CN111117794A - 一种洗碗机复合洗涤剂的制备工艺 - Google Patents
一种洗碗机复合洗涤剂的制备工艺 Download PDFInfo
- Publication number
- CN111117794A CN111117794A CN201911387608.3A CN201911387608A CN111117794A CN 111117794 A CN111117794 A CN 111117794A CN 201911387608 A CN201911387608 A CN 201911387608A CN 111117794 A CN111117794 A CN 111117794A
- Authority
- CN
- China
- Prior art keywords
- parts
- weight
- washing
- preparing
- particles
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/825—Mixtures of compounds all of which are non-ionic
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0008—Detergent materials or soaps characterised by their shape or physical properties aqueous liquid non soap compositions
- C11D17/0013—Liquid compositions with insoluble particles in suspension
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/044—Hydroxides or bases
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/046—Salts
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/04—Water-soluble compounds
- C11D3/10—Carbonates ; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/1233—Carbonates, e.g. calcite or dolomite
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/1253—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
- C11D3/1266—Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in liquid compositions
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/02—Inorganic compounds ; Elemental compounds
- C11D3/12—Water-insoluble compounds
- C11D3/124—Silicon containing, e.g. silica, silex, quartz or glass beads
- C11D3/1246—Silicates, e.g. diatomaceous earth
- C11D3/128—Aluminium silicates, e.g. zeolites
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/18—Hydrocarbons
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2003—Alcohols; Phenols
- C11D3/2065—Polyhydric alcohols
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/2093—Esters; Carbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/20—Organic compounds containing oxygen
- C11D3/22—Carbohydrates or derivatives thereof
- C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
