CN111517826A - High-saturation amorphous photon structure colored glaze and preparation method thereof - Google Patents
High-saturation amorphous photon structure colored glaze and preparation method thereof Download PDFInfo
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Abstract
A high-saturation amorphous photon structure colored glaze and a preparation method thereof comprise the following steps; taking 60% of feldspar, 20% of quartz, 15% of calcite, 2% of talcum and 3% of kaolin according to the mass ratio as basic glaze, and adding 2-12% of Ca in the total mass of the basic glaze3(PO4)2As a phase separation promoter, 0.8 percent of sodium carboxymethylcellulose and 0.3 percent of sodium polyphosphate are used as dispersing agents, and meanwhile, a high-temperature light absorbing agent with the total mass of 5-30 percent of the basic glaze is introduced and uniformly mixed to obtain a mixed glaze; ball-milling the mixed glaze material by a wet method, and adjusting the specific gravity of glaze slip to 1.60-1.70g/cm3Uniformly applying glaze slip on the ceramic blank by adopting a glaze dipping method; and drying the glazed blank, then placing the dried glazed blank into an electric furnace for firing, adding a middle fire heat preservation process in a cooling stage, and finally cooling the glazed blank to room temperature along with the furnace to obtain the high-saturation amorphous photon structure colored glaze. The invention can not damage the glaze layer by introducing the high-temperature light absorbentThe amorphous photon structure can absorb incoherent scattered light, and the color saturation of the colored glaze of the amorphous photon structure is improved.
Description
Technical Field
The invention relates to the technical field of ceramic material manufacturing, in particular to a high-saturation amorphous photon structure colored glaze and a preparation method thereof.
Background
The color and decoration of the ceramic glaze layer are based on pigments introduced in the glaze, but the pigments are complex in preparation process, high in energy consumption and serious in pollution, and become a great obstacle to the green sustainable development of the ceramic industry. Compared with the traditional pigment, the structural color avoids environmental pollution caused by using a chemical pigment, can be never faded as long as the integrity of the micro-nano structure is kept, and has the characteristics of environmental protection, high brightness, high saturation and the like. Therefore, in the field of ceramic decoration, the structural color is used for replacing the traditional coloring material to generate color, so that the ceramic decoration has wide application prospect.
According to different sources of the structural color, the structural colored glaze can be divided into amorphous photon structural colored glaze and structural colored glaze formed by Rayleigh scattering and Mie scattering. As the amorphous photon structure has the characteristics of isotropic photonic band gap, non-iridescence effect, light localization and the like, the ceramic glaze is soft and bright and has a color rendering effect which is not changed along with the angle, and the ceramic glaze has a wider application space in the field of ceramic decoration (material guide, 2017,31(1): 43-55). However, in the amorphous photonic structure colored glaze, the color saturation of the structural color formed by Bragg scattering is reduced due to the influence of incoherent scattering (Advanced Materials,2018,30(28):1706654), and the color visibility is not strong, so that the wide application of the amorphous photonic structure colored glaze in the ceramic industry is limited.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention aims to provide the high-saturation amorphous photon structure colored glaze and the preparation method thereof.
In order to achieve the purpose, the invention adopts the technical scheme that:
a high-saturation amorphous photon structure colored glaze comprises the following components in parts by weight: 60% of feldspar, 20% of quartz, 15% of calcite, 2% of talcum, 3% of kaolin as base glaze, and Ca3(PO4)2The phase separation promoter is 2-12% of the total mass of the basic glaze, 0.8% of sodium carboxymethyl cellulose and 0.3% of sodium polyphosphate are used as dispersing agents, and the high-temperature light absorbent is 5-30% of the total mass of the basic glaze.
