CN111218350A - Fulvic acid feather cleaning agent and preparation method thereof - Google Patents
Fulvic acid feather cleaning agent and preparation method thereof Download PDFInfo
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
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- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
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- C11D1/02—Anionic compounds
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Abstract
The invention discloses a fulvic acid feather cleaning agent which comprises fulvic acid, a complexing agent, sodium dodecyl benzene sulfonate, fatty alcohol-polyoxyethylene ether, alkylphenol polyoxyethylene, tea saponin, an inorganic auxiliary agent, sodium carboxymethylcellulose and a cosolvent. Also discloses a preparation method of the fulvic acid feather cleaning agent, which has the advantages of simple preparation process, low requirement on production equipment and production cost reduction.
Description
Technical Field
The invention belongs to the field of fine chemical product preparation processes, and particularly relates to a fulvic acid feather cleaning agent and a preparation method thereof.
Background
The feather can be made into the badminton after being processed, so that the economic value is high, the requirement on the quality of the feather is high, and the resource intensification, environmental protection and green sustainable development can be realized in the feather cleaning process besides the chromaticity, toughness and rigidity of the feather. The existing feather cleaning agent is easy to cause feather damage due to improper use and unscientific component proportion, so that the feather is poor in color and integrity, the cleaning efficiency and the cleaning quality are not up to the standard, a certain degree of pollution can be caused to a water body after the feather cleaning agent is used, and the feather cleaning agent does not meet the development requirement of modern productivity.
Disclosure of Invention
The invention aims to provide a fulvic acid feather cleaning agent which has the performances of environmental protection, high efficiency and cleanness, effectively prevents the feather from being damaged in the cleaning process, and has good color and integrity.
The invention also aims to provide a preparation method of the fulvic acid feather cleaning agent, which is simple in preparation process and easy to operate.
The invention is realized by the following technical scheme:
the fulvic acid feather cleaning agent comprises the following components in parts by weight: 5-20 parts of fulvic acid, 1-5 parts of a complexing agent, 5-15 parts of sodium dodecyl benzene sulfonate, 1-3 parts of fatty alcohol-polyoxyethylene ether, 5-10 parts of alkylphenol ethoxylates, 1-3 parts of tea saponin, 1-4 parts of an inorganic auxiliary agent, 1-1.5 parts of sodium carboxymethylcellulose, 2-4 parts of a cosolvent and 100-120 parts of water.
Further, the fulvic acid is mineral fulvic acid or biochemical fulvic acid.
Further, the complexing agent is an ammonia-carboxyl complexing agent.
Further, the fatty alcohol-polyoxyethylene ether is one of AEO-7 and AEO-9.
Further, the alkylphenol polyoxyethylene ether is one of nonylphenol polyoxyethylene ether and octylphenol polyoxyethylene ether.
Further, the inorganic auxiliary agent is one or more of sodium hydroxide, sodium sulfate and sodium silicate.
Further, the cosolvent is one of sodium toluene sulfonate, sodium xylene sulfonate and urea.
The preparation method of the fulvic acid feather cleaning agent comprises the following steps:
1) preparing fulvic acid into a fulvic acid aqueous solution, and preparing sodium carboxymethylcellulose into a sodium carboxymethylcellulose aqueous solution;
2) mixing fulvic acid aqueous solution with a complexing agent to obtain an agent A;
3) mixing sodium carboxymethylcellulose aqueous solution with the agent A to obtain an agent B;
4) and mixing the agent B with sodium dodecyl benzene sulfonate, fatty alcohol-polyoxyethylene ether, alkylphenol polyoxyethylene, tea saponin, an inorganic auxiliary agent, a cosolvent and water to obtain a mixed solution, namely the fulvic acid feather cleaning agent.
Further, preparing the fulvic acid into a fulvic acid aqueous solution with the concentration of 3-8 wt%.
Further, sodium carboxymethylcellulose is prepared into 1-1.5 wt% sodium carboxymethylcellulose aqueous solution.
