CN111560771A - Embroidery anticorrosion and antioxidation method for three-dimensional pattern - Google Patents
Embroidery anticorrosion and antioxidation method for three-dimensional pattern Download PDFInfo
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- CN111560771A CN111560771A CN202010435327.7A CN202010435327A CN111560771A CN 111560771 A CN111560771 A CN 111560771A CN 202010435327 A CN202010435327 A CN 202010435327A CN 111560771 A CN111560771 A CN 111560771A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D05—SEWING; EMBROIDERING; TUFTING
- D05C—EMBROIDERING; TUFTING
- D05C17/00—Embroidered or tufted products; Base fabrics specially adapted for embroidered work; Inserts for producing surface irregularities in embroidered products
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/228—Cyclic esters, e.g. lactones
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/238—Tannins, e.g. gallotannic acids
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M23/00—Treatment of fibres, threads, yarns, fabrics or fibrous goods made from such materials, characterised by the process
- D06M23/12—Processes in which the treating agent is incorporated in microcapsules
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Abstract
The invention provides an embroidery anticorrosion and antioxidation method of a three-dimensional pattern, which mainly comprises the following four steps: the processing method comprises the steps of soaking a base material cloth and an upper layer of cloth in natural plant essential oil, wherein the natural plant essential oil has obvious broad-spectrum antibacterial activity, so that the base material cloth and the upper layer of cloth soaked in the natural plant essential oil have effective corrosion prevention and oxidation resistance, and microcapsule powder of the natural plant essential oil is filled in the elastic rubber plate, and the microcapsule powder is water-soluble microcapsule powder.
Description
Technical Field
The invention relates to a protection method for embroidery of a three-dimensional pattern, in particular to an embroidery anticorrosion and antioxidation method for the three-dimensional pattern.
Background
Embroidery is the general term for various decorative patterns embroidered on fabric by needles and threads. The embroidery is divided into silk thread embroidery and feather embroidery. Namely, the silk thread or other fibers and yarns are punctured on the embroidery material by a needle in a certain pattern and color to embroider the decorative fabric forming the patterns. It is an art of adding the design and fabrication of people to any existing fabric with needles and threads. Embroidery is one of the traditional handicraft in China, and has at least two to three thousand years of history in China. The Chinese embroidery mainly comprises Suzhou embroidery, Hunan embroidery, Shu embroidery and Guangdong embroidery. The embroidery techniques include: the embroidery includes mainly life and artistic decoration, such as clothing, bedding, table cloth, stage, artwork decoration, etc.
Plant essential oils are composed of natural volatile compounds, also known as essences, essential oils, aromatic oils. As known from international standards for essential oils and european pharmacopoeia, essential oils are products obtained from raw materials by physical methods such as distillation, pressing (citrus fruits), extraction (leaching), or adsorption. Plant essential oils are very complex natural mixtures containing about 20-60 components at varying concentrations. They are characterized by a single or multiple main components (concentration 20-70%). However, experiments have shown that minor components also play a key role in the preservation and antioxidant of essential oils and may also exhibit synergistic effects with other compounds.
At present, the three-dimensional embroidery is favored by people due to beautiful and three-dimensional patterns, and in the real production of people, the three-dimensional embroidery is easy to corrode and oxidize due to the fact that the three-dimensional embroidery is partially protruded, so that the attractiveness and the appreciation are affected.