A preparation method of high-saturation amorphous photon structure colored glaze comprises the following steps;
the method comprises the following steps: taking 60% of feldspar, 20% of quartz, 15% of calcite, 2% of talcum and 3% of kaolin according to the mass ratio as basic glaze, and adding 2-12% of Ca in the total mass of the basic glaze3(PO4)2As a phase separation promoter, 0.8 percent of sodium carboxymethylcellulose and 0.3 percent of sodium polyphosphate are used as dispersing agents, and meanwhile, a high-temperature light absorbing agent with the total mass of 5-30 percent of the basic glaze is introduced, and the raw materials are fully and uniformly mixed to obtain a mixed glaze;
step two: ball-milling the mixed glaze material by a wet method to obtain glaze slip with the fineness of 250 meshes and the screened screen allowance of less than 0.5 percent, and adjusting the specific gravity of the glaze slip to be 1.60-1.70g/cm3Uniformly applying the glaze slip on the ceramic blank by adopting a glaze dipping method, wherein the glazing thickness is controlled to be 0.8-1.5 mm;
step three: and drying the glazed blank, then placing the dried glazed blank into an electric furnace for firing, adding a middle fire heat preservation process in a cooling stage, and finally cooling the glazed blank to room temperature along with the furnace to obtain the high-saturation amorphous photon structure colored glaze.
In the second step, the rotating speed of the ball mill is 300r/min, the ball milling time is 40min, and the mass ratio of the materials to the balls to the water is 1:2: 0.7.
The high-temperature light absorbing agent in the first step comprises but is not limited to various black pigments such as ferrochrome black, ferrochrome cobalt black and the like and any one of various black slags such as iron slag, manganese slag and the like.
The firing temperature of the electric furnace in the third step is 1160-.
The temperature of the heat preservation in the third step is 600-900 ℃, and the time duration is 10-60 min.
The invention has the beneficial effects that:
the invention introduces the high-temperature light absorbent into the amorphous photon structure colored glaze to absorb incoherent scattered light, is beneficial to improving the color saturation of the porcelain glaze and provides a new idea for widening the application range of the structure colored glaze. In addition, the preparation process is simple and convenient, can effectively replace pigments for color generation, can open up a new way for the color generation technology of ceramic color glaze, green and environment-friendly production of ceramic glaze and integration of structure and function, and has better industrial production application prospect.
Drawings
FIG. 1 shows the UV-VIS reflectance spectra of the surface of the amorphous photonic structure colored glaze at different iron ore slag addition amounts.
Detailed Description
The present invention will be described in further detail with reference to examples.
As shown in fig. 1: as can be seen from the figure, when the addition amount of the high temperature light absorbent iron ore slag was increased from 15 wt% to 25 wt%, the reflection peak of the glaze became high and the width became narrow, indicating that the color saturation of the structural color was enhanced.
The base glaze comprises 60% of feldspar, 20% of quartz, 15% of calcite, 2% of talcum and 3% of kaolin by mass. Ca accounting for 2 to 12 percent of the total mass of the basic glaze is added3(PO4)2As a phase separation promoter, 0.8% of sodium carboxymethylcellulose and 0.3% of sodium polyphosphate are used as dispersing agents. Meanwhile, a high-temperature light absorbing agent which accounts for 5-30% of the total mass of the base glaze is introduced, wherein the high-temperature light absorbing agent comprises but is not limited to various black pigments such as ferrochrome black and ferrochrome cobalt black and any one of various black slags such as iron slag and manganese slag.
The first embodiment is as follows:
the method comprises the following steps: 60 percent of feldspar, 20 percent of quartz, 15 percent of calcite, 2 percent of talcum and 3 percent of kaolin are taken as basic glaze according to the mass ratio, and Ca accounting for 2 percent of the total mass of the basic glaze is added3(PO4)2As a phase separation promoter, 0.8% of sodium carboxymethylcellulose and 0.3% of sodium polyphosphate are used as dispersing agents. Meanwhile, a high-temperature light absorbing agent with the total mass of 5% of the basic glaze is introduced, and the high-temperature light absorbing agent comprises but is not limited to various black pigments such as chromium iron black, chromium iron cobalt black and the like and any one of various black slag such as iron slag, manganese slag and the like. Fully and uniformly mixing the raw materials to obtain a mixed glaze material;
step two: ball-milling the mixed glaze material by a wet method to obtain glaze slip with the fineness of 250 meshes and the screened screen allowance of less than 0.5 percent, and adjusting the specific gravity of the glaze slip to be 1.60-1.70g/cm3Uniformly applying the glaze slip on the ceramic blank by adopting a glaze dipping method, wherein the glazing thickness is controlled to be 0.8-1.5 mm;
step three: drying the glazed blank, then placing the dried glazed blank into an electric furnace for firing, wherein the firing temperature is 1160 ℃, keeping the temperature for 20min, and in the cooling stage, increasing the middle-fire heat preservation process, wherein the heat preservation temperature is 600 ℃, and the duration is 10 min. And finally, cooling to room temperature along with the furnace to obtain the high-saturation amorphous photon structure colored glaze.
