CN110983819A - Preparation method of modified tencel fiber fabric suitable for children clothes - Google Patents
Preparation method of modified tencel fiber fabric suitable for children clothes Download PDFInfo
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- CN110983819A CN110983819A CN201911341999.5A CN201911341999A CN110983819A CN 110983819 A CN110983819 A CN 110983819A CN 201911341999 A CN201911341999 A CN 201911341999A CN 110983819 A CN110983819 A CN 110983819A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/04—Physical treatment combined with treatment with chemical compounds or elements
- D06M10/08—Organic compounds
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
- D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
- D06M15/37—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M15/643—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain
- D06M15/6436—Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds containing silicon in the main chain containing amino groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/52—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing synthetic macromolecular substances
- D06P1/5264—Macromolecular compounds obtained otherwise than by reactions involving only unsaturated carbon-to-carbon bonds
- D06P1/5292—Macromolecular compounds obtained otherwise than by reactions involving only unsaturated carbon-to-carbon bonds containing Si-atoms
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
- D06M2101/06—Vegetal fibres cellulosic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
- D06M2200/35—Abrasion, pilling or fibrillation resistance
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The invention discloses a preparation method of a modified tencel fiber fabric suitable for children clothes, which comprises the steps of firstly carrying out ultrasonic pretreatment on tencel fibers by adopting a glycerol solution, then treating the tencel fibers by adopting a modified treatment solution consisting of an acetal crosslinking agent, organic acid, poly-polycarboxylic acid, amino silicone oil microemulsion and water, dyeing by using a natural dye liquor, and directly weaving or blending. According to the invention, the glycerol solution is adopted for ultrasonic pretreatment, so that the treatment effect of the modified treatment solution on the tencel fibers can be improved, and the treatment time is shortened; after the tencel fiber is treated by the modified treatment liquid, the fluffing and pilling performance of the fiber can be obviously improved, the fiber can be effectively prevented from hardening, and the dyeing performance of the fiber can be improved. The preparation method of the modified tencel fiber fabric suitable for children clothes adopts natural plant dye for dyeing, does not add chemical additives, and is safe and pollution-free; the adopted modified treatment solution can be recycled for multiple times, and has small harm to the environment.
Description
Technical Field
The invention relates to the technical field of fabrics, in particular to a preparation method of a modified tencel fiber fabric suitable for children clothes.
Background
Tencel (Tencel) is a solvent-based cellulose fiber that was developed by Acordis corporation of the United kingdom over ten years until the nineties of the last century to complete its commercial application, and is the most typical green, environmentally friendly fiber. In 2004, 5 months, the materials were combined by lanjing corporation and produced in unison. The environment-friendly characteristic is as follows: the raw material is from wood, can be regenerated continuously and naturally, make wood pulp, adopt (NMMO) spinning process, dissolve wood pulp in the ammonium oxide solvent and spin directly, finish under the physical action completely, the ammonium oxide solvent is recycled, the recovery rate is more than 99%, non-toxic, pollution-free, biodegradable after the tencel product uses, will not cause the pollution to the environment, so called "green fiber of twenty-one century".
It has the comfort of cotton, the strength of terylene, the luxurious aesthetic feeling of wool fabric and the unique touch feeling and soft drooping of real silk, and has high toughness no matter in wet state. In the wet state, it is the first wet strength much superior to cotton cellulose fiber. The novel environment-friendly decomposable fiber has unique fiber performance and has the characteristics of natural fibers and synthetic fibers. Moisture absorption and ventilation, high strength, less curling, easy straightening and less fiber entanglement.
Tencel fibers have uniform cross sections, but have weak interfibrillary bonds and no elasticity, and if the tencel fibers are subjected to mechanical friction, the outer layers of the tencel fibers can be broken to form fuzz with the length of about 1-4 mu m, the fuzz is easier to generate particularly in a wet state, and the tencel fibers can be entangled into cotton grains in severe cases, and the fabric can be slightly hardened. In order to improve the defects and make the fabric more suitable for children to take, the invention provides a preparation method of a modified tencel fiber fabric suitable for children clothes.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a preparation method of a modified tencel fiber fabric suitable for children clothes.