Compared with the prior art, the invention has the following beneficial technical effects:
the invention discloses a fulvic acid feather cleaning agent which comprises fulvic acid, a complexing agent, sodium dodecyl benzene sulfonate, fatty alcohol-polyoxyethylene ether, alkylphenol polyoxyethylene, tea saponin, an inorganic auxiliary agent, sodium carboxymethylcellulose and a cosolvent, wherein the fulvic acid is used as a raw material, is a component with the minimum molecular weight and the maximum activity in humic acid and is an essence in active ingredients of the humic acid, and the fulvic acid has various active functional groups in a structure and can effectively complex heavy metal ions in a water body; meanwhile, the fulvic acid belongs to a natural polymer compound, has a certain interface effect, can improve the flocculation resistance of the surfactant, the dirt-removing capacity and the environmental protection performance of the cleaning agent, and also has a protection effect on the feather surface.
The sodium dodecyl benzene sulfonate, the fatty alcohol-polyoxyethylene ether, the alkylphenol polyoxyethylene and the tea saponin are used as surfactants, and the washing decontamination effect is achieved mainly through the comprehensive effect of the basic actions of wetting, permeating, emulsifying, dispersing, solubilizing and the like. These surfactant components reduce the interfacial tension between water (liquid phase) -solid (solid-solid phase) and make it easier for the liquid phase water to adsorb and spread to the feather surface and penetrate into the feather, and this wetting action destroys the attraction between the feather and the dirt and also the mutual attraction between dirt particles. In the feather cleaning process, when a proper external force is applied for kneading, the existing state of the original structural force is destroyed, dirt is changed into solid micro-particles, and the solid particles are uniformly dispersed in water to form a dispersion liquid by reducing the interfacial tension between water and the solid micro-particles and forming a hydrophilic adsorption film around the solid micro-particles. The synergistic effect of the surfactant and the synergistic effect of the fulvic acid ensure that the cleaning agent has the effects of environmental protection, high efficiency and cleanness.
Furthermore, the complexing agent is an ammonia-carboxyl complexing agent which is a derivative taking aminodiacetic acid as a matrix, and the molecules contain ammonia nitrogen and carboxyl oxygen coordination atoms, so that the complexing ability of the derivatives is strong, the derivatives can form a complex with a ring structure with various metal ions, and the metal ions can be prevented from being precipitated, thereby removing the metal ions in water.
According to the preparation method of the fulvic acid feather cleaning agent, disclosed by the invention, fulvic acid is combined with a complexing agent through a scientific proportion, the fulvic acid feather cleaning agent is mixed with sodium carboxymethylcellulose, and finally the mixture is compounded with a surfactant, so that the stability of a product can be ensured, and the product performance is improved. The preparation process is simple, the requirement on production equipment is low, and the production cost is reduced.
Drawings
FIG. 1 is a schematic diagram of the formation of micelles of a surfactant in an aqueous solution;
FIG. 2 is a view of the structure of a differently treated shuttlecock.
Detailed Description
The present invention will now be described in further detail with reference to specific examples, which are intended to be illustrative, but not limiting, of the invention.
The fulvic acid feather cleaning agent comprises the following components in parts by weight: 5-20 parts of fulvic acid, 1-5 parts of a complexing agent, 5-15 parts of sodium dodecyl benzene sulfonate, 1-3 parts of fatty alcohol-polyoxyethylene ether, 5-10 parts of alkylphenol ethoxylates, 1-3 parts of tea saponin, 1-4 parts of an inorganic auxiliary agent, 1-1.5 parts of sodium carboxymethylcellulose, 2-4 parts of a cosolvent and 100-120 parts of water.
The raw materials used in the following examples are all commercially available products, and are not limited to manufacturers.
Example 1
The embodiment provides a preparation method of a fulvic acid feather cleaning agent, which specifically comprises the following steps:
1) taking the following components in parts by mass: 5 parts of mineral fulvic acid, 1 part of sodium ethylene diamine tetracetate, 5 parts of sodium dodecyl benzene sulfonate, 1 part of AEO-9, 5 parts of octylphenol polyoxyethylene ether, 1 part of tea saponin, 1 part of sodium hydroxide, 1 part of sodium carboxymethylcellulose, 2 parts of sodium xylene sulfonate and 100 parts of water;
2) preparing mineral fulvic acid into a 3 wt% mineral fulvic acid aqueous solution;
3) preparing sodium carboxymethylcellulose into a 1 wt% sodium carboxymethylcellulose aqueous solution;
4) mixing mineral fulvic acid aqueous solution with sodium ethylene diamine tetracetate to obtain an agent A;
5) mixing sodium carboxymethylcellulose with the agent A to obtain an agent B;
6) and mixing the agent B with sodium dodecyl benzene sulfonate, AEO-9, polyoxyethylene octylphenol ether, tea saponin, sodium hydroxide, sodium xylene sulfonate and water to obtain a mixed solution, namely the fulvic acid feather cleaning agent.
