CN110668977B - 一种月桂酰精氨酸乙酯盐酸盐的制备工艺 - Google Patents
一种月桂酰精氨酸乙酯盐酸盐的制备工艺 Download PDFInfo
- Publication number
- CN110668977B CN110668977B CN201911022274.XA CN201911022274A CN110668977B CN 110668977 B CN110668977 B CN 110668977B CN 201911022274 A CN201911022274 A CN 201911022274A CN 110668977 B CN110668977 B CN 110668977B
- Authority
- CN
- China
- Prior art keywords
- ethyl ester
- lauroyl
- hydrochloride
- arginine
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C277/00—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups
- C07C277/08—Preparation of guanidine or its derivatives, i.e. compounds containing the group, the singly-bound nitrogen atoms not being part of nitro or nitroso groups of substituted guanidines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201911022274.XA CN110668977B (zh) | 2019-10-25 | 2019-10-25 | 一种月桂酰精氨酸乙酯盐酸盐的制备工艺 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201911022274.XA CN110668977B (zh) | 2019-10-25 | 2019-10-25 | 一种月桂酰精氨酸乙酯盐酸盐的制备工艺 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN110668977A CN110668977A (zh) | 2020-01-10 |
CN110668977B true CN110668977B (zh) | 2022-03-18 |
Family
ID=69084237
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201911022274.XA Active CN110668977B (zh) | 2019-10-25 | 2019-10-25 | 一种月桂酰精氨酸乙酯盐酸盐的制备工艺 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN110668977B (zh) |
Families Citing this family (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN111778509B (zh) * | 2020-07-16 | 2023-03-21 | 太原工业学院 | 一种含精氨酸衍生物的碳钢缓蚀剂及其制备方法与应用 |
CN113527145A (zh) * | 2021-08-31 | 2021-10-22 | 浙江圣达生物研究院有限公司 | 一种月桂酰精氨酸乙酯盐酸盐的制备工艺 |
Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5780658A (en) * | 1995-01-10 | 1998-07-14 | Laboratorios Miret, S.A. | Process for the synthesis of cationic surfactants comprising esterification with basic character amino acids |
WO2001094292A1 (en) * | 2000-06-03 | 2001-12-13 | Lamirsa (Laboratorios Miret, S.A.) | Process for the preparation of cationic surfactants |
WO2012130621A1 (en) * | 2011-03-28 | 2012-10-04 | Laboratorios Miret, S.A. | Use of cationic surfactants against acne |
WO2013098659A1 (en) * | 2011-12-28 | 2013-07-04 | Viridis Biopharma Pvt Ltd | Process for the synthesis of highly pure cationic surfactant products |
CN105037216A (zh) * | 2015-08-05 | 2015-11-11 | 上海应用技术学院 | 一种月桂酰精氨酸盐酸盐的制备方法 |
CN105061266A (zh) * | 2015-07-17 | 2015-11-18 | 武汉志邦化学技术有限公司 | 一种月桂酰精氨酸乙酯盐酸盐的制备方法 |
CN107400069A (zh) * | 2017-08-01 | 2017-11-28 | 浙江大学 | 一种月桂酰精氨酸乙酯盐酸盐的制备方法 |
CN107814754A (zh) * | 2017-11-16 | 2018-03-20 | 中国日用化学工业研究院 | 一种月桂酰精氨酸乙酯盐酸盐的制备方法 |
CN108101812A (zh) * | 2018-01-02 | 2018-06-01 | 成都傲飞生物化学品有限责任公司 | 一种月桂酰精氨酸乙酯盐酸盐的生产纯化工艺 |
CN108929247A (zh) * | 2018-06-08 | 2018-12-04 | 中南大学 | 一种Nα-烷基酰精氨酸酯抗菌剂及其制备和应用 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US20100152480A1 (en) * | 2008-12-16 | 2010-06-17 | Ghare Vishwas Sadhu | Process for synthesis of cationic surfactants |
US20160030317A1 (en) * | 2014-07-31 | 2016-02-04 | Johnson & Johnson Consumer Inc. | HIGHLY BIOAVAILABLE Na-ACYL ACIDIC AMINO ACID ESTER SALT COMPOSITONS WITH ZWITTERIONIC SURFACTANTS |
-
2019
- 2019-10-25 CN CN201911022274.XA patent/CN110668977B/zh active Active