- C11D3/225—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin etherified, e.g. CMC
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/34—Organic compounds containing sulfur
- C11D3/3418—Toluene -, xylene -, cumene -, benzene - or naphthalene sulfonates or sulfates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/38—Products with no well-defined composition, e.g. natural products
- C11D3/381—Microorganisms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/50—Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
- C11D1/66—Non-ionic compounds
- C11D1/72—Ethers of polyoxyalkylene glycols
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Inorganic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Molecular Biology (AREA)
- Microbiology (AREA)
- Detergent Compositions (AREA)
Abstract
本发明公开一种洗碗机复合洗涤剂的制备工艺,属于洗涤剂技术领域,包括如下步骤:第1步、制备洗碗液基础液;第2步、制备洗涤颗粒;第3步、按重量份计,将洗碗液基础液、洗涤颗粒、羧甲基纤维素、液体石蜡、氯化钠、山梨醇、益生菌和香,混合搅拌,搅拌均匀即可。本发明提供的洗碗机洗涤剂,是通过改进洗涤基础液,并通过加入具有颗粒较小的洗涤颗粒,在洗碗机洗涤过程中,利用洗涤颗粒对表面污渍的冲击作用,有效并快速去除污渍,同时利用洗涤成分对碗碟表面进行二次洁净处理,由此达到非常理想的洗涤效果,更为重要的是,洗涤颗粒的加入,可以有效降低表面活性剂的配比,进而有效控制残留,洗涤效果更为优异。
Description
技术领域
本发明公开一种洗碗机复合洗涤剂的制备工艺,属于生活技术领域,具体为一种洗碗机复合洗涤剂的制备工艺。
背景技术
洗碗机洗涤剂是一种适合洗碗机冲洗工序的专用洗涤剂,因其溶液呈碱性,故一般称作洗碗机碱液,富含高浓度洗涤助剂及软水剂。现有的洗涤剂包括液体和粉体,其作用机理是都是利用洗碗机冲洗喷嘴所产生的高温高压水流从不同的角度将洗涤剂喷射到餐具上,从而对餐具的产生较大的摩擦力,迅速冲洗、分解掉残留在餐具上的油污、饭粒等食物残渣。
现有技术中,洗碗机洗涤剂均为浓缩的清洗剂,包括洗涤主剂和助剂,洗涤主剂为一般的洗涤剂,包括表面活性剂等材料,为适应洗碗机的工作程序,目前洗涤剂均具有一定的渗透、皂化、乳化等作用,以达到去除油污之作用,但是,又不同于传统的洗涤剂,洗碗机具有一定的高压冲洗过程,因此,对于洗涤剂也有一定的要求,即快速去污能力,故,洗碗机洗涤剂对其的要求应当是快递去污和有效去污两个方面,而且必须适合洗碗机的洗涤程序。
CN 105087177A专利文献公开了“一种洗碗机用洗涤剂”,包括按照重量份计的下列物质:AES25-30份,磺酸4-8份,柠檬香精3-6份,十二烷基硫酸钠15-21份,烷醇酰胺11-31份,甘氨酸1-3份,脂肪醇聚氧乙烯3-8份,醚乙酸钠7-10份,烷基苯磺酸钠2-3份,烷基酚聚氧乙烯醚4-6份,二丙二醇丁醚1-6份,脂肪醇硫酸钠2-4份,水100份。
由此可知,上述洗涤剂的技术方案,主要是阴离子表面活性剂加上常规组分构成的技术方案,其洗涤效果在常规条件下尚可,但是很显然这个技术方案对于洗碗机并没有针对性,洗碗机高压冲洗过程,实际上两个过程,分别是“冲”和“洗”的过程,对于“洗”的过程,该技术方案具有一定效果,但是,对于“冲”的过程,依然没有改变现有技术中水溶液冲洗的过程;而且,在洗碗机洗涤过程中,“冲”的作用要明显优于“洗”的过程,高压水流会把污渍冲掉,能否“冲”干净也决定下一步“洗”的过程是否充分,因此,该方案只有“洗”,而缺少较为理想的“冲”的效果。
发明内容
本发明的目的是解决目前洗碗机洗涤液冲洗效果不理想的缺陷,主要是在通过制备洗涤基础液和加入洗涤颗粒,由此制备得到具有优良冲洗效果的洗碗机洗涤剂。
技术方案:
一种洗碗机复合洗涤剂的制备工艺,包括如下步骤:
第1步、制备洗碗液基础液:按重量计,取非离子聚丙烯酰胺20~40份、肉豆蔻酸异丙酯5~15份、柠檬酸甘油酯12~25份、丙烯酸丁酯2~5份、ETDA二钠3~8份和辛基酚聚氧乙烯醚2~4份放入反应器中,加入碱金属氢氧化物的水溶液15~35份混合均匀,即制备得到洗碗液基础液;
第2步、制备洗涤颗粒:按重量份计,取碳酸钙1~3份、碳酸钠2~5份、硅酸铝1~3份、二甲苯磺酸钠1~2份、白炭黑1~2份、沸石粉2~5份和膨润土2~5份放入模具中,置于高温炉中进行高温高压煅烧,煅烧时间1~3h,冷却后破碎,放入纳米研磨机中研磨至平均粒径200~500nm,得到洗涤颗粒;
第3步、按重量份计,将洗碗液基础液、洗涤颗粒、羧甲基纤维素5~12份、液体石蜡1~3份、氯化钠1~2份、山梨醇3~8份、益生菌1~2份和香精1~2份,混合搅拌,搅拌均匀即可。
作为优选,所述第1步中,碱金属氢氧化物为氢氧化钾,氢氧化钾物质的量浓度为1.2~3.0mol/L。
作为优选,所述第2步中,高温高压煅烧的温度为950~1050℃。
作为优选,所述第2步中,高温高压煅烧的压力为100~200MPa。
作为优选,所述第3步中,所述益生菌为乳酸菌、双歧杆菌或两者的组合。
有益效果
本发明提供的洗碗机洗涤剂,是通过改进洗涤基础液,并通过加入具有颗粒较小的洗涤颗粒,在洗碗机洗涤过程中,利用洗涤颗粒对表面污渍的冲击作用,有效并快速去除污渍,同时利用洗涤成分对碗碟表面进行二次洁净处理,由此达到非常理想的洗涤效果,更为重要的是,洗涤颗粒的加入,可以有效降低表面活性剂的配比,进而有效控制残留,洗涤效果更为优异。
具体实施方式
为了进一步理解本发明,下面结合实施例对本发明优选实施方案进行描述,但是应当理解,这些描述只是为进一步说明本发明的特征和优点,而不是对本发明权利要求的限制。
实施例1
一种洗碗机复合洗涤剂的制备工艺,包括如下步骤:
第1步、制备洗碗液基础液:取非离子聚丙烯酰胺40份、肉豆蔻酸异丙酯15份、柠檬酸甘油酯25份、丙烯酸丁酯5份、ETDA二钠8份和辛基酚聚氧乙烯醚4份放入反应器中,加入物质的量浓度为2.8mol/L的氢氧化钾溶液32份混合均匀,即制备得到洗碗液基础液;
第2步、制备洗涤颗粒:取碳酸钙3份、碳酸钠5份、硅酸铝3份、二甲苯磺酸钠2份、白炭黑2份、沸石粉5份和膨润土5份放入模具中,置于高温炉中进行高温高压煅烧,温度1050℃,压力200MPa,煅烧时间3h,冷却后破碎,放入纳米研磨机中研磨至平均粒径300nm,得到洗涤颗粒;
第3步、将洗碗液基础液、洗涤颗粒、羧甲基纤维素12份、液体石蜡3份、氯化钠2份、山梨醇8份、乳酸菌2份和香精2份,混合搅拌,搅拌均匀即可。
实施例2
一种洗碗机复合洗涤剂的制备工艺,包括如下步骤:
第1步、制备洗碗液基础液:取非离子聚丙烯酰胺20份、肉豆蔻酸异丙酯5份、柠檬酸甘油酯12份、丙烯酸丁酯2份、ETDA二钠3份和辛基酚聚氧乙烯醚2份放入反应器中,加入物质的量浓度为1.5mol/L的氢氧化钾溶液18份混合均匀,即制备得到洗碗液基础液;
第2步、制备洗涤颗粒:取碳酸钙1份、碳酸钠2份、硅酸铝1份、二甲苯磺酸钠1份、白炭黑1份、沸石粉2份和膨润土2份放入模具中,置于高温炉中进行高温高压煅烧,温度1050℃,压力200MPa,煅烧时间1h,冷却后破碎,放入纳米研磨机中研磨至平均粒径300nm,得到洗涤颗粒;
第3步、按重量份计,将洗碗液基础液、洗涤颗粒、羧甲基纤维素5份、液体石蜡1份、氯化钠1份、山梨醇3份、乳酸菌1份和香精1份,混合搅拌,搅拌均匀即可。
实施例3
一种洗碗机复合洗涤剂的制备工艺,包括如下步骤:
第1步、制备洗碗液基础液:取非离子聚丙烯酰胺36份、肉豆蔻酸异丙酯13份、柠檬酸甘油酯21份、丙烯酸丁酯4份、ETDA二钠7份和辛基酚聚氧乙烯醚3份放入反应器中,加入物质的量浓度为2.2mol/L的氢氧化钾溶液24份混合均匀,即制备得到洗碗液基础液;
第2步、制备洗涤颗粒:取碳酸钙2.5份、碳酸钠4.2份、硅酸铝2.2份、二甲苯磺酸钠1.7份、白炭黑1.8份、沸石粉4.3份和膨润土4.5份放入模具中,置于高温炉中进行高温高压煅烧,温度1000℃,压力180MPa,煅烧时间2h,冷却后破碎,放入纳米研磨机中研磨至平均粒径300nm,得到洗涤颗粒;
第3步、将洗碗液基础液、洗涤颗粒、羧甲基纤维素10份、液体石蜡2.4份、氯化钠1.7份、山梨醇7.1份、双歧杆菌1.6份和香精1.7份,混合搅拌,搅拌均匀即可。
实施例4
一种洗碗机复合洗涤剂的制备工艺,包括如下步骤:
第1步、制备洗碗液基础液:按重量计,取非离子聚丙烯酰胺26份、肉豆蔻酸异丙酯8份、柠檬酸甘油酯17份、丙烯酸丁酯3份、ETDA二钠5份和辛基酚聚氧乙烯醚3份放入反应器中,加入物质的量浓度为1.8mol/L的氢氧化钾溶液19份混合均匀,即制备得到洗碗液基础液;