Disclosure of Invention
In order to solve the problems, the invention provides an embroidery anticorrosion and antioxidation method of a three-dimensional pattern, which can effectively inhibit the corrosion and oxidation of the three-dimensional pattern embroidery, prolong the storage time and improve the ornamental value of the three-dimensional pattern embroidery, and the specific technical scheme is as follows:
an embroidery anticorrosion and antioxidation method of a three-dimensional pattern, wherein the embroidery of the three-dimensional pattern is to stack an elastic rubber plate and an upper layer of cloth on a base material cloth in sequence, place the elastic rubber plate and the upper layer of cloth on an embroidery machine and embroider according to a pre-related pattern, and the technical scheme is as follows: the embroidery anticorrosion and antioxidation method of the three-dimensional pattern comprises the following steps:
s1, processing of cloth: selecting proper base material cloth and upper layer cloth according to actual needs, and completely soaking the base material cloth and the upper layer cloth in the natural plant essential oil;
s2, preparing an elastic rubber plate: forming a plurality of holes with the particle size of 0.5-10 mu m on the elastic rubber plate, and filling microcapsule powder containing the natural plant essential oil obtained in the step S1 on the elastic rubber plate with the holes;
s3, embroidering the three-dimensional pattern: sequentially stacking the elastic rubber sheet prepared in S2 and the upper layer cloth processed in S1 on the base cloth processed in S1, and placing them on an embroidering machine to embroider according to a pre-related pattern;
s4, cleaning the elastic rubber plate: and (5) rinsing the embroidery finished in the step S3 with clear water, and removing the elastic rubber plate at the non-embroidery part to obtain the three-dimensional pattern embroidery with corrosion resistance and oxidation resistance.
In some embodiments of the present invention, the method for preparing the natural plant essential oil in step S1 includes the following steps:
a. taking plant tissues in nature, and drying the cleaned plant tissues at 90-120 ℃ for 2-10 h;
b. crushing the dried plant tissues by using a crusher, and sieving by using a sieve of 80-120 meshes;
c. extracting plant tissue powder with a mixed solution of acetone and ethyl-methyl ketone;
d. removing acetone and ethyl-methyl ketone by rotary evaporation to obtain mixed solution, and decolorizing to obtain natural plant essential oil from the extractive solution.
In some embodiments of the present invention, the plant tissue in step b is one of roots, stems, leaves, flowers, seeds and fruits of natural plants.
In a further embodiment of the present invention, the natural plant essential oil is prepared by a method wherein the natural plant in step a is selected from the group consisting of ilex purpurea hassk, star anise, chrysanthemum and calendula officinalis.
In some embodiments of the invention, the soaking time in the step S1 is 0.5-2 hours.
In some embodiments of the invention, the natural plant essential oil microcapsule powder in the step S2 is water-soluble natural plant essential oil microcapsule powder, and the filling amount of the natural plant essential oil microcapsule powder is 0.5 to 5 μ g/g.
In some embodiments of the present invention, the preparation method of the natural plant essential oil microcapsule powder in the step S2 is as follows:
a. stirring and heating 0.1-0.5 part by weight of core natural plant essential oil to 30-70 ℃, adding 0.003-0.05 part by weight of oil-soluble emulsifier and 0.001-0.003 part by weight of oil-soluble antioxidant, and stirring until complete dissolution to prepare a core phase;
b. adding 0.12-0.72 weight part of wall material into 1-3 times of water, stirring and heating to 50-90 ℃, adding 0.001-0.01 weight part of water-soluble antioxidant, 0.025-0.08 weight part of water-soluble emulsifier and 0.001-0.03 weight part of stabilizer, and stirring until complete dissolution to obtain a wall material phase;
c. mixing a core material phase and a wall material phase, and carrying out high-speed shearing emulsification and homogenization by a high-pressure homogenizer to form a stable emulsion, wherein the shearing speed is 3000-20000 rpm, and the homogenization pressure is 20-80 MPa;
d. and carrying out spray drying and embedding on the emulsion, and then carrying out secondary embedding on the emulsion by a starch fluidized bed, wherein the fluidizing temperature is 0-60 ℃, and the weight part of the starch is 0.15-0.20, so as to prepare the natural plant essential oil microcapsule powder.
In some embodiments of the present invention, the wall material of the method for preparing natural plant essential oil microcapsule powder is one or a mixture of two or more of carrageenan, modified starch, maltodextrin, chitosan, gelatin, gum arabic, protein, and cellulose derivatives.
In some embodiments of the present invention, the water-soluble antioxidant is any one or more of sodium L-ascorbate, L-ascorbic acid, and tea polyphenol.