Patent Citations (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5780658A (en) * | 1995-01-10 | 1998-07-14 | Laboratorios Miret, S.A. | Process for the synthesis of cationic surfactants comprising esterification with basic character amino acids |
WO2001094292A1 (en) * | 2000-06-03 | 2001-12-13 | Lamirsa (Laboratorios Miret, S.A.) | Process for the preparation of cationic surfactants |
WO2012130621A1 (en) * | 2011-03-28 | 2012-10-04 | Laboratorios Miret, S.A. | Use of cationic surfactants against acne |
WO2013098659A1 (en) * | 2011-12-28 | 2013-07-04 | Viridis Biopharma Pvt Ltd | Process for the synthesis of highly pure cationic surfactant products |
CN105061266A (zh) * | 2015-07-17 | 2015-11-18 | 武汉志邦化学技术有限公司 | 一种月桂酰精氨酸乙酯盐酸盐的制备方法 |
CN105037216A (zh) * | 2015-08-05 | 2015-11-11 | 上海应用技术学院 | 一种月桂酰精氨酸盐酸盐的制备方法 |
CN107400069A (zh) * | 2017-08-01 | 2017-11-28 | 浙江大学 | 一种月桂酰精氨酸乙酯盐酸盐的制备方法 |
CN107814754A (zh) * | 2017-11-16 | 2018-03-20 | 中国日用化学工业研究院 | 一种月桂酰精氨酸乙酯盐酸盐的制备方法 |
CN108101812A (zh) * | 2018-01-02 | 2018-06-01 | 成都傲飞生物化学品有限责任公司 | 一种月桂酰精氨酸乙酯盐酸盐的生产纯化工艺 |
CN108929247A (zh) * | 2018-06-08 | 2018-12-04 | 中南大学 | 一种Nα-烷基酰精氨酸酯抗菌剂及其制备和应用 |
Non-Patent Citations (3)
Title |
---|
"月桂酰精氨酸乙酯盐酸盐(LAE)的合成研究";吴闯;《中国优秀硕士学位论文全文数据库 工程科技I辑》;20170315;第2-3章 * |
月桂酰精氨酸乙酯盐酸盐的合成与性能研究;柯回春等;《日用化学工业》;20180722(第07期);第378-381页 * |
氨基酸表面活性剂的合成及对脂双层膜的修饰;侯新朴等;《齐齐哈尔大学学报》;19901230(第04期);第37-40页 * |
Also Published As
Publication number | Publication date |
---|---|
CN110668977A (zh) | 2020-01-10 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN110668977B (zh) | 一种月桂酰精氨酸乙酯盐酸盐的制备工艺 | |
CN104176968A (zh) | 一种萘系高浓减水剂的生产方法 | |
CN110590867A (zh) | 一种d-氨基葡萄糖盐酸盐的合成方法 | |
CN106631852A (zh) | 一种从l‑鸟氨酸发酵液中提取l‑鸟氨酸盐酸盐的方法 | |
CN104119243B (zh) | 一种亚氨基二乙酸的节能清洁生产方法 | |
CN109553550B (zh) | 一种合成二氢燕麦生物碱的方法 | |
CN112552167B (zh) | 葡萄糖酸钙的制备方法 | |
CN103265443B (zh) | 一种工业生产高纯度亚氨基二乙酸的方法 | |
CN108586493A (zh) | 一种结晶型头孢呋辛酯的制备方法 | |
CN110938020B (zh) | 一种月桂酰精氨酸乙酯盐酸盐的制备工艺 | |
CN111440171A (zh) | 一种鸟苷水解法合成鸟嘌呤的方法 | |
CN107383418B (zh) | 一种抗紫外线塑料添加剂及其制备方法 | |
CN113501771B (zh) | 一种n-(2-氨乙基)甘氨酸衍生物的制备方法 | |
CN113025679B (zh) | 一种叔丁氧羰基头孢卡品前体酸的酶法制备工艺 | |
CN114436930A (zh) | 一种Boc-L-羟脯氨酸的合成方法 | |
CN104327049B (zh) | 右旋雷贝拉唑钠单水合物晶体的制备方法 | |
CN107365223A (zh) | 一种壳聚糖‑海藻酸钠交联包覆的沼渣复合颗粒及其制备方法 | |
CN106631872A (zh) | 一种氟苯尼考类似物中间体的合成方法 | |
CN111574387A (zh) | 一种对氨甲基苯甲酸及其制备方法 | |
CN107245060B (zh) | 一种3-乙酰基-4-硝基亚氨基-1,3,5-恶二嗪的合成方法 | |
CN112250621A (zh) | 炔草酯的合成方法 | |
CN113527145A (zh) | 一种月桂酰精氨酸乙酯盐酸盐的制备工艺 | |
CN109705609A (zh) | 一种母液水低苯胺值颜料红57:1的工业化生产方法 | |
CN108623598A (zh) | 一种亚胺培南中间体及亚胺培南的制备方法 | |
CN108084064B (zh) | 一种d-(-)-酒石酸的新制备方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20210507 Address after: Room 5-302-2, 291 Fucheng Road, Xiasha street, Hangzhou Economic and Technological Development Zone, Zhejiang Province, 310018 Applicant after: Zhejiang Shengda Biological Research Institute Co.,Ltd. Applicant after: ZHEJIANG SHENGDA BIO-PHARM Co.,Ltd. Address before: 310018 room 5-302-2, 291 Fucheng Road, Xiasha street, Hangzhou Economic Development Zone, Zhejiang Province Applicant before: Zhejiang Shengda Biological Research Institute Co.,Ltd. |
|
TA01 | Transfer of patent application right | ||
GR01 | Patent grant | ||
GR01 | Patent grant |