The technical scheme of the invention is as follows:
a preparation method of a modified tencel fiber fabric suitable for children clothes comprises the following steps:
A. immersing the tencel fiber yarns into a glycerol solution, and stirring to uniformly disperse the tencel fiber yarns in the solution;
B. carrying out ultrasonic treatment on the solution, wherein the ultrasonic power is 600-800W, and the bath ratio is 1: (6-10), treating for 3-5min, taking out the tencel fiber yarns after the treatment is finished, and airing;
C. placing the aired tencel fiber yarn into a modification treatment solution, wherein the bath ratio is 1: (18-25), then treating for 8-15min at the temperature of 40-50 ℃, and airing;
D. immersing the tencel fiber yarns into natural dye liquor, adding a pH regulator, and dyeing the tencel fiber yarns by using a natural dye by adopting a dip-dyeing process, wherein the bath ratio is 1 (12-15);
E. taking the tencel fiber out, washing with water, drying at 40-50 ℃, fixing color at 80-90 ℃ for 2-3min, and spinning the tencel fiber into fabric.
Preferably, in the step a, the volume fraction of glycerol in the glycerol solution is 28-35%.
Preferably, in the step C, the modification treatment liquid includes the following components: acetal crosslinking agent, organic acid, poly-polycarboxylic acid, amino silicone oil microemulsion and water.
Preferably, in the step C, the modifying treatment solution comprises the following components in percentage by weight: 8-15% of acetal crosslinking agent, 5-8% of organic acid, 18-25% of poly polycarboxylic acid, 8-12% of amino silicone oil microemulsion and water.
Preferably, in the step C, the organic acid is any one of tartaric acid and citric acid.
Preferably, in the step D, the natural dye liquor is prepared by dissolving 2-10 wt% of natural dye in deionized water.
Preferably, in the step D, the dip dyeing process parameters are as follows: pH 3.5-4.5, temperature: 85-90 ℃, dyeing time: 15-25 min.
Preferably, in the step E, the tencel fiber can be directly woven into the fabric, and can also be blended with other fibers to obtain a blended fabric.
The invention has the advantages that: the preparation method of the modified tencel fiber fabric suitable for children clothes comprises the steps of firstly carrying out ultrasonic pretreatment on tencel fibers by adopting a glycerol solution, then treating the tencel fibers by adopting a modification treatment solution consisting of an acetal crosslinking agent, an organic acid, a poly-polycarboxylic acid, an amino silicone oil microemulsion and water, dyeing by using a natural dye solution, and directly spinning or blending to obtain the modified tencel fiber fabric suitable for children clothes.
According to the invention, the glycerol solution is adopted for ultrasonic pretreatment, so that the treatment effect of the modified treatment solution on the tencel fibers can be improved, and the treatment time is shortened; after the tencel fiber is treated by the modified treatment liquid, the fluffing and pilling performance of the fiber can be obviously improved, the fiber can be effectively prevented from hardening, and the dyeing performance of the fiber can be improved.
The preparation method of the modified tencel fiber fabric suitable for children clothes adopts natural plant dye for dyeing, does not add chemical additives, and is safe and pollution-free; the adopted modified treatment solution can be recycled for multiple times, and has small harm to the environment. In conclusion, the preparation method of the modified tencel fiber fabric suitable for children clothes is an environment-friendly and safe fabric preparation method, and meets the national requirements on the textile industry.
Detailed Description
Example 1
A preparation method of a modified tencel fiber fabric suitable for children clothes comprises the following steps:
A. immersing the tencel fiber yarns into a glycerol solution, and stirring to uniformly disperse the tencel fiber yarns in the solution;
B. carrying out ultrasonic treatment on the solution, wherein the ultrasonic power is 650W, and the bath ratio is 1: 8, treating for 4min, taking out the tencel fiber yarns after the treatment is finished, and airing;
C. placing the aired tencel fiber yarn into a modification treatment solution, wherein the bath ratio is 1: 20, then treating for 12min at the temperature of 42 ℃, and airing;
D. immersing the tencel fiber yarns into natural dye liquor, adding a pH regulator, and dyeing the tencel fiber yarns with natural dye by adopting a dip-dyeing process, wherein the bath ratio is 1: 13;
E. and taking the tencel fiber out, washing with water, drying at 47 ℃, fixing color at 85 ℃ for 2.5min, and spinning the tencel fiber into fabric.
In the step A, the volume fraction of glycerol in the glycerol solution is 30%.
In the step C, the modification treatment liquid comprises the following components in percentage by weight: 10% of acetal crosslinking agent, 6% of organic acid, 22% of poly-polycarboxylic acid, 10% of amino silicone oil microemulsion and water.
In the step C, the organic acid is tartaric acid.
In the step D, the natural dye liquor is prepared by dissolving 6.5 wt% of natural dye in deionized water.
In the step D, the dip dyeing process parameters are as follows: pH 3.8, temperature: 88 ℃, dyeing time: and 20 min.
In the step E, the tencel fiber can be directly woven into the fabric, and can also be blended with other fibers to obtain the blended fabric.