In some embodiments of the present invention, the particle size of the natural plant essential oil microcapsule powder is 0.5 to 10 μm.
The invention has the beneficial effects that:
1. according to the embroidery anticorrosion and antioxidation method for the three-dimensional patterns, the base material cloth and the upper layer cloth are soaked in the natural plant essential oil, most of the natural plant essential oil has obvious broad-spectrum antibacterial activity, and compared with a chemical antibacterial agent, the side effect and the residual toxicity of the natural plant essential oil are obviously reduced, so that the base material cloth and the upper layer cloth soaked in the natural plant essential oil have effective anticorrosion and antioxidation effects.
2. The invention provides an embroidery anticorrosion and antioxidation method of a three-dimensional pattern, wherein microcapsule powder of natural plant essential oil is filled in an elastic rubber plate, wherein the microcapsule powder is water-soluble microcapsule powder, in the cleaning process, a shell material is dissolved in water, and core material natural plant essential oil is adsorbed on embroidery of the three-dimensional pattern, so that the corruption and oxidation of the core material natural plant essential oil can be effectively inhibited.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below so that those skilled in the art can better understand the advantages and features of the present invention, and thus the scope of the present invention will be more clearly defined. The embodiments described herein are only a few embodiments of the present invention, rather than all embodiments, and all other embodiments that can be derived by one of ordinary skill in the art without inventive faculty based on the embodiments described herein are intended to fall within the scope of the present invention.
Example 1
Preparation of natural plant essential oil
Taking the seeds of the natural star anise, and drying the cleaned seeds of the star anise at 90 ℃ for 2 hours;
crushing the dried illicium verum seeds by using a crusher, and sieving the crushed illicium verum seeds by using a 80-mesh sieve;
thirdly, extracting the seed powder of the star anise by using a mixed solution obtained by acetone and ethyl-methyl ketone;
and step four, removing acetone and ethyl-methyl ketone by adopting a rotary evaporation mode to obtain a mixed solution, and decoloring to obtain the seed essential oil containing the star anise obtained from the extract liquor.
Preparation of plant essential oil microcapsule
Step one, stirring and heating 0.1-0.5 part by weight of seed essential oil of star anise as a core material to 30 ℃, adding 0.003 part by weight of oil-soluble emulsifier and 0.001 part by weight of oil-soluble antioxidant, and stirring until the oil-soluble emulsifier and the oil-soluble antioxidant are completely dissolved to prepare a core material phase;
adding 0.03 weight part of maltodextrin, 0.03 weight part of chitosan and 0.03 weight part of gelatin into water with the weight 1 time of that of the maltodextrin, stirring and heating to 50 ℃, adding 0.001 weight part of L-ascorbic acid, 0.025 weight part of water-soluble emulsifier and 0.001 weight part of stabilizer, and stirring until the materials are completely dissolved to prepare a wall material phase;
mixing the core material phase and the wall material phase, and performing high-speed shearing emulsification and homogenization by using a high-pressure homogenizer to form stable emulsion, wherein the shearing speed is 3000rpm, and the homogenization pressure is 20 MPa;
and step four, carrying out spray drying and embedding on the emulsion, and then carrying out secondary embedding on the emulsion by a starch fluidized bed, wherein the fluidizing temperature is 0 ℃, and the weight part of the starch is 0.15, so as to prepare the star anise seed essential oil microcapsule powder with the particle size of 0.5 mu m.
Embroidery of stereo pattern is anticorrosive anti-oxidant
S1, processing of cloth: selecting proper base material cloth and upper layer cloth according to actual needs, and completely soaking the base material cloth and the upper layer cloth in the natural plant essential oil for 0.5 h;
s2, preparing an elastic rubber plate: forming a plurality of holes with the grain diameter of 0.5 mu m on the elastic rubber plate, and filling 0.5 mu g/g of microcapsule powder containing the seed essential oil of the star anise in the step S1 on the elastic rubber plate with the holes;
s3, embroidering the three-dimensional pattern: sequentially stacking the elastic rubber sheet prepared in S2 and the upper layer cloth processed in S1 on the base cloth processed in S1, and placing them on an embroidering machine to embroider according to a pre-related pattern;
s4, cleaning the elastic rubber plate: and (5) rinsing the embroidery finished in the step S3 with clear water, and removing the elastic rubber plate at the non-embroidery part to obtain the three-dimensional pattern embroidery with corrosion resistance and oxidation resistance.