In the second step, the rotating speed of the ball mill is 300r/min, the ball milling time is 40min, and the mass ratio of the materials to the balls to the water is 1:2: 0.7.
Example two:
the method comprises the following steps: 60 percent of feldspar, 20 percent of quartz, 15 percent of calcite, 2 percent of talcum and 3 percent of kaolin are taken as basic glaze according to the mass ratio, and Ca accounting for 8 percent of the total mass of the basic glaze is added3(PO4)2As a phase separation promoter, 0.8% of sodium carboxymethylcellulose and 0.3% of sodium polyphosphate are used as dispersing agents. Meanwhile, a high-temperature light absorbing agent accounting for 15 percent of the total mass of the base glaze is introduced, and the high-temperature light absorbing agent comprises but is not limited to various black pigments such as chromium iron black, chromium iron cobalt black and the like and any one of various black slag such as iron slag, manganese slag and the like. Fully and uniformly mixing the raw materials to obtain a mixed glaze material;
step two: ball-milling the mixed glaze material by a wet method to obtain glaze slip with the fineness of 250 meshes and the screened screen allowance of less than 0.5 percent, and adjusting the specific gravity of the glaze slip to be 1.60-1.70g/cm3Uniformly applying the glaze slip on the ceramic blank by adopting a glaze dipping method, wherein the glazing thickness is controlled to be 0.8-1.5 mm;
step three: drying the glazed blank, then placing the dried glazed blank into an electric furnace for firing, wherein the firing temperature is 1250 ℃, preserving heat for 20min, and in the cooling stage, increasing the middle-fire heat preservation process, wherein the heat preservation temperature is 800 ℃, and the duration is 40 min. And finally, cooling to room temperature along with the furnace to obtain the high-saturation amorphous photon structure colored glaze.
In the second step, the rotating speed of the ball mill is 300r/min, the ball milling time is 40min, and the mass ratio of the materials to the balls to the water is 1:2: 0.7.
Example three:
the method comprises the following steps: 60 percent of feldspar, 20 percent of quartz, 15 percent of calcite, 2 percent of talcum and 3 percent of kaolin are taken as basic glaze according to the mass ratio, and Ca accounting for 12 percent of the total mass of the basic glaze is added3(PO4)2As a phase separation promoter, 0.8% of sodium carboxymethylcellulose and 0.3% of sodium polyphosphate are used as dispersing agents. Meanwhile, a high-temperature light absorbing agent with the total mass of 30% of the basic glaze is introduced, and the high-temperature light absorbing agent comprises but is not limited to various black pigments such as chromium iron black, chromium iron cobalt black and the like and any one of various black slag such as iron slag, manganese slag and the like. Fully and uniformly mixing the raw materials to obtain a mixed glaze material;
step two: ball-milling the mixed glaze material by a wet method to obtain glaze slip with the fineness of 250 meshes and the screened screen allowance of less than 0.5 percent, and adjusting the specific gravity of the glaze slip to be 1.60-1.70g/cm3Uniformly applying the glaze slip on the ceramic blank by adopting a glaze dipping method, wherein the glazing thickness is controlled to be 0.8-1.5 mm;
step three: drying the glazed blank, then placing the dried glazed blank into an electric furnace for firing, wherein the firing temperature is 1310 ℃, keeping the temperature for 20min, and in the cooling stage, increasing the middle-fire heat preservation process, wherein the heat preservation temperature is 900 ℃, and the duration is 60 min. And finally, cooling to room temperature along with the furnace to obtain the high-saturation amorphous photon structure colored glaze.