Example 2
The embodiment provides a preparation method of a fulvic acid feather cleaning agent, which specifically comprises the following steps:
1) taking the following components in parts by mass: 10 parts of biochemical fulvic acid, 5 parts of sodium ethylene diamine tetracetate, 10 parts of sodium dodecyl benzene sulfonate, 2 parts of AEO-9, 8 parts of octylphenol polyoxyethylene ether, 3 parts of tea saponin, 2 parts of sodium silicate, 1.5 parts of sodium carboxymethylcellulose, 3 parts of sodium xylene sulfonate and 120 parts of water;
2) preparing biochemical fulvic acid into 8 wt% biochemical fulvic acid aqueous solution;
3) preparing sodium carboxymethylcellulose into 1.5 wt% sodium carboxymethylcellulose aqueous solution;
4) mixing the biochemical fulvic acid aqueous solution with sodium ethylene diamine tetracetate to obtain an agent A;
5) mixing sodium carboxymethylcellulose aqueous solution with the agent A to obtain an agent B;
6) and mixing the agent B with sodium dodecyl benzene sulfonate, AEO-9, polyoxyethylene octylphenol ether, tea saponin, sodium silicate, sodium xylene sulfonate and water to obtain a mixed solution, namely the fulvic acid feather cleaning agent.
Example 3
The embodiment provides a preparation method of a fulvic acid feather cleaning agent, which specifically comprises the following steps:
1) taking the following components in parts by mass: 20 parts of biochemical fulvic acid, 5 parts of sodium ethylene diamine tetracetate, 15 parts of sodium dodecyl benzene sulfonate, 3 parts of AEO-9, 10 parts of octylphenol polyoxyethylene ether, 3 parts of tea saponin, 4 parts of sodium sulfate, 1.5 parts of sodium carboxymethylcellulose, 4 parts of sodium xylene sulfonate and 120 parts of water;
2) preparing biochemical fulvic acid into 5 wt% biochemical fulvic acid aqueous solution;
3) preparing sodium carboxymethylcellulose into a 1 wt% sodium carboxymethylcellulose aqueous solution;
4) mixing the biochemical fulvic acid aqueous solution with sodium ethylene diamine tetracetate to obtain an agent A;
5) mixing sodium carboxymethylcellulose aqueous solution with the agent A to obtain an agent B;
6) and mixing the agent B with sodium dodecyl benzene sulfonate, AEO-9, polyoxyethylene octylphenol ether, tea saponin, sodium sulfate, sodium xylene sulfonate and water to obtain a mixed solution, namely the fulvic acid feather cleaning agent.
Example 4
The embodiment provides a preparation method of a fulvic acid feather cleaning agent, which specifically comprises the following steps:
1) taking the following components in parts by mass: 8 parts of mineral fulvic acid, 3 parts of sodium ethylene diamine tetracetate, 10 parts of sodium dodecyl benzene sulfonate, 3 parts of AEO-9, 8 parts of nonylphenol polyoxyethylene ether, 1 part of tea saponin, 2 parts of sodium hydroxide, 1 part of sodium carboxymethylcellulose, 2 parts of urea and 110 parts of water;
2) preparing mineral fulvic acid into a 5 wt% mineral fulvic acid aqueous solution;
3) preparing sodium carboxymethylcellulose into a 1 wt% sodium carboxymethylcellulose aqueous solution;
4) mixing mineral fulvic acid aqueous solution with sodium ethylene diamine tetracetate to obtain an agent A;
5) mixing sodium carboxymethylcellulose aqueous solution with the agent A to obtain an agent B;
6) and mixing the agent B with sodium dodecyl benzene sulfonate, AEO-7, nonylphenol polyoxyethylene ether, tea saponin, sodium hydroxide, urea and water to obtain a mixed solution, namely the fulvic acid feather cleaning agent.