第2步、制备洗涤颗粒:取碳酸钙1.2份、碳酸钠2.6份、硅酸铝1.5份、二甲苯磺酸钠1.3份、白炭黑1.3份、沸石粉3.2份和膨润土2.9份放入模具中,置于高温炉中进行高温高压煅烧,温度1000℃,压力150MPa,煅烧时间2h,冷却后破碎,放入纳米研磨机中研磨至平均粒径300nm,得到洗涤颗粒;
第3步、按重量份计,将洗碗液基础液、洗涤颗粒、羧甲基纤维素7份、液体石蜡1.4份、氯化钠1.3份、山梨醇4.8份、双歧杆菌1.2份和香精1.3份,混合搅拌,搅拌均匀即可。
实施例5
一种洗碗机复合洗涤剂的制备工艺,包括如下步骤:
第1步、制备洗碗液基础液:取非离子聚丙烯酰胺32份、肉豆蔻酸异丙酯11份、柠檬酸甘油酯19份、丙烯酸丁酯3.5份、ETDA二钠5.8份和辛基酚聚氧乙烯醚2.8份放入反应器中,加入物质的量浓度为2.5mol/L的氢氧化钾溶液24份混合均匀,即制备得到洗碗液基础液;
第2步、制备洗涤颗粒:按重量份计,取碳酸钙2.1份、碳酸钠3.6份、硅酸铝2.2份、二甲苯磺酸钠1.5份、白炭黑1.7份、沸石粉3.6份和膨润土3.8份放入模具中,置于高温炉中进行高温高压煅烧,温度1000℃,压力180MPa,煅烧时间2h,冷却后破碎,放入纳米研磨机中研磨至平均粒径300nm,得到洗涤颗粒;
第3步、将洗碗液基础液、洗涤颗粒、羧甲基纤维素9份、液体石蜡2.2份、氯化钠1.6份、山梨醇6.5份、乳酸菌1.6份和香精1.2份,混合搅拌,搅拌均匀即可。
对照例1
与实施例5的区别在于:第1步中未加入非离子聚丙烯酰胺。
一种洗碗机复合洗涤剂的制备工艺,包括如下步骤:
第1步、制备洗碗液基础液:取肉豆蔻酸异丙酯11份、柠檬酸甘油酯19份、丙烯酸丁酯3.5份、ETDA二钠5.8份和辛基酚聚氧乙烯醚2.8份放入反应器中,加入物质的量浓度为2.5mol/L的氢氧化钾溶液24份混合均匀,即制备得到洗碗液基础液;
第2步、制备洗涤颗粒:按重量份计,取碳酸钙2.1份、碳酸钠3.6份、硅酸铝2.2份、二甲苯磺酸钠1.5份、白炭黑1.7份、沸石粉3.6份和膨润土3.8份放入模具中,置于高温炉中进行高温高压煅烧,温度1000℃,压力180MPa,煅烧时间2h,冷却后破碎,放入纳米研磨机中研磨至平均粒径300nm,得到洗涤颗粒;
第3步、将洗碗液基础液、洗涤颗粒、羧甲基纤维素9份、液体石蜡2.2份、氯化钠1.6份、山梨醇6.5份、乳酸菌1.6份和香精1.2份,混合搅拌,搅拌均匀即可。
对照例2
与实施例5的区别在于:未加入洗涤颗粒。
一种洗碗机复合洗涤剂的制备工艺,包括如下步骤:
第1步、制备洗碗液基础液:取非离子聚丙烯酰胺32份、肉豆蔻酸异丙酯11份、柠檬酸甘油酯19份、丙烯酸丁酯3.5份、ETDA二钠5.8份和辛基酚聚氧乙烯醚2.8份放入反应器中,加入物质的量浓度为2.5mol/L的氢氧化钾溶液24份混合均匀,即制备得到洗碗液基础液;
第2步、将洗碗液基础液、羧甲基纤维素9份、液体石蜡2.2份、氯化钠1.6份、山梨醇6.5份、乳酸菌1.6份和香精1.2份,混合搅拌,搅拌均匀即可。
将上述实施例和对照例制备得到的洗碗机洗涤剂,根据《GB/T 24692 2009》进行性能测试:
首先,检测洗碗机洗涤剂本身的基本参数,结果如表1所示:
表1 实施例和对照例基本参数
由上表可知,实施例和对照例的洗碗机洗涤剂基本参数均符合要求,无明显差异;均具有良好的稳定性。
其次,选取洗碗机,型号方太Q5,按照要求组装洗碗机之后,加入洗涤剂分别进行测试,并加入空白对照例3,即不适用洗涤剂,结果如表2所示:
表2 实施例和对照例清洗效果测试
由上表可知,实施例1~5的清洗效果要优于对照例1~3,性能等级达到最高级别5级别,对照例1清洗效果为4级,清洗过后有小污点,因未加入非离子聚丙烯酰胺,对清洗效果有一定的影响;对照例2清洗效果未4级,说明加入洗涤颗粒之后,洗涤效果明显增强;对照例3为空白对照。以上说明,经过对洗涤基础液的改进和加入洗涤颗粒之后,洗碗机洗涤液的洗涤效果更为理想。
Claims (5)
1.一种洗碗机复合洗涤剂的制备工艺,其特征在于,包括如下步骤:
第1步、制备洗碗液基础液:按重量计,取非离子聚丙烯酰胺20~40份、肉豆蔻酸异丙酯5~15份、柠檬酸甘油酯12~25份、丙烯酸丁酯2~5份、ETDA二钠3~8份和辛基酚聚氧乙烯醚2~4份放入反应器中,加入碱金属氢氧化物的水溶液15~35份混合均匀,即制备得到洗碗液基础液;
第2步、制备洗涤颗粒:按重量份计,取碳酸钙1~3份、碳酸钠2~5份、硅酸铝1~3份、二甲苯磺酸钠1~2份、白炭黑1~2份、沸石粉2~5份和膨润土2~5份放入模具中,置于高温炉中进行高温高压煅烧,煅烧时间1~3h,冷却后破碎,放入纳米研磨机中研磨至平均粒径200~500nm,得到洗涤颗粒;