Example 2
A preparation method of a modified tencel fiber fabric suitable for children clothes comprises the following steps:
A. immersing the tencel fiber yarns into a glycerol solution, and stirring to uniformly disperse the tencel fiber yarns in the solution;
B. carrying out ultrasonic treatment on the solution, wherein the ultrasonic power is 600W, and the bath ratio is 1: 10, treating for 3min, taking out the tencel fiber yarns after the treatment is finished, and airing;
C. placing the aired tencel fiber yarn into a modification treatment solution, wherein the bath ratio is 1: 25, then treating for 15min at the temperature of 40 ℃, and airing;
D. immersing the tencel fiber yarns into natural dye liquor, adding a pH regulator, and dyeing the tencel fiber yarns with natural dye by adopting a dip-dyeing process, wherein the bath ratio is 1: 12;
E. and taking the tencel fiber out, washing with water, drying at 50 ℃, fixing color at 80 ℃ for 3min, and spinning the tencel fiber into fabric.
In the step A, the volume fraction of glycerol in the glycerol solution is 28%.
In the step C, the modification treatment liquid comprises the following components in percentage by weight: acetal crosslinker 15%, organic acid 5%, poly-polycarboxylic acid 25%, amino silicone oil microemulsion 8% and water.
In the step C, the organic acid is tartaric acid.
In the step D, the natural dye liquor is prepared by dissolving 10 wt% of natural dye in deionized water.
In the step D, the dip dyeing process parameters are as follows: pH 3.5, temperature: 90 ℃, dyeing time: and 15 min.
In the step E, the tencel fiber can be directly woven into the fabric, and can also be blended with other fibers to obtain the blended fabric.
Example 3
A preparation method of a modified tencel fiber fabric suitable for children clothes comprises the following steps:
A. immersing the tencel fiber yarns into a glycerol solution, and stirring to uniformly disperse the tencel fiber yarns in the solution;
B. carrying out ultrasonic treatment on the solution, wherein the ultrasonic power is 800W, and the bath ratio is 1: 6, treating for 5min, taking out the tencel fiber yarns after the treatment is finished, and airing;
C. placing the aired tencel fiber yarn into a modification treatment solution, wherein the bath ratio is 1: 18, then treating for 8min at the temperature of 50 ℃, and airing;
D. immersing the tencel fiber yarns into natural dye liquor, adding a pH regulator, and dyeing the tencel fiber yarns with natural dye by adopting a dip-dyeing process, wherein the bath ratio is 1: 15;
E. and taking the tencel fiber out, washing with water, drying at 40 ℃, fixing color at 90 ℃ for 2min, and spinning the tencel fiber into fabric.
In the step A, the volume fraction of glycerol in the glycerol solution is 35%.
In the step C, the modification treatment liquid comprises the following components in percentage by weight: 8% of acetal crosslinking agent, 8% of organic acid, 18% of poly polycarboxylic acid, 12% of amino silicone oil microemulsion and water.
In the step C, the organic acid is citric acid.
In the step D, the natural dye liquor is prepared by dissolving 2 wt% of natural dye in deionized water.
In the step D, the dip dyeing process parameters are as follows: pH 4.5, temperature: 85 ℃, dyeing time: and (5) 25 min.
In the step E, the tencel fiber can be directly woven into the fabric, and can also be blended with other fibers to obtain the blended fabric.
Comparative example 1
The step of pretreatment of the glycerol solution in example 1 was eliminated, and the rest of the formulation and preparation method were unchanged.
Comparative example 2
The steps of pretreatment of the glycerol solution and treatment of the modified treatment solution in example 1 were removed, and the rest of the formulation and the preparation method were unchanged.
The samples prepared in examples 1 to 3 and comparative examples 1 to 2 were examined for pilling properties and the results of the specific tests are shown in Table 1.
Table 1: results of testing the pilling performance of the samples prepared in examples 1 to 3 and comparative examples 1 to 2;
| examples1 | Example 2 | Example 3 | Comparative example 1 | Comparative example 2 | |
| Pilling performance/grade | 4-5 | 4-5 | 4-5 | 2-3 | 3-4 |
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (8)
1. A preparation method of a modified tencel fiber fabric suitable for children clothes is characterized by comprising the following steps:
A. immersing the tencel fiber yarns into a glycerol solution, and stirring to uniformly disperse the tencel fiber yarns in the solution;
B. carrying out ultrasonic treatment on the solution, wherein the ultrasonic power is 600-800W, and the bath ratio is 1: (6-10), treating for 3-5min, taking out the tencel fiber yarns after the treatment is finished, and airing;
C. placing the aired tencel fiber yarn into a modification treatment solution, wherein the bath ratio is 1: (18-25), then treating for 8-15min at the temperature of 40-50 ℃, and airing;
D. immersing the tencel fiber yarns into natural dye liquor, adding a pH regulator, and dyeing the tencel fiber yarns by using a natural dye by adopting a dip-dyeing process, wherein the bath ratio is 1 (12-15);
E. taking the tencel fiber out, washing with water, drying at 40-50 ℃, fixing color at 80-90 ℃ for 2-3min, and spinning the tencel fiber into fabric.