Example 5
The embodiment provides a preparation method of a fulvic acid feather cleaning agent, which specifically comprises the following steps:
1) taking the following components in parts by mass: 18 parts of mineral fulvic acid, 5 parts of sodium ethylene diamine tetracetate, 15 parts of sodium dodecyl benzene sulfonate, 2 parts of AEO-7, 5 parts of nonylphenol polyoxyethylene ether, 2 parts of tea saponin, 2 parts of sodium hydroxide, 1.5 parts of sodium carboxymethylcellulose, 3 parts of sodium toluene sulfonate and 120 parts of water;
2) preparing mineral fulvic acid into a 3 wt% mineral fulvic acid aqueous solution;
3) preparing sodium carboxymethylcellulose into a 1 wt% sodium carboxymethylcellulose aqueous solution;
4) mixing mineral fulvic acid aqueous solution with sodium ethylene diamine tetracetate to obtain an agent A;
5) mixing sodium carboxymethylcellulose aqueous solution with the agent A to obtain an agent B;
6) and mixing the agent B with sodium dodecyl benzene sulfonate, AEO-9, nonylphenol polyoxyethylene ether, tea saponin, sodium hydroxide, sodium toluenesulfonate and water to obtain a mixed solution, namely the fulvic acid feather cleaning agent.
Example 6
The embodiment provides a preparation method of a fulvic acid feather cleaning agent, which specifically comprises the following steps:
1) taking the following components in parts by mass: 10 parts of mineral fulvic acid, 2 parts of sodium ethylene diamine tetracetate, 15 parts of sodium dodecyl benzene sulfonate, 3 parts of AEO-7, 8 parts of octylphenol polyoxyethylene ether, 1 part of tea saponin, 3 parts of sodium hydroxide, 1.5 parts of sodium carboxymethylcellulose, 3 parts of sodium toluene sulfonate and 120 parts of water;
2) preparing mineral fulvic acid into a 5 wt% mineral fulvic acid aqueous solution;
3) preparing sodium carboxymethylcellulose into a 1 wt% sodium carboxymethylcellulose aqueous solution;
4) mixing mineral fulvic acid aqueous solution with sodium ethylene diamine tetracetate to obtain an agent A;
5) mixing sodium carboxymethylcellulose aqueous solution with the agent A to obtain an agent B;
6) and mixing the agent B with sodium dodecyl benzene sulfonate, AEO-9, polyoxyethylene octylphenol ether, tea saponin, sodium hydroxide, sodium toluene sulfonate and water to obtain a mixed solution, namely the fulvic acid feather cleaning agent.
Example 7
The embodiment provides a preparation method of a fulvic acid feather cleaning agent, which specifically comprises the following steps:
1) taking the following components in parts by mass: 15 parts of mineral fulvic acid, 2 parts of sodium ethylene diamine tetracetate, 10 parts of sodium dodecyl benzene sulfonate, 2 parts of AEO-9, 10 parts of octylphenol polyoxyethylene ether, 2 parts of tea saponin, 2 parts of sodium hydroxide, 1.3 parts of sodium carboxymethylcellulose, 2 parts of sodium xylene sulfonate and 110 parts of water;
2) preparing mineral fulvic acid into a 5 wt% mineral fulvic acid aqueous solution;
3) preparing sodium carboxymethylcellulose into 1.5 wt% sodium carboxymethylcellulose aqueous solution;
4) mixing mineral fulvic acid aqueous solution with sodium ethylene diamine tetracetate to obtain an agent A;
5) mixing sodium carboxymethylcellulose aqueous solution with the agent A to obtain an agent B;
6) and mixing the agent B with sodium dodecyl benzene sulfonate, AEO-9, polyoxyethylene octylphenol ether, tea saponin, sodium hydroxide, sodium xylene sulfonate and water to obtain a mixed solution, namely the fulvic acid feather cleaning agent.
Example 8
The embodiment provides a preparation method of a fulvic acid feather cleaning agent, which specifically comprises the following steps:
1) taking the following components in parts by mass: 20 parts of mineral fulvic acid, 3 parts of sodium ethylene diamine tetracetate, 11 parts of sodium dodecyl benzene sulfonate, 1 part of AEO-9, 9 parts of octylphenol polyoxyethylene ether, 2 parts of tea saponin, 2 parts of sodium hydroxide, 1.5 parts of sodium carboxymethylcellulose, 3 parts of sodium xylene sulfonate and 120 parts of water;
2) preparing mineral fulvic acid into a 3 wt% mineral fulvic acid aqueous solution;
3) preparing sodium carboxymethylcellulose into a 1 wt% sodium carboxymethylcellulose aqueous solution;
4) mixing mineral fulvic acid aqueous solution with sodium ethylene diamine tetracetate to obtain an agent A;
5) mixing sodium carboxymethylcellulose aqueous solution with the agent A to obtain an agent B;
6) and mixing the agent B with sodium dodecyl benzene sulfonate, AEO-9, polyoxyethylene octylphenol ether, tea saponin, sodium hydroxide, sodium xylene sulfonate and water to obtain a mixed solution, namely the fulvic acid feather cleaning agent.