Example 2
Preparation of natural plant essential oil
Step one, taking stems of holly, and drying the cleaned stems of the holly at 105 ℃ for 6 hours;
step two, crushing the dried stems of the hollies by a crusher, and sieving the crushed stems by a 100-mesh sieve;
step three, extracting the stem powder of the holly by using a mixed solution obtained by acetone and ethyl-methyl ketone;
and step four, removing the acetone and the ethyl-methyl ketone by adopting a rotary evaporation mode to obtain a mixed solution, and decoloring to obtain the essential oil containing the stems of the holly obtained from the extract liquor.
Preparation of plant essential oil microcapsule
Step one, stirring and heating 0.4 part by weight of essential oil of stems of core materials of ilex chinensis to 50 ℃, adding 0.01 part by weight of oil-soluble emulsifier and 0.002 part by weight of oil-soluble antioxidant, and stirring until the essential oil is completely dissolved to prepare a core material phase;
step two, uniformly mixing 0.21 part by weight of carrageenan and 0.21 part by weight of modified starch, adding the mixture into water with the weight 2 times that of the carrageenan, stirring and heating the mixture to 70 ℃, adding 0.005 part by weight of sodium L-ascorbate, 0.05 part by weight of water-soluble emulsifier and 0.015 part by weight of stabilizer, and stirring the mixture until the mixture is completely dissolved to prepare a wall material phase;
mixing the core material phase and the wall material phase, and performing high-speed shearing emulsification and homogenization by using a high-pressure homogenizer to form stable emulsion, wherein the shearing speed is 11500rpm, and the homogenization pressure is 50 MPa;
and step four, carrying out spray drying and embedding on the emulsion, and then carrying out secondary embedding on the emulsion by a starch fluidized bed, wherein the fluidizing temperature is 30 ℃, and the weight part of starch is 0.175, so as to prepare the ilex chinensis essential oil microcapsule powder with the particle size of 5 mu m.
Embroidery of stereo pattern is anticorrosive anti-oxidant
S1, processing of cloth: selecting proper base material cloth and upper layer cloth according to actual needs, and completely soaking the base material cloth and the upper layer cloth in the natural plant essential oil for 1 h;
s2, preparing an elastic rubber plate: forming a plurality of holes with the grain diameter of 5 mu m on the elastic rubber plate, and filling 2.5 mu g/g of microcapsule powder containing the stems of the holly in the S1 step on the elastic rubber plate with the holes;
s3, embroidering the three-dimensional pattern: sequentially stacking the elastic rubber sheet prepared in S2 and the upper layer cloth processed in S1 on the base cloth processed in S1, and placing them on an embroidering machine to embroider according to a pre-related pattern;
s4, cleaning the elastic rubber plate: and (5) rinsing the embroidery finished in the step S3 with clear water, and removing the elastic rubber plate at the non-embroidery part to obtain the three-dimensional pattern embroidery with corrosion resistance and oxidation resistance.
Example 3
Preparation of natural plant essential oil
Firstly, taking petals of chrysanthemum in nature, and drying the cleaned petals of the chrysanthemum at 120 ℃ for 2 hours;
crushing the dried petals of the chrysanthemum by using a crusher, and sieving by using a 120-mesh sieve;
extracting petal powder of chrysanthemum with mixed solution of acetone and ethyl-methyl ketone;
and step four, removing acetone and ethyl-methyl ketone by adopting a rotary evaporation mode to obtain a mixed solution, and decoloring to obtain the chrysanthemum petal essential oil containing the chrysanthemum flower obtained from the extract liquor.