第3步、按重量份计,将洗碗液基础液、洗涤颗粒、羧甲基纤维素5~12份、液体石蜡1~3份、氯化钠1~2份、山梨醇3~8份、益生菌1~2份和香精1~2份,混合搅拌,搅拌均匀即可。
2.根据权利要求1所述的洗碗机复合洗涤剂的制备工艺,其特征在于:所述第1步中,碱金属氢氧化物为氢氧化钾,氢氧化钾物质的量浓度为1.2~3.0mol/L。
3.根据权利要求1所述的洗碗机复合洗涤剂的制备工艺,其特征在于:所述第2步中,高温高压煅烧的温度为950~1050℃。
4.根据权利要求1所述的洗碗机复合洗涤剂的制备工艺,其特征在于:所述第2步中,高温高压煅烧的压力为100~200MPa。
5.根据权利要求1所述的洗碗机复合洗涤剂的制备工艺,其特征在于:所述第3步中,所述益生菌为乳酸菌、双歧杆菌或两者的组合。
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201911387608.3A CN111117794A (zh) | 2019-12-30 | 2019-12-30 | 一种洗碗机复合洗涤剂的制备工艺 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201911387608.3A CN111117794A (zh) | 2019-12-30 | 2019-12-30 | 一种洗碗机复合洗涤剂的制备工艺 |
Publications (1)
Publication Number | Publication Date |
---|---|
CN111117794A true CN111117794A (zh) | 2020-05-08 |
Family
ID=70504485
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201911387608.3A Pending CN111117794A (zh) | 2019-12-30 | 2019-12-30 | 一种洗碗机复合洗涤剂的制备工艺 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN111117794A (zh) |
Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3627686A (en) * | 1968-09-30 | 1971-12-14 | Chemed Corp | Machine dishwashing compositions containing sodium polyacrylate and nta |
CN1283221A (zh) * | 1997-12-30 | 2001-02-07 | 亨克尔两合股份公司 | 洗碟机用洗涤剂成型物的制备方法 |
US20050075258A1 (en) * | 2001-08-17 | 2005-04-07 | Arnd Kessler | Dishwasher detergent with improved protection against glass corrosion |
CN102876475A (zh) * | 2012-08-21 | 2013-01-16 | 青岛叁鼎卫生制品有限公司 | 一种洗碗机用杀菌洗涤剂 |
CN105087177A (zh) * | 2015-08-30 | 2015-11-25 | 王璐 | 一种洗碗机用洗涤剂 |
CN106854576A (zh) * | 2017-01-05 | 2017-06-16 | 长沙协浩吉生物工程有限公司 | 一种生物洗碗机专用洗涤剂的配制方法 |
CN107779299A (zh) * | 2016-08-26 | 2018-03-09 | 游从鑫 | 洗碗机及洗锅机用顽固污垢强力去除剂 |
CN109504569A (zh) * | 2018-12-10 | 2019-03-22 | 沈阳化工大学 | 一种洗碗机用洗涤剂 |
CN110982638A (zh) * | 2019-12-24 | 2020-04-10 | 郭廷昌 | 一种泡沫清洗剂的制备工艺 |
-
2019
- 2019-12-30 CN CN201911387608.3A patent/CN111117794A/zh active Pending
Patent Citations (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3627686A (en) * | 1968-09-30 | 1971-12-14 | Chemed Corp | Machine dishwashing compositions containing sodium polyacrylate and nta |