In the second step, the rotating speed of the ball mill is 300r/min, the ball milling time is 40min, and the mass ratio of the materials to the balls to the water is 1:2: 0.7.
Claims (6)
1. The high-saturation amorphous photon structure colored glaze is characterized by comprising the following components in parts by weight: 60% of feldspar, 20% of quartz, 15% of calcite, 2% of talcum and 3% of calcium carbonateKaolin as a base glaze, Ca3(PO4)2The phase separation promoter is 2-12% of the total mass of the basic glaze, 0.8% of sodium carboxymethyl cellulose and 0.3% of sodium polyphosphate are used as dispersing agents, and the high-temperature light absorbent is 5-30% of the total mass of the basic glaze.
2. The method for preparing the high-saturation amorphous photon structure colored glaze based on claim 1, which is characterized by comprising the following steps of;
the method comprises the following steps: taking 60% of feldspar, 20% of quartz, 15% of calcite, 2% of talcum and 3% of kaolin according to the mass ratio as basic glaze, and adding 2-12% of Ca in the total mass of the basic glaze3(PO4)2As a phase separation promoter, 0.8 percent of sodium carboxymethylcellulose and 0.3 percent of sodium polyphosphate are used as dispersing agents, and meanwhile, a high-temperature light absorbing agent with the total mass of 5-30 percent of the basic glaze is introduced, and the raw materials are fully and uniformly mixed to obtain a mixed glaze;
step two: ball-milling the mixed glaze material by a wet method to obtain glaze slip with the fineness of 250 meshes and the screened screen allowance of less than 0.5 percent, and adjusting the specific gravity of the glaze slip to be 1.60-1.70g/cm3Uniformly applying the glaze slip on the ceramic blank by adopting a glaze dipping method, wherein the glazing thickness is controlled to be 0.8-1.5 mm;
step three: and drying the glazed blank, then placing the dried glazed blank into an electric furnace for firing, adding a middle fire heat preservation process in a cooling stage, and finally cooling the glazed blank to room temperature along with the furnace to obtain the high-saturation amorphous photon structure colored glaze.
3. The method for preparing the high-saturation amorphous photon structure colored glaze according to claim 2, wherein the rotating speed of a ball mill in the second step is 300r/min, the ball milling time is 40min, and the mass ratio of material to ball to water is 1:2: 0.7.
4. The method for preparing a high-saturation colored glaze with an amorphous photonic structure according to claim 2, wherein the high-temperature light absorber in the first step includes but is not limited to black pigments such as ferrochrome black and ferrochrome cobalt black, and any one of black slags such as iron slag and manganese slag.
5. The method for preparing the high-saturation amorphous photon structure colored glaze according to claim 2, wherein the firing temperature of the electric furnace in the third step is 1160-.
6. The method for preparing the colored glaze with the high saturation amorphous photon structure according to claim 2, wherein the temperature of the heat preservation in the third step is 600-900 ℃ and the time duration is 10-60 min.
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113354280A (en) * | 2021-07-25 | 2021-09-07 | 景德镇陶瓷大学 | Preparation method of ceramic photon glaze with high photo-thermal conversion efficiency |
| CN114409376A (en) * | 2022-01-24 | 2022-04-29 | 陕西科技大学 | Preparation method of high-saturation amorphous photonic crystal structure colored glaze |
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| CN113354280A (en) * | 2021-07-25 | 2021-09-07 | 景德镇陶瓷大学 | Preparation method of ceramic photon glaze with high photo-thermal conversion efficiency |
| CN114409376A (en) * | 2022-01-24 | 2022-04-29 | 陕西科技大学 | Preparation method of high-saturation amorphous photonic crystal structure colored glaze |
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Application publication date: 20200811 |