The cleaning agent prepared by the invention takes the fulvic acid as a raw material, the fulvic acid is a plant growth regulator, can promote the growth of plants, has important effects on drought resistance, can improve the stress resistance of the plants, has the effects of increasing yield and improving quality, and simultaneously has various active functional groups, can effectively complex heavy metal ions in water, softens water quality and improves the dirt-removing capacity of the cleaning agent. The natural high molecular compound fulvic acid is used as a raw material, so that heavy metal ions in a water body can be effectively complexed, the water quality is softened, and the dirt-removing capacity of the cleaning agent is improved. The sodium dodecyl benzene sulfonate, the fatty alcohol-polyoxyethylene ether, the alkylphenol polyoxyethylene and the tea saponin are used as surfactants, and the washing decontamination effect is achieved through the comprehensive effect of the basic actions of wetting, permeating, emulsifying, dispersing, solubilizing and the like.
As shown in fig. 1, the surfactant-formed micelles dissolve the oil in the hydrophobic group moiety, resulting in increased solubility of the substance in the solvent. The comprehensive effect of the surfactant and the synergistic effect of the fulvic acid on the surfactant ensure that the cleaning agent has the effects of environmental protection, high efficiency and cleanness.
The fulvic acid feather cleaning agent prepared in the examples 1 to 8 and a certain cleaning agent (comparative example) sold in the market are respectively cleaned according to the same cleaning method, and the comparative cleaning results are shown in the following table 1-5:
TABLE 1 Effect of different treatments on feather cleanliness
As can be seen from Table 1, the feather cleanliness of the fulvic acid feather cleaner-treated feathers was, on average, 98.33% higher than that of the blank water treatment sample and the commercial product, 63.03% higher than that of the blank water treatment sample and 17.83% higher than that of the commercial product. In example 2, the feather cleanliness is the highest and reaches 99.8%.
As can be seen from Table 2, the feather damage degree of the fulvic acid feather cleaning agent treatment was 0%, 7.5% higher than that of the blank water treatment and 11.3% higher than that of the commercial product, compared with the blank water treatment and the commercial product.
TABLE 2 Effect of different treatments on feather damage
As can be seen from Table 3, the yellow humic acid feather cleaning agent has no pollution to water after processing feathers, compared with the commercial products, which cause slight pollution to water.
TABLE 3 influence of different treatments on the water pollution situation
TABLE 4 appearance and stability of cleaning agent
As can be seen from Table 4, the appearance was partly yellowish clear, and both the fulvic acid cleaner and the commercial product had good stability. On one hand, the cleaning agent is light yellow because the inherent color of the raw material fulvic acid, a large number of chromogenic groups are conjugated in the molecular structure of the fulvic acid, so that the absorption section can be moved to the direction of longer wavelength, and the color can be developed when the wavelength of the absorbed light is moved to the visible light region; on the other hand, the color appears when the used surfactant is compounded, but the product performance is not influenced.
TABLE 5 foaming power of cleaning agent
As can be seen from Table 5, the foaming power of the fulvic acid cleaning agent is generally lower than that of the commercial product, the situation of difficult cleaning can occur due to abundant foam in consideration of the problem of wastewater treatment in the feather cleaning process, and the low-foam formula better meets the requirement of productivity.
The fulvic acid feather cleaning agent is taken to clean the same shuttlecock with a certain cleaning agent sold in the market according to the same cleaning method respectively to obtain the result shown in figure 2, and as can be seen from figure 2, the fulvic acid feather cleaning agent does not damage the feather twig structure, the inner feather sheet and the outer feather sheet can keep the original forms, and the feathers have good flexibility, color and integrity.
The commercial product comprises non-anionic SAA, an emulsifier and an inorganic salt builder, the consumption is large, the foam is large, and the abundant foam is not easy to be subsequently treated in terms of environmental protection. Meanwhile, the structure of the cleaned feather is damaged, so that the subsequent processing and utilization of the feather are limited. Besides the components of the commercial product, the components of the invention also contain fulvic acid, complexing agent and cosolvent, which can ensure the stability and cleaning performance of the product, and in addition, the added sodium carboxymethyl cellulose, tea saponin and the like are all environment-friendly raw materials, the proportion of the whole system is scientific, the use concentration is low, and the requirements of sustainable development are better met.