CN1283221A (zh) * | 1997-12-30 | 2001-02-07 | 亨克尔两合股份公司 | 洗碟机用洗涤剂成型物的制备方法 |
US20050075258A1 (en) * | 2001-08-17 | 2005-04-07 | Arnd Kessler | Dishwasher detergent with improved protection against glass corrosion |
CN102876475A (zh) * | 2012-08-21 | 2013-01-16 | 青岛叁鼎卫生制品有限公司 | 一种洗碗机用杀菌洗涤剂 |
CN105087177A (zh) * | 2015-08-30 | 2015-11-25 | 王璐 | 一种洗碗机用洗涤剂 |
CN107779299A (zh) * | 2016-08-26 | 2018-03-09 | 游从鑫 | 洗碗机及洗锅机用顽固污垢强力去除剂 |
CN106854576A (zh) * | 2017-01-05 | 2017-06-16 | 长沙协浩吉生物工程有限公司 | 一种生物洗碗机专用洗涤剂的配制方法 |
CN109504569A (zh) * | 2018-12-10 | 2019-03-22 | 沈阳化工大学 | 一种洗碗机用洗涤剂 |
CN110982638A (zh) * | 2019-12-24 | 2020-04-10 | 郭廷昌 | 一种泡沫清洗剂的制备工艺 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN102296004B (zh) | 一种用于厨房中硬表面清洗的膏体洗涤剂及其制备方法 | |
EP3099775B1 (en) | Aqueous detergent compositions | |
EP0289312B1 (en) | Process for the preparation of a granular detergent composition | |
AU697812B2 (en) | Descaling and cleaning formulations based on cellulose microfibrils | |
MX2008002310A (es) | Una composicion de detergente solida de lavanderia que comprende un surfactante detergente anionico y tecnologia de calcio aumentado. | |
CN104005039A (zh) | 一种铝合金模具清洁剂及其制备方法 | |
CN109097215B (zh) | 一种环保型洗衣皂粉组合物及其制备方法 | |
CN102732389A (zh) | 一种车辆清洁剂 | |
TW201708528A (zh) | 水性清潔劑組成物 | |
EP2801606A1 (en) | Spray-dried particle comprising sulphate | |
CN103146504A (zh) | 一种环保节能浓缩洗衣粉及其制备方法 | |
CN111117794A (zh) | 一种洗碗机复合洗涤剂的制备工艺 | |
CN107970939A (zh) | 一种脂肪酸甲酯乙氧基化催化剂及其制法和用途 | |
CN110982638A (zh) | 一种泡沫清洗剂的制备工艺 | |
CN106833930A (zh) | 一种环保型轻垢液体洗涤剂 | |
JPH0848999A (ja) | 洗浄剤組成物 | |
CN104293510A (zh) | 一种纺织品清洗剂 | |
CN106566685A (zh) | 高效低泡洗衣液及其制备方法 | |
CN104789396B (zh) | 利用高塔喷雾干燥制备香果油皂粉的方法 | |
JP2670404B2 (ja) | 高密度粒状洗浄剤組成物 | |
CN107541350A (zh) | 一种列车座椅用洗涤剂 | |
CN105542993A (zh) | 一种环保型浓缩洗衣粉 | |
CN107090366A (zh) | 一种冷水洗涤剂及其制备方法 | |
CN102876488A (zh) | 一种高效环保印染皂洗剂的复配方法 | |
CN108192742A (zh) | 一种去污粉及其制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20200508 |
|
WD01 | Invention patent application deemed withdrawn after publication |