Preparation of plant essential oil microcapsule
Step one, stirring and heating 0.5 part by weight of petal essential oil of core material chrysanthemum to 70 ℃, adding 0.05 part by weight of oil-soluble emulsifier and 0.003 part by weight of oil-soluble antioxidant, and stirring until the petal essential oil is completely dissolved to prepare a core material phase;
adding 0.24 weight part of Arabic gum, 0.24 weight part of protein and 0.24 weight part of cellulose derivative into 3 times of water, stirring and heating to 90 ℃, adding 0.01 weight part of tea polyphenol, 0.08 weight part of water-soluble emulsifier and 0.03 weight part of stabilizer, stirring until the materials are completely dissolved, and preparing a wall material phase;
mixing the core material phase and the wall material phase, and homogenizing the mixture by a high-speed shearing emulsifying machine and a high-pressure homogenizer to form stable emulsion, wherein the shearing speed is 20000rpm, and the homogenizing pressure is 80 MPa;
and step four, carrying out spray drying and embedding on the emulsion, and then carrying out secondary embedding on the emulsion by a starch fluidized bed, wherein the fluidizing temperature is 60 ℃, and the weight part of the starch is 00.20, thus obtaining the chrysanthemum petal essential oil microcapsule powder with the particle size of 10 mu m.
Embroidery of stereo pattern is anticorrosive anti-oxidant
S1, processing of cloth: selecting proper base material cloth and upper layer cloth according to actual needs, and completely soaking the base material cloth and the upper layer cloth in the petal essential oil of the chrysanthemum for 2 hours;
s2, preparing an elastic rubber plate: forming a plurality of holes with the particle size of 10 mu m on the elastic rubber plate, and filling 5 mu g/g of microcapsule powder containing the chrysanthemum petal essential oil in the S1 step on the elastic rubber plate with the holes;
s3, embroidering the three-dimensional pattern: sequentially stacking the elastic rubber sheet prepared in S2 and the upper layer cloth processed in S1 on the base cloth processed in S1, and placing them on an embroidering machine to embroider according to a pre-related pattern;
s4, cleaning the elastic rubber plate: and (5) rinsing the embroidery finished in the step S3 with clear water, and removing the elastic rubber plate at the non-embroidery part to obtain the three-dimensional pattern embroidery with corrosion resistance and oxidation resistance.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention, and not for limiting the protection scope of the present invention, although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (10)
1. An embroidery anticorrosion antioxidation method of a three-dimensional pattern, the embroidery of the three-dimensional pattern is to stack an elastic rubber plate and an upper layer cloth on a base material cloth in sequence, place the elastic rubber plate and the upper layer cloth on an embroidery machine, and embroider according to a pre-related pattern, and is characterized in that: the embroidery anticorrosion and antioxidation method of the three-dimensional pattern comprises the following steps:
s1, processing of cloth: selecting proper base material cloth and upper layer cloth according to actual needs, and completely soaking the base material cloth and the upper layer cloth in the natural plant essential oil;
s2, preparing an elastic rubber plate: forming a plurality of holes with the particle size of 0.5-10 mu m on the elastic rubber plate, and filling microcapsule powder containing the natural plant essential oil obtained in the step S1 on the elastic rubber plate with the holes;
s3, embroidering the three-dimensional pattern: sequentially stacking the elastic rubber sheet prepared in S2 and the upper layer cloth processed in S1 on the base cloth processed in S1, and placing them on an embroidering machine to embroider according to a pre-related pattern;
s4, cleaning the elastic rubber plate: and (5) rinsing the embroidery finished in the step S3 with clear water, and removing the elastic rubber plate at the non-embroidery part to obtain the three-dimensional pattern embroidery with corrosion resistance and oxidation resistance.