In conclusion, the fulvic acid is used as a raw material, so that heavy metal ions in a water body can be effectively complexed, the decontamination capability and the environmental protection performance of the cleaning agent are improved, and the cleaning agent is ensured to have green, environment-friendly, efficient and clean effects through the synergistic effect of the surfactants and the synergistic effect of the fulvic acid on the surfactants. Compared with a certain cleaning agent sold in the market, the fulvic acid feather cleaning agent disclosed by the invention is good in cleaning effect, scientific in component proportion, less in foaming and easy to clean, the feather is effectively prevented from being damaged in the cleaning process, the obtained feather is good in color and integrity, and pollution is avoided.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (10)
1. The fulvic acid feather cleaning agent is characterized by comprising the following components in parts by mass: 5-20 parts of fulvic acid, 1-5 parts of a complexing agent, 5-15 parts of sodium dodecyl benzene sulfonate, 1-3 parts of fatty alcohol-polyoxyethylene ether, 5-10 parts of alkylphenol ethoxylates, 1-3 parts of tea saponin, 1-4 parts of an inorganic auxiliary agent, 1-1.5 parts of sodium carboxymethylcellulose, 2-4 parts of a cosolvent and 100-120 parts of water.
2. The fulvic acid feather cleaning agent according to claim 1, wherein the fulvic acid is a mineral source fulvic acid or a biochemical fulvic acid.
3. The fulvic acid feather cleaning agent according to claim 1, wherein the complexing agent is an ammonia-carboxylic acid complexing agent.
4. The fulvic acid feather cleaning agent according to claim 1, wherein the fatty alcohol-polyoxyethylene ether is one of AEO-7 and AEO-9.
5. The fulvic acid feather cleaning agent according to claim 1, wherein the alkylphenol ethoxylate is one of nonylphenol ethoxylate and octylphenol ethoxylate.
6. The fulvic acid feather cleaning agent according to claim 1, wherein the inorganic auxiliary agent is one or more of sodium hydroxide, sodium sulfate and sodium silicate.
7. The fulvic acid feather cleaning agent according to claim 1, wherein the cosolvent is one of sodium toluene sulfonate, sodium xylene sulfonate and urea.
8. The preparation method of the fulvic acid feather cleaning agent as defined in any one of claims 1 to 7, comprising the following steps:
1) preparing fulvic acid into a fulvic acid aqueous solution, and preparing sodium carboxymethylcellulose into a sodium carboxymethylcellulose aqueous solution;
2) mixing fulvic acid aqueous solution with a complexing agent to obtain an agent A;
3) mixing sodium carboxymethylcellulose aqueous solution with the agent A to obtain an agent B;
4) and mixing the agent B with sodium dodecyl benzene sulfonate, fatty alcohol-polyoxyethylene ether, alkylphenol polyoxyethylene, tea saponin, an inorganic auxiliary agent, a cosolvent and water to obtain a mixed solution, namely the fulvic acid feather cleaning agent.
9. The method according to claim 8, wherein the fulvic acid is prepared as a 3-8 wt% fulvic acid aqueous solution.
10. The preparation method according to claim 8, wherein the sodium carboxymethylcellulose is prepared as a 1-1.5 wt% sodium carboxymethylcellulose aqueous solution.
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| CN202210003787.1A CN114292710A (en) | 2020-02-12 | 2020-02-12 | Feather cleaning agent and preparation method thereof |
| CN202010089223.5A CN111218350A (en) | 2020-02-12 | 2020-02-12 | Fulvic acid feather cleaning agent and preparation method thereof |
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| CN202010089223.5A CN111218350A (en) | 2020-02-12 | 2020-02-12 | Fulvic acid feather cleaning agent and preparation method thereof |
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| CN202010089223.5A Pending CN111218350A (en) | 2020-02-12 | 2020-02-12 | Fulvic acid feather cleaning agent and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113293067A (en) * | 2021-05-28 | 2021-08-24 | 陕西科技大学 | Fulvic acid type green environment-friendly down feather cleaning agent and preparation method thereof |
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| CN114292710A (en) | 2022-04-08 |
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