating thick paste slice with the water content of 8%;
(10) and removing wrinkles of the thick paste coated thin sheet, shaping and rolling to obtain a finished product.
The coffee aroma slice finished product prepared by the method is applied to preparing a tobacco product which is not combusted by heating.
The coffee aroma style coating thick paste method sheet reduces the content of harmful substances such as methanol in tobacco stems due to enzymolysis of wood structural materials and addition of baked coffee powder, and addictive components such as nicotine are not added in the coating thick paste method sheet, so that the content of substances harmful to human bodies in the coating thick paste method sheet is reduced.
The invention finely processes the coffee bean raw material, and adopts the integrated processes of extrusion forming, grading drying and the like, and the prepared sheet material has the advantages of large smoke agent loading capacity, high coffee component proportion, large product smoke release amount, high release stability, good processing resistance and the like.
Claims (9)
1. The preparation method of the coffee aroma style coating thick paste slice is characterized by comprising the following steps:
(1) preparing roasted coffee beans, a smoke agent, an adhesive, an edible spice, plant fibers, biological enzyme and warm water;
(2) soaking plant fibers in warm water 4-5 times the weight of the plant fibers, keeping the water temperature at 35-40 ℃, soaking for 2-2.5 hours, performing enzyme treatment on the soaked plant fibers for 2.5-3 hours by using a biological enzyme preparation, and then dehydrating and drying to obtain dried plant fibers after the enzyme treatment;
(3) crushing coffee beans into 300-400-mesh coffee powder;
(4) mechanically defibering the plant fiber after enzyme treatment and drying, and then uniformly mixing the plant fiber with coffee powder, wherein the mass percentage of the plant fiber to the coffee powder is 80-60%: 20% -40%, and then laying the mixed material on a forming net to form a fiber thin layer; the plant fiber is a compound product of bagasse fiber and bamboo fiber, wherein the bagasse fiber accounts for 20-80% by weight, and the balance is bamboo fiber;
(5) spraying an aqueous solution of an adhesive on the surface of the fiber thin layer, and drying to obtain a substrate; the aqueous solution of the adhesive is prepared by adding water into the adhesive, and has the mass concentration of 1-12%, and the mass ratio of the aqueous solution of the adhesive to the fiber thin layer is 3-4%;
(6) according to the mass percentage, 15-20% of edible spice, 15-25% of smoke agent and 70-55% of coffee powder prepared in the step (3) are poured into a material barrel and are uniformly stirred to form a base material;
(7) placing the substrate prepared in the step (5) on a stainless steel strip, and uniformly coating the base material prepared in the step (6) on the substrate, wherein the coating amount of the base material is 30-40% of the mass of the substrate;
(8) introducing hot steam penetrating through the stainless steel strip along the vertical direction, carrying out primary drying on the substrate on the stainless steel strip, and demolding the substrate after primary drying to obtain a semi-finished substrate;
(9) turning over the demolded semi-finished substrate, and uniformly coating the base material on the surface which is not coated with the base material;
(10) drying the substrate for the second time by adopting drying equipment to obtain a thick slurry coating sheet;
(11) and removing wrinkles of the thick paste coated thin sheet, shaping and rolling to obtain a finished product.
2. The method of preparing a coffee aroma-style coated thick paste sheet according to claim 1, wherein the bio-enzyme is one or a mixture of several of pectinase, cellulase, hemicellulase, alpha-L-arabinofuranosidase, and amylase.
3. The method for preparing a coffee aroma-style coated thick paste sheet according to claim 1 or 2, wherein in the step (2), when the soaked plant fiber is subjected to enzyme treatment with the bio-enzyme preparation, the amount of bio-enzyme added is 0.3% to 0.5% of the weight of the plant fiber before soaking.
4. The method of preparing a coffee aroma style coated thick paste sheet according to claim 1, wherein the smoking agent is one or a mixture of propylene glycol, glycerin, sorbitol, and diammonium hydrogen phosphate.
5. The method for preparing the coffee aroma style coated thick paste sheet according to claim 1, wherein the adhesive is one or more of modified starch glue, sodium carboxymethyl cellulose, guar gum and chitosan.
6. The method for preparing a coffee aroma style coated thick paste sheet according to claim 1, wherein the step (7) of placing the base sheet on a stainless steel belt and uniformly coating the base material on the base sheet comprises coating the anti-sticking agent on the stainless steel belt and coating the base material on the upper surface of the base sheet by using a single-die or double-die screw extruder.
7. The method for preparing a coffee aroma style coated thick paste sheet according to claim 1, wherein the moisture content of the semi-finished substrate after the first drying in the step (8) is 12% to 18% when a steel strip is released from the semi-finished substrate, and the moisture content of the coated thick paste sheet obtained by the second drying in the step (10) is 8% to 15%.
8. The method for preparing the coffee aroma style coating thick pulp sheet as claimed in claim 1, wherein the base material obtained by the pulp blending in the step (6) is ground by a twin-screw kneading machine, wherein the grinding temperature is 50-55 ℃, and the grinding flow rate is 20-25L/min.
9. The coffee aroma-style coated thick paste sheet prepared by the method according to any one of claims 1 to 8 is applied to the preparation of a heat-not-burn tobacco product.
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| GB1330999A (en) * | 1971-03-17 | 1973-09-19 | Philip Morris Inc | Smoking product from coffee bean hulls and method for making same |
| CN104824827A (en) * | 2015-04-15 | 2015-08-12 | 江西中烟工业有限责任公司 | Agilawood fragrance style dry-method slice preparation method |
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