2. The embroidery anticorrosion and antioxidation method of a three-dimensional pattern according to claim 1, characterized in that: the preparation method of the natural plant essential oil in the step S1 comprises the following steps:
a. taking plant tissues in nature, and drying the cleaned plant tissues at 90-120 ℃ for 2-10 h;
b. crushing the dried plant tissues by using a crusher, and sieving by using a sieve of 80-120 meshes;
c. extracting plant tissue powder with a mixed solution of acetone and ethyl-methyl ketone;
d. removing acetone and ethyl-methyl ketone by rotary evaporation to obtain mixed solution, and decolorizing to obtain natural plant essential oil from the extractive solution.
3. The embroidery anticorrosion and antioxidation method of the three-dimensional pattern according to claim 2, characterized in that: the plant tissue in the step b is one of roots, stems, leaves, flowers, seeds and fruits of natural plants.
4. The embroidery anticorrosion and antioxidation method of the three-dimensional pattern according to claim 2, characterized in that: the natural plant in the step a is selected from one of wintergreen, star anise, chrysanthemum and calendula.
5. The embroidery anticorrosion and antioxidation method of a three-dimensional pattern according to claim 1, characterized in that: the soaking time in the step S1 is 0.5-2 h.
6. The embroidery anticorrosion and antioxidation method of a three-dimensional pattern according to claim 1, characterized in that: the natural plant essential oil microcapsule powder in the step S2 is water-soluble natural plant essential oil microcapsule powder, and the filling amount of the natural plant essential oil microcapsule powder is 0.5-5 mu g/g.
7. The embroidery anticorrosion and antioxidation method of a three-dimensional pattern according to claim 1, characterized in that: the preparation method of the natural plant essential oil microcapsule powder in the step S2 is as follows:
a. stirring and heating 0.1-0.5 part by weight of core natural plant essential oil to 30-70 ℃, adding 0.003-0.05 part by weight of oil-soluble emulsifier and 0.001-0.003 part by weight of oil-soluble antioxidant, and stirring until complete dissolution to prepare a core phase;
b. adding 0.12-0.72 weight part of wall material into 1-3 times of water, stirring and heating to 50-90 ℃, adding 0.001-0.01 weight part of water-soluble antioxidant, 0.025-0.08 weight part of water-soluble emulsifier and 0.001-0.03 weight part of stabilizer, and stirring until complete dissolution to obtain a wall material phase;
c. mixing a core material phase and a wall material phase, and carrying out high-speed shearing emulsification and homogenization by a high-pressure homogenizer to form a stable emulsion, wherein the shearing speed is 3000-20000 rpm, and the homogenization pressure is 20-80 MPa;
d. and carrying out spray drying and embedding on the emulsion, and then carrying out secondary embedding on the emulsion by a starch fluidized bed, wherein the fluidizing temperature is 0-60 ℃, and the weight part of the starch is 0.15-0.20, so as to prepare the natural plant essential oil microcapsule powder.
8. The embroidery anticorrosion and antioxidation method of a three-dimensional pattern according to claim 7, characterized in that: the wall material is one or a mixture of two or more of carrageenan, modified starch, maltodextrin, chitosan, gelatin, Arabic gum, protein and cellulose derivatives.
9. The embroidery anticorrosion and antioxidation method of a three-dimensional pattern according to claim 1, characterized in that: the water-soluble antioxidant is one or more of L-sodium ascorbate, L-ascorbic acid and tea polyphenol.
10. The embroidery anticorrosion and antioxidation method of a three-dimensional pattern according to claim 1, characterized in that: the particle size of the natural plant essential oil microcapsule powder is 0.5-10 mu m.
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| CN105028706A (en) * | 2015-08-11 | 2015-11-11 | 刘进 | Peony seed oil microcapsule and preparation method of peony seed oil microcapsule |
| CN206733721U (en) * | 2017-03-15 | 2017-12-12 | 爱德纺织（杭州）有限公司 | A kind of antibiotic fabric |
| CN107232636A (en) * | 2017-07-28 | 2017-10-10 | 美泰科技（青岛）股份有限公司 | A kind of preparation method of water-soluble antarctic krill oil microcapsule powder |
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