2. The method for preparing a modified tencel fiber fabric suitable for children's clothing as claimed in claim 1, wherein in the step a, the volume fraction of glycerin in the glycerin solution is 28-35%.
3. The method for preparing modified tencel fiber fabric suitable for children's clothing according to claim 1, wherein in the step C, the modifying treatment solution comprises the following components: acetal crosslinking agent, organic acid, poly-polycarboxylic acid, amino silicone oil microemulsion and water.
4. The method for preparing modified tencel fiber fabric suitable for children clothes as claimed in claim 1, wherein in the step C, the modifying treatment solution comprises the following components in percentage by weight: 8-15% of acetal crosslinking agent, 5-8% of organic acid, 18-25% of poly-polycarboxylic acid, 8-12% of amino silicone oil microemulsion and water.
5. The method for preparing modified tencel fiber fabric suitable for children's clothing as claimed in claim 3 or 4, wherein in the step C, the organic acid is tartaric acid or citric acid.
6. The method for preparing modified tencel fiber fabric suitable for children's clothing as claimed in claim 1, wherein in the step D, the natural dye solution is prepared by dissolving 2-10 wt% of natural dye in deionized water.
7. The method for preparing the modified tencel fiber fabric suitable for children clothes as claimed in claim 1, wherein in the step D, the dip dyeing process parameters are as follows: pH 3.5-4.5, temperature: 85-90 ℃, dyeing time: 15-25 min.
8. The method for preparing modified tencel fiber fabric suitable for children clothes as claimed in claim 1, wherein in the step E, the tencel fiber can be directly woven into the fabric, and can also be blended with other fibers to obtain a blended fabric.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201911341999.5A CN110983819A (en) | 2019-12-23 | 2019-12-23 | Preparation method of modified tencel fiber fabric suitable for children clothes |
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| CN201911341999.5A CN110983819A (en) | 2019-12-23 | 2019-12-23 | Preparation method of modified tencel fiber fabric suitable for children clothes |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3960686A (en) * | 1974-01-04 | 1976-06-01 | Chemische Werke Huls Aktiengesellschaft | Method for preparing low pilling effect polyester fiber products |
| CN101638847A (en) * | 2009-07-24 | 2010-02-03 | 东莞市德能化工有限公司 | Formaldehyde-free durable crease-proof finishing agent used for cellulosic fiber fabric |
| CN101760846A (en) * | 2009-11-06 | 2010-06-30 | 苏州双轮化纤有限公司 | Low balling-up degradation fabric |
| CN105544241A (en) * | 2016-01-26 | 2016-05-04 | 青岛百草纤维科技股份有限公司 | Method for dyeing regenerated cellulose fibers through isatis root natural dyestuff and application of method to mask |
| CN108948781A (en) * | 2018-07-04 | 2018-12-07 | 武汉纺织大学 | The preparation method of spun gold emperor's chrysanthemum natural dye and the natural dye and colouring method prepared by this method |
-
2019
- 2019-12-23 CN CN201911341999.5A patent/CN110983819A/en not_active Withdrawn
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3960686A (en) * | 1974-01-04 | 1976-06-01 | Chemische Werke Huls Aktiengesellschaft | Method for preparing low pilling effect polyester fiber products |
| CN101638847A (en) * | 2009-07-24 | 2010-02-03 | 东莞市德能化工有限公司 | Formaldehyde-free durable crease-proof finishing agent used for cellulosic fiber fabric |
| CN101760846A (en) * | 2009-11-06 | 2010-06-30 | 苏州双轮化纤有限公司 | Low balling-up degradation fabric |
| CN105544241A (en) * | 2016-01-26 | 2016-05-04 | 青岛百草纤维科技股份有限公司 | Method for dyeing regenerated cellulose fibers through isatis root natural dyestuff and application of method to mask |
| CN108948781A (en) * | 2018-07-04 | 2018-12-07 | 武汉纺织大学 | The preparation method of spun gold emperor's chrysanthemum natural dye and the natural dye and colouring method prepared by this method |
Non-Patent Citations (1)
| Title |
|---|
| 梅自强等: "《纺织辞典》", 31 January 2007, 中国纺织出版社 * |
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Application publication date: 20200410 |
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